CN106577981A - Preparation method of globe artichoke aquatic product preservation film coating solution - Google Patents
Preparation method of globe artichoke aquatic product preservation film coating solution Download PDFInfo
- Publication number
- CN106577981A CN106577981A CN201611166705.6A CN201611166705A CN106577981A CN 106577981 A CN106577981 A CN 106577981A CN 201611166705 A CN201611166705 A CN 201611166705A CN 106577981 A CN106577981 A CN 106577981A
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- Prior art keywords
- preservation
- fishery
- carlina
- coating liquid
- preparation
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- 238000004321 preservation Methods 0.000 title claims abstract description 37
- 238000002360 preparation method Methods 0.000 title claims abstract description 17
- 244000019459 Cynara cardunculus Species 0.000 title abstract description 5
- 235000019106 Cynara scolymus Nutrition 0.000 title abstract description 4
- 239000007888 film coating Substances 0.000 title abstract 4
- 238000009501 film coating Methods 0.000 title abstract 4
- 235000003230 Helianthus tuberosus Nutrition 0.000 title abstract 2
- 238000000034 method Methods 0.000 claims abstract description 12
- 239000002994 raw material Substances 0.000 claims abstract description 6
- 238000000605 extraction Methods 0.000 claims abstract description 3
- 240000001789 Carlina acaulis Species 0.000 claims description 46
- 235000005882 Carlina acaulis Nutrition 0.000 claims description 46
- 239000007788 liquid Substances 0.000 claims description 32
- 239000011248 coating agent Substances 0.000 claims description 31
- 238000000576 coating method Methods 0.000 claims description 31
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims description 20
- 239000000284 extract Substances 0.000 claims description 15
- 239000012153 distilled water Substances 0.000 claims description 11
- QTBSBXVTEAMEQO-UHFFFAOYSA-N Acetic acid Chemical compound CC(O)=O QTBSBXVTEAMEQO-UHFFFAOYSA-N 0.000 claims description 10
- 229960000583 acetic acid Drugs 0.000 claims description 5
- 239000012141 concentrate Substances 0.000 claims description 5
- 239000012467 final product Substances 0.000 claims description 5
- 239000012362 glacial acetic acid Substances 0.000 claims description 5
- 239000000463 material Substances 0.000 claims description 5
- 239000007787 solid Substances 0.000 claims description 5
- 239000006228 supernatant Substances 0.000 claims description 5
- 238000001035 drying Methods 0.000 claims 1
- 230000000694 effects Effects 0.000 abstract description 5
- 230000003647 oxidation Effects 0.000 abstract description 4
- 238000007254 oxidation reaction Methods 0.000 abstract description 4
- 230000003111 delayed effect Effects 0.000 abstract description 2
- 230000001953 sensory effect Effects 0.000 abstract description 2
- 241000894006 Bacteria Species 0.000 abstract 1
- 238000000926 separation method Methods 0.000 abstract 1
- 239000000047 product Substances 0.000 description 11
- 238000003756 stirring Methods 0.000 description 4
- 238000001514 detection method Methods 0.000 description 3
- 244000005700 microbiome Species 0.000 description 3
- 239000002245 particle Substances 0.000 description 3
- 241000196324 Embryophyta Species 0.000 description 2
- 230000003115 biocidal effect Effects 0.000 description 2
- 235000013305 food Nutrition 0.000 description 2
- 238000007710 freezing Methods 0.000 description 2
- 230000008014 freezing Effects 0.000 description 2
- 231100000252 nontoxic Toxicity 0.000 description 2
- 230000003000 nontoxic effect Effects 0.000 description 2
- 230000035943 smell Effects 0.000 description 2
- 238000012360 testing method Methods 0.000 description 2
- 241000251468 Actinopterygii Species 0.000 description 1
- 229920001661 Chitosan Polymers 0.000 description 1
- 241000252230 Ctenopharyngodon idella Species 0.000 description 1
- 206010059866 Drug resistance Diseases 0.000 description 1
- 241001465754 Metazoa Species 0.000 description 1
- 241000904014 Pappus Species 0.000 description 1
- 244000061458 Solanum melongena Species 0.000 description 1
- 230000002159 abnormal effect Effects 0.000 description 1
- 239000013543 active substance Substances 0.000 description 1
- 230000000844 anti-bacterial effect Effects 0.000 description 1
- 238000009360 aquaculture Methods 0.000 description 1
- 244000144974 aquaculture Species 0.000 description 1
- 230000001580 bacterial effect Effects 0.000 description 1
- 230000009286 beneficial effect Effects 0.000 description 1
- 230000000975 bioactive effect Effects 0.000 description 1
- 239000003795 chemical substances by application Substances 0.000 description 1
- 210000001951 dura mater Anatomy 0.000 description 1
- 238000011156 evaluation Methods 0.000 description 1
- 238000002474 experimental method Methods 0.000 description 1
- 239000000796 flavoring agent Substances 0.000 description 1
- 235000019634 flavors Nutrition 0.000 description 1
- 239000013505 freshwater Substances 0.000 description 1
- 230000001408 fungistatic effect Effects 0.000 description 1
- 239000008187 granular material Substances 0.000 description 1
- 238000007654 immersion Methods 0.000 description 1
- 239000002932 luster Substances 0.000 description 1
- 238000004519 manufacturing process Methods 0.000 description 1
- 235000016709 nutrition Nutrition 0.000 description 1
- 230000001590 oxidative effect Effects 0.000 description 1
- 238000012856 packing Methods 0.000 description 1
- 239000003755 preservative agent Substances 0.000 description 1
- 230000002335 preservative effect Effects 0.000 description 1
- 238000005057 refrigeration Methods 0.000 description 1
- 238000012827 research and development Methods 0.000 description 1
- 230000001954 sterilising effect Effects 0.000 description 1
- 238000004659 sterilization and disinfection Methods 0.000 description 1
- 239000000126 substance Substances 0.000 description 1
- 210000001835 viscera Anatomy 0.000 description 1
Classifications
-
- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
- A23B—PRESERVING, e.g. BY CANNING, MEAT, FISH, EGGS, FRUIT, VEGETABLES, EDIBLE SEEDS; CHEMICAL RIPENING OF FRUIT OR VEGETABLES; THE PRESERVED, RIPENED, OR CANNED PRODUCTS
- A23B4/00—General methods for preserving meat, sausages, fish or fish products
- A23B4/10—Coating with a protective layer; Compositions or apparatus therefor
-
- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
- A23L—FOODS, FOODSTUFFS, OR NON-ALCOHOLIC BEVERAGES, NOT COVERED BY SUBCLASSES A21D OR A23B-A23J; THEIR PREPARATION OR TREATMENT, e.g. COOKING, MODIFICATION OF NUTRITIVE QUALITIES, PHYSICAL TREATMENT; PRESERVATION OF FOODS OR FOODSTUFFS, IN GENERAL
- A23L3/00—Preservation of foods or foodstuffs, in general, e.g. pasteurising, sterilising, specially adapted for foods or foodstuffs
- A23L3/34—Preservation of foods or foodstuffs, in general, e.g. pasteurising, sterilising, specially adapted for foods or foodstuffs by treatment with chemicals
- A23L3/3454—Preservation of foods or foodstuffs, in general, e.g. pasteurising, sterilising, specially adapted for foods or foodstuffs by treatment with chemicals in the form of liquids or solids
- A23L3/3463—Organic compounds; Microorganisms; Enzymes
- A23L3/3472—Compounds of undetermined constitution obtained from animals or plants
-
- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
- A23V—INDEXING SCHEME RELATING TO FOODS, FOODSTUFFS OR NON-ALCOHOLIC BEVERAGES AND LACTIC OR PROPIONIC ACID BACTERIA USED IN FOODSTUFFS OR FOOD PREPARATION
- A23V2002/00—Food compositions, function of food ingredients or processes for food or foodstuffs
Abstract
The invention belongs to the technical field of aquatic product preservation, and in particular relates to a preparation method of globe artichoke aquatic product preservation film coating solution, which comprises the specific steps: A, raw material pretreatment; B, extraction; C, separation and concentration; D, preservation film coating solution preparation. The preservation film coating solution preparation prepared by the method has the advantages that a bacteria resisting effect is good, unpleasant odor such as fishlike smell and the like of an aquatic product can be covered up effectively, surface glossiness is good, sensory quality of the aquatic product is improved, and attraction of the aquatic to customers is increased; oxidation and rancidity of the aquatic product can be delayed effectively, the method is simple, the cost is low, and the aquatic product is natural and safe.
Description
Technical field
The invention belongs to Aquatic product preservation field, and in particular to a kind of preparation method of Carlina acauliss preservation of fishery coating liquid.
Background technology
Aquatic products are animals and plants and its general designations of converted productss of ocean and fresh water fishery production.
Aquaculture nutritional value is abundant, but easily putrid and deteriorated.At present conventional preservation method has freezing method and chemistry guarantor
Fresh method, freezing method needs refrigeration plant, and the color and luster quality structure, taste flavor to aquatic products can be damaged, and reduce commodity value；
Sterilization or bacteriostasis of the fresh chemically rule by various antibiotic or bioactive substance, method is easy, but antibiotic
Using there is residual quantity and bacterial drug resistance, the antibacterial corrosion-resistanting fresh-keeping effect of most biologic active substances is limited.Cause
This, the research and development of Nantural non-toxic and the good antistaling agent of corrosion-resistanting fresh-keeping effect seem more urgent.
The content of the invention
In view of this, it is an object of the invention to provide a kind of preparation method of Carlina acauliss preservation of fishery coating liquid.Should
Preservation of fishery film Nantural non-toxic obtained in method, corrosion-resistanting fresh-keeping effect is good.
To realize object above, the technical scheme is that：
The preparation method of Carlina acauliss preservation of fishery coating liquid, concretely comprises the following steps：
A. pretreatment of raw material：After Carlina acauliss bract is dried, crush；
B is extracted：Water is added in the Carlina acauliss bract of pretreatment, the water-bath extraction 3-7h at a temperature of 45-60 DEG C；
C. separate, concentrate：Step B gained is carried out into centrifugal treating, supernatant is taken, is concentrated, obtain Carlina acaulis extract；
D. preservation coating liquid is prepared：Add in 5.0-80.0 mass parts shitosans in 900 mass parts distilled water and shake
10min, adds 5.25-31.5 mass parts glacial acetic acid, stirs, and adds Carlina acaulis extract 200-350 mass parts, treats each
Material is settled to volume equivalent to 1000 mass parts water after being completely dissolved with distilled water, obtains final product the Carlina acauliss aquatic products and protects
Fresh coating liquid.
The Carlina acauliss are also called Cynara scolymus L (Cyhara cardunculus.), food support Cynara scolymus L (Cyhara cardunculus.), arithoke, towards Ji, be that Compositae Cynara scolymus L (Cyhara cardunculus.) belongs to herbaceos perennial, it is high
Up to 2 meters.Stem is sturdy, and uprightly, branch, the big shape of leaf, basal leaf rosette-stape are arranged at top；Bottom stem and leaf ellipse or wide lanceolar,
1 meter is about, two times pinniform is totally cleaved, and has long petiole；Thin, the herbaceous stem in whole food value of leaf ground, above green, below canescence, head inflorescence
Greatly, involucre multilamellar, without hair, imbricate arrangement, Radix Aconiti Lateralis Preparata dura mater matter, circular, avette, triangle or shape of tail, little Hua aubergines, flower
9 millimeters of hat sliver length.Achene oblong, edge of having no result.Pappus white, July yields positive results.
Further, the temperature dried described in step A is 50-70 DEG C, and the time is 8-15h.
Further, in step A, the degree of the crushing is to be crushed to more than 90% grain diameter≤10 μm.
Further, in step B, the consumption of the water is 3-6 times of Carlina acauliss bract quality.
Further, in step C, the degree of the concentration is 40-50% to be concentrated into solid content.
The second object of the present invention is Carlina acauliss preservation of fishery coating liquid obtained in protection said method.
The present invention also aims to protect Carlina acauliss preservation of fishery coating liquid obtained in said method to protect in aquatic products
Application in fresh, when using, aquatic products is put in coating liquid and soaks 2-8min, is picked up, and is dried naturally, is solidificated in coating liquid
Aquatic products surface.
The beneficial effects of the present invention is：
(1) preservation coating liquid fungistatic effect is preferable obtained in the application；(2) fishlike smell of aquatic products etc. can effectively be covered no
Good abnormal smells from the patient, and surface gloss is good, improves the aesthetic quality of aquatic products, increased captivation of the aquatic products to consumer；(3)
The oxidative rancidity of fat in aquatic products can effectively be delayed；(4) method is simple, with low cost, natural safety.
Specific embodiment
Embodiment of the present invention is described in detail below in conjunction with embodiment, but those skilled in the art will
Understand, the following example is merely to illustrate the present invention, and should not be taken as limiting the scope of the invention.It is unreceipted in preferred embodiment
The experimental technique of actual conditions, generally according to normal condition.
Embodiment 1
The preparation method of Carlina acauliss preservation of fishery coating liquid, concretely comprises the following steps：
A. pretreatment of raw material：Carlina acauliss bract 1000g is dried after 15h at a temperature of 50 DEG C, more than 90% is crushed to
Grain particle diameter≤10 μm；
B is extracted：To 3000g water is added in the Carlina acauliss bract of pretreatment, the water-bath at a temperature of 45 DEG C extracts 3h；
C. separate, concentrate：Step B gained is carried out into centrifugal treating, supernatant is taken, it is 50% to be concentrated into solid content,
Obtain Carlina acaulis extract；
D. preservation coating liquid is prepared：Weigh 5.0g shitosans and add in 900g distilled water and shake 10min, add 5.25g
Glacial acetic acid, stirs, and adds Carlina acaulis extract 350g, and 1000mL is settled to distilled water after each material is completely dissolved,
Obtain final product the Carlina acauliss preservation of fishery coating liquid.
Embodiment 2
The preparation method of Carlina acauliss preservation of fishery coating liquid, concretely comprises the following steps：
A. pretreatment of raw material：Carlina acauliss bract 1000g is dried after 8h at a temperature of 70 DEG C, more than 90% granule is crushed to
Particle diameter≤10 μm；
B is extracted：To 6000g water is added in the Carlina acauliss bract of pretreatment, the water-bath at a temperature of 60 DEG C extracts 7h；
C. separate, concentrate：Step B gained is carried out into centrifugal treating, supernatant is taken, it is 40% to be concentrated into solid content,
Obtain Carlina acaulis extract；
D. preservation coating liquid is prepared：Weigh 80.0g shitosans and add in 900g distilled water and shake 10min, add 31.5g
Glacial acetic acid, stirs, and adds Carlina acaulis extract 200g, and 1000mL is settled to distilled water after each material is completely dissolved,
Obtain final product the Carlina acauliss preservation of fishery coating liquid.
Embodiment 3
The preparation method of Carlina acauliss preservation of fishery coating liquid, concretely comprises the following steps：
A. pretreatment of raw material：Carlina acauliss bract 1000g is dried after 11h at a temperature of 60 DEG C, more than 90% is crushed to
Grain particle diameter≤10 μm；
B is extracted：To 5000g water is added in the Carlina acauliss bract of pretreatment, the water-bath at a temperature of 50 DEG C extracts 6h；
C. separate, concentrate：Step B gained is carried out into centrifugal treating, supernatant is taken, it is 48% to be concentrated into solid content,
Obtain Carlina acaulis extract；
D. preservation coating liquid is prepared：Weigh 40.0g shitosans and add in 900g distilled water and shake 10min, add 22.5g
Glacial acetic acid, stirs, and adds Carlina acaulis extract 240g, and 1000mL is settled to distilled water after each material is completely dissolved,
Obtain final product the Carlina acauliss preservation of fishery coating liquid.
Carlina acauliss preservation of fishery coating liquid fresh-keeping effect is verified
Fresh and alive Ctenopharyngodon idellus are slaughtered, and decaptitated, remove the peel, are removed internal organs, are cut into 3.0cm × 3.0cm × 1.0cm's parallel to fish spine
Fish block.Be separately immersed in distilled water, be not added with Carlina acaulis extract chitosan coating liquid and this law prepare preservation coating liquid
Middle immersion 6min, carries out preservative film and covers pallet packing after draining on sterile gauze, then preserve 15 days under the conditions of 4 DEG C.
Fat oxidation value, microorganism and organoleptic indicator detection was carried out every 3 days.Fat oxidation value result is as shown in table 1, microorganism detection
As a result as shown in table 2, organoleptic indicator's testing result is as shown in table 3.
The fat oxidation value TBARS testing result of table 1
The microorganism detection result of table 2
The sensory evaluation result of table 3
Finally illustrate, above example is only unrestricted to illustrate technical scheme, although with reference to compared with
Good embodiment has been described in detail to the present invention, it will be understood by those within the art that, can be to the skill of the present invention
Art scheme is modified or equivalent, and without deviating from the objective and scope of technical solution of the present invention, it all should cover at this
In the middle of the right of invention.
Claims (7)
1. the preparation method of Carlina acauliss preservation of fishery coating liquid, it is characterised in that concretely comprise the following steps：
A. pretreatment of raw material：After Carlina acauliss bract is dried, crush；
B. extract：Water is added in the Carlina acauliss bract of pretreatment, the water-bath extraction 3-7h at a temperature of 45-60 DEG C；
Separate, concentrate：Step B gained is carried out into centrifugal treating, supernatant is taken, is concentrated, obtain Carlina acaulis extract；
D. preservation coating liquid is prepared：Add in 900 mass parts distilled water in 5.0-80.0 mass parts shitosans and shake 10min,
5.25-31.5 mass parts glacial acetic acid is added, is stirred, add Carlina acaulis extract 200-350 mass parts, treat that each material is complete
The volume equivalent to 1000 mass parts water is settled to distilled water after CL, the Carlina acauliss preservation of fishery film is obtained final product
Liquid.
2. the preparation method of Carlina acauliss preservation of fishery coating liquid according to claim 1, it is characterised in that step A institute
The temperature for stating drying is 50-70 DEG C, and the time is 8-15h.
3. the preparation method of Carlina acauliss preservation of fishery coating liquid according to claim 1, it is characterised in that in step A,
The degree of the crushing is to be crushed to more than 90% grain diameter≤10 μm.
4. the preparation method of Carlina acauliss preservation of fishery coating liquid according to claim 1, it is characterised in that in step B,
The consumption of the water is 3-6 times of Carlina acauliss bract quality.
5. the preparation method of Carlina acauliss preservation of fishery coating liquid according to claim 1, it is characterised in that in step C,
The degree of the concentration is 40-50% to be concentrated into solid content.
6. the preparation method of Carlina acauliss preservation of fishery coating liquid obtained in any one of claim 1-5 methods described.
7. application of the Carlina acauliss preservation of fishery coating liquid in preservation of fishery obtained in claim 1.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201611166705.6A CN106577981A (en) | 2016-12-16 | 2016-12-16 | Preparation method of globe artichoke aquatic product preservation film coating solution |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201611166705.6A CN106577981A (en) | 2016-12-16 | 2016-12-16 | Preparation method of globe artichoke aquatic product preservation film coating solution |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| CN106577981A true CN106577981A (en) | 2017-04-26 |
Family
ID=58801940
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN201611166705.6A Pending CN106577981A (en) | 2016-12-16 | 2016-12-16 | Preparation method of globe artichoke aquatic product preservation film coating solution |
Country Status (1)
| Country | Link |
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| CN (1) | CN106577981A (en) |
Cited By (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN107183578A (en) * | 2017-06-05 | 2017-09-22 | 舟山市齐晟水产有限公司 | A kind of Pu burns sliced eel preparation technology |
| CN107242462A (en) * | 2017-06-05 | 2017-10-13 | 舟山市齐晟水产有限公司 | A kind of mackerel is according to burning flavouring material formula |
| CN107259417A (en) * | 2017-06-05 | 2017-10-20 | 舟山市齐晟水产有限公司 | A kind of mackerel is according to burning preparation technology |
| CN107373448A (en) * | 2017-06-05 | 2017-11-24 | 舟山市齐晟水产有限公司 | A kind of Pu burns eel silk preparation technology |
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| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN102276465A (en) * | 2011-09-08 | 2011-12-14 | 南京泽朗医药科技有限公司 | Method for purifying cynarin |
| CN103749667A (en) * | 2013-12-18 | 2014-04-30 | 广西科技大学 | Siraitia grosvenorii fresh-keeping film coating liquid and preparation method thereof |
| CN104365831A (en) * | 2014-11-01 | 2015-02-25 | 东莞市青麦田数码科技有限公司 | Fruit and vegetable fresh-keeping agent |
| CN105010523A (en) * | 2014-04-28 | 2015-11-04 | 蔡联兵 | Fresh-keeping film coating solution for bitter gourds |
| CN106070584A (en) * | 2016-06-08 | 2016-11-09 | 务川自治县大坪镇官学村果蔬种植农民专业合作社 | A kind of preservation coating liquid of Fructus Pruni salicinae and preparation method thereof |
| CN106070531A (en) * | 2016-07-29 | 2016-11-09 | 华南理工大学 | A kind of Cortex Cinnamomi, the preparation method and application of bergamot fruit extract edible fresh-keeping film-coating agent |
-
2016
- 2016-12-16 CN CN201611166705.6A patent/CN106577981A/en active Pending
Patent Citations (6)
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|---|---|---|---|---|
| CN102276465A (en) * | 2011-09-08 | 2011-12-14 | 南京泽朗医药科技有限公司 | Method for purifying cynarin |
| CN103749667A (en) * | 2013-12-18 | 2014-04-30 | 广西科技大学 | Siraitia grosvenorii fresh-keeping film coating liquid and preparation method thereof |
| CN105010523A (en) * | 2014-04-28 | 2015-11-04 | 蔡联兵 | Fresh-keeping film coating solution for bitter gourds |
| CN104365831A (en) * | 2014-11-01 | 2015-02-25 | 东莞市青麦田数码科技有限公司 | Fruit and vegetable fresh-keeping agent |
| CN106070584A (en) * | 2016-06-08 | 2016-11-09 | 务川自治县大坪镇官学村果蔬种植农民专业合作社 | A kind of preservation coating liquid of Fructus Pruni salicinae and preparation method thereof |
| CN106070531A (en) * | 2016-07-29 | 2016-11-09 | 华南理工大学 | A kind of Cortex Cinnamomi, the preparation method and application of bergamot fruit extract edible fresh-keeping film-coating agent |
Cited By (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN107183578A (en) * | 2017-06-05 | 2017-09-22 | 舟山市齐晟水产有限公司 | A kind of Pu burns sliced eel preparation technology |
| CN107242462A (en) * | 2017-06-05 | 2017-10-13 | 舟山市齐晟水产有限公司 | A kind of mackerel is according to burning flavouring material formula |
| CN107259417A (en) * | 2017-06-05 | 2017-10-20 | 舟山市齐晟水产有限公司 | A kind of mackerel is according to burning preparation technology |
| CN107373448A (en) * | 2017-06-05 | 2017-11-24 | 舟山市齐晟水产有限公司 | A kind of Pu burns eel silk preparation technology |
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Application publication date: 20170426 |
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