CN106566676A - Powerful decontaminating and toilet cleaning detergent and preparation method thereof - Google Patents

Powerful decontaminating and toilet cleaning detergent and preparation method thereof Download PDF

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Publication number
CN106566676A
CN106566676A CN201610890009.3A CN201610890009A CN106566676A CN 106566676 A CN106566676 A CN 106566676A CN 201610890009 A CN201610890009 A CN 201610890009A CN 106566676 A CN106566676 A CN 106566676A
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CN
China
Prior art keywords
sodium
agent
toilet cleaning
parts
cleaning agent
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Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Pending
Application number
CN201610890009.3A
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Chinese (zh)
Inventor
向洋
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
Chongqing Wuyi Clean New Material Co Ltd
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Chongqing Wuyi Clean New Material Co Ltd
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Priority to CN201610890009.3A priority Critical patent/CN106566676A/en
Publication of CN106566676A publication Critical patent/CN106566676A/en
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    • C—CHEMISTRY; METALLURGY
    • C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
    • C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
    • C11D1/00—Detergent compositions based essentially on surface-active compounds; Use of these compounds as a detergent
    • C11D1/66—Non-ionic compounds
    • C11D1/72—Ethers of polyoxyalkylene glycols
    • C11D1/721—End blocked ethers
    • C—CHEMISTRY; METALLURGY
    • C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
    • C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
    • C11D1/00—Detergent compositions based essentially on surface-active compounds; Use of these compounds as a detergent
    • C11D1/66—Non-ionic compounds
    • C11D1/825—Mixtures of compounds all of which are non-ionic
    • C11D1/8255—Mixtures of compounds all of which are non-ionic containing a combination of compounds differently alcoxylised or with differently alkylated chains
    • C—CHEMISTRY; METALLURGY
    • C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
    • C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
    • C11D3/00—Other compounding ingredients of detergent compositions covered in group C11D1/00
    • C11D3/0005—Other compounding ingredients characterised by their effect
    • C11D3/0036—Soil deposition preventing compositions; Antiredeposition agents
    • C—CHEMISTRY; METALLURGY
    • C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
    • C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
    • C11D3/00—Other compounding ingredients of detergent compositions covered in group C11D1/00
    • C11D3/0005—Other compounding ingredients characterised by their effect
    • C11D3/0047—Other compounding ingredients characterised by their effect pH regulated compositions
    • C—CHEMISTRY; METALLURGY
    • C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
    • C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
    • C11D3/00—Other compounding ingredients of detergent compositions covered in group C11D1/00
    • C11D3/02—Inorganic compounds ; Elemental compounds
    • C11D3/04—Water-soluble compounds
    • C11D3/046—Salts
    • C—CHEMISTRY; METALLURGY
    • C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
    • C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
    • C11D3/00—Other compounding ingredients of detergent compositions covered in group C11D1/00
    • C11D3/02—Inorganic compounds ; Elemental compounds
    • C11D3/04—Water-soluble compounds
    • C11D3/08—Silicates
    • C—CHEMISTRY; METALLURGY
    • C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
    • C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
    • C11D3/00—Other compounding ingredients of detergent compositions covered in group C11D1/00
    • C11D3/02—Inorganic compounds ; Elemental compounds
    • C11D3/04—Water-soluble compounds
    • C11D3/10—Carbonates ; Bicarbonates
    • C—CHEMISTRY; METALLURGY
    • C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
    • C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
    • C11D3/00—Other compounding ingredients of detergent compositions covered in group C11D1/00
    • C11D3/16—Organic compounds
    • C11D3/20—Organic compounds containing oxygen
    • C11D3/2075—Carboxylic acids-salts thereof
    • C11D3/2086—Hydroxy carboxylic acids-salts thereof
    • C—CHEMISTRY; METALLURGY
    • C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
    • C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
    • C11D3/00—Other compounding ingredients of detergent compositions covered in group C11D1/00
    • C11D3/16—Organic compounds
    • C11D3/20—Organic compounds containing oxygen
    • C11D3/2093—Esters; Carbonates
    • C—CHEMISTRY; METALLURGY
    • C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
    • C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
    • C11D3/00—Other compounding ingredients of detergent compositions covered in group C11D1/00
    • C11D3/39—Organic or inorganic per-compounds
    • C11D3/3942—Inorganic per-compounds

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  • Chemical & Material Sciences (AREA)
  • Life Sciences & Earth Sciences (AREA)
  • Engineering & Computer Science (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Oil, Petroleum & Natural Gas (AREA)
  • Wood Science & Technology (AREA)
  • Organic Chemistry (AREA)
  • Inorganic Chemistry (AREA)
  • Health & Medical Sciences (AREA)
  • Emergency Medicine (AREA)
  • Detergent Compositions (AREA)

Abstract

The invention belongs to the technical field of detergent, and particularly relates to powerful decontaminating and toilet cleaning detergent. The detergent is composed of, by mass, 5.4-7.2 parts of sodium citrate, 2.7-3.5 parts of glycollic acid, 1.7-2.5 parts of alkylphenol ethoxylates, 1.2-1.7 parts of sodium sulfate, 2.5-2.8 parts of a pH regulator, 0.48-0.63 part of an anti-redeposition agent, 0.84-1.21 parts of a blenching agent and 64-88 parts of water. The detergent is good in cleaning effect and high in decontaminating capacity, a preparation method of the powerful decontaminating and toilet cleaning detergent is simple, and industrialized production is easy to achieve.

Description

Potent decontamination toilet cleaning agent and preparation method thereof
Technical field
The invention belongs to cleaning agent technical field, and in particular to a kind of potent decontamination toilet cleaning agent and preparation method thereof.
Background technology
In actual life, due to life process in accumulate over a long period so that the health of family, hotel, restaurant etc. lavatory There are many dead angles in situation, occurs some dirts for being difficult to remove in each corner and toilet, and these are throughout the year accumulative Dirt, relies solely on common cleaning agent clean effect not strong, it is difficult to realize quickly, thoroughly cleaning.
The content of the invention
In view of this, it is an object of the invention to provide a kind of potent decontamination toilet cleaning agent.The toilet cleaning agent cleaning Effect is good.
To realize object above, technical scheme is as follows：
A kind of potent decontamination toilet cleaning agent, is made up of following content of component：Sodium citrate 5.4-7.2 parts, glycolic 2.7-3.5 parts, APES 1.7-2.5 parts, sodium sulphate 1.2-1.7 parts, pH adjusting agent 2.5-2.8 part, anti-sink again Product agent 0.48-0.63 parts, bleaching agent 0.84-1.21 parts and water 64-88 parts.
The sodium citrate calls sodium citrate, is a kind of organic compound, and outward appearance is white to clear crystal.Odorless, There is refrigerant salty pungent.Sodium citrate is used as acidity regulator, flavouring agent, stabilizer in food, beverage industry；In medical industry In be used as anticoagulant, apophlegmatisant and diuretics；In detergent industry, alternative sodium tripolyphosphate is used as non-toxic detergent Auxiliary agent；Be additionally operable to brewage, parenteral solution, photographic chemical and plating etc..
Further, the APES be NPE, OPEO or the two Composition.
The APES (English abbreviation is APEO) is a kind of important polyoxyethylene-type non-ionic surface Activating agent, it has stable in properties, acid and alkali-resistance and the low feature of cost, is that printing and dyeing are helped mainly to produce high-performance detergent One of the most frequently used primary raw material in agent.
Further, the APES by NPE and OPEO according to 4： 3 quality is formed than proportioning.
Further, the pH adjusting agent by anhydrous sodium metasilicate and sodium carbonate according to 3:2 quality is formed than proportioning.The PH Conditioning agent is also called pH value conditioning agent, acidity regulator or pH value controlling agent.
Further, the anti redeposition agent is methyl acrylate.Antiredeposition is from fabric fibre or other object wash-outs The not Fu solution solids foul for getting off so as to disperse and be suspended in wash solution, and do not return again to deposit to fabric or other objects On a kind of cleaning function.Material with this anti-redeposition is referred to as anti redeposition agent, such as sodium carboxymethylcellulose.It is interior Olefin(e) acid homopolymers etc..
Further, the bleaching agent is SODIUM PERCARBONATE, sodium perborate or combination thing.The bleaching agent be destruction, Suppress the chromogenic factors of food so as to fade or make food to avoid the material of brown stain.
Further, the bleaching agent by SODIUM PERCARBONATE and sodium perborate according to 1:2 quality is formed than proportioning.
The present invention also aims to protect the preparation method of the potent decontamination toilet cleaning agent, following step is specifically included Suddenly：
S1:Sodium citrate and glycolic is soluble in water, 50-55 DEG C is heated to, add APES and stir Mix uniform, be cooled to room temperature；
S2:Sodium sulphate, bleaching agent, anti redeposition agent, pH adjusting agent are sequentially added in step S1 gained mixture；Stirring Uniformly.
The beneficial effects of the present invention is：
The cleaning agent cleaning performance of the present invention is good, and dirt-removing power is strong, and its preparation method is simple, it is easy to industrialized production.
Specific embodiment
Embodiment of the present invention is described in detail below in conjunction with embodiment, but those skilled in the art will Understand, the following example is merely to illustrate the present invention, and should not be taken as limiting the scope of the invention.It is unreceipted in preferred embodiment The experimental technique of actual conditions, generally according to normal condition.
Embodiment 1
A kind of potent decontamination toilet cleaning agent, consisting of：Sodium citrate 7.2kg, glycolic 2.7kg, polyoxyethylene nonyl phenyl Vinethene 1.7kg, sodium sulphate 1.7kg, anhydrous sodium metasilicate 1.68kg, sodium carbonate 1.12kg, methyl acrylate 0.63kg, percarbonic acid Sodium 0.84kg and water 88kg.
The preparation method of the potent decontamination toilet cleaning agent is：
S1:Sodium citrate and glycolic is soluble in water, 55 DEG C are heated to, add NPE and stir Uniformly, it is cooled to room temperature；
S2:Sodium sulphate, SODIUM PERCARBONATE, methyl acrylate, anhydrous sodium metasilicate are sequentially added in step S1 gained mixture And sodium carbonate；Stir.
Embodiment 2
A kind of potent decontamination toilet cleaning agent, consisting of：Sodium citrate 5.4kg, glycolic 3.5kg, octyl phenol polyoxy Vinethene 2.5kg, sodium sulphate 1.2kg, anhydrous sodium metasilicate 1.5kg, sodium carbonate 1.0kg, methyl acrylate 0.48kg, sodium perborate 1.21kg and water 64kg.
The preparation method of the potent decontamination toilet cleaning agent is：
S1:Sodium citrate and glycolic is soluble in water, 50 DEG C are heated to, add OPEO and stir equal It is even, it is cooled to room temperature；
S2:Sodium sulphate, sodium perborate, methyl acrylate, anhydrous sodium metasilicate are sequentially added in step S1 gained mixture And sodium carbonate；Stir.
Embodiment 3
A kind of potent decontamination toilet cleaning agent, consisting of：Sodium citrate 6.7kg, glycolic 3.2kg, polyoxyethylene nonyl phenyl Vinethene 1.2kg, OPEO 0.9kg, sodium sulphate 1.35kg, anhydrous sodium metasilicate 1.56kg, sodium carbonate 1.04kg, Methyl acrylate 0.57kg, SODIUM PERCARBONATE 0.72kg, sodium perborate 0.24kg and water 72kg.
The preparation method of the potent decontamination toilet cleaning agent is：
S1:Sodium citrate and glycolic is soluble in water, 53 DEG C are heated to, add NPE, octyl phenol APEO simultaneously stirs, and is cooled to room temperature；
S2:Sodium sulphate, SODIUM PERCARBONATE, sodium perborate, methyl acrylate, nothing are sequentially added in step S1 gained mixture Water sodium metasilicate and sodium carbonate；Stir.
Comparative example 1
A kind of potent decontamination toilet cleaning agent, consisting of：Sodium citrate 5.8kg, glycolic 2.8kg, polyoxyethylene nonyl phenyl Vinethene 2.1kg, anhydrous sodium metasilicate 1.5kg, sodium carbonate 1.0kg, methyl acrylate 0.53kg, SODIUM PERCARBONATE 0.94kg and water 68kg。
The preparation method of the potent decontamination toilet cleaning agent is：
S1:Sodium citrate and glycolic is soluble in water, 51 DEG C are heated to, add NPE and stir equal It is even, it is cooled to room temperature；
S2:SODIUM PERCARBONATE, methyl acrylate, anhydrous sodium metasilicate and carbonic acid are sequentially added in step S1 gained mixture Sodium；Stir.
Comparative example 2
A kind of potent decontamination toilet cleaning agent, consisting of：Sodium citrate 8.1kg, glycolic 3.4kg, octyl phenol polyoxy Vinethene 2.0kg, sodium sulphate 1.27kg, anhydrous sodium metasilicate 1.53kg, sodium carbonate 1.02kg, excessively methyl acrylate 0.58kg, carbon Sour sodium 0.88kg and water 69kg.
The preparation method of the potent decontamination toilet cleaning agent is：
S1:Sodium citrate and glycolic is soluble in water, 54 DEG C are heated to, add OPEO and stir equal It is even, it is cooled to room temperature；
S2:Sodium sulphate, SODIUM PERCARBONATE, methyl acrylate, anhydrous sodium metasilicate are sequentially added in step S1 gained mixture And sodium carbonate；Stir.
Comparative example 3
A kind of potent decontamination toilet cleaning agent, consisting of：Sodium citrate 6.2kg, glycolic 2.9kg, polyoxyethylene nonyl phenyl Vinethene, 1.75kg, sodium sulphate 1.32kg, anhydrous sodium metasilicate 1.62kg, excessively sodium carbonate 1.08kg methyl acrylate 0.53kg, boron Sour sodium 1.11kg and water 78kg.
The preparation method of the potent decontamination toilet cleaning agent is：
S1:Sodium citrate and glycolic is soluble in water, 51 DEG C are heated to, add NPE and stir Uniformly, it is cooled to room temperature；
S2:Methyl acrylate, sodium sulphate, sodium perborate, anhydrous sodium metasilicate are sequentially added in step S1 gained mixture And sodium carbonate；Stir.
Cleaning agent outward appearance and performance test
Sensory evaluation in terms of outward appearance, smell, stability is carried out to the cleaning agent that embodiment 1-3 and comparative example 1-3 are obtained, As a result it is as shown in the table：
Remarks：Outward appearance method of testing is：Take appropriate amount of sample to be placed in dried and clean test tube, enter under non-direct projection light condition Row observation.Low-temperature stability method of testing is：Sample is poured in the 60mL glass ground joint reagent bottles of cleaning, -5 ± 2 DEG C are placed in In refrigerator, take out after 24h, it is disposed within to recover to room temperature, check outward appearance.High-temperature stability method of testing is：Sample is fallen In entering the 60mL glass ground joint reagent bottles of cleaning, in being placed in 40 ± 2 DEG C of refrigerators, take out after 24h, outward appearance, smell are checked immediately.
The toilet cleaning agent that embodiment 1-3 and comparative example 1-3 are obtained is sprayed on the toilet surface for speckling with spot, 5 minutes Afterwards, scrubbed with brush, it is as a result as shown in the table：
Finally illustrate, above example is only unrestricted to illustrate technical scheme, although with reference to compared with Good embodiment has been described in detail to the present invention, it will be understood by those within the art that, can be to the skill of the present invention Art scheme is modified or equivalent, and without deviating from the objective and scope of technical solution of the present invention, it all should cover at this In the middle of the right of invention.

Claims (8)

1. a kind of potent decontamination toilet cleaning agent, it is characterised in that be made up of following content of component：Sodium citrate 5.4-7.2 Part, glycolic 2.7-3.5 parts, APES 1.7-2.5 parts, sodium sulphate 1.2-1.7 parts, pH adjusting agent 2.5-2.8 Part, anti redeposition agent 0.48-0.63 parts, bleaching agent 0.84-1.21 parts and water 64-88 parts.
2. a kind of potent decontamination toilet cleaning agent according to claim 1, it is characterised in that the alkylphenol-polyethenoxy Ether is NPE, OPEO or combination thing.
3. a kind of potent decontamination toilet cleaning agent according to claim 2, it is characterised in that the alkylphenol-polyethenoxy Ether is by NPE and OPEO according to 4：3 quality is formed than proportioning.
4. a kind of potent decontamination toilet cleaning agent according to claim 1, it is characterised in that the pH adjusting agent is by anhydrous Sodium metasilicate and sodium carbonate are according to 3:2 quality is formed than proportioning.
5. a kind of potent decontamination toilet cleaning agent according to claim 1, it is characterised in that the anti redeposition agent is third E pioic acid methyl ester.
6. a kind of potent decontamination toilet cleaning agent according to claim 1, it is characterised in that the bleaching agent is percarbonic acid Sodium, sodium perborate or combination thing.
7. a kind of potent decontamination toilet cleaning agent according to claim 6, it is characterised in that the bleaching agent is by percarbonic acid Sodium and sodium perborate are according to 1:2 quality is formed than proportioning.
8. the preparation method of the potent decontamination toilet cleaning agent described in claim 1, it is characterised in that comprise the following steps：
S1:Sodium citrate and glycolic is soluble in water, 50-55 DEG C is heated to, add APES and stir equal It is even, it is cooled to room temperature；
S2:Sodium sulphate, bleaching agent, anti redeposition agent, pH adjusting agent are sequentially added in step S1 gained mixture；Stirring is equal It is even.
CN201610890009.3A 2016-10-12 2016-10-12 Powerful decontaminating and toilet cleaning detergent and preparation method thereof Pending CN106566676A (en)

Priority Applications (1)

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Application Number Priority Date Filing Date Title
CN201610890009.3A CN106566676A (en) 2016-10-12 2016-10-12 Powerful decontaminating and toilet cleaning detergent and preparation method thereof

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Citations (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN103215144A (en) * 2013-03-22 2013-07-24 于文 Acidic lasting wall built-up type toilet bowl cleaner and preparation method thereof
CN103666780A (en) * 2012-09-22 2014-03-26 青岛道合生物科技有限公司 Special cleaning disinfecting liquid for toilets
CN104073370A (en) * 2014-07-03 2014-10-01 谢伟杰 Toilet antibacterial cleaning agent

Patent Citations (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN103666780A (en) * 2012-09-22 2014-03-26 青岛道合生物科技有限公司 Special cleaning disinfecting liquid for toilets
CN103215144A (en) * 2013-03-22 2013-07-24 于文 Acidic lasting wall built-up type toilet bowl cleaner and preparation method thereof
CN104073370A (en) * 2014-07-03 2014-10-01 谢伟杰 Toilet antibacterial cleaning agent

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Application publication date: 20170419