CN106587213B - A kind of sewage-treating agent and preparation method thereof for handling fermentation waste water - Google Patents
A kind of sewage-treating agent and preparation method thereof for handling fermentation waste water Download PDFInfo
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- CN106587213B CN106587213B CN201611258498.7A CN201611258498A CN106587213B CN 106587213 B CN106587213 B CN 106587213B CN 201611258498 A CN201611258498 A CN 201611258498A CN 106587213 B CN106587213 B CN 106587213B
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- C—CHEMISTRY; METALLURGY
- C02—TREATMENT OF WATER, WASTE WATER, SEWAGE, OR SLUDGE
- C02F—TREATMENT OF WATER, WASTE WATER, SEWAGE, OR SLUDGE
- C02F1/00—Treatment of water, waste water, or sewage
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- C—CHEMISTRY; METALLURGY
- C02—TREATMENT OF WATER, WASTE WATER, SEWAGE, OR SLUDGE
- C02F—TREATMENT OF WATER, WASTE WATER, SEWAGE, OR SLUDGE
- C02F1/00—Treatment of water, waste water, or sewage
- C02F1/58—Treatment of water, waste water, or sewage by removing specified dissolved compounds
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- C—CHEMISTRY; METALLURGY
- C02—TREATMENT OF WATER, WASTE WATER, SEWAGE, OR SLUDGE
- C02F—TREATMENT OF WATER, WASTE WATER, SEWAGE, OR SLUDGE
- C02F2101/00—Nature of the contaminant
- C02F2101/10—Inorganic compounds
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- C—CHEMISTRY; METALLURGY
- C02—TREATMENT OF WATER, WASTE WATER, SEWAGE, OR SLUDGE
- C02F—TREATMENT OF WATER, WASTE WATER, SEWAGE, OR SLUDGE
- C02F2101/00—Nature of the contaminant
- C02F2101/10—Inorganic compounds
- C02F2101/20—Heavy metals or heavy metal compounds
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- C—CHEMISTRY; METALLURGY
- C02—TREATMENT OF WATER, WASTE WATER, SEWAGE, OR SLUDGE
- C02F—TREATMENT OF WATER, WASTE WATER, SEWAGE, OR SLUDGE
- C02F2103/00—Nature of the water, waste water, sewage or sludge to be treated
- C02F2103/32—Nature of the water, waste water, sewage or sludge to be treated from the food or foodstuff industry, e.g. brewery waste waters
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- C—CHEMISTRY; METALLURGY
- C02—TREATMENT OF WATER, WASTE WATER, SEWAGE, OR SLUDGE
- C02F—TREATMENT OF WATER, WASTE WATER, SEWAGE, OR SLUDGE
- C02F2103/00—Nature of the water, waste water, sewage or sludge to be treated
- C02F2103/32—Nature of the water, waste water, sewage or sludge to be treated from the food or foodstuff industry, e.g. brewery waste waters
- C02F2103/325—Nature of the water, waste water, sewage or sludge to be treated from the food or foodstuff industry, e.g. brewery waste waters from processes relating to the production of wine products
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- C—CHEMISTRY; METALLURGY
- C02—TREATMENT OF WATER, WASTE WATER, SEWAGE, OR SLUDGE
- C02F—TREATMENT OF WATER, WASTE WATER, SEWAGE, OR SLUDGE
- C02F2209/00—Controlling or monitoring parameters in water treatment
- C02F2209/08—Chemical Oxygen Demand [COD]; Biological Oxygen Demand [BOD]
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- C—CHEMISTRY; METALLURGY
- C02—TREATMENT OF WATER, WASTE WATER, SEWAGE, OR SLUDGE
- C02F—TREATMENT OF WATER, WASTE WATER, SEWAGE, OR SLUDGE
- C02F2209/00—Controlling or monitoring parameters in water treatment
- C02F2209/10—Solids, e.g. total solids [TS], total suspended solids [TSS] or volatile solids [VS]
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- C—CHEMISTRY; METALLURGY
- C02—TREATMENT OF WATER, WASTE WATER, SEWAGE, OR SLUDGE
- C02F—TREATMENT OF WATER, WASTE WATER, SEWAGE, OR SLUDGE
- C02F2303/00—Specific treatment goals
- C02F2303/22—Eliminating or preventing deposits, scale removal, scale prevention
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- Engineering & Computer Science (AREA)
- Environmental & Geological Engineering (AREA)
- Water Supply & Treatment (AREA)
- Chemical & Material Sciences (AREA)
- Organic Chemistry (AREA)
- Fertilizers (AREA)
- Water Treatment By Sorption (AREA)
- Biological Treatment Of Waste Water (AREA)
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Abstract
The invention discloses a kind of for handling the sewage-treating agent of fermentation waste water, is made of the raw material below according to parts by weight: 23-27 parts of diatomite, 14-18 parts of cross-linked rectorite, 10-15 parts of zeolite, 5-9 parts of polydimethyl diallyl ammonium chloride, 30-35 parts of stalk, 15-20 parts of polymeric aluminum sulfate iron, 12-16 parts of chitosan, 7-10 parts of sodium metasilicate, 3-6 parts of butyl stearate, 4-9 parts of aminotrimethylenephosphonic acid, 11-15 parts of polyethyleneimine.The invention also discloses described for handling the preparation method of the sewage-treating agent of fermentation waste water.Sewage-treating agent prepared by the present invention can be effectively reduced COD, BOD, SS and metal ion content in fermentation waste water to the high treating effect of fermentation waste water, and the physical and chemical index of fermentation waste water after treatment can reach discharge standard.
Description
Technical field
The present invention relates to technical field of sewage, it is specifically a kind of for handle fermentation waste water sewage-treating agent and its
Preparation method.
Background technique
Fermentation industry is using grain and agricultural and sideline product as the processing industry of primary raw material.It mainly includes alcohol, monosodium glutamate, shallow lake
The industries such as powder, white wine, citric acid, starch sugar.For China's national situation, deep processing and the industrialization of crops and industrial crops are
Promote Sustainable Development of Agriculture, improve farmers' income, improve Rural-urban Gap, realizes the core hand of national economy balanced development
Section.But since the problems such as fermentation industry water consumption is big, and waste discharge is seriously polluted, restricts the sustainable development of fermentation industry.Cause
This, developing efficient, energy conservation and the suitable actual wastewater treatment of China's fermentation industry and process for reclaiming technology is to solve above-mentioned ask
One of key link of topic.
Currently, processing fermentation industry pollution problem has the various methods such as physics, chemistry, biology, but physical method is deposited more
It is bad in treatment effect, handling rate instability problem；Biological method processing cost is excessively high, is not suitable for promoting the use of；It is more to use
Chemical method handles sewage, but existing sewage-treating agent, agent formulations have secondary pollution, also can to environment
It has a certain impact.
Summary of the invention
The purpose of the present invention is to provide a kind of sewage-treating agents and preparation method thereof for handling fermentation waste water, with solution
Certainly the problems mentioned above in the background art.
To achieve the above object, the invention provides the following technical scheme:
It is a kind of for handling the sewage-treating agent of fermentation waste water, be made of the raw material below according to parts by weight: diatomite 23-
27 parts, it is 14-18 parts of cross-linked rectorite, 10-15 parts of zeolite, 5-9 parts of polydimethyl diallyl ammonium chloride, 30-35 parts of stalk, poly-
Close aluminium iron sulfate 15-20 parts, 12-16 parts of chitosan, 7-10 parts of sodium metasilicate, 3-6 parts of butyl stearate, aminotrimethylenephosphonic acid 4-
9 parts, 11-15 parts of polyethyleneimine.
As a further solution of the present invention: the stalk is combined by corn stover and rape stalk according to weight ratio 2:1
It forms.
As further scheme of the invention: be made of the raw material below according to parts by weight: 24-26 parts of diatomite is handed over
Join rectorite 15-17 parts, 11-14 parts of zeolite, 6-8 parts of polydimethyl diallyl ammonium chloride, 31-34 parts of stalk, polyaluminum sulfate
16-19 parts of ferro-aluminum, 8-9 parts of sodium metasilicate, 4-5 parts of butyl stearate, 5-8 parts of aminotrimethylenephosphonic acid, gathers 13-15 parts of chitosan
12-14 parts of aziridine.
As further scheme of the invention: be made of the raw material below according to parts by weight: 25 parts of diatomite, crosslinking are tired
Hold in the palm 16 parts of stone, 13 parts of zeolite, 7 parts of polydimethyl diallyl ammonium chloride, 33 parts of stalk, 18 parts of polymeric aluminum sulfate iron, chitosan
14 parts, 9 parts of sodium metasilicate, 4 parts of butyl stearate, 7 parts of aminotrimethylenephosphonic acid, 13 parts of polyethyleneimine.
The preparation method of the sewage-treating agent for being used to handle fermentation waste water, steps are as follows:
1) diatomite and cross-linked rectorite are weighed, after crushing, ground and mixed 1-2h, cross 80-100 mesh, be then added to
In calcining furnace, the calcination processing 50-60min at 620-650 DEG C obtains calcining material；
2) will calcine feed powder it is broken after, cross 60-80 mesh, obtain calcined powder, it is spare；
3) stalk is weighed, after crushing, the drying and processing 2-3h at 120-150 DEG C obtains stalk powder, spare；
4) polydimethyl diallyl ammonium chloride, sodium metasilicate and aminotrimethylenephosphonic acid are weighed, after merging, 15-20 is added
The water of times weight, is stirred 30-40min at 75-80 DEG C, is then added calcined powder, after ball milling mixing 3-4h, is starched
Material；
5) butyl stearate is weighed, calcined powder and butyl stearate are added into slurry, is stirred at 75-80 DEG C mixed
50-60min is closed, mixture A is obtained；
6) it by after mixture A vacuum drying, crushes, crosses 60-80 mesh, obtain mixture B；
7) zeolite is weighed, after crushing, 60-80 mesh is crossed, obtains zeolite powder；
8) polymeric aluminum sulfate iron, chitosan and polyethyleneimine are weighed, after mixing, mixture B, stalk powder is added
And zeolite powder, after continueing to mix uniformly.
Compared with prior art, the beneficial effects of the present invention are:
Sewage-treating agent prepared by the present invention can be effectively reduced in fermentation waste water the high treating effect of fermentation waste water
The physical and chemical index of COD, BOD, SS and metal ion content, fermentation waste water after treatment can reach discharge standard.This hair
The sewage-treating agent of bright preparation is easy to use, and dosage is few, high treating effect, and performance is stablized, and stalk is used in its raw material,
Turn waste into wealth, reduces cost of sewage disposal.
Specific embodiment
Technical solution of the present invention is described in more detail With reference to embodiment.
Embodiment 1
It is a kind of for handling the sewage-treating agent of fermentation waste water, be made of the raw material below according to parts by weight: diatomite 23
Part, 14 parts of cross-linked rectorite, 10 parts of zeolite, 5 parts of polydimethyl diallyl ammonium chloride, 30 parts of stalk, polymeric aluminum sulfate iron 15
Part, 12 parts of chitosan, 7 parts of sodium metasilicate, 3 parts of butyl stearate, 4 parts of aminotrimethylenephosphonic acid, 11 parts of polyethyleneimine；Wherein,
The stalk is composed of corn stover and rape stalk according to weight ratio 2:1.
In the present embodiment, described for handling the preparation method of the sewage-treating agent of fermentation waste water, steps are as follows:
1) diatomite and cross-linked rectorite are weighed, after crushing, ground and mixed 1h crosses 80 meshes, is then added to calcining furnace
In, the calcination processing 50min at 620 DEG C obtains calcining material；
2) will calcine feed powder it is broken after, cross 60 meshes, obtain calcined powder, it is spare；
3) stalk is weighed, after crushing, the drying and processing 2h at 120 DEG C obtains stalk powder, spare；
4) polydimethyl diallyl ammonium chloride, sodium metasilicate and aminotrimethylenephosphonic acid are weighed, after merging, 15 times of weights are added
The water of amount is stirred 30min at 75 DEG C, is then added calcined powder, after ball milling mixing 3h, obtains slurry；
5) butyl stearate is weighed, calcined powder and butyl stearate are added into slurry, is stirred at 75 DEG C
50min obtains mixture A；
6) it by after mixture A vacuum drying, crushes, crosses 60 meshes, obtain mixture B；
7) zeolite is weighed, after crushing, 60 meshes is crossed, obtains zeolite powder；
8) polymeric aluminum sulfate iron, chitosan and polyethyleneimine are weighed, after mixing, mixture B, stalk powder is added
And zeolite powder, after continueing to mix uniformly.
Embodiment 2
It is a kind of for handling the sewage-treating agent of fermentation waste water, be made of the raw material below according to parts by weight: diatomite 24
Part, 15 parts of cross-linked rectorite, 11 parts of zeolite, 6 parts of polydimethyl diallyl ammonium chloride, 34 parts of stalk, polymeric aluminum sulfate iron 19
Part, 15 parts of chitosan, 9 parts of sodium metasilicate, 4 parts of butyl stearate, 5 parts of aminotrimethylenephosphonic acid, 14 parts of polyethyleneimine；Wherein,
The stalk is composed of corn stover and rape stalk according to weight ratio 2:1.
In the present embodiment, described for handling the preparation method of the sewage-treating agent of fermentation waste water, steps are as follows:
1) diatomite and cross-linked rectorite are weighed, after crushing, ground and mixed 1.5h crosses 80 meshes, is then added to calcining
In furnace, the calcination processing 50min at 630 DEG C obtains calcining material；
2) will calcine feed powder it is broken after, cross 70 meshes, obtain calcined powder, it is spare；
3) stalk is weighed, after crushing, the drying and processing 2h at 130 DEG C obtains stalk powder, spare；
4) polydimethyl diallyl ammonium chloride, sodium metasilicate and aminotrimethylenephosphonic acid are weighed, after merging, 16 times of weights are added
The water of amount is stirred 30min at 75 DEG C, is then added calcined powder, after ball milling mixing 3.5h, obtains slurry；
5) butyl stearate is weighed, calcined powder and butyl stearate are added into slurry, is stirred at 76 DEG C
52min obtains mixture A；
6) it by after mixture A vacuum drying, crushes, crosses 70 meshes, obtain mixture B；
7) zeolite is weighed, after crushing, 80 meshes is crossed, obtains zeolite powder；
8) polymeric aluminum sulfate iron, chitosan and polyethyleneimine are weighed, after mixing, mixture B, stalk powder is added
And zeolite powder, after continueing to mix uniformly.
Embodiment 3
It is a kind of for handling the sewage-treating agent of fermentation waste water, be made of the raw material below according to parts by weight: diatomite 25
Part, 16 parts of cross-linked rectorite, 13 parts of zeolite, 7 parts of polydimethyl diallyl ammonium chloride, 33 parts of stalk, polymeric aluminum sulfate iron 18
Part, 14 parts of chitosan, 9 parts of sodium metasilicate, 4 parts of butyl stearate, 7 parts of aminotrimethylenephosphonic acid, 13 parts of polyethyleneimine；Wherein,
The stalk is composed of corn stover and rape stalk according to weight ratio 2:1.
In the present embodiment, described for handling the preparation method of the sewage-treating agent of fermentation waste water, steps are as follows:
1) diatomite and cross-linked rectorite are weighed, after crushing, ground and mixed 1.5h crosses 90 meshes, is then added to calcining
In furnace, the calcination processing 55min at 640 DEG C obtains calcining material；
2) will calcine feed powder it is broken after, cross 70 meshes, obtain calcined powder, it is spare；
3) stalk is weighed, after crushing, the drying and processing 2.5h at 140 DEG C obtains stalk powder, spare；
4) polydimethyl diallyl ammonium chloride, sodium metasilicate and aminotrimethylenephosphonic acid are weighed, after merging, 18 times of weights are added
The water of amount is stirred 35min at 78 DEG C, is then added calcined powder, after ball milling mixing 3.5h, obtains slurry；
5) butyl stearate is weighed, calcined powder and butyl stearate are added into slurry, is stirred at 78 DEG C
55min obtains mixture A；
6) it by after mixture A vacuum drying, crushes, crosses 70 meshes, obtain mixture B；
7) zeolite is weighed, after crushing, 70 meshes is crossed, obtains zeolite powder；
8) polymeric aluminum sulfate iron, chitosan and polyethyleneimine are weighed, after mixing, mixture B, stalk powder is added
And zeolite powder, after continueing to mix uniformly.
Embodiment 4
It is a kind of for handling the sewage-treating agent of fermentation waste water, be made of the raw material below according to parts by weight: diatomite 26
Part, 17 parts of cross-linked rectorite, 14 parts of zeolite, 8 parts of polydimethyl diallyl ammonium chloride, 31 parts of stalk, polymeric aluminum sulfate iron 16
Part, 13 parts of chitosan, 8 parts of sodium metasilicate, 5 parts of butyl stearate, 8 parts of aminotrimethylenephosphonic acid, 12 parts of polyethyleneimine；Wherein,
The stalk is composed of corn stover and rape stalk according to weight ratio 2:1.
In the present embodiment, described for handling the preparation method of the sewage-treating agent of fermentation waste water, steps are as follows:
1) diatomite and cross-linked rectorite are weighed, after crushing, ground and mixed 1.5h is sieved with 100 mesh sieve, and is then added to calcining
In furnace, the calcination processing 55min at 640 DEG C obtains calcining material；
2) will calcine feed powder it is broken after, cross 80 meshes, obtain calcined powder, it is spare；
3) stalk is weighed, after crushing, the drying and processing 3h at 140 DEG C obtains stalk powder, spare；
4) polydimethyl diallyl ammonium chloride, sodium metasilicate and aminotrimethylenephosphonic acid are weighed, after merging, 20 times of weights are added
The water of amount is stirred 37min at 80 DEG C, is then added calcined powder, after ball milling mixing 3h, obtains slurry；
5) butyl stearate is weighed, calcined powder and butyl stearate are added into slurry, is stirred at 78 DEG C
55min obtains mixture A；
6) it by after mixture A vacuum drying, crushes, crosses 80 meshes, obtain mixture B；
7) zeolite is weighed, after crushing, 80 meshes is crossed, obtains zeolite powder；
8) polymeric aluminum sulfate iron, chitosan and polyethyleneimine are weighed, after mixing, mixture B, stalk powder is added
And zeolite powder, after continueing to mix uniformly.
Embodiment 5
It is a kind of for handling the sewage-treating agent of fermentation waste water, be made of the raw material below according to parts by weight: diatomite 27
Part, 18 parts of cross-linked rectorite, 15 parts of zeolite, 9 parts of polydimethyl diallyl ammonium chloride, 35 parts of stalk, polymeric aluminum sulfate iron 20
Part, 16 parts of chitosan, 10 parts of sodium metasilicate, 6 parts of butyl stearate, 9 parts of aminotrimethylenephosphonic acid, 15 parts of polyethyleneimine；Wherein,
The stalk is composed of corn stover and rape stalk according to weight ratio 2:1.
In the present embodiment, described for handling the preparation method of the sewage-treating agent of fermentation waste water, steps are as follows:
1) diatomite and cross-linked rectorite are weighed, after crushing, ground and mixed 2h is sieved with 100 mesh sieve, and is then added to calcining furnace
In, the calcination processing 60min at 650 DEG C obtains calcining material；
2) will calcine feed powder it is broken after, cross 80 meshes, obtain calcined powder, it is spare；
3) stalk is weighed, after crushing, the drying and processing 3h at 150 DEG C obtains stalk powder, spare；
4) polydimethyl diallyl ammonium chloride, sodium metasilicate and aminotrimethylenephosphonic acid are weighed, after merging, 20 times of weights are added
The water of amount is stirred 40min at 80 DEG C, is then added calcined powder, after ball milling mixing 4h, obtains slurry；
5) butyl stearate is weighed, calcined powder and butyl stearate are added into slurry, is stirred at 80 DEG C
60min obtains mixture A；
6) it by after mixture A vacuum drying, crushes, crosses 80 meshes, obtain mixture B；
7) zeolite is weighed, after crushing, 80 meshes is crossed, obtains zeolite powder；
8) polymeric aluminum sulfate iron, chitosan and polyethyleneimine are weighed, after mixing, mixture B, stalk powder is added
And zeolite powder, after continueing to mix uniformly.
Sewage-treating agent prepared by the present invention can be effectively reduced in fermentation waste water the high treating effect of fermentation waste water
The physical and chemical index of COD, BOD, SS and metal ion content, fermentation waste water after treatment can reach discharge standard.This hair
The sewage-treating agent of bright preparation is easy to use, and dosage is few, high treating effect, and performance is stablized, and stalk is used in its raw material,
Turn waste into wealth, reduces cost of sewage disposal.
Better embodiment of the invention is explained in detail above, but the present invention is not limited to above-mentioned embodiment party
Formula within the knowledge of one of ordinary skill in the art can also be without departing from the purpose of the present invention
Various changes can be made.
Claims (1)
1. a kind of for handling the sewage-treating agent of fermentation waste water, which is characterized in that be made of the raw material below according to parts by weight:
25 parts of diatomite, 16 parts of cross-linked rectorite, 13 parts of zeolite, 7 parts of polydimethyl diallyl ammonium chloride, 33 parts of stalk, polymerised sulphur
18 parts of sour ferro-aluminum, 14 parts of chitosan, 9 parts of sodium metasilicate, 4 parts of butyl stearate, 7 parts of aminotrimethylenephosphonic acid, polyethyleneimine 13
Part；
The stalk is composed of corn stover and rape stalk according to weight ratio 2:1；
The preparation method of the sewage-treating agent for handling fermentation waste water, steps are as follows:
1) diatomite and cross-linked rectorite are weighed, after crushing, ground and mixed 1-2h crosses 80-100 mesh, is then added to calcining
In furnace, the calcination processing 50-60min at 620-650 DEG C obtains calcining material；
2) will calcine feed powder it is broken after, cross 60-80 mesh, obtain calcined powder, it is spare；
3) stalk is weighed, after crushing, the drying and processing 2-3h at 120-150 DEG C obtains stalk powder, spare；
4) polydimethyl diallyl ammonium chloride, sodium metasilicate and aminotrimethylenephosphonic acid are weighed, after merging, 15-20 times is added and weighs
The water of amount is stirred 30-40min at 75-80 DEG C, is then added calcined powder, after ball milling mixing 3-4h, obtains slurry；
5) butyl stearate is weighed, calcined powder and butyl stearate are added into slurry, is stirred at 75-80 DEG C
50-60min obtains mixture A；
6) it by after mixture A vacuum drying, crushes, crosses 60-80 mesh, obtain mixture B；
7) zeolite is weighed, after crushing, 60-80 mesh is crossed, obtains zeolite powder；
8) polymeric aluminum sulfate iron, chitosan and polyethyleneimine are weighed, after mixing, mixture B, stalk powder and boiling is added
Mountain flour, after continueing to mix uniformly.
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| CN107522281A (en) * | 2017-10-19 | 2017-12-29 | 张永华 | A kind of preparation method for the algicide administered for water-surface blue-green algae |
| CN107793002A (en) * | 2017-11-22 | 2018-03-13 | 郑州源冉生物技术有限公司 | A kind of River Mud inorganic agent and preparation method thereof |
| CN108046346A (en) * | 2017-12-14 | 2018-05-18 | 张培磊 | It is a kind of for the inorganic agent in pollution administration river and preparation method thereof |
| CN108408864A (en) * | 2018-05-09 | 2018-08-17 | 东莞市石鼓污水处理有限公司 | A kind of sewage disposal precipitating reagent |
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| CN106241904A (en) * | 2016-08-18 | 2016-12-21 | 桂林市春晓环保科技有限公司 | A kind of high-efficiency sewage treatment agent and preparation method thereof |
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