CN106590186A - Waterproof and flame-retarding coating for fabric and preparation method thereof - Google Patents

Waterproof and flame-retarding coating for fabric and preparation method thereof Download PDF

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Publication number
CN106590186A
CN106590186A CN201611130467.3A CN201611130467A CN106590186A CN 106590186 A CN106590186 A CN 106590186A CN 201611130467 A CN201611130467 A CN 201611130467A CN 106590186 A CN106590186 A CN 106590186A
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China
Prior art keywords
parts
priming coat
following components
cross
coating
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CN201611130467.3A
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Chinese (zh)
Inventor
叶冬明
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Suzhou Chen Heng Weaves Co Ltd
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Suzhou Chen Heng Weaves Co Ltd
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Priority to CN201611130467.3A priority Critical patent/CN106590186A/en
Publication of CN106590186A publication Critical patent/CN106590186A/en
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    • C—CHEMISTRY; METALLURGY
    • C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
    • C09D—COATING COMPOSITIONS, e.g. PAINTS, VARNISHES OR LACQUERS; FILLING PASTES; CHEMICAL PAINT OR INK REMOVERS; INKS; CORRECTING FLUIDS; WOODSTAINS; PASTES OR SOLIDS FOR COLOURING OR PRINTING; USE OF MATERIALS THEREFOR
    • C09D123/00—Coating compositions based on homopolymers or copolymers of unsaturated aliphatic hydrocarbons having only one carbon-to-carbon double bond; Coating compositions based on derivatives of such polymers
    • C09D123/02—Coating compositions based on homopolymers or copolymers of unsaturated aliphatic hydrocarbons having only one carbon-to-carbon double bond; Coating compositions based on derivatives of such polymers not modified by chemical after-treatment
    • C09D123/04—Homopolymers or copolymers of ethene
    • C09D123/06—Polyethene
    • C—CHEMISTRY; METALLURGY
    • C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08K—Use of inorganic or non-macromolecular organic substances as compounding ingredients
    • C08K13/00—Use of mixtures of ingredients not covered by one single of the preceding main groups, each of these compounds being essential
    • C08K13/02—Organic and inorganic ingredients
    • C—CHEMISTRY; METALLURGY
    • C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08K—Use of inorganic or non-macromolecular organic substances as compounding ingredients
    • C08K3/00—Use of inorganic substances as compounding ingredients
    • C08K3/18—Oxygen-containing compounds, e.g. metal carbonyls
    • C08K3/20—Oxides; Hydroxides
    • C08K3/22—Oxides; Hydroxides of metals
    • C—CHEMISTRY; METALLURGY
    • C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08K—Use of inorganic or non-macromolecular organic substances as compounding ingredients
    • C08K3/00—Use of inorganic substances as compounding ingredients
    • C08K3/30—Sulfur-, selenium- or tellurium-containing compounds
    • C—CHEMISTRY; METALLURGY
    • C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08K—Use of inorganic or non-macromolecular organic substances as compounding ingredients
    • C08K3/00—Use of inorganic substances as compounding ingredients
    • C08K3/32—Phosphorus-containing compounds
    • C—CHEMISTRY; METALLURGY
    • C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08K—Use of inorganic or non-macromolecular organic substances as compounding ingredients
    • C08K3/00—Use of inorganic substances as compounding ingredients
    • C08K3/34—Silicon-containing compounds
    • C—CHEMISTRY; METALLURGY
    • C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08K—Use of inorganic or non-macromolecular organic substances as compounding ingredients
    • C08K5/00—Use of organic ingredients
    • C08K5/49—Phosphorus-containing compounds
    • C08K5/51—Phosphorus bound to oxygen
    • C08K5/52—Phosphorus bound to oxygen only
    • C08K5/521—Esters of phosphoric acids, e.g. of H3PO4
    • C—CHEMISTRY; METALLURGY
    • C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
    • C09D—COATING COMPOSITIONS, e.g. PAINTS, VARNISHES OR LACQUERS; FILLING PASTES; CHEMICAL PAINT OR INK REMOVERS; INKS; CORRECTING FLUIDS; WOODSTAINS; PASTES OR SOLIDS FOR COLOURING OR PRINTING; USE OF MATERIALS THEREFOR
    • C09D163/00—Coating compositions based on epoxy resins; Coating compositions based on derivatives of epoxy resins
    • C—CHEMISTRY; METALLURGY
    • C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
    • C09D—COATING COMPOSITIONS, e.g. PAINTS, VARNISHES OR LACQUERS; FILLING PASTES; CHEMICAL PAINT OR INK REMOVERS; INKS; CORRECTING FLUIDS; WOODSTAINS; PASTES OR SOLIDS FOR COLOURING OR PRINTING; USE OF MATERIALS THEREFOR
    • C09D175/00—Coating compositions based on polyureas or polyurethanes; Coating compositions based on derivatives of such polymers
    • C09D175/04—Polyurethanes
    • C—CHEMISTRY; METALLURGY
    • C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
    • C09D—COATING COMPOSITIONS, e.g. PAINTS, VARNISHES OR LACQUERS; FILLING PASTES; CHEMICAL PAINT OR INK REMOVERS; INKS; CORRECTING FLUIDS; WOODSTAINS; PASTES OR SOLIDS FOR COLOURING OR PRINTING; USE OF MATERIALS THEREFOR
    • C09D5/00—Coating compositions, e.g. paints, varnishes or lacquers, characterised by their physical nature or the effects produced; Filling pastes
    • C09D5/18—Fireproof paints including high temperature resistant paints
    • C—CHEMISTRY; METALLURGY
    • C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
    • C09D—COATING COMPOSITIONS, e.g. PAINTS, VARNISHES OR LACQUERS; FILLING PASTES; CHEMICAL PAINT OR INK REMOVERS; INKS; CORRECTING FLUIDS; WOODSTAINS; PASTES OR SOLIDS FOR COLOURING OR PRINTING; USE OF MATERIALS THEREFOR
    • C09D7/00—Features of coating compositions, not provided for in group C09D5/00; Processes for incorporating ingredients in coating compositions
    • C09D7/40—Additives
    • C09D7/60—Additives non-macromolecular
    • C09D7/61—Additives non-macromolecular inorganic
    • C—CHEMISTRY; METALLURGY
    • C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
    • C09D—COATING COMPOSITIONS, e.g. PAINTS, VARNISHES OR LACQUERS; FILLING PASTES; CHEMICAL PAINT OR INK REMOVERS; INKS; CORRECTING FLUIDS; WOODSTAINS; PASTES OR SOLIDS FOR COLOURING OR PRINTING; USE OF MATERIALS THEREFOR
    • C09D7/00—Features of coating compositions, not provided for in group C09D5/00; Processes for incorporating ingredients in coating compositions
    • C09D7/40—Additives
    • C09D7/60—Additives non-macromolecular
    • C09D7/63—Additives non-macromolecular organic
    • C—CHEMISTRY; METALLURGY
    • C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
    • C09D—COATING COMPOSITIONS, e.g. PAINTS, VARNISHES OR LACQUERS; FILLING PASTES; CHEMICAL PAINT OR INK REMOVERS; INKS; CORRECTING FLUIDS; WOODSTAINS; PASTES OR SOLIDS FOR COLOURING OR PRINTING; USE OF MATERIALS THEREFOR
    • C09D7/00—Features of coating compositions, not provided for in group C09D5/00; Processes for incorporating ingredients in coating compositions
    • C09D7/40—Additives
    • C09D7/70—Additives characterised by shape, e.g. fibres, flakes or microspheres
    • D—TEXTILES; PAPER
    • D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
    • D06N—WALL, FLOOR, OR LIKE COVERING MATERIALS, e.g. LINOLEUM, OILCLOTH, ARTIFICIAL LEATHER, ROOFING FELT, CONSISTING OF A FIBROUS WEB COATED WITH A LAYER OF MACROMOLECULAR MATERIAL; FLEXIBLE SHEET MATERIAL NOT OTHERWISE PROVIDED FOR
    • D06N3/00—Artificial leather, oilcloth or other material obtained by covering fibrous webs with macromolecular material, e.g. resins, rubber or derivatives thereof
    • D—TEXTILES; PAPER
    • D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
    • D06N—WALL, FLOOR, OR LIKE COVERING MATERIALS, e.g. LINOLEUM, OILCLOTH, ARTIFICIAL LEATHER, ROOFING FELT, CONSISTING OF A FIBROUS WEB COATED WITH A LAYER OF MACROMOLECULAR MATERIAL; FLEXIBLE SHEET MATERIAL NOT OTHERWISE PROVIDED FOR
    • D06N3/00—Artificial leather, oilcloth or other material obtained by covering fibrous webs with macromolecular material, e.g. resins, rubber or derivatives thereof
    • D06N3/0056—Artificial leather, oilcloth or other material obtained by covering fibrous webs with macromolecular material, e.g. resins, rubber or derivatives thereof characterised by the compounding ingredients of the macro-molecular coating
    • D06N3/0061—Organic fillers or organic fibrous fillers, e.g. ground leather waste, wood bark, cork powder, vegetable flour; Other organic compounding ingredients; Post-treatment with organic compounds
    • D—TEXTILES; PAPER
    • D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
    • D06N—WALL, FLOOR, OR LIKE COVERING MATERIALS, e.g. LINOLEUM, OILCLOTH, ARTIFICIAL LEATHER, ROOFING FELT, CONSISTING OF A FIBROUS WEB COATED WITH A LAYER OF MACROMOLECULAR MATERIAL; FLEXIBLE SHEET MATERIAL NOT OTHERWISE PROVIDED FOR
    • D06N3/00—Artificial leather, oilcloth or other material obtained by covering fibrous webs with macromolecular material, e.g. resins, rubber or derivatives thereof
    • D06N3/0056—Artificial leather, oilcloth or other material obtained by covering fibrous webs with macromolecular material, e.g. resins, rubber or derivatives thereof characterised by the compounding ingredients of the macro-molecular coating
    • D06N3/0063—Inorganic compounding ingredients, e.g. metals, carbon fibres, Na2CO3, metal layers; Post-treatment with inorganic compounds
    • D—TEXTILES; PAPER
    • D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
    • D06N—WALL, FLOOR, OR LIKE COVERING MATERIALS, e.g. LINOLEUM, OILCLOTH, ARTIFICIAL LEATHER, ROOFING FELT, CONSISTING OF A FIBROUS WEB COATED WITH A LAYER OF MACROMOLECULAR MATERIAL; FLEXIBLE SHEET MATERIAL NOT OTHERWISE PROVIDED FOR
    • D06N3/00—Artificial leather, oilcloth or other material obtained by covering fibrous webs with macromolecular material, e.g. resins, rubber or derivatives thereof
    • D06N3/04—Artificial leather, oilcloth or other material obtained by covering fibrous webs with macromolecular material, e.g. resins, rubber or derivatives thereof with macromolecular compounds obtained by reactions only involving carbon-to-carbon unsaturated bonds
    • D06N3/10—Artificial leather, oilcloth or other material obtained by covering fibrous webs with macromolecular material, e.g. resins, rubber or derivatives thereof with macromolecular compounds obtained by reactions only involving carbon-to-carbon unsaturated bonds with styrene-butadiene copolymerisation products or other synthetic rubbers or elastomers except polyurethanes
    • D—TEXTILES; PAPER
    • D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
    • D06N—WALL, FLOOR, OR LIKE COVERING MATERIALS, e.g. LINOLEUM, OILCLOTH, ARTIFICIAL LEATHER, ROOFING FELT, CONSISTING OF A FIBROUS WEB COATED WITH A LAYER OF MACROMOLECULAR MATERIAL; FLEXIBLE SHEET MATERIAL NOT OTHERWISE PROVIDED FOR
    • D06N3/00—Artificial leather, oilcloth or other material obtained by covering fibrous webs with macromolecular material, e.g. resins, rubber or derivatives thereof
    • D06N3/12—Artificial leather, oilcloth or other material obtained by covering fibrous webs with macromolecular material, e.g. resins, rubber or derivatives thereof with macromolecular compounds obtained otherwise than by reactions only involving carbon-to-carbon unsaturated bonds, e.g. gelatine proteins
    • D—TEXTILES; PAPER
    • D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
    • D06N—WALL, FLOOR, OR LIKE COVERING MATERIALS, e.g. LINOLEUM, OILCLOTH, ARTIFICIAL LEATHER, ROOFING FELT, CONSISTING OF A FIBROUS WEB COATED WITH A LAYER OF MACROMOLECULAR MATERIAL; FLEXIBLE SHEET MATERIAL NOT OTHERWISE PROVIDED FOR
    • D06N3/00—Artificial leather, oilcloth or other material obtained by covering fibrous webs with macromolecular material, e.g. resins, rubber or derivatives thereof
    • D06N3/12—Artificial leather, oilcloth or other material obtained by covering fibrous webs with macromolecular material, e.g. resins, rubber or derivatives thereof with macromolecular compounds obtained otherwise than by reactions only involving carbon-to-carbon unsaturated bonds, e.g. gelatine proteins
    • D06N3/14—Artificial leather, oilcloth or other material obtained by covering fibrous webs with macromolecular material, e.g. resins, rubber or derivatives thereof with macromolecular compounds obtained otherwise than by reactions only involving carbon-to-carbon unsaturated bonds, e.g. gelatine proteins with polyurethanes
    • D06N3/142—Artificial leather, oilcloth or other material obtained by covering fibrous webs with macromolecular material, e.g. resins, rubber or derivatives thereof with macromolecular compounds obtained otherwise than by reactions only involving carbon-to-carbon unsaturated bonds, e.g. gelatine proteins with polyurethanes mixture of polyurethanes with other resins in the same layer
    • D06N3/144—Artificial leather, oilcloth or other material obtained by covering fibrous webs with macromolecular material, e.g. resins, rubber or derivatives thereof with macromolecular compounds obtained otherwise than by reactions only involving carbon-to-carbon unsaturated bonds, e.g. gelatine proteins with polyurethanes mixture of polyurethanes with other resins in the same layer with polyurethane and polymerisation products, e.g. acrylics, PVC
    • D—TEXTILES; PAPER
    • D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
    • D06N—WALL, FLOOR, OR LIKE COVERING MATERIALS, e.g. LINOLEUM, OILCLOTH, ARTIFICIAL LEATHER, ROOFING FELT, CONSISTING OF A FIBROUS WEB COATED WITH A LAYER OF MACROMOLECULAR MATERIAL; FLEXIBLE SHEET MATERIAL NOT OTHERWISE PROVIDED FOR
    • D06N3/00—Artificial leather, oilcloth or other material obtained by covering fibrous webs with macromolecular material, e.g. resins, rubber or derivatives thereof
    • D06N3/12—Artificial leather, oilcloth or other material obtained by covering fibrous webs with macromolecular material, e.g. resins, rubber or derivatives thereof with macromolecular compounds obtained otherwise than by reactions only involving carbon-to-carbon unsaturated bonds, e.g. gelatine proteins
    • D06N3/14—Artificial leather, oilcloth or other material obtained by covering fibrous webs with macromolecular material, e.g. resins, rubber or derivatives thereof with macromolecular compounds obtained otherwise than by reactions only involving carbon-to-carbon unsaturated bonds, e.g. gelatine proteins with polyurethanes
    • D06N3/145—Artificial leather, oilcloth or other material obtained by covering fibrous webs with macromolecular material, e.g. resins, rubber or derivatives thereof with macromolecular compounds obtained otherwise than by reactions only involving carbon-to-carbon unsaturated bonds, e.g. gelatine proteins with polyurethanes two or more layers of polyurethanes
    • C—CHEMISTRY; METALLURGY
    • C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08K—Use of inorganic or non-macromolecular organic substances as compounding ingredients
    • C08K3/00—Use of inorganic substances as compounding ingredients
    • C08K3/18—Oxygen-containing compounds, e.g. metal carbonyls
    • C08K3/20—Oxides; Hydroxides
    • C08K3/22—Oxides; Hydroxides of metals
    • C08K2003/2237—Oxides; Hydroxides of metals of titanium
    • C08K2003/2241—Titanium dioxide
    • C—CHEMISTRY; METALLURGY
    • C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08K—Use of inorganic or non-macromolecular organic substances as compounding ingredients
    • C08K3/00—Use of inorganic substances as compounding ingredients
    • C08K3/30—Sulfur-, selenium- or tellurium-containing compounds
    • C08K2003/3045—Sulfates
    • C—CHEMISTRY; METALLURGY
    • C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08K—Use of inorganic or non-macromolecular organic substances as compounding ingredients
    • C08K3/00—Use of inorganic substances as compounding ingredients
    • C08K3/32—Phosphorus-containing compounds
    • C08K2003/321—Phosphates
    • C08K2003/324—Alkali metal phosphate
    • D—TEXTILES; PAPER
    • D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
    • D06N—WALL, FLOOR, OR LIKE COVERING MATERIALS, e.g. LINOLEUM, OILCLOTH, ARTIFICIAL LEATHER, ROOFING FELT, CONSISTING OF A FIBROUS WEB COATED WITH A LAYER OF MACROMOLECULAR MATERIAL; FLEXIBLE SHEET MATERIAL NOT OTHERWISE PROVIDED FOR
    • D06N2209/00—Properties of the materials
    • D06N2209/06—Properties of the materials having thermal properties
    • D06N2209/067—Flame resistant, fire resistant
    • D—TEXTILES; PAPER
    • D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
    • D06N—WALL, FLOOR, OR LIKE COVERING MATERIALS, e.g. LINOLEUM, OILCLOTH, ARTIFICIAL LEATHER, ROOFING FELT, CONSISTING OF A FIBROUS WEB COATED WITH A LAYER OF MACROMOLECULAR MATERIAL; FLEXIBLE SHEET MATERIAL NOT OTHERWISE PROVIDED FOR
    • D06N2209/00—Properties of the materials
    • D06N2209/12—Permeability or impermeability properties
    • D06N2209/126—Permeability to liquids, absorption
    • D06N2209/128—Non-permeable
    • D—TEXTILES; PAPER
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    • D06N—WALL, FLOOR, OR LIKE COVERING MATERIALS, e.g. LINOLEUM, OILCLOTH, ARTIFICIAL LEATHER, ROOFING FELT, CONSISTING OF A FIBROUS WEB COATED WITH A LAYER OF MACROMOLECULAR MATERIAL; FLEXIBLE SHEET MATERIAL NOT OTHERWISE PROVIDED FOR
    • D06N2209/00—Properties of the materials
    • D06N2209/16—Properties of the materials having other properties
    • D06N2209/1678—Resistive to light or to UV

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  • Chemical & Material Sciences (AREA)
  • Engineering & Computer Science (AREA)
  • Organic Chemistry (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Life Sciences & Earth Sciences (AREA)
  • Wood Science & Technology (AREA)
  • Textile Engineering (AREA)
  • Materials Engineering (AREA)
  • Polymers & Plastics (AREA)
  • Health & Medical Sciences (AREA)
  • Medicinal Chemistry (AREA)
  • Dispersion Chemistry (AREA)
  • Inorganic Chemistry (AREA)
  • Treatments For Attaching Organic Compounds To Fibrous Goods (AREA)
  • Laminated Bodies (AREA)
  • Fireproofing Substances (AREA)

Abstract

The invention provides a waterproof and flame-retarding coating for a fabric. The waterproof and flame-retarding coating is composed of a first bottom coating, a second bottom coating and a third bottom coating by overlapping, wherein the first bottom coating is prepared from the following components in parts by mass: 10 to 15 parts of polyurethane, 13 to 17 parts of carbon fiber powder, 5 to 13 parts of antimony trioxide, 15 to 20 parts of low-density polyethylene resin, 3 to 9 parts of polytetrafluoroethylene, 3 to 5 parts of an anionic surfactant, 1 to 3 parts of a thickening agent and 1 to 3 parts of an auxiliary agent; the second bottom coating is prepared from the following components in parts by mass: 18 to 26 parts of polyurethane emulsion, 3 to 7 parts of calcium sulfate powder, 10 to 14 parts of sodium tripolyphosphate, 2 to 6 parts of nano titanium dioxide, 3 to 7 parts of tributyl phosphate and 10 to 15 parts of an organic solvent; the third bottom coating is prepared from the following components in parts by mass: 15 to 22 parts of epoxy resin, 11 to 16 parts of diethyl phthalate, 8 to 15 parts of polychloroprene rubber latex, 5 to 10 parts of sodium n-butyl naphthalene sulfonate, 1 to 3 parts of phosphate esters flame-retarding oil, 5 to 9 parts of stearic acid, 6 to 8 parts of magnesium hydroxide and 3 to 7 parts of a cross-linking agent. The waterproof and flame-retarding coating for the fabric can both consider a waterproof property and a flame-retarding property of the fabric.

Description

A kind of fabric water proof fire retardant coating and preparation method thereof
Technical field
The invention belongs to textile fabric coatings technical field, and in particular to a kind of fabric water proof fire retardant coating.
Background technology
General garment material is combustibles, meets fire and easily burns, and causes damage to property, therefore in recent years to fire retardant Material research is relatively more, and the fire-retardant method or material itself using the addition fire retardant inside material of general fabric has fire-retardant Structure, can be with self-extinguishment when running into flame, but water resistance is particularly poor, and the water-proof air-moisture-permeable film thickness on cloth is very It is thin therefore infeasible using the method for addition fire retardant, losing issue, and the poor performance of material are there is, existing coating is produced Product have that fire-retardant and air permeable waterproof can not be taken into account.
The content of the invention
The technical problem to be solved is the shortcoming for overcoming prior art, there is provided a kind of fabric water proof fire retardant Coating, takes into account water proofing property and anti-flammability.
The present invention solves the technical scheme of above technical problem：A kind of fabric water proof fire retardant coating is provided, it is described anti- Water flame retardant coating is made up of the superposition of the first priming coat, the second priming coat and the 3rd priming coat, and first priming coat presses its matter Amount number meter includes following components：Polyurethane 10-15 parts, dimethyl methyl phosphonate 3-7 parts, nano silicon 2-5 parts, carbon Fiber powder 13-17 parts, antimony oxide 5-13 parts, ldpe resin 15-20 parts, politef 3-9 parts, it is cloudy from Sub- surfactant 3-5 parts, thickening agent 1-3 parts, auxiliary agent 1-3 parts；
Second priming coat is based on its mass fraction including following components：Polyaminoester emulsion 18-26 parts, calcium sulphate powders 3-7 Part, sodium tripolyphosphate 10-14 parts, nano titanium oxide 2-6 part TRI N BUTYL PHOSPHATE 3-7 parts, prodan 3-5 parts have Machine solvent 10-15 parts, cross-linked binder 2-6 part；
3rd priming coat is based on its mass fraction including following components：Epoxy resin 15-22, diethyl phthalate 11-16 parts, polychloroprene latex 8-15 part, normal-butyl sodium naphthalene sulfonate 5-10 parts, phosphoric acid ester flame retardant oil 1-3 parts, stearic acid 5-9 parts, magnesium hydroxide 6-8 parts, cross-linking agent 3-7 parts.
Further limits scheme of the invention：
Aforesaid first priming coat is based on its mass fraction including following components：Polyurethane 12-15 parts, dimethyl methyl phosphonate 3-5 parts, nano silicon 2-4 parts, carbon fiber powder 13-15 parts, antimony oxide 5-10 parts, ldpe resin 15- 17 parts, politef 3-6 parts, anion surfactant 3-4 parts, thickening agent 1-2 parts, auxiliary agent 1-2 parts；
Second priming coat is based on its mass fraction including following components：Polyaminoester emulsion 22-26 parts, calcium sulphate powders 3-5 part, Sodium tripolyphosphate 10-12 parts, nano titanium oxide 4-6 part TRI N BUTYL PHOSPHATE 3-5 parts, prodan 3-4 parts are organic Solvent 10-12 parts, cross-linked binder 2-4 part；
3rd priming coat is based on its mass fraction including following components：Epoxy resin 18-22, diethyl phthalate 11-13 Part, polychloroprene latex 8-12 part, normal-butyl sodium naphthalene sulfonate 5-8 parts, phosphoric acid ester flame retardant oil 1-2 parts；Stearic acid 5-7 parts, Magnesium hydroxide 6-7 parts, cross-linking agent 3-5 parts.
Aforesaid first priming coat is based on its mass fraction including following components：Polyurethane 12-15 parts, methylphosphonic acid diformazan Ester 3-5 parts, nano silicon 2-4 parts, carbon fiber powder 13-15 parts, antimony oxide 5-10 parts, ldpe resin 15-17 parts, politef 3-6 parts, anion surfactant 3-4 parts, thickening agent 1-2 parts, auxiliary agent 1-2 parts；
Second priming coat is based on its mass fraction including following components：Polyaminoester emulsion 22-26 parts, calcium sulphate powders 3-5 Part, sodium tripolyphosphate 10-12 parts, nano titanium oxide 4-6 part TRI N BUTYL PHOSPHATE 3-5 parts, prodan 3-4 parts have Machine solvent 10-12 parts, cross-linked binder 2-3 part.
3rd priming coat is based on its mass fraction including following components：Epoxy resin 18-22, diethyl phthalate 11-13 parts, polychloroprene latex 8-12 part, normal-butyl sodium naphthalene sulfonate 5-8 parts, phosphoric acid ester flame retardant oil 1-2 parts；Stearic acid 5- 7 parts, magnesium hydroxide 6-7 parts, cross-linking agent 3-5 parts.
Aforesaid thickening agent be methylcellulose, hydroxypropyl methyl cellulose or sodium carboxymethyl cellulose one of which or Various mixture.
Aforesaid cosolvent is butyl glycol ether or Propylene Glycol.
Aforesaid cross-linking agent is isocyanates cross-linking agent.
Aforesaid cross-linked binder by mass fraction agent include following components：4- isocyanatomethyls：18-23 Part, urethanes：18-25 parts, alpha-linolenic acid：3-5 parts, ethoxylated bisphenol A dimethylacrylates：3-7 parts, three hydroxyl first Base propane trimethyl acrylic ester：4-8 parts, butyl acrylate：3-9 parts, Crosslinkable Acrylic Polymer Emulsion：5-12 parts, 2- hydroxyls- 1,2- diphenylethans：2-6 parts, vinylacetate：1-3 parts.
Aforesaid fabric water proof fire retardant coating production is comprised the following steps：
Step one：Polyurethane, nano silicon, carbon fiber powder, ldpe resin are put into instead according to said ratio In answering kettle, stirred using agitator, speed controlling is heated simultaneously in 600-800r/min, stirring, and temperature is 40-60 DEG C, 45-60min is stirred, dimethyl methyl phosphonate, politef, antimony oxide are then placed in, continue to stir 60- 80min, temperature rises to 70-80 DEG C, and temperature successively adds anion surfactant, thickening agent and auxiliary agent after reaching reacts Kettle, stirs 2-3h, and temperature rises to 90-98 DEG C, is subsequently cooled to room temperature, and the slurry for obtaining is dried, and has made the first primary coat Layer；
Step 2;According to said ratio by polyaminoester emulsion, calcium sulphate powders, sodium tripolyphosphate, nano titanium oxide, tricresyl phosphate N-butyl, prodan, organic solvent and cross-linked binder are added sequentially in reactor, are stirred using agitator, speed Spend for 550-700r/min, stir 2-4h, temperature rises to 85-93 DEG C, is incubated 1-2h, is subsequently cooled to room temperature, then drying system Obtain the second priming coat；
Step 3：According to said ratio by epoxy resin, diethyl phthalate, phosphoric acid ester flame retardant oil, stearic acid and hydrogen Magnesium oxide is sequentially added in reactor, with 750-850r/min stirrings, stirs 1-2h, and temperature rises to 96-102 DEG C, then temperature 70-80 DEG C is cooled to, then polychloroprene latex, normal-butyl sodium naphthalene sulfonate and cross-linking agent are added, then temperature is added to 92- 98 DEG C, 2-3h is incubated, continues to stir with 300-400r/min, stir 3-4h, be subsequently cooled to room temperature, the slurry for obtaining is dried It is dry, make the 3rd priming coat；
Step 4：The first priming coat, the 2nd coating and the 3rd bottom bonding are combined in the presence of hot pressing, hot pressing combined temp For 180-200 DEG C, the time is 1-2min, and line pressure is 1.2-1.6 Kg/mm.
The invention has the beneficial effects as follows：The present invention adds antimony oxide, and itself has fire resistance, can be in burning When produce water composition, and play the role of isolating oxygen prevent fire burning, add phosphoric acid ester flame retardant oil can also play fire-retardant Effect, and can also improve the feel of fabric, add nano material so that coating structure is stable, improves the intensity of coating, Coating obtained in method prepared by the present invention is enabled to together with fabric takes into account water resistance with fire resistance, while also having There are Stability Analysis of Structures, good anti-ultraviolet ability.
Specific embodiment
Embodiment 1
The present embodiment provides a kind of fabric water proof fire retardant coating, is laminated by the first priming coat, the second priming coat and the 3rd primary coat Plus composition, the first priming coat is based on its mass fraction including following components：12 parts of polyurethane, 3 parts of dimethyl methyl phosphonate, 2 parts of nano silicon, 13 parts of carbon fiber powder, 7 parts of antimony oxide, 15 parts of ldpe resin, politef 4 Part, 3 parts of anion surfactant, 1 part of thickening agent, 1 part of butyl glycol ether；
Second priming coat is based on its mass fraction including following components：23 parts of polyaminoester emulsion, 3 parts of calcium sulphate powders, trimerization phosphorus 10 parts of sour sodium, 4 parts of nano titanium oxide, 3 parts of TRI N BUTYL PHOSPHATE, 3 parts of prodan, 10 parts of organic solvent, crosslinking 2 parts of binding agent；
3rd priming coat is based on its mass fraction including following components：Epoxy resin 18,11 parts of diethyl phthalate, polychlorostyrene 10 parts of butadiene latex, 6 parts of normal-butyl sodium naphthalene sulfonate, 1 part of phosphoric acid ester flame retardant oil；It is 5 parts of stearic acid, 6 parts of magnesium hydroxide, different 3 parts of cyanate cross-linking agent；
Thickening agent is the mixture of methylcellulose, hydroxypropyl methyl cellulose and sodium carboxymethyl cellulose；Cross-linked binder Include following components by mass fraction agent：4- isocyanatomethyls：20 parts, urethanes：22 parts, α-Caulis et Folium Lini Acid：3 parts, ethoxylated bisphenol A dimethylacrylates：4 parts, trimethylol-propane trimethacrylate：5 parts, acrylic acid fourth Ester：4 parts, Crosslinkable Acrylic Polymer Emulsion：7 parts, 2- hydroxyl -1,2- diphenylethans：3 parts, vinylacetate：2 parts.
The present embodiment fabric water proof fire retardant coating production is comprised the following steps：
Step one：Polyurethane, nano silicon, carbon fiber powder, ldpe resin are put into instead according to said ratio In answering kettle, stirred using agitator, speed controlling is heated simultaneously in 680r/min, stirring, temperature is 50 DEG C, stirring 55min, is then placed in dimethyl methyl phosphonate, politef, antimony oxide, continues to stir 65min, and temperature rises to 73 DEG C, anion surfactant, thickening agent and butyl glycol ether are added reactor by temperature successively after reaching, and stir 2h, temperature 94 DEG C are risen to, room temperature is subsequently cooled to, the slurry for obtaining is dried, made the first priming coat；
Step 2;According to said ratio by polyaminoester emulsion, calcium sulphate powders, sodium tripolyphosphate, nano titanium oxide, tricresyl phosphate N-butyl, prodan, organic solvent and cross-linked binder are added sequentially in reactor, are stirred using agitator, speed Spend for 630r/min, stir 2.5h, temperature rises to 88 DEG C, is incubated 1.5h, is subsequently cooled to room temperature, then dry and the second bottom is obtained Coating；
Step 3：According to said ratio by epoxy resin, diethyl phthalate, phosphoric acid ester flame retardant oil, stearic acid and hydrogen Magnesium oxide is sequentially added in reactor, with 780r/min stirrings, stirs 1.5h, and temperature rises to 98 DEG C, and then temperature is cooled to 73 DEG C, then polychloroprene latex, normal-butyl sodium naphthalene sulfonate and isocyanates cross-linking agent are added, then temperature is added to 95 DEG C, 2.5h is incubated, continue to stir with 330r/min, 3h is stirred, room temperature is subsequently cooled to, the slurry for obtaining is dried, and is made 3rd priming coat；
Step 4：The first priming coat, the 2nd coating and the 3rd bottom bonding are combined in the presence of hot pressing, hot pressing combined temp For 185 DEG C, the time is 1.3min, and line pressure is 1.4 Kg/mm.
Embodiment 2
The present embodiment provides a kind of fabric water proof fire retardant coating, is laminated by the first priming coat, the second priming coat and the 3rd primary coat Plus composition, the first priming coat is based on its mass fraction including following components：14 parts of polyurethane, dimethyl methyl phosphonate 3-5 Part, 3 parts of nano silicon, 15 parts of carbon fiber powder, 9 parts of antimony oxide, 16 parts of ldpe resin, polytetrafluoroethyl-ne 5 parts of alkene, 4 parts of anion surfactant, 2 parts of thickening agent, 2 parts of butyl glycol ether；
Second priming coat is based on its mass fraction including following components：25 parts of polyaminoester emulsion, 4 parts of calcium sulphate powders, trimerization phosphorus 11 parts of sour sodium, 5 parts of nano titanium oxide, 4 parts of TRI N BUTYL PHOSPHATE, 4 parts of prodan, 11 parts of organic solvent, crosslinking 3 parts of binding agent；
3rd priming coat is based on its mass fraction including following components：Epoxy resin 20,12 parts of diethyl phthalate, polychlorostyrene 9 parts of butadiene latex, 7 parts of normal-butyl sodium naphthalene sulfonate, 2 parts of phosphoric acid ester flame retardant oil；6 parts of stearic acid, 7 parts of magnesium hydroxide, isocyanide 4 parts of esters of gallic acid cross-linking agent；
Thickening agent is the mixture of methylcellulose, hydroxypropyl methyl cellulose and sodium carboxymethyl cellulose；Cross-linked binder Include following components by mass fraction agent：4- isocyanatomethyls：22 parts, urethanes：24 parts, α-Caulis et Folium Lini Acid：4 parts, ethoxylated bisphenol A dimethylacrylates：6 parts, trimethylol-propane trimethacrylate：6 parts, acrylic acid fourth Ester：7 parts, Crosslinkable Acrylic Polymer Emulsion：9 parts, 2- hydroxyl -1,2- diphenylethans：4 parts, vinylacetate：3 parts.
The fabric water proof fire retardant coating production is comprised the following steps：
Step one：Polyurethane, nano silicon, carbon fiber powder, ldpe resin are put into instead according to said ratio In answering kettle, stirred using agitator, speed controlling is heated simultaneously in 750r/min, stirring, temperature is 57 DEG C, stirring 60min, is then placed in dimethyl methyl phosphonate, politef, antimony oxide, continues to stir 72min, and temperature rises to 77 DEG C, anion surfactant, thickening agent and butyl glycol ether are added reactor by temperature successively after reaching, and stir 2-3h, temperature Degree rises to 97 DEG C, is subsequently cooled to room temperature, and the slurry for obtaining is dried, and has made the first priming coat；
Step 2;According to said ratio by polyaminoester emulsion, calcium sulphate powders, sodium tripolyphosphate, nano titanium oxide, tricresyl phosphate N-butyl, prodan, organic solvent and cross-linked binder are added sequentially in reactor, are stirred using agitator, speed Spend for 680r/min, stir 3h, temperature rises to 92 DEG C, is incubated 2h, is subsequently cooled to room temperature, then dry and the second primary coat is obtained Layer；
Step 3：According to said ratio by epoxy resin, diethyl phthalate, phosphoric acid ester flame retardant oil, stearic acid and hydrogen Magnesium oxide is sequentially added in reactor, with 820r/min stirrings, stirs 2h, and temperature rises to 100 DEG C, and then temperature is cooled to 76 DEG C, then polychloroprene latex, normal-butyl sodium naphthalene sulfonate and isocyanates cross-linking agent are added, then temperature is added to 93 DEG C, 3h is incubated, continue to stir with 370r/min, 3.5h is stirred, room temperature is subsequently cooled to, the slurry for obtaining is dried, and is made 3rd priming coat；
Step 4：The first priming coat, the 2nd coating and the 3rd bottom bonding are combined in the presence of hot pressing, hot pressing combined temp For 190 DEG C, the time is 1.7min, and line pressure is 1.2 Kg/mm.
In addition to the implementation, the present invention can also have other embodiment, all employing equivalents or equivalent transformation shape Into technical scheme, all fall within the protection domain of application claims.

Claims (8)

1. a kind of fabric water proof fire retardant coating, it is characterised in that：The water proof fire retardant coating is by the first priming coat, the second primary coat Layer and the 3rd priming coat are superimposed composition, and a coating is based on its mass fraction including following components：Polyurethane 10-15 Part, dimethyl methyl phosphonate 3-7 parts, nano silicon 2-5 parts, carbon fiber powder 13-17 parts, antimony oxide 5-13 parts, Ldpe resin 15-20 parts, politef 3-9 parts, anion surfactant 3-5 parts, thickening agent 1-3 parts, help Agent 1-3 parts；
Second priming coat is based on its mass fraction including following components：Polyaminoester emulsion 18-26 parts, calcium sulphate powders 3-7 Part, sodium tripolyphosphate 10-14 parts, nano titanium oxide 2-6 part TRI N BUTYL PHOSPHATE 3-7 parts, prodan 3-5 parts have Machine solvent 10-15 parts, cross-linked binder 2-6 part；
3rd priming coat is based on its mass fraction including following components：Epoxy resin 15-22, diethyl phthalate 11-16 parts, polychloroprene latex 8-15 part, normal-butyl sodium naphthalene sulfonate 5-10 parts, phosphoric acid ester flame retardant oil 1-3 parts, stearic acid 5-9 parts, magnesium hydroxide 6-8 parts, cross-linking agent 3-7 parts.
2. fabric according to claim 1 water proof fire retardant coating, it is characterised in that：First priming coat presses its quality Number meter includes following components：Polyurethane 12-15 parts, dimethyl methyl phosphonate 3-5 parts, nano silicon 2-4 parts, carbon are fine Dimension powder 13-15 parts, antimony oxide 5-10 parts, ldpe resin 15-17 parts, politef 3-6 parts, anion Surfactant 3-4 parts, thickening agent 1-2 parts, auxiliary agent 1-2 parts；
Second priming coat is based on its mass fraction including following components：Polyaminoester emulsion 22-26 parts, calcium sulphate powders 3-5 Part, sodium tripolyphosphate 10-12 parts, nano titanium oxide 4-6 part TRI N BUTYL PHOSPHATE 3-5 parts, prodan 3-4 parts have Machine solvent 10-12 parts, cross-linked binder 2-4 part；
3rd priming coat is based on its mass fraction including following components：Epoxy resin 18-22, diethyl phthalate 11-13 parts, polychloroprene latex 8-12 part, normal-butyl sodium naphthalene sulfonate 5-8 parts, phosphoric acid ester flame retardant oil 1-2 parts；Stearic acid 5- 7 parts, magnesium hydroxide 6-7 parts, cross-linking agent 3-5 parts.
3. fabric according to claim 1 water proof fire retardant coating, it is characterised in that：First priming coat presses its quality Number meter includes following components：Polyurethane 12-15 parts, dimethyl methyl phosphonate 3-5 parts, nano silicon 2-4 parts, carbon are fine Dimension powder 13-15 parts, antimony oxide 5-10 parts, ldpe resin 15-17 parts, politef 3-6 parts, anion Surfactant 3-4 parts, thickening agent 1-2 parts, auxiliary agent 1-2 parts；
Second priming coat is based on its mass fraction including following components：Polyaminoester emulsion 22-26 parts, calcium sulphate powders 3-5 Part, sodium tripolyphosphate 10-12 parts, nano titanium oxide 4-6 part TRI N BUTYL PHOSPHATE 3-5 parts, prodan 3-4 parts have Machine solvent 10-12 parts, cross-linked binder 2-3 part；
3rd priming coat is based on its mass fraction including following components：Epoxy resin 18-22, diethyl phthalate 11-13 parts, polychloroprene latex 8-12 part, normal-butyl sodium naphthalene sulfonate 5-8 parts, phosphoric acid ester flame retardant oil 1-2 parts；Stearic acid 5- 7 parts, magnesium hydroxide 6-7 parts, cross-linking agent 3-5 parts.
4. fabric according to claim 1 water proof fire retardant coating, it is characterised in that：The thickening agent is Methyl cellulose Element, hydroxypropyl methyl cellulose or sodium carboxymethyl cellulose one of which or various mixture.
5. fabric according to claim 1 water proof fire retardant coating, it is characterised in that：The cosolvent is butyl glycol ether Or Propylene Glycol.
6. fabric according to claim 1 water proof fire retardant coating, it is characterised in that：The cross-linking agent is isocyanates Cross-linking agent.
7. fabric according to claim 1 water proof fire retardant coating, it is characterised in that：The cross-linked binder by quality Number agent includes following components：4- isocyanatomethyls：18-23 parts, urethanes：18-25 parts, α-Caulis et Folium Lini Acid：3-5 parts, ethoxylated bisphenol A dimethylacrylates：3-7 parts, trimethylol-propane trimethacrylate：4-8 parts, third Olefin(e) acid butyl ester：3-9 parts, Crosslinkable Acrylic Polymer Emulsion：5-12 parts, 2- hydroxyl -1,2- diphenylethans：2-6 parts, vinyl acetate Ester：1-3 parts.
8. fabric according to claim 1 water proof fire retardant coating, it is characterised in that：Fabric water proof fire retardant coating Preparation method is comprised the following steps：
Step one：Polyurethane, nano silicon, carbon fiber powder, ldpe resin are put into instead according to said ratio In answering kettle, stirred using agitator, speed controlling is heated simultaneously in 600-800r/min, stirring, and temperature is 40-60 DEG C, 45-60min is stirred, dimethyl methyl phosphonate, politef, antimony oxide are then placed in, continue to stir 60- 80min, temperature rises to 70-80 DEG C, and temperature successively adds anion surfactant, thickening agent and auxiliary agent after reaching reacts Kettle, stirs 2-3h, and temperature rises to 90-98 DEG C, is subsequently cooled to room temperature, and the slurry for obtaining is dried, and has made the first primary coat Layer；
Step 2;According to said ratio by polyaminoester emulsion, calcium sulphate powders, sodium tripolyphosphate, nano titanium oxide, tricresyl phosphate N-butyl, prodan, organic solvent and cross-linked binder are added sequentially in reactor, are stirred using agitator, speed Spend for 550-700r/min, stir 2-4h, temperature rises to 85-93 DEG C, is incubated 1-2h, is subsequently cooled to room temperature, then drying system Obtain the second priming coat；
Step 3：According to said ratio by epoxy resin, diethyl phthalate, phosphoric acid ester flame retardant oil, stearic acid and hydrogen Magnesium oxide is sequentially added in reactor, with 750-850r/min stirrings, stirs 1-2h, and temperature rises to 96-102 DEG C, then temperature 70-80 DEG C is cooled to, then polychloroprene latex, normal-butyl sodium naphthalene sulfonate and cross-linking agent are added, then temperature is added to 92- 98 DEG C, 2-3h is incubated, continues to stir with 300-400r/min, stir 3-4h, be subsequently cooled to room temperature, the slurry for obtaining is dried It is dry, make the 3rd priming coat；
Step 4：The first priming coat, the 2nd coating and the 3rd bottom bonding are combined in the presence of hot pressing, hot pressing combined temp For 180-200 DEG C, the time is 1-2min, and line pressure is 1.2-1.6 Kg/mm.
CN201611130467.3A 2016-12-09 2016-12-09 Waterproof and flame-retarding coating for fabric and preparation method thereof Pending CN106590186A (en)

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CN113638232A (en) * 2021-09-03 2021-11-12 南通强生石墨烯科技有限公司 Insulating fabric with flame-retardant coating and preparation method thereof
CN113956776A (en) * 2021-12-06 2022-01-21 烟台大学 Preparation method of powderable self-repairing flame-retardant low-VOC (volatile organic compound) polyurethane coating and application of powderable self-repairing flame-retardant low-VOC polyurethane coating in automobile leather

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