CN106568772A - Multifunctional detection liquid - Google Patents
Multifunctional detection liquid Download PDFInfo
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- CN106568772A CN106568772A CN201610999283.4A CN201610999283A CN106568772A CN 106568772 A CN106568772 A CN 106568772A CN 201610999283 A CN201610999283 A CN 201610999283A CN 106568772 A CN106568772 A CN 106568772A
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- G01N—INVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES
- G01N21/00—Investigating or analysing materials by the use of optical means, i.e. using sub-millimetre waves, infrared, visible or ultraviolet light
- G01N21/75—Systems in which material is subjected to a chemical reaction, the progress or the result of the reaction being investigated
- G01N21/77—Systems in which material is subjected to a chemical reaction, the progress or the result of the reaction being investigated by observing the effect on a chemical indicator
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Abstract
The invention provides a multifunctional detection liquid, and belongs to the technical field of chemical detection reagent. The multifunctional detection liquid is prepared by taking lime, sulphur, alumen, mirabilite, chalcanthite, melanterite, vermilion, borax, and nitric acid as the main raw materials at a certain ratio. A preparation method of the multifunctional detection liquid is simple; the multifunctional detection liquid can be used for true and false inspection and quality detection of a plurality of substances including food and drugs, is low in cost, wide in application range, high in sensitivity and stability, rapid in reaction speed, and long in self life, and is convenient to use; obvious color development is achieved; and distinguish is easy to realize.
Description
【Technical field】
The present invention relates to chemical detection reagent technique field, and in particular to a kind of multi-functional detection liquid.
【Background technology】
With the development of social economy, market commodity are more and more diversified, but while also occur in that some fake and forged business
Product, disrupt the market, harm consumer's interests, especially food, the edible commodity such as medicine, fake and forged or adulterate, very
Extremely health may be worked the mischief.The more existing detection method for detecting commodity true and false quality, such as：Information optics side
Method, laser detecting method and Explosion-proof cap etc., the method for this anti-counterfeiting counterfeit or inferior quality goods need specific equipment and detection instrument, and
Cost is big, is not easy to consumers in general and is used.Therefore seek a kind of work that can quickly and efficiently differentiate material true and false quality
Tool or method become the urgent needss of people.
【The content of the invention】
For posed problems above, the invention provides a kind of quick, easy, reliable multi-functional detection liquid, the inspection
The preparation method for surveying liquid is simple, and obtained detection liquid is detectable to differentiate the true and false good of many kinds of substance (such as varieties of food items and medicine)
Bad, low cost, applied widely, easy to use, sensitivity is high, reaction is quick, develops the color obvious, easily distinguishable, and good stability,
Long shelf-life.
In order to realize object above, the technical scheme that the present invention takes is：
A kind of multi-functional detection liquid, is mainly made up of the raw material of following weight portion：It is Calx 6-8 parts, sulfur 14-16 parts, white
Vitriol 1-3 parts, Natrii Sulfas 7-9 parts, Chalcanthitum 3-5 parts, Melanteritum 2-4 parts, Vermilion 4-6 parts, Borax 2-4 parts, nitric acid 10-20 parts, distilled water
700-900 parts；Wherein, the mass concentration of the nitric acid is 50-70%.
Further, the multi-functional detection liquid is mainly made up of the raw material of following weight portion：6.9 parts of Calx, sulfur
15.6 parts, 1.9 parts of Alumen, 8 parts of Natrii Sulfas, 3.6 parts of Chalcanthitum, 3 parts of Melanteritum, 5 parts of Vermilion, 3.5 parts of Borax, 18 parts of nitric acid, distilled water
800 parts；Wherein, the mass concentration of the nitric acid is 69%.
Further, the multi-functional detection liquid is obtained as follows：
(1) each raw material is weighed by the weight portion；
(2) by Calx, sulfur, Alumen mixing, distilled water is then added, is stirred, be again heated to boiling, then stop
Heating, stands 24h releasing fire-toxin, obtains just mixed liquid；
(3) Vermilion is mixed with nitric acid and is stirred evenly, after placing 2h, be added in the just mixed liquid；Then sequentially add
Natrii Sulfas, Chalcanthitum, Melanteritum, are stirred well to dissolving, obtain final product.
The multi-functional detection liquid of the present invention can be applicable to qualitative detection, and the true and false quality of many kinds of substance can be detected,
Such as detect the quality of beans, medicine it is true and false and whether rotten.Specific detection method is as follows：
1st, treat the process of detection material：
Material to be detected is crushed to sufficiently fine；It is 1 again in mass ratio:The ratio of 50-100 takes material to be detected after crushing
It is sufficiently stirred for after mixing with distilled water, until soluble substance therein all dissolves, obtains prepare liquid.
2nd, detect：
Test tube is taken, taken test tube is cleaned up with distilled water, and in backward test tube, add 2mL distilled water, then use glue head
Dropper takes the prepare liquid of gained after 1 drop material to be detected is processed, and instills in the test tube containing distilled water, stirs；Finally,
Another glue head dropper takes the multi-functional detection liquid 1 of the present invention and drips, and instills in the test tube, after rocking or stirring 1-2min, observation examination
In the pipe color is presented by liquid.
Containing different chemical compositions in different material, and the detection liquid of the present invention and different chemical composition haptoreactions
Different colors can be presented.The fake products of material, chemical composition are different；After material degenerates, chemical constituent therein
Can also change, can be detected by the detection liquid of the present invention, differentiate its true and false quality.
The invention provides a kind of multi-functional detection liquid, relative to prior art, has the advantages that：
Multi-functional detection liquid provided by the present invention, is with Calx, sulfur, Alumen, Natrii Sulfas, Chalcanthitum, Melanteritum, Vermilion, boron
Sand, nitric acid are primary raw material, are prepared from when specific addition mixed processing method by certain.Its preparation method it is simple but
Strictly, obtained detection liquid can be applicable to the qualitative detection of material, can be to the true and false of many kinds of substance (such as varieties of food items and medicine)
Quality carries out detection and identification, its low cost, applied widely, easy to use, and sensitivity is high, reaction is quick, presents after reaction
Color is obvious, it is easy to distinguish, and good stability, long shelf-life.
【Specific embodiment】
The following examples can help those skilled in the art that the present invention is more fully understood, but cannot be with any
Mode limits the present invention.
Embodiment 1
A kind of multi-functional detection liquid, is mainly made up of the raw material of following weight portion：6 parts of Calx, 14 parts of sulfur, 1 part of Alumen,
7 parts of Natrii Sulfas, 3 parts of Chalcanthitum, 2 parts of Melanteritum, 6 parts of Vermilion, 4 parts of Borax, 20 parts of nitric acid, 700 parts of distilled water；Wherein, the nitric acid
Mass concentration is 70%.
Specifically preparation method is：
(1) each raw material is weighed by the weight portion；
(2) by Calx, sulfur, Alumen mixing, distilled water is then added, is stirred, be again heated to boiling, then stop
Heating, stands 24h releasing fire-toxin, obtains just mixed liquid；
(3) Vermilion is mixed with nitric acid and is stirred evenly, after placing 2h, be added in the just mixed liquid；Then sequentially add
Natrii Sulfas, Chalcanthitum, Melanteritum, are stirred well to dissolving, obtain final product.
Embodiment 2
A kind of multi-functional detection liquid, is mainly made up of the raw material of following weight portion：6.9 parts of Calx, 15.6 parts of sulfur, Alumen
1.9 parts, 8 parts of Natrii Sulfas, 3.6 parts of Chalcanthitum, 3 parts of Melanteritum, 5 parts of Vermilion, 3.5 parts of Borax, 18 parts of nitric acid, 800 parts of distilled water；Wherein,
The mass concentration of the nitric acid is 69%.
Concrete preparation method is with embodiment 1.
Embodiment 3
A kind of multi-functional detection liquid, is mainly made up of the raw material of following weight portion：8 parts of Calx, 16 parts of sulfur, 3 parts of Alumen,
9 parts of Natrii Sulfas, 5 parts of Chalcanthitum, 4 parts of Melanteritum, 4 parts of Vermilion, 2 parts of Borax, 10 parts of nitric acid, 900 parts of distilled water；Wherein, the nitric acid
Mass concentration is 50%.
Concrete preparation method is with embodiment 1.
Application example
(1) beans test experience
Using Semen Glyciness, Semen sojae atricolor, Semen Phaseoli, Seem Lablab Album, 6 kinds of beans of Fructus Crotonis and Semen phaseoli radiati as experimental subject, every kind of bean is 1 group, always
Totally 6 groups, per group of solarization for taking this kind of bean respectively makes a good job of bean and dries rotten bad bean and contrasted, made using the embodiment of the present invention 1
The detection liquid for obtaining carries out detection contrast to the good bean and bad bean of various beans.
Concrete detection method is operated as follows：
1) the good bean and bad bean of various beans are crushed respectively, is crossed 200 eye mesh screens, then respectively according to mass ratio 1:
100 ratio takes bean and distilled water after crushing, mixes and is sufficiently stirred for until soluble substance therein all dissolvings, obtain to be measured
Liquid；
2) test tube of cleaning is taken respectively, adds 2mL distilled water, then take 1 drop step with glue head dropper respectively in each test tube
1) the various bean prepare liquids obtained by, instill in each test tube for having added distilled water, stir；Glue head dropper is used still further
To in each test tube add the 1 drop present invention to implement the detection liquid obtained by 1 respectively, after rocking or stirring 2min, observe in each test tube
The color is presented by material, tests presented color after testing to the good bean and bad bean of various beans respectively and is observed and right
Than acquired results such as table 1 below：
Table 1：
From upper table 1：Good bean and bad bean are detected using the detection liquid obtained by the embodiment of the present invention 1, detected
Different colors can be presented after reaction, and it is obvious to develop the color, it is easy to be distinguished；After being gone bad due to beans, chemical constituent therein changes
Become, detected by present invention detection liquid, the different color presented from the detection reaction of good bean can be presented.
Successively using the detection liquid obtained by the embodiment of the present invention 2 and embodiment 3, using identical detection method, to Huang
Bean, Semen sojae atricolor, Semen Phaseoli, Seem Lablab Album, the good bean of 6 kinds of beans of Fructus Crotonis and Semen phaseoli radiati and bad bean carry out detection contrast experiment, acquired results with adopt
Result with the detection liquid detection gained obtained by the embodiment of the present invention 1 is basically identical, wherein, 2 obtained detection liquid of embodiment
The presented color of detection is the most obvious, it is easy to distinguish.
It follows that the detection liquid by adopting the present invention, detects to bean to be measured, detection reaction according to the observation is in
Existing color, can differentiate the quality of bean to be measured.
(2) drug detection experiment
JINSANGZI HOUPIAN (Guangxi Golden Throat Co., Ltd), the stomach invigorating do not spent the shelf-life and spent the shelf-life is taken respectively
XIAOSHI PIAN (Fushoutang Pharmaceutical Co., Ltd.), compound bismuth aluminate tabletses (Harbin City Kaicheng Pharmaceutical Co., Ltd.), hydroxytetracycline tablet (Guangdong
South China Pharmaceutical Group Co., Ltd), Loratadine capsule (Aobang Pharmaceutical Co., Ltd., Sichuan) is used as experimental subject.Using this
Detection liquid obtained by bright embodiment 1 is detected to the got it filled thing of the above, then to the not mistake shelf-life and has spent the shelf-life respectively
The color that presented of every kind of drug detection contrasted.
Concrete detection method is operated as follows：
1) the various flake drugs for being taken are ground, pharmaceutical capsules remove soft capsule；Then respectively according to mass ratio 1：50
Ratio take medicine and distilled water after each process, stir after mixing to whole dissolvings, obtain prepare liquid；
2) test tube of cleaning is taken respectively, adds 2mL distilled water, then take 1 drop step with glue head dropper respectively in each test tube
1) each medicine prepare liquid obtained by, instills in each test tube for having added distilled water, stirs；Glue head dropper is used still further
To in each test tube add the 1 drop present invention to implement the detection liquid obtained by 1 respectively, after rocking or stirring 2min, observe in each test tube
The color is presented by material, tests presented color after testing to not spending the shelf-life and having crossed every kind of medicine of shelf-life respectively
Observed and contrasted, acquired results such as table 2 below：
Table 2：
From upper table 2：Using the detection liquid obtained by the embodiment of the present invention 1 to not spending the shelf-life and having spent the shelf-life
Same drug is detected, can present different colors, and it is obvious to develop the color, it is easy to distinguish after detection reaction.Due to medicine mistake
After phase is rotten or manufacture counterfeit drug, chemical constituent therein changed, detected by present invention detection liquid, can be presented and guarantor
The different color presented by certified products drug detection reaction in the matter phase.
3 obtained detection liquid of the embodiment of the present invention 2 and embodiment is adopted successively, is protected to not crossing using identical detection method
The matter phase and crossed the shelf-life more than 6 kinds of medicines carry out detection contrast experiment respectively, acquired results implement 1 institute with using the present invention
The result of obtained detection liquid detection gained is basically identical, wherein, 2 obtained detection liquid of embodiment detects presented color most
For obvious, it is easy to distinguish.
It follows that the detection liquid by adopting the present invention, detects to medicine to be measured, institute is reacted in detection according to the observation
The color of presentation, can differentiate to the true and false quality of medicine.
In summary, multi-functional detection liquid provided by the present invention, can be by different from the presentation of different material haptoreaction
Color, so as to make a distinction to different material, and then can be used for the true and false good of many kinds of substance (such as varieties of food items and medicine)
It is bad to be differentiated.And the detection liquid prepare it is simple, it is with low cost, be widely used, easy to use, sensitivity is high, reaction is quick, shows
Color is obvious, it is easy to distinguish, and good stability, long shelf-life.
Described above is the detailed description for preferably possible embodiments of the invention, but embodiment is not limited to this
Bright patent claim, the equal change completed under the technical spirit suggested by all present invention or modification change, all should belong to
In the covered the scope of the claims of the present invention.
Claims (5)
1. a kind of multi-functional detection liquid, it is characterised in that the detection liquid is mainly made up of the raw material of following weight portion：Calx 6-
8 parts, sulfur 14-16 parts, Alumen 1-3 parts, Natrii Sulfas 7-9 parts, Chalcanthitum 3-5 parts, Melanteritum 2-4 parts, Vermilion 4-6 parts, Borax 2-4 parts,
Nitric acid 10-20 parts, distilled water 700-900 parts；Wherein, the mass concentration of the nitric acid is 50-70%.
2. multi-functional detection liquid as claimed in claim 1, it is characterised in that the detection liquid is mainly by the original of following weight portion
Material is made：6.9 parts of Calx, 15.6 parts of sulfur, 1.9 parts of Alumen, 8 parts of Natrii Sulfas, 3.6 parts of Chalcanthitum, 3 parts of Melanteritum, 5 parts of Vermilion, Borax
3.5 parts, 18 parts of nitric acid, 800 parts of distilled water；Wherein, the mass concentration of the nitric acid is 69%.
3. multi-functional detection liquid as claimed in claim 1, it is characterised in that the detection liquid is obtained as follows：
(1) each raw material is weighed by the weight portion；
(2) by Calx, sulfur, Alumen mixing, distilled water is then added, is stirred, be again heated to boiling, then stop adding
Heat, stands 24h releasing fire-toxin, obtains just mixed liquid；
(3) Vermilion is mixed with nitric acid and is stirred evenly, after placing 2h, be added in the just mixed liquid；Then sequentially add Natrii Sulfas,
Chalcanthitum, Melanteritum, are stirred well to dissolving, obtain final product.
4. application of the arbitrary described multi-functional detection liquid of claim 1-3 in terms of qualitative detection.
5. application of the arbitrary described multi-functional detection liquid of claim 1-3 on the true and false quality to food, medicine differentiates.
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| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201610999283.4A CN106568772A (en) | 2016-11-14 | 2016-11-14 | Multifunctional detection liquid |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201610999283.4A CN106568772A (en) | 2016-11-14 | 2016-11-14 | Multifunctional detection liquid |
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| CN106568772A true CN106568772A (en) | 2017-04-19 |
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Citations (5)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN102183615A (en) * | 2011-05-12 | 2011-09-14 | 北京市药品检验所 | Kit for rapidly testing flower herbs adulteration in traditional Chinese medicine |
| CN105699343A (en) * | 2016-01-05 | 2016-06-22 | 华南农业大学 | Method for nondestructively identifying authenticity of agilawood |
| CN105891172A (en) * | 2016-03-30 | 2016-08-24 | 李莉 | Method for detecting and recognizing different species and easily confused traditional Chinese medicine materials or traditional Chinese medicine decoction pieces |
| CN105954368A (en) * | 2016-04-15 | 2016-09-21 | 山东省食品药品检验研究院 | Authentication method for medicinal material sandalwood |
| CN106092950A (en) * | 2016-06-08 | 2016-11-09 | 常熟雷允上制药有限公司 | A kind of method differentiating dendrobium candidum medicinal material based near infrared spectrum |
-
2016
- 2016-11-14 CN CN201610999283.4A patent/CN106568772A/en active Pending
Patent Citations (5)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN102183615A (en) * | 2011-05-12 | 2011-09-14 | 北京市药品检验所 | Kit for rapidly testing flower herbs adulteration in traditional Chinese medicine |
| CN105699343A (en) * | 2016-01-05 | 2016-06-22 | 华南农业大学 | Method for nondestructively identifying authenticity of agilawood |
| CN105891172A (en) * | 2016-03-30 | 2016-08-24 | 李莉 | Method for detecting and recognizing different species and easily confused traditional Chinese medicine materials or traditional Chinese medicine decoction pieces |
| CN105954368A (en) * | 2016-04-15 | 2016-09-21 | 山东省食品药品检验研究院 | Authentication method for medicinal material sandalwood |
| CN106092950A (en) * | 2016-06-08 | 2016-11-09 | 常熟雷允上制药有限公司 | A kind of method differentiating dendrobium candidum medicinal material based near infrared spectrum |
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