CN106590155A - Modification and preparation process of quick-drying ink - Google Patents
Modification and preparation process of quick-drying ink Download PDFInfo
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- CN106590155A CN106590155A CN201611093024.1A CN201611093024A CN106590155A CN 106590155 A CN106590155 A CN 106590155A CN 201611093024 A CN201611093024 A CN 201611093024A CN 106590155 A CN106590155 A CN 106590155A
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- ink
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- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09D—COATING COMPOSITIONS, e.g. PAINTS, VARNISHES OR LACQUERS; FILLING PASTES; CHEMICAL PAINT OR INK REMOVERS; INKS; CORRECTING FLUIDS; WOODSTAINS; PASTES OR SOLIDS FOR COLOURING OR PRINTING; USE OF MATERIALS THEREFOR
- C09D11/00—Inks
- C09D11/02—Printing inks
- C09D11/08—Printing inks based on natural resins
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- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09D—COATING COMPOSITIONS, e.g. PAINTS, VARNISHES OR LACQUERS; FILLING PASTES; CHEMICAL PAINT OR INK REMOVERS; INKS; CORRECTING FLUIDS; WOODSTAINS; PASTES OR SOLIDS FOR COLOURING OR PRINTING; USE OF MATERIALS THEREFOR
- C09D11/00—Inks
- C09D11/02—Printing inks
- C09D11/03—Printing inks characterised by features other than the chemical nature of the binder
-
- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09D—COATING COMPOSITIONS, e.g. PAINTS, VARNISHES OR LACQUERS; FILLING PASTES; CHEMICAL PAINT OR INK REMOVERS; INKS; CORRECTING FLUIDS; WOODSTAINS; PASTES OR SOLIDS FOR COLOURING OR PRINTING; USE OF MATERIALS THEREFOR
- C09D11/00—Inks
- C09D11/02—Printing inks
- C09D11/10—Printing inks based on artificial resins
- C09D11/106—Printing inks based on artificial resins containing macromolecular compounds obtained by reactions only involving carbon-to-carbon unsaturated bonds
- C09D11/107—Printing inks based on artificial resins containing macromolecular compounds obtained by reactions only involving carbon-to-carbon unsaturated bonds from unsaturated acids or derivatives thereof
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- Chemical & Material Sciences (AREA)
- Life Sciences & Earth Sciences (AREA)
- Engineering & Computer Science (AREA)
- Materials Engineering (AREA)
- Wood Science & Technology (AREA)
- Organic Chemistry (AREA)
- Chemical Kinetics & Catalysis (AREA)
- General Chemical & Material Sciences (AREA)
- Inks, Pencil-Leads, Or Crayons (AREA)
Abstract
The invention discloses a modification and preparation process of quick-drying ink. Vegetable oil based ink is slow in drying speed, and the addition of a zinc neodecanoate dryer can improve the drying performance of the ink. The specific preparation process includes the following steps that vegetable oil, ethanol amine, an organosilicone defoaming agent, a soybean lecithin wetting agent and a proper amount of water are added into a dispersion tank according to a certain proportion, mixed and filtered to collect a filtered emulsion, the filtered emulsion is then mixed with a certain proportion of water soluble acrylic resin, water-based acrylic acid color paste and rosin resin, the mixture is filtered to collect a filtered emulsion, finally calcium naphthenate and a proper amount of defoaming agents are added into the filtered emulsion, and the quick-drying ink added with zinc naphthenate can be obtained. The preparation process has the advantages of being simple in technological process, and has a wide application prospect.
Description
Technical field
The present invention relates to a kind of ink, more particularly to a kind of addition naphthoic acid zinc drier is modified and prepares the preparation of quicksetting ink
Technique, belongs to ink synthesis field.
Background technology
Ink be it is a kind of equably mixed by pigment, link stuff and auxiliary agent etc. and Jing repeat-rollings a kind of viscosity glue
Shape fluid.As the continuous development of press, ink application are also increasingly extensive, yield constantly increases, in China, 2015 whole nation oil
Black gross annual output amount amounts to 800,000 tons, but ink manufacturing industry substantially produces is traditional synthetic resin ink, in this kind of ink
Organic (or inorganic) solvent will be contained mostly, thus containing more multiring aromatic hydrocarbon substance, and therein 3,4- benzo pyrrole,
3- nitro benzo ketone etc. also contains carcinogenic components, can endanger user health, develops the research heat that non-toxic ink is current ink
Point.
Make solvent with vegetable oil, not only resource that is environmentally friendly but also can use regeneration replaces non-renewable oil molten to the ink of preparation
Agent, and deinking is easier to than traditional ink to useless leaflet process when reclaiming, but plant oil base contains a large amount of unsaturated fatty acidss
Acid, slow drying speed are in order to overcome the shortcoming of slow drying speed, of the invention in ink-making process, by adding naphthoate
Drier so that consaturated oil occurs oxidation, after oxygen uptake, becomes solid-state from liquid, becomes macromole by small molecule, so as to
Accelerate oils and fatss conjunctival xerosiss.Naphthalene acid zinc urges dry auxiliary agent to be widely used in ink industry as one kind, can quickly improve ink
Drying property, so as to lift ink combination property.
The content of the invention
The present invention provides the ink that a kind of addition naphthoic acid zinc drier is modified preparation, and the ink includes following percentage by weight
Material：
Vegetable oil esters 20-40%
Ethanolamine 10-20%
Rosin resin 10-15%
Water soluble acrylic resin 10-15%
Water soluble acrylic acid mill base 10-20%
Soybean lecithin wetting agent 1-2%
Organic silicon defoamer 1-2%
Naphthalene acid zinc 1-2%
Water surplus.
A kind of addition naphthoic acid zinc drier be modified preparation ink preparation method, its method comprises the steps：
(1) a certain proportion of vegetable oil, ethanolamine, organic silicon defoamer and soybean lecithin wetting agent and suitable quantity of water are loaded and divided
In scattered cylinder；
(2) mixed solution system in dispersion cylinder is mixed under certain rotating speed, be uniformly dispersed；
(3), after disperseing, liquid is filtered；
(4) the emulsion of filtration is collected, then is poured in dispersion cylinder, sequentially add a certain amount of water soluble acrylic resin, rosin resin
With water soluble acrylic acid mill base；
(5) mixed solution system is mixed under certain rotating speed, be uniformly dispersed；
(6) it is eventually adding a certain amount of naphthoic acid zinc drier and organic silicon defoamer and filters, you can obtains a kind of addition naphthalene acid zinc
Quick-drying ink.
Preferentially, step (1) in, vegetable oil esters are soybean oil or Semen Maydiss oils and fatss.
Preferentially, step (2) in, by the rotating speed of 500-600 r/min, dispersed 2-3 hours.
Preferentially, step (5) in, by the rotating speed of 600-800r/min, dispersed 2-4 hours.
The present invention has following advantages and characteristic：
(1) good environmental protection；
(2) raw material sources are extensive, with low cost；
(3) flow process is short, process is simple.
Specific embodiment
Embodiment one：
With the soybean oil of a dispersion cylinder 20% ratio of loading, the ethanolamine of 10% ratio, the organic silicon defoamer of 1% ratio, 1% ratio
Mixed solution system is disperseed 3 under the conditions of rotating speed is 500 r/min by the water of the soybean lecithin wetting agent and 16% ratio of example
Hour, mixture is filtered after dispersion, collect filter emulsion put in dispersion cylinder again, and sequentially add 15% it is water-soluble
Property acrylic resin, 15% rosin resin, the water soluble acrylic acid mill base of 20% ratio, by mixed solution system rotating speed be 700
Disperse 3 hours under the conditions of r/min, after dispersion terminates, be eventually adding the organic silicon defoamer of the naphthalene acid zinc and 1% ratio of 1% ratio,
The quick-drying ink that a kind of addition naphthalene acid zinc can be obtained is filtered finally.
Embodiment two：
With a dispersion cylinder load the soybean oil of 30% ratio, the ethanolamine of 20% ratio, the organic silicon defoamer of 0.5% ratio, 2%
The water of the soybean lecithin wetting agent and 10.5% ratio of ratio, mixed solution system is divided under the conditions of rotating speed is 550 r/min
Dissipate 2.5 hours, mixture is filtered after dispersion, collect the emulsion for filtering and put in dispersion cylinder again, and sequentially add 10%
Water soluble acrylic resin, 15% rosin resin, the water soluble acrylic acid mill base of 10% ratio, by mixed solution system in rotating speed be
Under the conditions of 600 r/min disperse 4 hours, dispersion terminate after, be eventually adding 1.5% ratio naphthalene acid zinc and 0.5% ratio it is organic
Silicon defoaming agent, finally filters the quick-drying ink that can obtain a kind of addition naphthalene acid zinc.
Embodiment three：
With a dispersion cylinder load the soybean oil of 40% ratio, the ethanolamine of 15% ratio, the organic silicon defoamer of 0.5% ratio, 1%
The soybean lecithin wetting agent agent of ratio and the water of 6% ratio, mixed solution system is divided under the conditions of rotating speed is 600 r/min
Dissipate 2 hours, mixture is filtered after dispersion, collect the emulsion for filtering and put in dispersion cylinder again, and sequentially add 10% water
Soluble acrylic resin, 10% rosin resin, the water soluble acrylic acid mill base of 15% ratio, by mixed solution system in rotating speed be
Disperse 2 hours under the conditions of 800 r/min, after dispersion terminates, be eventually adding the organosilicon of the naphthalene acid zinc and 0.5% ratio of 2% ratio
Defoamer, finally filters the quick-drying ink that can obtain a kind of addition naphthalene acid zinc.
Claims (4)
1. the modified preparation technology of a kind of quicksetting ink, it is characterised in that the preparation technology comprises the steps：
(1) a certain proportion of vegetable oil, ethanolamine, organic silicon defoamer and soybean lecithin wetting agent and suitable quantity of water are loaded and divided
In scattered cylinder；
(2) mixed solution system in dispersion cylinder is mixed under certain rotating speed, be uniformly dispersed；
(3), after dispersion a period of time, liquid is filtered；
(4) the emulsion of filtration is collected, then is poured in dispersion cylinder, sequentially add a certain amount of water soluble acrylic resin, rosin resin
With water soluble acrylic acid mill base；
(5) mixed solution system is mixed under certain rotating speed, be uniformly dispersed；
(6) it is eventually adding a certain amount of naphthoic acid zinc drier and organic silicon defoamer and filters, you can obtains a kind of addition naphthalene acid zinc
Quick-drying ink.
2. the modified preparation technology of a kind of quicksetting ink according to claim 1, it is characterised in that step (1) in, plant
Thing grease is soybean oil or Semen Maydiss oils and fatss.
3. the modified preparation technology of a kind of quicksetting ink according to claim 1, it is characterised in that step (2) in, press
The rotating speed of 500-600 r/min, dispersed 2-3 hours.
4. the modified preparation technology of a kind of quicksetting ink according to claim 1, it is characterised in that step (5) in, press
The rotating speed of 600-800r/min, dispersed 2-4 hours.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201611093024.1A CN106590155A (en) | 2016-12-02 | 2016-12-02 | Modification and preparation process of quick-drying ink |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201611093024.1A CN106590155A (en) | 2016-12-02 | 2016-12-02 | Modification and preparation process of quick-drying ink |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| CN106590155A true CN106590155A (en) | 2017-04-26 |
Family
ID=58595953
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN201611093024.1A Pending CN106590155A (en) | 2016-12-02 | 2016-12-02 | Modification and preparation process of quick-drying ink |
Country Status (1)
| Country | Link |
|---|---|
| CN (1) | CN106590155A (en) |
Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN113122046A (en) * | 2021-04-27 | 2021-07-16 | 中山市富日印刷材料有限公司 | High-gloss quick-drying non-skinning printing ink and preparation method thereof |
Citations (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN104559466A (en) * | 2014-12-28 | 2015-04-29 | 乐渭林 | Mixed oleoresin printing ink |
-
2016
- 2016-12-02 CN CN201611093024.1A patent/CN106590155A/en active Pending
Patent Citations (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN104559466A (en) * | 2014-12-28 | 2015-04-29 | 乐渭林 | Mixed oleoresin printing ink |
Non-Patent Citations (1)
| Title |
|---|
| 田庆华等: "《钴氧化物无氨草酸沉淀-热分解制备新工艺研究》", 31 October 2015, 冶金工业出版社 * |
Cited By (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN113122046A (en) * | 2021-04-27 | 2021-07-16 | 中山市富日印刷材料有限公司 | High-gloss quick-drying non-skinning printing ink and preparation method thereof |
| CN113122046B (en) * | 2021-04-27 | 2022-06-28 | 中山市富日印刷材料有限公司 | High-gloss quick-drying non-skinning printing ink and preparation method thereof |
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Application publication date: 20170426 |
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