CN106578790A - Duck egg white polypeptide beverage and preparation method thereof - Google Patents
Duck egg white polypeptide beverage and preparation method thereof Download PDFInfo
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- CN106578790A CN106578790A CN201611052738.8A CN201611052738A CN106578790A CN 106578790 A CN106578790 A CN 106578790A CN 201611052738 A CN201611052738 A CN 201611052738A CN 106578790 A CN106578790 A CN 106578790A
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- anas domestica
- ovum anas
- domestica album
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- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
- A23L—FOODS, FOODSTUFFS, OR NON-ALCOHOLIC BEVERAGES, NOT COVERED BY SUBCLASSES A21D OR A23B-A23J; THEIR PREPARATION OR TREATMENT, e.g. COOKING, MODIFICATION OF NUTRITIVE QUALITIES, PHYSICAL TREATMENT; PRESERVATION OF FOODS OR FOODSTUFFS, IN GENERAL
- A23L2/00—Non-alcoholic beverages; Dry compositions or concentrates therefor; Their preparation
- A23L2/38—Other non-alcoholic beverages
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Abstract
The invention provides a duck egg white polypeptide beverage and a preparation method thereof. The preparation method comprises the following steps: with yolk-free duck egg white from a salted duck egg as a raw material, carrying out desalination, enzymatic hydrolysis and purification so as to prepare duck egg white polypeptide liquid with antioxidation activity; blending the duck egg white polypeptide liquid with a composite functional sweetener and water so as to obtain mixed beverage liquid; and carrying out filling and sterilization so as to obtain the duck egg white polypeptide beverage, wherein the duck egg white polypeptide liquid accounts for 2 to 5% of the total mass of the beverage. The prepared duck egg white polypeptide beverage is rich in nutrients, clear and transparent, tastes slippery and agreeably sour and sweet, and has substantial health-care functions; and the preparation method is rational in process, simple to operate and suitable for industrial mass production.
Description
Technical field
The present invention relates to technical field of beverage production, and in particular to a kind of Ovum Anas domestica album polypeptide beverage and preparation method thereof.
Background technology
The nutrition of fowl egg is extremely enriched, containing protein excellent necessary to human body, fat, lipoids, mineral and
The nutrient substance such as vitamin, and digestibility is very high, can be rated as high quality food.Ovum Anas domestica protein is not only required rich in eight kinds
Aminoacid, and ratio is appropriate, needs to be very close to human body.Albumen protein is comparatively ideal high quality protein in food, but
Due to itself intrinsic properties, its application in food processing is limited.Can improve Ovum Anas domestica album using hydrolysis
The functional character of protein, so as to more food can be applied in.
Preserved egg yellow is one of food ingredient that people like, current China's preserved egg yellow industry flourishes and gradually scale
Change, leave lower nearly ten thousand tons of salted egg albumens because producing preserved egg yellow every year, be huge protein resource.Protein content in salted egg albumen
It is abundant, about 10%～11%, but due to salinity height, about 5% in salted egg albumen, high salinity makes its value of exploiting and utilizing
It is extremely limited.Salted egg albumen is only used on a small quantity in the processing of feedstuff, cookiess and sausage；Also someone produces salted egg with salted egg albumen
The product of clear powder fermented bean curd similar with some.But it is very high that these all can not farthest make good use of nutritive value in salted egg albumen
Protein resource.
In recent years, by people's extensive concern, research shows the master of absorption of human body protein to the physiological function of biologically active peptide
Form is wanted not to be aminoacid but polypeptide, the peptide that protein digestion is obtained has the incomparable superiority of protein.So sharp
Biodegradation being carried out with remaining salted egg albumen this high quality protein resource and preparing polypeptide, enzymatic hydrolysate is carried out to isolate and purify desalination
It is a high effective way for improving the additional output value of salted egg albumen to obtain polypeptide products, with significant Development volue.
The content of the invention
It is an object of the invention to provide a kind of Ovum Anas domestica album polypeptide beverage and preparation method thereof, to take out preserved egg yellow after Ovum Anas domestica
Clearly it is raw material, Jing desalinations, enzymolysis, purification are prepared into the Ovum Anas domestica album polypeptide liquid with antioxidant activity, then allocate with other adjuvants,
Fill, sterilization, product is nutritious, clear, sour-sweet moderate, smooth in taste, and has significant health care.
To achieve these goals, the technical solution used in the present invention is as follows：
A kind of Ovum Anas domestica album polypeptide beverage, to take out preserved egg yellow after Ovum Anas domestica album as raw material, Jing desalinations, enzymolysis, purification are prepared into tool
There is the Ovum Anas domestica album polypeptide liquid of antioxidant activity, then beverage blends liquid, Jing fills, sterilization are deployed into complex function sweeting agent and water
Process.
According to above scheme, the complex function sweeting agent includes following component and its accounts for the percentage ratio of beverage gross mass：
Sucrose 5%～8%, sodium carboxymethyl cellulose (CMC-Na) 0.05%～0.15%, xanthan gum 0.05%～0.15%, sucrose ester
0.005%～0.025%, cycloheptaamylose 0.5%～1.5%, citric acid 0.3%～0.8%, Mel 3%～5%.
According to above scheme, it is 2%～5% that the Ovum Anas domestica album polypeptide liquid accounts for the percentage ratio of beverage gross mass.
A kind of preparation method of Ovum Anas domestica album polypeptide beverage, comprises the steps：
1) Ovum Anas domestica album desalination：
1. pretreatment：The drinking water of 1～5 times of quality is added in the Ovum Anas domestica album taken out after preserved egg yellow, stirs homogenizing to reduce duck
The viscosity of Ovum Gallus domesticus album, then with filtered through gauze, remove coarse impurities in Ovum Gallus domesticus album；
2. ultrasonic Treatment：Ultrasonic Treatment will be carried out through the Ovum Anas domestica album of pretreatment；
3. ultrafiltration desalination：Pouring the Ovum Anas domestica album of Jing ultrasonic Treatment into ultrafiltration apparatus carries out ultrafiltration；
4. concentrate：The Ovum Anas domestica album after desalination is carried out into rotary evaporation concentration under water bath using Rotary Evaporators, is concentrated into
0.5～1.5 times of former Ovum Anas domestica album volume；
2) enzymolysis of Ovum Anas domestica album：
1. digest：Add the water of 10～20 times of its quality to be diluted to the Ovum Anas domestica album after desalting processing, add Papain
Enzyme, flavor protease, pH value is 5.0～6.0, and hydrolysis temperature is 50 DEG C, 5～8h of enzyme digestion reaction；
2. enzyme denaturing：Adjust hydrolyzed solution pH value to 4.2-4.5 with citric acid, at 80 DEG C 30min enzyme denaturing is maintained, obtain Ovum Anas domestica album enzymolysis many
Peptide liquid；
3) Ovum Anas domestica album enzymolysis polypeptide liquid purification：
1. eliminating sargassum smell：The Ovum Anas domestica album enzymolysis polypeptide liquid for obtaining is added into the yeast powder of its quality 0.3%～0.8%, temperature 30 is controlled
～50 DEG C, stir, stand 1～2h, carry out defishying；
2. hardship is taken off：Ovum Anas domestica album enzymolysis polypeptide liquid after eliminating sargassum smell is added into the cycloheptaamylose of its quality 0.5%～1%, control temperature
45～55 DEG C of degree, stirs, and carries out de- suffering and manages 5～10min；
3. decolourize：Ovum Anas domestica album enzymolysis polypeptide liquid after de- hardship is added into the kieselguhr of its quality 1%～3% and 1%～3% active
Charcoal, controls 50～70 DEG C of temperature, stirs, and carries out 1～2h of desolventing technology；
4. sucking filtration：The Ovum Anas domestica album enzymolysis polypeptide liquid of Jing desolventing technologies is carried out into vacuum filtration, transparent, free from extraneous odour Ovum Anas domestica album is obtained final product
Polypeptide liquid；
5. concentrate：Transparent, free from extraneous odour Ovum Anas domestica album polypeptide liquid is concentrated in vacuo for the 1/3～1/5 of original volume, it is standby；
4) prepared by Ovum Anas domestica album polypeptide beverage：
1. allocate：Sucrose is added water post-heating dissolving, sodium carboxymethyl cellulose, xanthan gum, sucrose ester is added, fully dissolving
Afterwards, cycloheptaamylose, citric acid, Mel are added, and is stirred, Ovum Anas domestica album polypeptide liquid is added while stirring, obtain Ovum Anas domestica album many
Peptide mixed liquor；
2. fill, sterilization：Deployed Ovum Anas domestica album polypeptide mixed liquor is carried out into fill, sterilization, the sterilization process is：Heat up
10min, sterilize 15～40min at a temperature of 105～115 DEG C, is cooled to central temperature less than 40 DEG C, gets product.
According to above scheme, during the ultrasonic Treatment, ultrasonic power is 1.0kw, and ultrasonic time is 20min, every time
After processing 10S, stop 10S, reprocessing is so recycled to end.
According to above scheme, the pressure during ultrafiltration is 5kPa, and unit temp is 20 DEG C, and the ultrafiltration time is 2h.
According to above scheme, during the concentration, the pressure of Rotary Evaporators is 5kPa, and rotary speed is 50r/min, water-bath
Temperature is 65-75 DEG C, and rotary evaporation concentration time is 1～3h.
According to above scheme, during the enzymolysis, papain, the consumption of flavor protease are：Per the addition of 1ml Ovum Anas domestica album
4000～6000 enzyme-activity units (u/ml substrates).
According to above scheme, during the enzymolysis, papain is 1 with the mass ratio of flavor protease:0.5～2.
According to above scheme, during the decolouring, diatomaceous earth is 1 with the mass ratio of activated carbon:1～3.
Ultrafiltration desalination is a kind of mode using infiltration, is dissolved in water using salt, and the effect sieved by size is by salt
Divide and remove.The relative molecular mass of protein is substantially tens of thousands of in Ovum Gallus domesticus album, it is minimum it is also thousand of more than, and salinity is relative to egg
Just seem very little for white matter, hence with the centrifugation of ultrafiltration, can not only carry out desalting processing, and the material that desalination is obtained
Liquid can be directly thickened to desired concn into the operation of next step again.
The invention has the beneficial effects as follows：
1) present invention carries out clearly desalination and enzymolysis using ultrafiltration apparatus to Salted duck egg, will take the Ovum Anas domestica album proteolysiss after preserved egg yellow
Into easily digested polypeptide and aminoacid, Jing takes off hardship, eliminating sargassum smell, decolouring, sucking filtration and concentration and prepares tool antioxidant activity
Ovum Anas domestica album polypeptide beverage, product is nutritious, smooth in taste, and solves that Ovum Anas domestica album transport is difficult, and cost of transportation is high and dirty
The problem of dye environment；
2) present invention propose a kind of preparation method of Ovum Anas domestica album beverage, solve Ovum Anas domestica album denaturation temperature it is low and hydrolysis after have
The problem of bitterness, makes to become the aminoacid or polypeptide that are conducive to absorption of human body after Ovum Anas domestica album hydrolysis and have good mouthfeel；
3) preparation method rational technology of the invention, it is simple to operate, mass industrialized production can be carried out.
Specific embodiment
Technical scheme is illustrated with reference to embodiment.
Embodiment 1：
The present invention provides a kind of Ovum Anas domestica album polypeptide beverage and preparation method thereof, comprises the steps：
1) Ovum Anas domestica album desalination：
1. pretreatment：The drinking water of 2 times of quality is added in the Ovum Anas domestica album taken out after preserved egg yellow, stirs homogenizing to reduce Ovum Anas domestica album
Viscosity, then with filtered through gauze, remove coarse impurities in Ovum Gallus domesticus album；
2. ultrasonic Treatment：Ultrasonic Treatment will be carried out through the Ovum Anas domestica album of pretreatment, ultrasonic power is 1.0kw, when ultrasonic
Between be 20min, after 10S per treatment, stop 10S, reprocessing, be so recycled to end；
3. ultrafiltration desalination：Pouring the Ovum Anas domestica album of Jing ultrasonic Treatment into ultrafiltration apparatus carries out ultrafiltration, ultrafiltration pressure 5kPa, device temperature
20 DEG C of degree, ultrafiltration time 2h；
4. concentrate：The Ovum Anas domestica album after desalination is carried out into rotary evaporation concentration under water bath using Rotary Evaporators, pressure is
5kPa, rotary speed is 50r/min, and bath temperature is 65 DEG C, and rotary evaporation concentration 1h is concentrated into the 0.8 of former Ovum Anas domestica album volume
Times；2) enzymolysis of Ovum Anas domestica album：
1. digest：Add the water of 18 times of its quality to be diluted to the Ovum Anas domestica album after desalting processing, add papain, wind
Taste protease, pH value is 6.0, and hydrolysis temperature is 50 DEG C, enzyme digestion reaction 5h, the quality of the papain and flavor protease
Than for 1:2, consumption is：Add 5500 enzyme-activity units (u/ml substrates) per 1ml Ovum Anas domestica album；
2. enzyme denaturing：Adjust hydrolyzed solution pH value to 4.3 with citric acid, at 80 DEG C 30min enzyme denaturing is maintained, obtain Ovum Anas domestica album enzymolysis polypeptide
Liquid；3) Ovum Anas domestica album enzymolysis polypeptide liquid purification：
1. eliminating sargassum smell：The Ovum Anas domestica album enzymolysis polypeptide liquid for obtaining is added into the yeast powder of its quality 0.5%, 35 DEG C of temperature, stirring is controlled
Uniformly, 1h is stood, carries out defishying；
2. hardship is taken off：Ovum Anas domestica album enzymolysis polypeptide liquid after eliminating sargassum smell is added into the cycloheptaamylose of its quality 0.7%, temperature 51 is controlled
DEG C, stir, carry out de- suffering reason 8min；
3. decolourize：Ovum Anas domestica album enzymolysis polypeptide liquid after de- hardship is added into the kieselguhr and 1% activated carbon of its quality 1%, control temperature
60 DEG C of degree, stirs, and carries out desolventing technology 1.5h；
4. sucking filtration：The Ovum Anas domestica album enzymolysis polypeptide liquid of Jing desolventing technologies is carried out into vacuum filtration, transparent, free from extraneous odour Ovum Anas domestica album is obtained final product
Polypeptide liquid；
5. concentrate：Transparent, free from extraneous odour Ovum Anas domestica album polypeptide liquid is concentrated in vacuo for the 1/3 of original volume, it is standby；
4) prepared by Ovum Anas domestica album polypeptide beverage：
1. allocate：Add 6% sucrose by beverage gross mass, the post-heating that adds water dissolving adds 0.08%CMC-Na, 0.09% yellow
After virgin rubber and 0.015% sucrose ester, fully dissolving, 1.0% cycloheptaamylose, 0.6% citric acid and 5% Mel are added, and stirred
Mix uniform, 4% Ovum Anas domestica album polypeptide liquid is added while stirring, obtain Ovum Anas domestica album polypeptide mixed liquor；
2. fill, sterilization：Deployed Ovum Anas domestica album polypeptide mixed liquor is carried out into fill, sterilization, the sterilization process is：Heat up
10min, sterilize 30min at a temperature of 110 DEG C, is cooled to central temperature less than 40 DEG C, gets product.
Embodiment 2：
The present invention provides a kind of Ovum Anas domestica album polypeptide beverage and preparation method thereof, comprises the steps：
1) Ovum Anas domestica album desalination：
1. pretreatment：The drinking water of 3 times of quality is added in the Ovum Anas domestica album taken out after preserved egg yellow, stirs homogenizing to reduce Ovum Anas domestica album
Viscosity, then with filtered through gauze, remove coarse impurities in Ovum Gallus domesticus album；
2. ultrasonic Treatment：Ultrasonic Treatment will be carried out through the Ovum Anas domestica album of pretreatment, ultrasonic power is 1.0kw, when ultrasonic
Between be 20min, after 10S per treatment, stop 10S, reprocessing, be so recycled to end；
3. ultrafiltration desalination：Pouring the Ovum Anas domestica album of Jing ultrasonic Treatment into ultrafiltration apparatus carries out ultrafiltration, ultrafiltration pressure 5kPa, device temperature
20 DEG C of degree, ultrafiltration time 2h；
4. concentrate：The Ovum Anas domestica album after desalination is carried out into rotary evaporation concentration under water bath using Rotary Evaporators, pressure is
5kPa, rotary speed is 50r/min, and bath temperature is 70 DEG C, and rotary evaporation concentration 1h is concentrated into 1 times of former Ovum Anas domestica album volume；
2) enzymolysis of Ovum Anas domestica album：
1. digest：Add the water of 20 times of its quality to be diluted to the Ovum Anas domestica album after desalting processing, add papain, wind
Taste protease, pH value is 5.5, and hydrolysis temperature is 50 DEG C, enzyme digestion reaction 6h, the quality of the papain and flavor protease
Than for 1:1.5, consumption is：Add 4500 enzyme-activity units (u/ml substrates) per 1ml Ovum Anas domestica album；
2. enzyme denaturing：Adjust hydrolyzed solution pH value to 4.4 with citric acid, at 80 DEG C 30min enzyme denaturing is maintained, obtain Ovum Anas domestica album enzymolysis polypeptide
Liquid；3) Ovum Anas domestica album enzymolysis polypeptide liquid purification：
1. eliminating sargassum smell：The Ovum Anas domestica album enzymolysis polypeptide liquid for obtaining is added into the yeast powder of its quality 0.6%, 40 DEG C of temperature, stirring is controlled
Uniformly, 1.5h is stood, carries out defishying；
2. hardship is taken off：Ovum Anas domestica album enzymolysis polypeptide liquid after eliminating sargassum smell is added into the cycloheptaamylose of its quality 0.6%, temperature 52 is controlled
DEG C, stir, carry out de- suffering reason 7min；
3. decolourize：Ovum Anas domestica album enzymolysis polypeptide liquid after de- hardship is added into the kieselguhr and 2% activated carbon of its quality 2%, control temperature
55 DEG C of degree, stirs, and carries out desolventing technology 2h；
4. sucking filtration：The Ovum Anas domestica album enzymolysis polypeptide liquid of Jing desolventing technologies is carried out into vacuum filtration, transparent, free from extraneous odour Ovum Anas domestica album is obtained final product
Polypeptide liquid；
5. concentrate：Transparent, free from extraneous odour Ovum Anas domestica album polypeptide liquid is concentrated in vacuo for the 1/4 of original volume, it is standby；
4) prepared by Ovum Anas domestica album polypeptide beverage：
1. allocate：Add 7% sucrose by beverage gross mass, the post-heating that adds water dissolving adds 0.1%CMC-Na, 0.08% yellow
After virgin rubber and 0.02% sucrose ester, fully dissolving, 0.7% cycloheptaamylose, 0.4% citric acid and 3% Mel are added, and stirred
Uniformly, 4% Ovum Anas domestica album polypeptide liquid is added while stirring, obtains Ovum Anas domestica album polypeptide mixed liquor；
2. fill, sterilization：Deployed Ovum Anas domestica album polypeptide mixed liquor is carried out into fill, sterilization, the sterilization process is：Heat up
10min, sterilize 20min at a temperature of 115 DEG C, is cooled to central temperature less than 40 DEG C, gets product.
Embodiment 3：
The present invention provides a kind of Ovum Anas domestica album polypeptide beverage and preparation method thereof, comprises the steps：
1) Ovum Anas domestica album desalination：
1. pretreatment：The drinking water of 5 times of quality is added in the Ovum Anas domestica album taken out after preserved egg yellow, stirs homogenizing to reduce Ovum Anas domestica album
Viscosity, then with filtered through gauze, remove coarse impurities in Ovum Gallus domesticus album；
2. ultrasonic Treatment：Ultrasonic Treatment will be carried out through the Ovum Anas domestica album of pretreatment, ultrasonic power is 1.0kw, when ultrasonic
Between be 20min, after 10S per treatment, stop 10S, reprocessing, be so recycled to end；
3. ultrafiltration desalination：Pouring the Ovum Anas domestica album of Jing ultrasonic Treatment into ultrafiltration apparatus carries out ultrafiltration, ultrafiltration pressure 5kPa, device temperature
20 DEG C of degree, ultrafiltration time 2h；
4. concentrate：The Ovum Anas domestica album after desalination is carried out into rotary evaporation concentration under water bath using Rotary Evaporators, pressure is
5kPa, rotary speed is 50r/min, and bath temperature is 75 DEG C, and rotary evaporation concentration 1h is concentrated into the 1.5 of former Ovum Anas domestica album volume
Times；
2) enzymolysis of Ovum Anas domestica album：
1. digest：Add the water of 12 times of its quality to be diluted to the Ovum Anas domestica album after desalting processing, add papain, wind
Taste protease, pH value is 5.0, and hydrolysis temperature is 50 DEG C, enzyme digestion reaction 7h, the quality of the papain and flavor protease
Than for 1:1.5, consumption is：Add 5000 enzyme-activity units (u/ml substrates) per 1ml Ovum Anas domestica album；
2. enzyme denaturing：Adjust hydrolyzed solution pH value to 4.2 with citric acid, at 80 DEG C 30min enzyme denaturing is maintained, obtain Ovum Anas domestica album enzymolysis polypeptide
Liquid；
3) Ovum Anas domestica album enzymolysis polypeptide liquid purification：
1. eliminating sargassum smell：The Ovum Anas domestica album enzymolysis polypeptide liquid for obtaining is added into the yeast powder of its quality 0.6%, 38 DEG C of temperature, stirring is controlled
Uniformly, 2h is stood, carries out defishying；
2. hardship is taken off：Ovum Anas domestica album enzymolysis polypeptide liquid after eliminating sargassum smell is added into the cycloheptaamylose of its quality 1%, 55 DEG C of temperature is controlled,
Stir, carry out de- suffering reason 5min；
3. decolourize：Ovum Anas domestica album enzymolysis polypeptide liquid after de- hardship is added into the kieselguhr and 3% activated carbon of its quality 1%, control temperature
60 DEG C of degree, stirs, and carries out desolventing technology 1.5h；
4. sucking filtration：The Ovum Anas domestica album enzymolysis polypeptide liquid of Jing desolventing technologies is carried out into vacuum filtration, transparent, free from extraneous odour Ovum Anas domestica album is obtained final product
Polypeptide liquid；
5. concentrate：Transparent, free from extraneous odour Ovum Anas domestica album polypeptide liquid is concentrated in vacuo for the 1/3 of original volume, it is standby；
4) prepared by Ovum Anas domestica album polypeptide beverage：
1. allocate：Add 5% sucrose by beverage gross mass, the post-heating that adds water dissolving adds 0.11%CMC-Na, 0.15% yellow
After virgin rubber and 0.009% sucrose ester, fully dissolving, 0.8% cycloheptaamylose, 0.4% citric acid and 5% Mel are added, and stirred
Mix uniform, 5% Ovum Anas domestica album polypeptide liquid is added while stirring, obtain Ovum Anas domestica album polypeptide mixed liquor；
2. fill, sterilization：Deployed Ovum Anas domestica album polypeptide mixed liquor is carried out into fill, sterilization, the sterilization process is：Heat up
10min, sterilize 40min at a temperature of 105 DEG C, is cooled to central temperature less than 40 DEG C, gets product.
Above example only to illustrative and not limiting technical scheme, although above-described embodiment enters to the present invention
Detailed description is gone, the person skilled of this area should be understood：The present invention can be modified or be replaced on an equal basis, but
Any modification and local without departing from spirit and scope of the invention is replaced and all should covered in scope of the presently claimed invention.
Claims (10)
1. a kind of Ovum Anas domestica album polypeptide beverage, it is characterised in that the Ovum Anas domestica album after to take out preserved egg yellow as raw material, Jing desalinations, enzymolysis,
Purification is prepared into the Ovum Anas domestica album polypeptide liquid with antioxidant activity, then is deployed into beverage blends with complex function sweeting agent and water
Liquid, Jing fills, sterilization are processed.
2. Ovum Anas domestica album polypeptide beverage according to claim 1, it is characterised in that the complex function sweeting agent includes as follows
Component and its account for the percentage ratio of beverage gross mass：Sucrose 5%～8%, sodium carboxymethyl cellulose 0.05%～0.15%, xanthan gum
0.05%～0.15%, sucrose ester 0.005%～0.025%, cycloheptaamylose 0.5%～1.5%, citric acid 0.3%～
0.8%th, Mel 3%～5%.
3. Ovum Anas domestica album polypeptide beverage according to claim 1, it is characterised in that the Ovum Anas domestica album polypeptide liquid accounts for the total matter of beverage
The percentage ratio of amount is 2%～5%.
4. a kind of preparation method of Ovum Anas domestica album polypeptide beverage, it is characterised in that comprise the steps：
1) Ovum Anas domestica album desalination：
1. pretreatment：The drinking water of 1～5 times of quality is added in the Ovum Anas domestica album taken out after preserved egg yellow, stirs homogenizing to reduce duck
The viscosity of Ovum Gallus domesticus album, then with filtered through gauze, remove coarse impurities in Ovum Gallus domesticus album；
2. ultrasonic Treatment：Ultrasonic Treatment will be carried out through the Ovum Anas domestica album of pretreatment；
3. ultrafiltration desalination：Pouring the Ovum Anas domestica album of Jing ultrasonic Treatment into ultrafiltration apparatus carries out ultrafiltration；
4. concentrate：The Ovum Anas domestica album after desalination is carried out into rotary evaporation concentration under water bath using Rotary Evaporators, is concentrated into
0.5～1.5 times of former Ovum Anas domestica album volume；
2) enzymolysis of Ovum Anas domestica album：
1. digest：Add the water of 10～20 times of its quality to be diluted to the Ovum Anas domestica album after desalting processing, add Papain
Enzyme, flavor protease, pH value is 5.0～6.0, and hydrolysis temperature is 50 DEG C, 5～8h of enzyme digestion reaction；
2. enzyme denaturing：Adjust hydrolyzed solution pH value to 4.2-4.5 with citric acid, at 80 DEG C 30min enzyme denaturing is maintained, obtain Ovum Anas domestica album enzymolysis many
Peptide liquid；
3) Ovum Anas domestica album enzymolysis polypeptide liquid purification：
1. eliminating sargassum smell：The Ovum Anas domestica album enzymolysis polypeptide liquid for obtaining is added into the yeast powder of its quality 0.3%～0.8%, temperature 30 is controlled
～50 DEG C, stir, stand 1～2h, carry out defishying；
2. hardship is taken off：Ovum Anas domestica album enzymolysis polypeptide liquid after eliminating sargassum smell is added into the cycloheptaamylose of its quality 0.5%～1%, control temperature
45～55 DEG C of degree, stirs, and carries out de- suffering and manages 5～10min；
3. decolourize：Ovum Anas domestica album enzymolysis polypeptide liquid after de- hardship is added into the kieselguhr of its quality 1%～3% and 1%～3% active
Charcoal, controls 50～70 DEG C of temperature, stirs, and carries out 1～2h of desolventing technology；
4. sucking filtration：The Ovum Anas domestica album enzymolysis polypeptide liquid of Jing desolventing technologies is carried out into vacuum filtration, transparent, free from extraneous odour Ovum Anas domestica album is obtained final product
Polypeptide liquid；
5. concentrate：Transparent, free from extraneous odour Ovum Anas domestica album polypeptide liquid is concentrated in vacuo for the 1/3～1/5 of original volume, it is standby；
4) prepared by Ovum Anas domestica album polypeptide beverage：
1. allocate：Sucrose is added water post-heating dissolving, sodium carboxymethyl cellulose, xanthan gum, sucrose ester is added, fully dissolving
Afterwards, cycloheptaamylose, citric acid, Mel are added, and is stirred, Ovum Anas domestica album polypeptide liquid is added while stirring, obtain Ovum Anas domestica album many
Peptide mixed liquor；
2. fill, sterilization：Deployed Ovum Anas domestica album polypeptide mixed liquor is carried out into fill, sterilization, the sterilization process is：Heat up
10min, sterilize 15～40min at a temperature of 105～115 DEG C, is cooled to central temperature less than 40 DEG C, gets product.
5. the preparation method of Ovum Anas domestica album polypeptide beverage according to claim 4, it is characterised in that the ultrasonic Treatment
When, ultrasonic power is 1.0kw, and ultrasonic time is 20min, after 10S per treatment, stops 10S, and reprocessing is so recycled to
Terminate.
6. the preparation method of Ovum Anas domestica album polypeptide beverage according to claim 4, it is characterised in that the pressure during ultrafiltration
For 5kPa, unit temp is 20 DEG C, and the ultrafiltration time is 2h.
7. the preparation method of Ovum Anas domestica album polypeptide beverage according to claim 4, it is characterised in that during the concentration, rotation
The pressure of evaporimeter is 5kPa, and rotary speed is 50r/min, and bath temperature is 65-75 DEG C, rotary evaporation concentration time is 1～
3h。
8. the preparation method of Ovum Anas domestica album polypeptide beverage according to claim 4, it is characterised in that during the enzymolysis, Fructus Chaenomeliss
Protease, the consumption of flavor protease are：Add 4000～6000 enzyme-activity units per 1ml Ovum Anas domestica album.
9. the preparation method of Ovum Anas domestica album polypeptide beverage according to claim 4, it is characterised in that during the enzymolysis, Fructus Chaenomeliss
Protease is 1 with the mass ratio of flavor protease:0.5～2.
10. the preparation method of Ovum Anas domestica album polypeptide beverage according to claim 4, it is characterised in that during the decolouring, diatomaceous earth
It is 1 with the mass ratio of activated carbon:1～3.
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| CN109123262A (en) * | 2018-08-24 | 2019-01-04 | 湖北神丹健康食品有限公司 | A kind of lime-preserved egg polypeptide beverage and preparation method thereof |
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| CN109452446A (en) * | 2018-09-25 | 2019-03-12 | 金太阳粮油股份有限公司 | A kind of preparation method of sunflower seeds antioxidation polypeptide beverage |
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| CN109452446A (en) * | 2018-09-25 | 2019-03-12 | 金太阳粮油股份有限公司 | A kind of preparation method of sunflower seeds antioxidation polypeptide beverage |
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| CN111202198A (en) * | 2020-01-20 | 2020-05-29 | 广东蛋能量生物科技有限公司 | Egg white peptide oral drink and preparation method thereof |
| CN111493195A (en) * | 2020-04-07 | 2020-08-07 | 江西农业大学 | Salted egg white zymolyte soft sweets and preparation method thereof |
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| CN117099890A (en) * | 2023-09-28 | 2023-11-24 | 泰昊乐生物科技有限公司 | Colorless and odorless oligopeptide liquid beverage capable of promoting uric acid reduction, blood sugar reduction and blood lipid reduction and processing method thereof |
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