CN106582546A - Plant dip dyeing liquid used for purifying nitrogen and phosphorus polluted water body and preparation method thereof - Google Patents
Plant dip dyeing liquid used for purifying nitrogen and phosphorus polluted water body and preparation method thereof Download PDFInfo
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- CN106582546A CN106582546A CN201611257026.XA CN201611257026A CN106582546A CN 106582546 A CN106582546 A CN 106582546A CN 201611257026 A CN201611257026 A CN 201611257026A CN 106582546 A CN106582546 A CN 106582546A
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- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
- B01J20/00—Solid sorbent compositions or filter aid compositions; Sorbents for chromatography; Processes for preparing, regenerating or reactivating thereof
- B01J20/22—Solid sorbent compositions or filter aid compositions; Sorbents for chromatography; Processes for preparing, regenerating or reactivating thereof comprising organic material
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- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
- B01J20/00—Solid sorbent compositions or filter aid compositions; Sorbents for chromatography; Processes for preparing, regenerating or reactivating thereof
- B01J20/02—Solid sorbent compositions or filter aid compositions; Sorbents for chromatography; Processes for preparing, regenerating or reactivating thereof comprising inorganic material
- B01J20/10—Solid sorbent compositions or filter aid compositions; Sorbents for chromatography; Processes for preparing, regenerating or reactivating thereof comprising inorganic material comprising silica or silicate
- B01J20/12—Naturally occurring clays or bleaching earth
-
- C—CHEMISTRY; METALLURGY
- C02—TREATMENT OF WATER, WASTE WATER, SEWAGE, OR SLUDGE
- C02F—TREATMENT OF WATER, WASTE WATER, SEWAGE, OR SLUDGE
- C02F1/00—Treatment of water, waste water, or sewage
- C02F1/28—Treatment of water, waste water, or sewage by sorption
- C02F1/288—Treatment of water, waste water, or sewage by sorption using composite sorbents, e.g. coated, impregnated, multi-layered
-
- C—CHEMISTRY; METALLURGY
- C02—TREATMENT OF WATER, WASTE WATER, SEWAGE, OR SLUDGE
- C02F—TREATMENT OF WATER, WASTE WATER, SEWAGE, OR SLUDGE
- C02F2101/00—Nature of the contaminant
- C02F2101/10—Inorganic compounds
- C02F2101/105—Phosphorus compounds
-
- C—CHEMISTRY; METALLURGY
- C02—TREATMENT OF WATER, WASTE WATER, SEWAGE, OR SLUDGE
- C02F—TREATMENT OF WATER, WASTE WATER, SEWAGE, OR SLUDGE
- C02F2101/00—Nature of the contaminant
- C02F2101/10—Inorganic compounds
- C02F2101/16—Nitrogen compounds, e.g. ammonia
Abstract
The invention discloses plant dip dyeing liquid used for purifying a nitrogen and phosphorus polluted water body and a preparation method thereof. According to a formula, the plant dip dyeing liquid is composed of the following raw materials of, by weight, 10-50 parts of calamus, 10-50 parts of water spinach, 1-10 parts of a potassium permanganate solution, 100-200 parts of allyl monomers, 60-150 parts of clay, 10-30 parts of auxiliary raw materials and 500-1000 parts of sterile water. The calamus and the water spinach are used as the plant raw materials, extracted and combined with the two materials of the allyl monomers and the clay, the nitrogen and phosphorus treatment degree is improved, the plant dip dyeing liquid is low in cost, and only swells instead of being dissolved, the mass transfer resistance to an adsorbent in the adsorption process can be reduced to enable an adsorption system to rapidly reach adsorption equilibrium, and the using range of the plant dip dyeing liquid prepared from the calamus and the water spinach through dilution is enlarged.
Description
Technical field
The present invention relates to technical field of water body purification, specially a kind of plant dip-dyeing solution for purifying water body nitrogen and phosphorus pollution
And preparation method thereof.
Background technology
With China's industrial progress and social development, water pollution is also on the rise, into a difficult problem for environmental improvement.According to environment
Department monitors, and the daily at least 100,000,000 tons sewage in national cities and towns are unprocessed to be directly discharged into water body.In national seven big water systems half with
Upper section water quality is contaminated, and the water body in the whole nation 1/3 is unsuitable for Fish Survival, and 1/4 water body is unsuitable for irrigating, 90% city
Water pollution is serious, and 50% cities and towns water source does not meet drinking water standard.With economic continuous development, these statistical datas are also
Continuing to increase.
Water pollution is mainly caused by the pollutant of mankind's activity generation, and it includes industrial pollution source, agricultural pollution source
With domestic pollution source three parts.Industrial wastewater is the important polluter in waters, with big, the wide, complicated component of amount, toxicity
Greatly, be difficult purification, it is difficult the features such as.Agricultural pollution source includes excrement of animals, pesticide, chemical fertilizer etc..China is water and soil in the world
One of country of most serious is lost in, about 5,000,000,000 tons of annual ground surface soil number of dropouts causes a large amount of pesticide, chemical fertilizer to flow into ground surface soil
River, river, lake, storehouse, the nitrogen being lost in therewith, phosphorus, potassium nutrition element, the lake for making 2/3 is subject to different degrees of eutrophication pollution
Harm, causes algae and other biological distorted proliferation, causes the change of water transparency and dissolved oxygen, so as to cause water quality to be disliked
Change.Domestic pollution source is mainly the various detergents used in urban life and sewage, rubbish, feces etc., mostly nontoxic nothing
Machine salt, many containing nitrogen phosphate and sulfur in sanitary sewage, malignant bacteria is more.
Nitrogen and phosphorus, as inorganic nutrient substance, are the main matters for causing water pollution and eutrophication.Therefore, effectively go
Except nitrogen and phosphorus in sewage, to protecting water environment significant.That what is reported both at home and abroad at present denitrogenates phosphorus method
Mainly there are chemical method, the sedimentation method, biochemical process and absorption method.In these methods, adsorption technology is because with convenient and swift, efficient
The features such as, more and more concerns for causing people.The core of adsorption technology is to select suitable adsorbing material.Activated carbon is most normal
Water treatment absorbent, but its is expensive, separates difficult, regeneration condition harshness, and adsorption effect is undesirable.In recent years,
Adsorption treatment is carried out using molecular sieve or cheap clay to Nitrogen-and Phosphorus-containing waste water also to have been reported that, but adsorption time is long, adsorption capacity
It is low.
Therefore a kind of plant dip-dyeing solution for purifying water body nitrogen and phosphorus pollution is designed, is reached with reference to the purification of plant
The effect of water body purification.
The content of the invention
For achieving the above object, the present invention provides following technical scheme：A kind of plant for purifying water body nitrogen and phosphorus pollution
Dip-dyeing solution, its formula is made up of according to parts by weight the following raw material：
Rhizoma Acori Graminei 10-50 parts, water spinach 10-50 parts, potassium permanganate solution 1-10 parts, vinyl monomer 100-200 parts, clay
60-150 parts, auxiliary material 10-30 parts, sterilized water 500-1000 parts.
Preferably, its formula is made up of according to parts by weight the following raw material：
10 parts of Rhizoma Acori Graminei, 10 parts of water spinach, 1 part of potassium permanganate solution, 100 parts of vinyl monomer, 60 parts of clay, auxiliary material 10
Part, 500 parts of sterilized water.
Preferably, its formula is made up of according to parts by weight the following raw material：
50 parts of Rhizoma Acori Graminei, 50 parts of water spinach, 10 parts of potassium permanganate solution, 200 parts of vinyl monomer, 150 parts of clay, auxiliary material
30 parts, 1000 parts of sterilized water.
In addition the present invention have also been devised a kind of preparation method of the plant dip-dyeing solution for purifying water body nitrogen and phosphorus pollution, including
Following steps：
(1) two kinds of plants of Rhizoma Acori Graminei and water spinach are selected to extract raw material as dip-dyeing solution；
(2) above two plant is completely won, with clean water 2-4 time, and with clear water soaks 4-6 hours again；
(3) after being crushed, sieved with Microdisintegrator, 6-8 gram of plant coarse powder is weighed respectively；
(4) the plant coarse powder for obtaining is used respectively with potassium permanganate solution after soak at room temperature extracts 40-60 hour
Filter paper filters extracting solution；
(5) extracting solution after filtration is added into vinyl monomer, clay and auxiliary material, and 50-100 is diluted with sterilized water
Times, mix homogeneously；
(6) again impurity is filtered by filtration and obtains plant dip-dyeing solution.
Used as a kind of preferred scheme of the present invention, the potassium permanganate solution is 0.1% potassium permanganate solution.
As a kind of preferred scheme of the present invention, the auxiliary material be it is a kind of in shitosan, humic acid, polyvinyl alcohol or
Several combinations.
Used as a kind of preferred scheme of the present invention, the clay needs first to be suspended in the aqueous solution of alcohol, adds extraction
In liquid.
Compared with prior art, the invention has the beneficial effects as follows：By the use of Rhizoma Acori Graminei and water spinach as plant material, Jing Guoti
Take and with reference to vinyl monomer and clay bi-material, strengthen the degree for the treatment of of nitrogen phosphorus, the dip-dyeing solution cost is relatively low, in nitrogen phosphorus solution
In it is only swelling and insoluble, the resistance to mass tranfer in adsorbent adsorption process can be reduced, make absorption system quickly reach adsorption equilibrium,
And plant dip-dyeing solution is prepared into using Rhizoma Acori Graminei and water spinach, and by dilution, expands its use range.
Specific embodiment
In below in conjunction with the embodiment of the present invention, the technical scheme in the embodiment of the present invention is clearly and completely retouched
State, it is clear that described embodiment is only a part of embodiment of the invention, rather than the embodiment of whole.Based on the present invention
In embodiment, the every other enforcement that those of ordinary skill in the art are obtained under the premise of creative work is not made
Example, belongs to the scope of protection of the invention.
Embodiment 1：
A kind of plant dip-dyeing solution for purifying water body nitrogen and phosphorus pollution, its formula is according to parts by weight by the following raw material group
Into：
10 parts of Rhizoma Acori Graminei, 10 parts of water spinach, 1 part of potassium permanganate solution, 100 parts of vinyl monomer, 60 parts of clay, auxiliary material 10
Part, 500 parts of sterilized water.
Its preparation method comprises the steps：
(1) two kinds of plants of Rhizoma Acori Graminei and water spinach are selected to extract raw material as dip-dyeing solution；
(2) above two plant is completely won, with clean water 2 times, and is soaked 4 hours with clear water again；
(3) after being crushed, sieved with Microdisintegrator, 6 grams of plant coarse powder are weighed respectively；
(4) the plant coarse powder for obtaining is used respectively with 0.1% potassium permanganate solution after soak at room temperature extracts 40 hours
Filter paper filters extracting solution；
(5) vinyl monomer, clay and auxiliary material, clay is added to need the water for first being suspended in alcohol the extracting solution after filtration
In solution, in adding extracting solution, and 50 times are diluted with sterilized water, mix homogeneously；
(6) again impurity is filtered by filtration and obtains plant dip-dyeing solution.
The auxiliary material is one or more combination in shitosan, humic acid, polyvinyl alcohol.
Embodiment 2：
A kind of plant dip-dyeing solution for purifying water body nitrogen and phosphorus pollution, its formula is according to parts by weight by the following raw material group
Into：
25 parts of Rhizoma Acori Graminei, 25 parts of water spinach, 5 parts of potassium permanganate solution, 150 parts of vinyl monomer, 90 parts of clay, auxiliary material 20
Part, 750 parts of sterilized water.
Its preparation method comprises the steps：
(1) two kinds of plants of Rhizoma Acori Graminei and water spinach are selected to extract raw material as dip-dyeing solution；
(2) above two plant is completely won, with clean water 3 times, and is soaked 5 hours with clear water again；
(3) after being crushed, sieved with Microdisintegrator, 7 grams of plant coarse powder are weighed respectively；
(4) the plant coarse powder for obtaining is used respectively with 0.1% potassium permanganate solution after soak at room temperature extracts 50 hours
Filter paper filters extracting solution；
(5) vinyl monomer, clay and auxiliary material, clay is added to need first to be suspended in alcohol the extracting solution after filtration
In aqueous solution, in adding extracting solution, and 75 times are diluted with sterilized water, mix homogeneously；
(6) again impurity is filtered by filtration and obtains plant dip-dyeing solution.
The auxiliary material is one or more combination in shitosan, humic acid, polyvinyl alcohol.
Embodiment 3：
A kind of plant dip-dyeing solution for purifying water body nitrogen and phosphorus pollution, its formula is according to parts by weight by the following raw material group
Into：
50 parts of Rhizoma Acori Graminei, 50 parts of water spinach, 10 parts of potassium permanganate solution, 200 parts of vinyl monomer, 150 parts of clay, auxiliary material
30 parts, 1000 parts of sterilized water.
Its preparation method comprises the steps：
(1) two kinds of plants of Rhizoma Acori Graminei and water spinach are selected to extract raw material as dip-dyeing solution；
(2) above two plant is completely won, with clean water 5 times, and is soaked 6 hours with clear water again；
(3) after being crushed, sieved with Microdisintegrator, 8 grams of plant coarse powder are weighed respectively；
(4) the plant coarse powder for obtaining is used respectively with 0.1% potassium permanganate solution after soak at room temperature extracts 60 hours
Filter paper filters extracting solution；
(5) vinyl monomer, clay and auxiliary material, clay is added to need the water for first being suspended in alcohol the extracting solution after filtration
In solution, in adding extracting solution, and 100 times are diluted with sterilized water, mix homogeneously；
(6) again impurity is filtered by filtration and obtains plant dip-dyeing solution.
The auxiliary material is one or more combination in shitosan, humic acid, polyvinyl alcohol.
By the use of Rhizoma Acori Graminei and water spinach as plant material, through extracting and with reference to vinyl monomer and clay bi-material increase
The degree for the treatment of of strong nitrogen phosphorus, the dip-dyeing solution cost is relatively low, only swelling and insoluble in nitrogen phosphorus solution, can reduce adsorbent absorption
During resistance to mass tranfer, make absorption system quickly reach adsorption equilibrium, and plant leaching is prepared into using Rhizoma Acori Graminei and water spinach
Dye liquor, and by dilution, expand its use range.
The present invention is as follows for the dependence test of Rhizoma Acori Graminei and water spinach：
By Rhizoma Acori Graminei and water spinach using two kinds of strains of A.delicata, G.mosseae and aseptic culture, determine its CDD,
The concentration for the treatment of of TN and TP.Such as following table：(1-9 is Rhizoma Acori Graminei；10-18 is water spinach).
| Sequence number | Botanical name | Strain | Concentration for the treatment of |
| 1 | Rhizoma Acori Graminei | A.delicata | COD 40mg/L TN 2mg/L TP 0.4mg/L |
| 2 | Rhizoma Acori Graminei | A.delicata | COD 200mg/L TN 10mg/L TP 2mg/L |
| 3 | Rhizoma Acori Graminei | A.delicata | COD 800mg/L TN 40mg/L TP 8mg/L |
| 4 | Rhizoma Acori Graminei | G.mosseae | COD 40mg/L TN 2mg/L TP 0.5mg/L |
| 5 | Rhizoma Acori Graminei | G.mosseae | COD 200mg/L TN 10mg/L TP 3mg/L |
| 6 | Rhizoma Acori Graminei | G.mosseae | COD 800mg/L TN 40mg/L TP 9mg/L |
| 7 | Rhizoma Acori Graminei | It is blank | COD 40mg/L TN 2mg/L TP 0.6mg/L |
| 8 | Rhizoma Acori Graminei | It is blank | COD 200mg/L TN 10mg/L TP 4mg/L |
| 9 | Rhizoma Acori Graminei | It is blank | COD 800mg/L TN 40mg/L TP 10mg/L |
| 10 | Water spinach | A.delicata | COD 40mg/L TN 2mg/L TP 0.7mg/L |
| 11 | Water spinach | A.delicata | COD 200mg/L TN 10mg/L TP 5mg/L |
| 12 | Water spinach | A.delicata | COD 800mg/L TN 40mg/L TP 11mg/L |
| 13 | Water spinach | G.mosseae | COD 40mg/L TN 2mg/L TP 0.8mg/L |
| 14 | Water spinach | G.mosseae | COD 200mg/L TN 10mg/L TP 6mg/L |
| 15 | Water spinach | G.mosseae | COD 800mg/L TN 40mg/L TP 12mg/L |
| 16 | Water spinach | It is blank | COD 40mg/L TN 2mg/L TP 0.9mg/L |
| 17 | Water spinach | It is blank | COD 200mg/L TN 10mg/L TP 7mg/L |
| 18 | Water spinach | It is blank | COD 800mg/L TN 40mg/L TP 13mg/L |
(1) for the improving activity of root system test such as following table of water spinach and Rhizoma Acori Graminei：AMF mycorhiza enhance root system of plant to hormone,
The synthesis capability of the nutrient substance such as aminoacid, for the metaboilic level of aerial partss.
(2) it is as follows for the test data of nitrogen phosphorus：AMF mycorhiza promotes the metabolism of plant, thus improving activity of root system is more
It is vigorous, finally accelerate utilization of the plant to nutrients such as moisture, organic matter, Organic carbon and nitrogen phosphorus.
(2) it is as follows for the test data of phosphorus：
(3) test data for COD is as follows：
(4) it is as follows for chlorophyllous test data：AMF mycorhiza promotes the metabolism of plant, improves the work of enzyme
Property, so as to be conducive to the absorption and conversion of Plant To Nutrient material.
It is obvious to a person skilled in the art that the invention is not restricted to the details of above-mentioned one exemplary embodiment, Er Qie
In the case of spirit or essential attributes without departing substantially from the present invention, the present invention can be in other specific forms realized.Therefore, no matter
From the point of view of which point, embodiment all should be regarded as exemplary, and be nonrestrictive, the scope of the present invention is by appended power
Profit is required rather than described above is limited, it is intended that by the institute in the implication and scope of the equivalency of claim that falls
Change and include in the present invention.
Claims (7)
1. a kind of plant dip-dyeing solution for purifying water body nitrogen and phosphorus pollution, it is characterised in that：Its formula is according to parts by weight by such as
Lower raw material composition：
Rhizoma Acori Graminei 10-50 parts, water spinach 10-50 parts, potassium permanganate solution 1-10 parts, vinyl monomer 100-200 parts, clay 60-150
Part, auxiliary material 10-30 parts, sterilized water 500-1000 parts.
2. a kind of plant dip-dyeing solution for purifying water body nitrogen and phosphorus pollution according to claim 1, it is characterised in that：It is matched somebody with somebody
Side is made up of according to parts by weight the following raw material：
10 parts of Rhizoma Acori Graminei, 10 parts of water spinach, 1 part of potassium permanganate solution, 100 parts of vinyl monomer, 60 parts of clay, 10 parts of auxiliary material,
500 parts of sterilized water.
3. a kind of plant dip-dyeing solution for purifying water body nitrogen and phosphorus pollution according to claim 1, it is characterised in that：It is matched somebody with somebody
Side is made up of according to parts by weight the following raw material：
50 parts of Rhizoma Acori Graminei, 50 parts of water spinach, 10 parts of potassium permanganate solution, 200 parts of vinyl monomer, 150 parts of clay, auxiliary material 30
Part, 1000 parts of sterilized water.
4. a kind of preparation method of the plant dip-dyeing solution for purifying water body nitrogen and phosphorus pollution, it is characterised in that：Comprise the steps：
(1) two kinds of plants of Rhizoma Acori Graminei and water spinach are selected to extract raw material as dip-dyeing solution；
(2) above two plant is completely won, with clean water 2-4 time, and with clear water soaks 4-6 hours again；
(3) after being crushed, sieved with Microdisintegrator, 6-8 gram of plant coarse powder is weighed respectively；
(4) the plant coarse powder for obtaining is used into filter paper mistake respectively with potassium permanganate solution after soak at room temperature extracts 40-60 hour
Filter extracting solution；
(5) extracting solution after filtration is added into vinyl monomer, clay and auxiliary material, and 50-100 times is diluted with sterilized water, mixed
Close uniform；
(6) again impurity is filtered by filtration and obtains plant dip-dyeing solution.
5. a kind of plant dip-dyeing solution for purifying water body nitrogen and phosphorus pollution according to claim 4 and preparation method thereof, its
It is characterised by：The potassium permanganate solution is 0.1% potassium permanganate solution.
6. a kind of plant dip-dyeing solution for purifying water body nitrogen and phosphorus pollution according to claim 4 and preparation method thereof, its
It is characterised by：The auxiliary material is one or more combination in shitosan, humic acid, polyvinyl alcohol.
7. a kind of plant dip-dyeing solution for purifying water body nitrogen and phosphorus pollution according to claim 4 and preparation method thereof, its
It is characterised by：The clay needs first to be suspended in the aqueous solution of alcohol, in adding extracting solution.
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| Application Number | Priority Date | Filing Date | Title |
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| CN201611257026.XA CN106582546A (en) | 2016-12-30 | 2016-12-30 | Plant dip dyeing liquid used for purifying nitrogen and phosphorus polluted water body and preparation method thereof |
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|---|---|---|---|
| CN201611257026.XA CN106582546A (en) | 2016-12-30 | 2016-12-30 | Plant dip dyeing liquid used for purifying nitrogen and phosphorus polluted water body and preparation method thereof |
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Cited By (2)
| Publication number | Priority date | Publication date | Assignee | Title |
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| CN107434303A (en) * | 2017-07-31 | 2017-12-05 | 兰溪市普润斯水产养殖技术有限公司 | The processing method of eutrophication aquiculture waste water |
| CN115136969A (en) * | 2022-08-02 | 2022-10-04 | 山西首爱动物药业有限公司 | Modifying agent for water ecological damage |
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| CB03 | Change of inventor or designer information |
Inventor after: Ju Shuming Inventor after: Sun Meng Inventor after: Ji Lingzhen Inventor after: Yin Tingchao Inventor after: Wang Nana Inventor after: Tong Lu Inventor after: Lin Yuanyuan Inventor after: Xu Delan Inventor before: Sun Meng Inventor before: Ju Shuming Inventor before: Ji Lingzhen Inventor before: Yin Tingchao Inventor before: Wang Nana Inventor before: Tong Lu Inventor before: Lin Yuanyuan Inventor before: Xu Delan |
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| RJ01 | Rejection of invention patent application after publication | ||
| RJ01 | Rejection of invention patent application after publication |
Application publication date: 20170426 |