CN106596364A - Tracer method based particle concentration measurement system for closed cyclic spray drying system - Google Patents
Tracer method based particle concentration measurement system for closed cyclic spray drying system Download PDFInfo
- Publication number
- CN106596364A CN106596364A CN201611202467.XA CN201611202467A CN106596364A CN 106596364 A CN106596364 A CN 106596364A CN 201611202467 A CN201611202467 A CN 201611202467A CN 106596364 A CN106596364 A CN 106596364A
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- China
- Prior art keywords
- hothouse
- spray drying
- light source
- laser light
- drying system
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- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
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- 238000001694 spray drying Methods 0.000 title claims abstract description 28
- 238000000034 method Methods 0.000 title claims abstract description 18
- 239000000700 radioactive tracer Substances 0.000 title claims abstract description 17
- 239000002245 particle Substances 0.000 title claims abstract description 10
- 238000005259 measurement Methods 0.000 title abstract description 9
- 125000004122 cyclic group Chemical group 0.000 title abstract description 3
- XAGFODPZIPBFFR-UHFFFAOYSA-N aluminium Chemical compound [Al] XAGFODPZIPBFFR-UHFFFAOYSA-N 0.000 claims abstract description 15
- 239000012530 fluid Substances 0.000 claims abstract description 12
- 239000000084 colloidal system Substances 0.000 claims abstract description 8
- 238000000889 atomisation Methods 0.000 claims abstract description 5
- 239000000463 material Substances 0.000 claims description 34
- 239000007788 liquid Substances 0.000 claims description 24
- 239000008187 granular material Substances 0.000 claims description 18
- 230000008676 import Effects 0.000 claims description 14
- 229910052782 aluminium Inorganic materials 0.000 claims description 13
- 239000000843 powder Substances 0.000 claims description 13
- 239000004411 aluminium Substances 0.000 claims description 11
- 239000006199 nebulizer Substances 0.000 claims description 10
- 239000002904 solvent Substances 0.000 claims description 5
- 238000012546 transfer Methods 0.000 claims description 5
- 230000005540 biological transmission Effects 0.000 claims description 3
- 239000012780 transparent material Substances 0.000 claims description 3
- 230000003760 hair shine Effects 0.000 claims 1
- 238000001035 drying Methods 0.000 abstract description 11
- 238000011160 research Methods 0.000 abstract description 3
- 239000002994 raw material Substances 0.000 abstract description 2
- 238000005457 optimization Methods 0.000 abstract 1
- 230000000638 stimulation Effects 0.000 abstract 1
- 239000007789 gas Substances 0.000 description 6
- 238000004458 analytical method Methods 0.000 description 2
- 238000005516 engineering process Methods 0.000 description 2
- 238000010438 heat treatment Methods 0.000 description 2
- 238000004519 manufacturing process Methods 0.000 description 2
- 239000000203 mixture Substances 0.000 description 2
- 239000007787 solid Substances 0.000 description 2
- 230000002159 abnormal effect Effects 0.000 description 1
- QVGXLLKOCUKJST-UHFFFAOYSA-N atomic oxygen Chemical compound [O] QVGXLLKOCUKJST-UHFFFAOYSA-N 0.000 description 1
- 230000009286 beneficial effect Effects 0.000 description 1
- 239000003054 catalyst Substances 0.000 description 1
- 239000003795 chemical substances by application Substances 0.000 description 1
- 239000012141 concentrate Substances 0.000 description 1
- 230000007547 defect Effects 0.000 description 1
- 239000003814 drug Substances 0.000 description 1
- 230000000694 effects Effects 0.000 description 1
- 230000007613 environmental effect Effects 0.000 description 1
- 239000000446 fuel Substances 0.000 description 1
- 238000009434 installation Methods 0.000 description 1
- 239000008267 milk Substances 0.000 description 1
- 210000004080 milk Anatomy 0.000 description 1
- 235000013336 milk Nutrition 0.000 description 1
- 239000003960 organic solvent Substances 0.000 description 1
- 239000001301 oxygen Substances 0.000 description 1
- 229910052760 oxygen Inorganic materials 0.000 description 1
- 239000013618 particulate matter Substances 0.000 description 1
- 238000000053 physical method Methods 0.000 description 1
- 231100000614 poison Toxicity 0.000 description 1
- 230000007096 poisonous effect Effects 0.000 description 1
- 238000012545 processing Methods 0.000 description 1
- 238000004064 recycling Methods 0.000 description 1
- 230000011514 reflex Effects 0.000 description 1
- 230000035943 smell Effects 0.000 description 1
- 239000007921 spray Substances 0.000 description 1
- 239000000126 substance Substances 0.000 description 1
- 230000009897 systematic effect Effects 0.000 description 1
Classifications
-
- G—PHYSICS
- G01—MEASURING; TESTING
- G01N—INVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES
- G01N15/00—Investigating characteristics of particles; Investigating permeability, pore-volume or surface-area of porous materials
- G01N15/06—Investigating concentration of particle suspensions
-
- G—PHYSICS
- G01—MEASURING; TESTING
- G01N—INVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES
- G01N15/00—Investigating characteristics of particles; Investigating permeability, pore-volume or surface-area of porous materials
- G01N15/06—Investigating concentration of particle suspensions
- G01N15/075—Investigating concentration of particle suspensions by optical means
Landscapes
- Chemical & Material Sciences (AREA)
- Dispersion Chemistry (AREA)
- Physics & Mathematics (AREA)
- Health & Medical Sciences (AREA)
- Life Sciences & Earth Sciences (AREA)
- Analytical Chemistry (AREA)
- Biochemistry (AREA)
- General Health & Medical Sciences (AREA)
- General Physics & Mathematics (AREA)
- Immunology (AREA)
- Pathology (AREA)
- Investigating Or Analysing Materials By Optical Means (AREA)
- Sampling And Sample Adjustment (AREA)
Abstract
The invention discloses a tracer method based particle concentration measurement system for a closed cyclic spray drying system. The tracer method based particle concentration measurement system comprises a laser source, aluminum powder colloid, an image acquisition device and a spray drying system. The laser source is positioned on one side of a drying chamber to illuminate fluid in the drying chamber. The image acquisition device is positioned on the other side of the drying chamber and opposite to the laser source and is used for recording the position of fluid tracer particle aluminum powder illuminated by the laser source. The tracer method based particle concentration measurement system is used for displaying particle concentration of raw material fluid in the drying chamber under atomization and rotating hot air action and can be used for research stimulation and structural optimization in a drying process.
Description
Technical field
The present invention relates to a kind of close type circulation spray drying system tracer method granule density measuring system, belongs to physical measurement
Technical field.
Background technology
Spray drying is that material liquid nebulizer is dispersed into droplet by one kind, and is carried out with droplet directly contact with hot-air
Heat and mass heat exchange and obtain the drying meanss of dry particle, its application widely, from milk powder manufacture develop into doctor
Nearly all processing such as medicine, chemical industry, catalyst, fuel, environmental protection and production field.Centrifugal spray drying system be divided into it is open with
Two kinds of enclosed, at present the country use open spray drying system in a large number, but when running into material liquid by solid and organic molten
Agent is constituted, it is desirable to which organic solvent is all reclaimed, the poisonous solid, powdery product of drying, does not allow abnormal smells from the patient and particulate matter effusion dirty
Dye environment and recycling thermophore need to select close type circulation spray drying system when reducing economic input.Enclosed is followed
Ring drying system is mainly by drying machine main body, feeding system, circulating fan and pipe-line system, online oxygen concentration analyser, receipts
A few part compositions of collecting system, retracting device, heating system.At present, people are for the research master of close type circulation spray drying system
Concentrate in overall cyclic drying systematic research, and for material liquid is being dried liquid of the indoor dry run through atomization
Then rarely people is related to the real-time concentration of drop and dried material.For the measurement of the granule density of close type circulation spray drying system
Can be used to be optimized the structure of spray-drying installation, reduce material wall sticking phenomenon, recycle thermophore, reduce fund
Input, increases spray-drying efficiency.
The content of the invention
The technical problem to be solved is the defect for overcoming prior art, there is provided a kind of closed cycle spray is dried
System tracer method granule density measuring system, simply and easily can be tracked measurement to being dried indoor granule density.
To solve above-mentioned technical problem, the present invention provides a kind of close type circulation spray drying system tracer method granule density and surveys
Amount system, including LASER Light Source, aluminium powder colloid, image collecting device and spray drying system；The spray drying system includes
Scroll casing type hot air distributor, nebulizer, material liquid import, hothouse, carrying object loop exit and material outlet；The hothouse
For the chamber of a closing, top is cylinder, and bottom is cone, sets heat transfer medium circuit and go out on the bottom chamber locular wall of cylinder
Mouthful, the bottom opening of cone is material outlet；The center of top of the cylinder opens up material liquid import；The scroll casing type heat
Wind distributor 2 is installed on the top of hothouse, and positioned at the surface of material liquid import, for importing carrying object and by carrying object
Flowing is changed into rotary wind；The nebulizer is located at the top position inside hothouse；The LASER Light Source is located at the one of hothouse
Side, is illuminated to being dried fluid inside；Described image harvester be located at hothouse opposite side, LASER Light Source it is just right
Face, the position of the fluid trace particle aluminium powder illuminated for recording laser light source；The aluminium powder colloid is mixed with solvent fluid
Material liquid is formed, and nebulizer is delivered to via material liquid import.
Aforesaid LASER Light Source is arc light source.
Aforesaid LASER Light Source has three groups, accordingly three image collecting devices of configuration, LASER Light Source and image collector
Put it is adjacent two-by-two be evenly distributed on around hothouse, and ensure every group of LASER Light Source just to an image collecting device.
The light that aforesaid LASER Light Source sends is directional light.
It is that pure white surface is used to receive the laser that hothouse transmission comes that aforesaid image collecting device receives laser side.
Aforesaid hothouse selects transparent material.
Aforesaid hothouse is from large diameter cylinder as chamber.
Beneficial effects of the present invention：
1. measurement can be tracked to being dried indoor granule density simply and easily.
2., for the measurement of running orbit can be used to optimizing drying system structure, the viscous wall of material is reduced.
Description of the drawings
Fig. 1 is the measuring system overall structure figure of the present invention；
Fig. 2 is the measuring system top view of the present invention；
In figure：1- material liquid imports, 2- scroll casing type hot air distributors, 3- nebulizers, 4-1 ~ 4-3 LASER Light Sources, 5-1 ~ 5-3 images
Harvester, the outlet of 6- heat transfer medium circuits, 7- material outlets, 8- hothouses.
Specific embodiment
The invention will be further described below.Following examples are only used for the technical side for clearly illustrating the present invention
Case, and can not be limited the scope of the invention with this.
As shown in figure 1, the close type circulation spray drying system tracer method granule density measuring system of the present invention, including laser
Light source 4, aluminium powder colloid, image collecting device 5, solvent fluid and spray drying system.
Specifically, spray drying system includes scroll casing type hot air distributor 2, nebulizer 3, material liquid import 1, hothouse 8,
Carrying object loop exit 6 and material outlet 7.Hothouse 8 is the chamber of a closing, and top is cylinder, and bottom is cone, circle
Heat transfer medium circuit outlet 6 is set on the bottom chamber locular wall of cylinder, the bottom opening of cone is material outlet 7.The top of cylinder
Central authorities open up material liquid import 1.Scroll casing type hot air distributor 2 is installed on the top of hothouse, and positioned at material liquid import 1 just
Top, for importing carrying object and carrying object flowing being changed into rotary wind.Nebulizer 3 is located at the top position inside hothouse.
Aluminium powder colloid is mixed to form material liquid with solvent fluid, is delivered to nebulizer 3 via material liquid import 1.
Further, LASER Light Source 4 is arc light source, positioned at the side of hothouse 8, diameter of the width for hothouse 8, figure
As harvester 5 is located at the opposite side of hothouse 8, the right opposite of arc light source.
As shown in Fig. 2 LASER Light Source has three groups of 4-1,4-2,4-3, corresponding configuration three image collecting device 5-1,5-
2,5-3, LASER Light Source and image collecting device are adjacent two-by-two to be evenly distributed on around hothouse 8, it is ensured that every group of laser light
Source just to an image collecting device, from comprehensive analysis granule density on three directions.
Preferably, the light that LASER Light Source sends is directional light, reflexes to other image acquisition to reduce light Jing aluminium powders surface
Phenomenon on device.It is that pure white surface is used to receive the laser that transmission comes that image collecting device receives laser side.
Preferably, hothouse 8 selects transparent material, it is ensured that the directional light that LASER Light Source sends is by the parallel photograph in hothouse side
It is mapped on the image collecting device of opposite side right opposite.Hothouse 8 selects larger diameter, reduces wall sticking phenomenon to measurement result
Affect.
The specific work process of the present invention is as follows：After current-carrying gas heating, Jing scroll casing types hot air distributor 2 enters hothouse
8, aluminium powder colloid is mixed to form material liquid with solvent fluid and enters the centrifugal energy nozzle of nebulizer 3 by a high speed by material liquid import 1
The nebulizer 3 of rotation is atomized into drop, and the flow of material liquid gradually increases by 0, can be used to observe raw material flow quantity to
The impact of grain concentration.Current-carrying gas are converted into rotation hot blast, hot current-carrying gas of the drop in rotation at scroll casing type hot air distributor 2
Caloic exchange is completed with gas motion and in hothouse 8 under body effect, is gone out from materials at bottom of tower by dried granular material
Mouth 7 is discharged, and the flow gas for being evaporated mix current-carrying gas 6 discharge of Jing heat transfer medium circuits outlet under fan action and reclaimed
Circulation.In whole process, LASER Light Source 4 sends directional light and is irradiated in the material liquid of 8 atomization mistake of hothouse, due to aluminium powder
Opaqueness, can be shown by the aluminum particle of parallel light irradiation, by just collecting aluminum to the image collecting device of position
The position of powder, three groups of light sources of comprehensive analysis and image collecting device judge the granule density of droplets of feed.
The above is only the preferred embodiment of the present invention, it is noted that for the ordinary skill people of the art
For member, on the premise of without departing from the technology of the present invention principle, some improvement and deformation can also be made, these improve and deform
Also should be regarded as protection scope of the present invention.
Claims (7)
1. a kind of close type circulation spray drying system tracer method granule density measuring system, it is characterised in that including LASER Light Source,
Aluminium powder colloid, image collecting device and spray drying system；The spray drying system includes scroll casing type hot air distributor, atomization
Device, material liquid import, hothouse, carrying object loop exit and material outlet；The hothouse is the chamber of a closing, and top is
Cylinder, bottom are cone, and heat transfer medium circuit outlet is set on the bottom chamber locular wall of cylinder, and the bottom opening of cone is thing
Material outlet；The center of top of the cylinder opens up material liquid import；The scroll casing type hot air distributor 2 is installed on hothouse
Top, and positioned at the surface of material liquid import, for importing carrying object and carrying object flowing being changed into rotary wind；The atomization
Device is located at the top position inside hothouse；The LASER Light Source is located at the side of hothouse, shines to being dried fluid inside
It is bright；Described image harvester is located at the opposite side of hothouse, and the right opposite of LASER Light Source is illuminated for recording laser light source
Fluid trace particle aluminium powder position；The aluminium powder colloid is mixed to form material liquid with solvent fluid, via material liquid import
It is delivered to nebulizer.
2. a kind of close type circulation spray drying system tracer method granule density measuring system according to claim 1, which is special
Levy and be, the LASER Light Source is arc light source.
3. a kind of close type circulation spray drying system tracer method granule density measuring system according to claim 2, which is special
Levy and be, the LASER Light Source there are three groups, accordingly three image collecting devices of configuration, LASER Light Source and image collecting device two
Two it is adjacent be evenly distributed on around hothouse, and ensure every group of LASER Light Source just to an image collecting device.
4. a kind of close type circulation spray drying system tracer method granule density measuring system according to claim 3, which is special
Levy and be, the light that the LASER Light Source sends is directional light.
5. a kind of close type circulation spray drying system tracer method granule density measuring system according to claim 1, which is special
Levy and be, it is that pure white surface is used to receive the laser that hothouse transmission comes that described image harvester receives laser side.
6. a kind of close type circulation spray drying system tracer method granule density measuring system according to claim 1, which is special
Levy and be, the hothouse selects transparent material.
7. a kind of close type circulation spray drying system tracer method granule density measuring system according to claim 1, which is special
Levy and be, the hothouse is from large diameter cylinder as chamber.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201611202467.XA CN106596364A (en) | 2016-12-23 | 2016-12-23 | Tracer method based particle concentration measurement system for closed cyclic spray drying system |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201611202467.XA CN106596364A (en) | 2016-12-23 | 2016-12-23 | Tracer method based particle concentration measurement system for closed cyclic spray drying system |
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| Publication Number | Publication Date |
|---|---|
| CN106596364A true CN106596364A (en) | 2017-04-26 |
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Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN201611202467.XA Pending CN106596364A (en) | 2016-12-23 | 2016-12-23 | Tracer method based particle concentration measurement system for closed cyclic spray drying system |
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| CN (1) | CN106596364A (en) |
Cited By (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN109269952A (en) * | 2018-10-16 | 2019-01-25 | 东南大学 | A kind of measuring device and method of filamentary material three dimensional particles concentration information in air flow bed rectangle riser |
| CN114699503A (en) * | 2022-03-30 | 2022-07-05 | 湖南东健药业有限公司 | Spray drying method for Chinese medicinal extract and preparation method of granule |
| CN114768277A (en) * | 2022-04-29 | 2022-07-22 | 湖南东健药业有限公司 | Spray drying system for traditional Chinese medicine preparation |
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| WO1993023129A1 (en) * | 1992-05-21 | 1993-11-25 | Niro Holding A/S | A method and an apparatus for minimizing deposits in a drying chamber |
| WO2011063808A1 (en) * | 2009-11-24 | 2011-06-03 | Gea Process Engineering A/S | A method of monitoring a spray dryer and a spray dryer comprising one or more infrared cameras |
| CN104535563A (en) * | 2014-12-25 | 2015-04-22 | 浙江大学 | Detection system for spraying droplet density and size capable of being well used under both dry and wet environments, preparation method and detection method |
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2016
- 2016-12-23 CN CN201611202467.XA patent/CN106596364A/en active Pending
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|---|---|---|---|---|
| WO1993023129A1 (en) * | 1992-05-21 | 1993-11-25 | Niro Holding A/S | A method and an apparatus for minimizing deposits in a drying chamber |
| WO2011063808A1 (en) * | 2009-11-24 | 2011-06-03 | Gea Process Engineering A/S | A method of monitoring a spray dryer and a spray dryer comprising one or more infrared cameras |
| CN105582683A (en) * | 2014-10-21 | 2016-05-18 | 中国科学院上海药物研究所 | Dynamically-monitored high-frequency ultrasound atomized particle preparation system |
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| Title |
|---|
| MACIEJ JASKULSKI 等: ""PARTICLE SIZE DISTRIBUTION AND MOISTURE CONTENT INLINE MEASUREMENT SYSTEMS FOR THE SPRAY DRYERS"", 《THE 22ND POLISH CONFERENCE OF CHEMICAL AND PROCESS ENGINEERING》 * |
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Cited By (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN109269952A (en) * | 2018-10-16 | 2019-01-25 | 东南大学 | A kind of measuring device and method of filamentary material three dimensional particles concentration information in air flow bed rectangle riser |
| CN114699503A (en) * | 2022-03-30 | 2022-07-05 | 湖南东健药业有限公司 | Spray drying method for Chinese medicinal extract and preparation method of granule |
| CN114768277A (en) * | 2022-04-29 | 2022-07-22 | 湖南东健药业有限公司 | Spray drying system for traditional Chinese medicine preparation |
| CN114768277B (en) * | 2022-04-29 | 2023-09-05 | 湖南东健药业有限公司 | Spray drying system for traditional Chinese medicine preparation |
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Application publication date: 20170426 |