CN106587745A - High efficient insulation material of pipeline - Google Patents
High efficient insulation material of pipeline Download PDFInfo
- Publication number
- CN106587745A CN106587745A CN201610932184.4A CN201610932184A CN106587745A CN 106587745 A CN106587745 A CN 106587745A CN 201610932184 A CN201610932184 A CN 201610932184A CN 106587745 A CN106587745 A CN 106587745A
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- insulation material
- thermal insulation
- straw
- red mud
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- C—CHEMISTRY; METALLURGY
- C04—CEMENTS; CONCRETE; ARTIFICIAL STONE; CERAMICS; REFRACTORIES
- C04B—LIME, MAGNESIA; SLAG; CEMENTS; COMPOSITIONS THEREOF, e.g. MORTARS, CONCRETE OR LIKE BUILDING MATERIALS; ARTIFICIAL STONE; CERAMICS; REFRACTORIES; TREATMENT OF NATURAL STONE
- C04B26/00—Compositions of mortars, concrete or artificial stone, containing only organic binders, e.g. polymer or resin concrete
- C04B26/02—Macromolecular compounds
- C04B26/28—Polysaccharides or derivatives thereof
- C04B26/285—Cellulose or derivatives thereof
-
- C—CHEMISTRY; METALLURGY
- C04—CEMENTS; CONCRETE; ARTIFICIAL STONE; CERAMICS; REFRACTORIES
- C04B—LIME, MAGNESIA; SLAG; CEMENTS; COMPOSITIONS THEREOF, e.g. MORTARS, CONCRETE OR LIKE BUILDING MATERIALS; ARTIFICIAL STONE; CERAMICS; REFRACTORIES; TREATMENT OF NATURAL STONE
- C04B20/00—Use of materials as fillers for mortars, concrete or artificial stone according to more than one of groups C04B14/00 - C04B18/00 and characterised by shape or grain distribution; Treatment of materials according to more than one of the groups C04B14/00 - C04B18/00 specially adapted to enhance their filling properties in mortars, concrete or artificial stone; Expanding or defibrillating materials
- C04B20/02—Treatment
- C04B20/04—Heat treatment
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- Chemical & Material Sciences (AREA)
- Engineering & Computer Science (AREA)
- Ceramic Engineering (AREA)
- Materials Engineering (AREA)
- Structural Engineering (AREA)
- Organic Chemistry (AREA)
- Physics & Mathematics (AREA)
- Thermal Sciences (AREA)
- Silicates, Zeolites, And Molecular Sieves (AREA)
Abstract
The invention discloses a high efficient insulation material of pipelines. The material comprises the following raw materials in parts by mass: 30-50 parts of red mud, 5-9 parts of metasilicic acid, 3-5 parts of perlite, 30-40 parts of straw, 5-11 parts of turpentine, 6-9 parts of ethanol, 2-4 parts of hydrogen peroxide, 0.3-1.3 parts of tannin, 7-9 parts of diatom mud, 5-11 parts of sodium carbonate, 1-3 parts of pectin, 1-3 parts of cellulose, and 1-3 parts of an activator. Because of self characteristics of the material, and in the utilization process of high efficient insulation of pipelines, the material has good insulation effects, and extremely good insulation effects; further, the high efficient insulation material of pipelines has the advantages of simple preparation, preparation for current usage, wide raw material resources, low cost, and easy popular promotion.
Description
Technical field
The present invention relates to a kind of insulating layer material, more particularly to a kind of pipeline thermal insulation material.
Background technology
Red mud be with bauxite as raw material production alumina process in produce fines strong basicity solid waste, often give birth to
One ton of aluminium oxide is produced, 0.8～1.5 ton of red mud is about produced.China is alumina producing big country, produces aluminium oxide 2378 within 2009
Ten thousand tons, the 30% of Gross World Product is accounted for, the red mud of generation is nearly 30,000,000 tons.At present China's red mud comprehensive utilization ratio is only 4%,
Accumulation volume of cargo in storage reaches 200,000,000 tons.With increasing year by year for China's aluminium oxide yield and being gradually lowered for bauxite grade, red mud
Yield will also be continuously increased in year, and by 2015, the accumulative volume of cargo in storage of red mud was up to 3.5 hundred million tons.Red mud is stored up in a large number, both takes
Soil, waste of resource easily causes environmental pollution and potential safety hazard again.
Now factory's either chemical pipeline conveying liquid charging stock or during heat exchange material, needs to raw material or heat exchange material
It is incubated, but most chemical pipeline is not only longer, and having many bends or curves, the mistake of raw material or heat exchange material in conveying
It is easier to lose the temperature of its own in journey, causes process materials conveying more difficult.At present, in most chemical plant using asbestos or
Person sponge is wrapped up pipeline, or seals one layer of cement in pipeline outer-layer, to reaching the effect of insulation, but such as comprehensive institute
State, play more chemical pipeline and go, in corner, easily turned round using asbestos and the more difficult operation of sponge wrapping, and energy
Place is lost in.Pipeline can be incubated using cement, although effect is good not as sponge and asbestos, easy to operate, low cost.Cause
This, needs at present a kind of low cost, easy to operate, high insulating effect pipe insulation material badly.
The information for being disclosed in the background section is merely intended to increase the understanding of the general background to the present invention, and should not
When the prior art for being considered to recognize or imply in any form the information structure well known to persons skilled in the art.
The content of the invention
, for the high-efficiency insulated effect on driving birds is not good of chemical pipeline in prior art, operating process is wordy, high cost for the present invention
Problem, invents a kind of pipeline thermal insulation material, it is intended to which obtaining one kind can effectively play heat insulation effect, and cost is again cheap, fits
Close to the popular heat-barrier material promoted.
For achieving the above object, the technical scheme that the present invention is provided is as follows：
A kind of pipeline thermal insulation material, according to quality parts ratio following components raw material is included：30～50 parts of red mud, inclined silicon
5～9 parts of acid, 3～5 parts of perlite, 30～40 parts of straw, 5～11 parts of Colophonium, 6～9 parts of ethanol, 2～4 parts of hydrogen peroxide, tannin
1～3 part of 0.3～1.3 part, 7～9 parts of diatom ooze, 5～11 parts of sodium carbonate, 1～3 part of pectin, 1～3 part of cellulose and activating agent.
Wherein, described red mud 1～3h of roasting at 250～300 DEG C, takes out, add sulphuric acid react 30 at normal temperatures～
45min, obtains final product.
Wherein, the sulphuric acid of addition and red mud are into 0.4～0.7:1 mass ratio.
Wherein, described sulphuric acid volumetric concentration is 20～30%.
Wherein, described activating agent is by silicon dioxide, alkali lignin, plant amylum, zingiberone, flyash, glycine betaine, Canis familiaris L. alkene
With calcium chloride composition.
Wherein, described activating agent is made up of according to quality parts ratio following components raw material：31～41 parts of silicon dioxide, alkali
21～31 parts of lignin, 11～21 parts of plant amylum, 0.3～0.9 part of zingiberone, 3～7 parts of flyash, 11～15 parts of glycine betaine, Canis familiaris L.
5～8 parts of 1～3 part of alkene and calcium chloride.
Wherein, described straw is wheat-straw or rice straw, and straw granularity is 0.5～1.0mm.
Wherein, described plant amylum is a kind of in tapioca starch, dehydrated potato powder, flour or rice flour.
A kind of preparation method of pipeline thermal insulation material as described above, comprising following operating procedure：
(1) following components raw material is taken according to quality parts ratio：30～50 parts of red mud, 5～9 parts of metasilicic acid, perlite 3～5
Part, 30～40 parts of straw, 5～11 parts of Colophonium, 6～9 parts of ethanol, 2～4 parts of hydrogen peroxide, 0.3～1.3 part of tannin, diatom ooze 7～9
Part, 5～11 parts of sodium carbonate, 1～3 part of pectin, 1～3 part of cellulose and 1～3 part of activating agent, by red mud, metasilicic acid, perlite,
Straw, Colophonium, ethanol, diatom ooze, sodium carbonate and activating agent mixing and stirring, are subsequently adding tannin, pectin and cellulose, mix
Conjunction stirs, and places 10～20min；
(2) hydrogen peroxide is added in gained material after placing in step (1), 30～40min is stood, is obtained final product.
Compared with prior art, the present invention has the advantages that：
Inventive pipeline thermal insulation material during the high-efficiency insulated utilization of pipeline, can be risen due to material self-characteristic
To good insulation effect, heat insulation effect is fabulous；Further, inventive pipeline thermal insulation material prepares simple and direct, can now match somebody with somebody
Now use, extensively, cost is relatively low for raw material sources, it is easy to popular popularization.
Specific embodiment
It is described in detail with reference to specific embodiment, it is to be understood that protection scope of the present invention is not by concrete
The restriction of embodiment.
Embodiment 1
Red mud roasting 3h at 250 DEG C, takes out, according to sulphuric acid and red mud into 0.4:1 mass ratio add volumetric concentration be
20% sulphuric acid reacts at normal temperatures 45min, obtains final product, standby；Activating agent weighs following components raw material in units of g：Titanium dioxide
Silicon 31g, alkali lignin 21g, dehydrated potato powder 11g, zingiberone 0.3g, flyash 3g, glycine betaine 11g, Canis familiaris L. alkene 1g and calcium chloride 5g, will
Each component raw material mixing and stirring, obtains final product.
A kind of preparation method of pipeline thermal insulation material, operating procedure is as follows：
(1) following components raw material is weighed in units of g：Above-mentioned standby red mud 30g, metasilicic acid 5g, perlite 3g, straw
Granularity is wheat-straw 30g, Colophonium 5g, ethanol 6g, hydrogen peroxide 2g, tannin 0.3g, diatom ooze 7g, sodium carbonate 5g, the pectin of 0.5mm
1g, cellulose 1g and above-mentioned standby activating agent 1g, by red mud, metasilicic acid, perlite, straw, Colophonium, ethanol, diatom ooze, carbon
Sour sodium and activating agent mixing and stirring, are subsequently adding tannin, pectin and cellulose, and mixing and stirring places 10min；
(2) hydrogen peroxide is added in gained material after placing in step (1), 30min is stood, is obtained final product.
Embodiment 2
Red mud roasting 1h at 300 DEG C, takes out, according to sulphuric acid and red mud into 0.7:1 mass ratio add volumetric concentration be
30% sulphuric acid reacts at normal temperatures 30min, obtains final product, standby；Activating agent weighs following components raw material in units of g：Titanium dioxide
Silicon 41g, alkali lignin 31g, flour 21g, zingiberone 0.9g, flyash 7g, glycine betaine 15g, Canis familiaris L. alkene 3g and calcium chloride 8g, by each group
Divide raw material mixing and stirring, obtain final product.
A kind of preparation method of pipeline thermal insulation material, operating procedure is as follows：
(1) following components raw material is weighed in units of g：Above-mentioned standby red mud 50g, metasilicic acid 9g, perlite 5g, straw
Granularity is rice straw 40g, Colophonium 11g, ethanol 9g, hydrogen peroxide 4g, tannin 1.3g, diatom ooze 9g, sodium carbonate 11g, the pectin of 1.0mm
3g, cellulose 3g and above-mentioned standby activating agent 3g, by red mud, metasilicic acid, perlite, straw, Colophonium, ethanol, diatom ooze, carbon
Sour sodium and activating agent mixing and stirring, are subsequently adding tannin, pectin and cellulose, and mixing and stirring places 20min；
(2) hydrogen peroxide is added in gained material after placing in step (1), 40min is stood, is obtained final product.
Embodiment 3
Red mud roasting 2h at 275 DEG C, takes out, according to sulphuric acid and red mud into 0.6:1 mass ratio add volumetric concentration be
25% sulphuric acid reacts at normal temperatures 378min, obtains final product, standby；Activating agent weighs following components raw material in units of g：Titanium dioxide
Silicon 36g, alkali lignin 26g, tapioca starch 16g, zingiberone 0.6g, flyash 5g, glycine betaine 13g, Canis familiaris L. alkene 2g and calcium chloride 6g, will be each
Component raw material mixing and stirring, obtains final product.
A kind of preparation method of pipeline thermal insulation material, operating procedure is as follows：
(1) following components raw material is weighed in units of g：Above-mentioned standby red mud 40g, metasilicic acid 7g, perlite 4g, straw
Granularity is rice straw 35g, Colophonium 8g, ethanol 7g, hydrogen peroxide 3g, tannin 0.8g, diatom ooze 8g, sodium carbonate 8g, the pectin of 0.7mm
2g, cellulose 2g and above-mentioned standby activating agent 2g, by red mud, metasilicic acid, perlite, straw, Colophonium, ethanol, diatom ooze, carbon
Sour sodium and activating agent mixing and stirring, are subsequently adding tannin, pectin and cellulose, and mixing and stirring places 15min；
(2) hydrogen peroxide is added in gained material after placing in step (1), 35min is stood, is obtained final product.
Embodiment 4
Red mud roasting 2h at 275 DEG C, takes out, according to sulphuric acid and red mud into 0.6:1 mass ratio add volumetric concentration be
25% sulphuric acid reacts at normal temperatures 378min, obtains final product, standby.
A kind of preparation method of pipeline thermal insulation material, operating procedure is as follows：
(1) following components raw material is weighed in units of g：Above-mentioned standby red mud 40g, metasilicic acid 7g, perlite 4g, straw
Granularity is rice straw 35g, Colophonium 8g, ethanol 7g, hydrogen peroxide 3g, tannin 0.8g, diatom ooze 8g, sodium carbonate 8g, the pectin of 0.7mm
2g, cellulose 2g, by red mud, metasilicic acid, perlite, straw, Colophonium, ethanol, diatom ooze, sodium carbonate mixing and stirring, so
Tannin, pectin and cellulose, mixing and stirring is added to place 15min afterwards；
(2) hydrogen peroxide is added in gained material after placing in step (1), 35min is stood, is obtained final product.
Detection
Long 2000 meters with 3, outer aperture is 150mm, and internal orifice dimension is the pipeline of 148mm, is respectively labeled as 1#, 2# and, 3#
And 4#；Wherein, 1# is left intact；2# wraps up the asbestos that a layer thickness is 80mm outside caliber；3# is real using the present invention
Apply the preparation gained pipeline thermal insulation material of example 3 and smear pipeline external surface, smearing thickness is 80mm；4# is prepared using embodiment 4
Gained pipeline thermal insulation material smears pipeline external surface, and smearing thickness is 80mm.4 cement boxes are placed on into 10 during measurement
～20 DEG C of outdoor, temperature of liquid to be conveyed is 100 DEG C, and again flow velocity is 3.4m/s in pipeline to keep liquid, and measurement pipeline is final
Conveying gained temperature of liquid, measures 3 times, averages, and acquired results are as shown in the table：
Table 1
| Detection content | 1# temperature | 2# temperature | 3# temperature | 4# temperature |
| Water | 72.8℃ | 91.2℃ | 91.8℃ | 85.3℃ |
| Diesel oil | 74.9℃ | 92.9 | 93.2 | 86.5 |
| Rosin liquid | 73.8℃ | 90.0 | 90.7 | 85.0 |
In from table 1, using material of the present invention, after processing pipeline external surface, heat insulation effect is obvious；By table 1
In further illustrate, the activating agent of the present invention is high-efficiency insulated to pipeline with greatly facilitating effect.
It is aforementioned to the present invention specific illustrative embodiment description be in order to illustrate and illustration purpose.These descriptions
It is not wishing to limit the invention to disclosed precise forms, and it will be apparent that according to above-mentioned teaching, can be much changed
And change.The purpose of selecting and describing the exemplary embodiment is that explaining that the certain principles and its reality of the present invention should
With so that those skilled in the art can realize and using the present invention a variety of exemplaries and
A variety of selections and change.The scope of the present invention is intended to be limited by claims and its equivalents.
Claims (9)
1. a kind of pipeline thermal insulation material, it is characterised in that include following components raw material according to quality parts ratio：Red mud 30～
50 parts, 5～9 parts of metasilicic acid, 3～5 parts of perlite, 30～40 parts of straw, 5～11 parts of Colophonium, 6～9 parts of ethanol, hydrogen peroxide 2～4
Part, 0.3～1.3 part of tannin, 7～9 parts of diatom ooze, 5～11 parts of sodium carbonate, 1～3 part of pectin, 1～3 part of cellulose and activating agent 1
～3 parts.
2. pipeline thermal insulation material according to claim 1, it is characterised in that：Described red mud is at 250～300 DEG C
1～3h of roasting, takes out, and adds sulphuric acid to react 30～45min at normal temperatures, obtains final product.
3. pipeline thermal insulation material according to claim 2, it is characterised in that：The sulphuric acid of addition and red mud into 0.4～
0.7:1 mass ratio.
4. the pipeline thermal insulation material according to Claims 2 or 3, it is characterised in that：Described sulphuric acid volumetric concentration is
20～30%.
5. pipeline thermal insulation material according to claim 1, it is characterised in that：Described activating agent by silicon dioxide,
Alkali lignin, plant amylum, zingiberone, flyash, glycine betaine, Canis familiaris L. alkene and calcium chloride composition.
6. pipeline thermal insulation material according to claim 1, it is characterised in that：Described activating agent is according to mass fraction
Than being made up of following components raw material：31～41 parts of silicon dioxide, 21～31 parts of alkali lignin, 11～21 parts of plant amylum, zingiberone
5～8 parts of 0.3～0.9 part, 3～7 parts of flyash, 11～15 parts of glycine betaine, 1～3 part of Canis familiaris L. alkene and calcium chloride.
7. pipeline thermal insulation material according to claim 6, it is characterised in that：Described plant amylum be tapioca starch,
It is a kind of in dehydrated potato powder, flour or rice flour.
8. pipeline thermal insulation material according to claim 1, it is characterised in that：Described straw is wheat-straw or rice
Bar, straw granularity is 0.5～1.0mm.
9. a kind of preparation method of pipeline thermal insulation material as claimed in claim 1, it is characterised in that comprising following operation
Step：
(1) following components raw material is taken according to quality parts ratio：30～50 parts of red mud, 5～9 parts of metasilicic acid, 3～5 parts of perlite, straw
30～40 parts of stalk, 5～11 parts of Colophonium, 6～9 parts of ethanol, 2～4 parts of hydrogen peroxide, 0.3～1.3 part of tannin, 7～9 parts of diatom ooze, carbon
1～3 part of 5～11 parts of sour sodium, 1～3 part of pectin, 1～3 part of cellulose and activating agent, by red mud, metasilicic acid, perlite, straw,
Colophonium, ethanol, diatom ooze, sodium carbonate and activating agent mixing and stirring, are subsequently adding tannin, pectin and cellulose, and mixing is stirred
Mix uniform, place 10～20min；
(2) hydrogen peroxide is added in gained material after placing in step (1), 30～40min is stood, is obtained final product.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201610932184.4A CN106587745A (en) | 2016-10-31 | 2016-10-31 | High efficient insulation material of pipeline |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201610932184.4A CN106587745A (en) | 2016-10-31 | 2016-10-31 | High efficient insulation material of pipeline |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| CN106587745A true CN106587745A (en) | 2017-04-26 |
Family
ID=58556339
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN201610932184.4A Pending CN106587745A (en) | 2016-10-31 | 2016-10-31 | High efficient insulation material of pipeline |
Country Status (1)
| Country | Link |
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| CN (1) | CN106587745A (en) |
Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN108298861A (en) * | 2018-02-27 | 2018-07-20 | 合肥帧讯低温科技有限公司 | A kind of chemical pipeline heat-insulating material and preparation method thereof |
Citations (5)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN1880259A (en) * | 2005-06-14 | 2006-12-20 | 刘贵堂 | Water-preserving materials and process for preparing same |
| CN101671157A (en) * | 2009-09-22 | 2010-03-17 | 中国人民解放军海军工程大学 | High-efficiency insulating material used for high-temperature pipeline and preparation method thereof |
| CN101781112A (en) * | 2009-01-19 | 2010-07-21 | 陈冠廷 | Air-entrapping sodium silicate perlite thermal insulation material |
| CN103073066A (en) * | 2012-11-01 | 2013-05-01 | 吕富华 | Innocent treatment and resource utilization method for red mud |
| CN104844263A (en) * | 2015-06-01 | 2015-08-19 | 中国科学院青海盐湖研究所 | Thermal insulation material |
-
2016
- 2016-10-31 CN CN201610932184.4A patent/CN106587745A/en active Pending
Patent Citations (5)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN1880259A (en) * | 2005-06-14 | 2006-12-20 | 刘贵堂 | Water-preserving materials and process for preparing same |
| CN101781112A (en) * | 2009-01-19 | 2010-07-21 | 陈冠廷 | Air-entrapping sodium silicate perlite thermal insulation material |
| CN101671157A (en) * | 2009-09-22 | 2010-03-17 | 中国人民解放军海军工程大学 | High-efficiency insulating material used for high-temperature pipeline and preparation method thereof |
| CN103073066A (en) * | 2012-11-01 | 2013-05-01 | 吕富华 | Innocent treatment and resource utilization method for red mud |
| CN104844263A (en) * | 2015-06-01 | 2015-08-19 | 中国科学院青海盐湖研究所 | Thermal insulation material |
Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN108298861A (en) * | 2018-02-27 | 2018-07-20 | 合肥帧讯低温科技有限公司 | A kind of chemical pipeline heat-insulating material and preparation method thereof |
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Application publication date: 20170426 |