CN106566333A - Preparation method of composite fragrance type environment-friendly coating - Google Patents

Preparation method of composite fragrance type environment-friendly coating Download PDF

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Publication number
CN106566333A
CN106566333A CN201610886891.4A CN201610886891A CN106566333A CN 106566333 A CN106566333 A CN 106566333A CN 201610886891 A CN201610886891 A CN 201610886891A CN 106566333 A CN106566333 A CN 106566333A
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China
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parts
environmental protection
coating material
protection coating
type environmental
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Pending
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CN201610886891.4A
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Chinese (zh)
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王胜利
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Individual
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Individual
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    • CCHEMISTRY; METALLURGY
    • C09DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
    • C09DCOATING COMPOSITIONS, e.g. PAINTS, VARNISHES OR LACQUERS; FILLING PASTES; CHEMICAL PAINT OR INK REMOVERS; INKS; CORRECTING FLUIDS; WOODSTAINS; PASTES OR SOLIDS FOR COLOURING OR PRINTING; USE OF MATERIALS THEREFOR
    • C09D133/00Coating compositions based on homopolymers or copolymers of compounds having one or more unsaturated aliphatic radicals, each having only one carbon-to-carbon double bond, and at least one being terminated by only one carboxyl radical, or of salts, anhydrides, esters, amides, imides, or nitriles thereof; Coating compositions based on derivatives of such polymers
    • CCHEMISTRY; METALLURGY
    • C09DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
    • C09DCOATING COMPOSITIONS, e.g. PAINTS, VARNISHES OR LACQUERS; FILLING PASTES; CHEMICAL PAINT OR INK REMOVERS; INKS; CORRECTING FLUIDS; WOODSTAINS; PASTES OR SOLIDS FOR COLOURING OR PRINTING; USE OF MATERIALS THEREFOR
    • C09D103/00Coating compositions based on starch, amylose or amylopectin or on their derivatives or degradation products
    • C09D103/02Starch; Degradation products thereof, e.g. dextrin
    • CCHEMISTRY; METALLURGY
    • C09DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
    • C09DCOATING COMPOSITIONS, e.g. PAINTS, VARNISHES OR LACQUERS; FILLING PASTES; CHEMICAL PAINT OR INK REMOVERS; INKS; CORRECTING FLUIDS; WOODSTAINS; PASTES OR SOLIDS FOR COLOURING OR PRINTING; USE OF MATERIALS THEREFOR
    • C09D7/00Features of coating compositions, not provided for in group C09D5/00; Processes for incorporating ingredients in coating compositions
    • C09D7/40Additives
    • C09D7/60Additives non-macromolecular
    • C09D7/61Additives non-macromolecular inorganic
    • CCHEMISTRY; METALLURGY
    • C09DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
    • C09DCOATING COMPOSITIONS, e.g. PAINTS, VARNISHES OR LACQUERS; FILLING PASTES; CHEMICAL PAINT OR INK REMOVERS; INKS; CORRECTING FLUIDS; WOODSTAINS; PASTES OR SOLIDS FOR COLOURING OR PRINTING; USE OF MATERIALS THEREFOR
    • C09D7/00Features of coating compositions, not provided for in group C09D5/00; Processes for incorporating ingredients in coating compositions
    • C09D7/40Additives
    • C09D7/60Additives non-macromolecular
    • C09D7/63Additives non-macromolecular organic
    • CCHEMISTRY; METALLURGY
    • C09DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
    • C09DCOATING COMPOSITIONS, e.g. PAINTS, VARNISHES OR LACQUERS; FILLING PASTES; CHEMICAL PAINT OR INK REMOVERS; INKS; CORRECTING FLUIDS; WOODSTAINS; PASTES OR SOLIDS FOR COLOURING OR PRINTING; USE OF MATERIALS THEREFOR
    • C09D7/00Features of coating compositions, not provided for in group C09D5/00; Processes for incorporating ingredients in coating compositions
    • C09D7/40Additives
    • C09D7/65Additives macromolecular
    • CCHEMISTRY; METALLURGY
    • C08ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08LCOMPOSITIONS OF MACROMOLECULAR COMPOUNDS
    • C08L2205/00Polymer mixtures characterised by other features
    • C08L2205/03Polymer mixtures characterised by other features containing three or more polymers in a blend

Abstract

The invention relates to a preparation method of a composite fragrance type environment-friendly coating. The composite fragrance type environment-friendly coating comprises the following components: a Chinese scholartree leave extract, jasminum sambac concrete, peppermint oil, hydroxyethyl cellulose, titanium dioxide, calcium carbonate powder, an acrylic acid emulsion, mung bean flour, absolute ethyl alcohol and an assistant. The coating is environment-friendly, has a composite fragrance of jasmine fragrance and mint fragrance, is good for physical and psychological health of people, and pleases people.

Description

A kind of preparation method of compound fragrant type environmental protection coating material
Technical field
The present invention relates to building material technical field, more particularly to a kind of coating.
Background technology
Coating is one of indispensable material of building field, and being applied to body surface can form with protection, decoration Or the solid coated film of property.In recent years, with the raising of living standards of the people, the environmental consciousness of people and health requirements day Benefit strengthens, the poisonous and harmful substance pollution on the environment in building and ornament materials, the impact caused to human health also day Benefit is prominent.
Contain more volatile organic principle in traditional coating, abnormal flavour is produced after construction, what human body was worked the mischief is same When, allow people to smell one unpleasant, even nauseous abnormal smells from the patient.
Therefore, work out it is a kind of with fragrance and environmental protection coating, expected by people always.
The content of the invention
The purpose of the present invention, be provide it is a kind of with fragrance and environmental protection coating.
The above-mentioned purpose of the present invention is achieved through the following technical solutions:A kind of compound fragrant type environmental protection coating material, including Following components:Sophora japonica L. leaf extract, concrete of jasmine, Oleum menthae, hydroxyethyl cellulose, titanium dioxide, calcium carbonate powder, propylene yogurt Liquid, Semen phaseoli radiati powder, dehydrated alcohol and auxiliary agent.
Preferably, above-mentioned each component weight proportion is:Sophora japonica L. leaf extract 10-30 parts, concrete of jasmine 1-5 parts, Oleum menthae It is 1-6 parts, hydroxyethyl cellulose 5-10 parts, titanium dioxide 15-35 parts, calcium carbonate powder 20-45 parts, acrylic emulsion 10-15 parts, green Semen Glycines powder 5-15 parts, dehydrated alcohol 5-10 parts, auxiliary agent 1-10 parts.
More preferably, above-mentioned each component weight proportion is:Sophora japonica L. leaf extract 15-25 parts, concrete of jasmine 2-4 parts, Oleum menthae It is 2-5 parts, hydroxyethyl cellulose 5-8 parts, titanium dioxide 20-30 parts, calcium carbonate powder 30-40 parts, acrylic emulsion 12-13 parts, green Semen Glycines powder 8-10 parts, dehydrated alcohol 6-9 parts, auxiliary agent 3-5 parts.
Wherein, above-mentioned auxiliary agent is defoamer, wetting agent, drier, suspending agent, levelling agent, flatting agent or ultra-violet absorption Agent or its mixing.
The preparation method of above-mentioned Sophora japonica L. leaf extract is:
A. pretreatment of raw material:The clean Folium sophorae of roguing is dried into process;
B. pure water impregnation stage:By Folium sophorae and water according to 1:5~1:7 ratio mixing, is positioned over multi-function extractor, After stirring, 2~6h is soaked;
C. heating extraction method:The mixture of Folium sophorae in step b and water is led to and is steam heated to 80~90 DEG C, circulation is carried 1.5~4h is taken, by extracting solution through coarse filtration, pump to receiver, during second extraction, water and Folium sophorae are mixed in 2~4 times of ratio Close, Extracting temperature and time are identical with first time;
D. concentrate drying method:By the extracting solution in step c, through membrane separation concentration adjustment, and membrance separation circulation is controlled Pump inlet pressure keeps 0.5MPa, 0.2~0.3MPa of outlet pressure, when concentrated solution density is 1.10~1.15g/mL, squeezes into true Empty pump;Spray-dried again to be prepared into finished product, when carrying out centrifugal spray drying, it is 160~180 DEG C to control inlet temperature, air-out 60~80 DEG C of temperature.
Preferably, the coating of above-mentioned not release formaldehyde, also including gas-phase silica and silicon dioxide powder.
Wherein, above-mentioned gas-phase silica and silicon dioxide are 1-5 parts.
Preferably, above-mentioned gas-phase silica and silicon dioxide are 2-3 parts.
Wherein, above-mentioned gas-phase silica and the weight ratio of silicon dioxide are 1:1-0.3.
The invention has the beneficial effects as follows:The coating environmental protection of the present invention and the compound fragrant with jasmin Yu minty note, It is easy to the physical and mental health of human body, allows people to be in a cheerful frame of mind.
Below in conjunction with preferred embodiment, the invention will be further described.
Specific embodiment
Embodiment 1
10 parts of Sophora japonica L. leaf extract, 1 part of concrete of jasmine, 1 part of Oleum menthae, 5 parts of hydroxyethyl cellulose, 15 parts of titanium dioxide, carbon 20 parts of sour calcium powder, 10 parts of acrylic emulsion, 5 parts of Semen phaseoli radiati powder, 10 parts of dehydrated alcohol, 1 part of suspending agent.
Embodiment 2
30 parts of Sophora japonica L. leaf extract, 5 parts of concrete of jasmine, 6 parts of Oleum menthae, 10 parts of hydroxyethyl cellulose, 35 parts of titanium dioxide, carbon 30 parts of sour calcium powder, 15 parts of acrylic emulsion, 15 parts of Semen phaseoli radiati powder, 5 parts of dehydrated alcohol, 1 part of suspending agent, 2 parts of defoamer.
Embodiment 3
15 parts of Sophora japonica L. leaf extract, 2 parts of concrete of jasmine, 2 parts of Oleum menthae, 5 parts of hydroxyethyl cellulose, 20 parts of titanium dioxide, carbon 30 parts of sour calcium powder, 12 parts of acrylic emulsion, 8 parts of Semen phaseoli radiati powder, 6 parts of dehydrated alcohol, 3 parts of UV absorbent.
Embodiment 4
20 parts of Sophora japonica L. leaf extract, 4 parts of concrete of jasmine, 5 parts of Oleum menthae, 8 parts of hydroxyethyl cellulose, 30 parts of titanium dioxide, carbon 40 parts of sour calcium powder, 13 parts of acrylic emulsion, 10 parts of Semen phaseoli radiati powder, 9 parts of dehydrated alcohol, 5 parts of UV absorbent, 1 part of suspending agent.
Embodiment 5
11 parts of Sophora japonica L. leaf extract, 3 parts of concrete of jasmine, 4 parts of Oleum menthae, 7 parts of hydroxyethyl cellulose, 35 parts of titanium dioxide, carbon 3 parts of 35 parts of sour calcium powder, 10 parts of acrylic emulsion, 10 parts of Semen phaseoli radiati powder, 5 parts of dehydrated alcohol, gas-phase silica and silicon dioxide powder, 5 parts of suspending agent.
Wherein, gas-phase silica and the weight ratio of silicon dioxide powder are 1:1.
Embodiment 6
15 parts of Sophora japonica L. leaf extract, 3 parts of concrete of jasmine, 5 parts of Oleum menthae, 10 parts of hydroxyethyl cellulose, 35 parts of titanium dioxide, carbon 3 parts of 35 parts of sour calcium powder, 10 parts of acrylic emulsion, 10 parts of Semen phaseoli radiati powder, 5 parts of dehydrated alcohol, gas-phase silica and silicon dioxide powder, 5 parts of suspending agent.
Wherein, gas-phase silica and the weight ratio of silicon dioxide powder are 1:0.3.
In above-described embodiment, the preparation method of above-mentioned Sophora japonica L. leaf extract is:
A. preprocessing method of raw materials:The clean Folium sophorae of roguing is dried into process;
B. pure water immersion process:By Folium sophorae and water according to 1:5~1:7 ratio mixing, is positioned over multi-function extractor, After stirring, 2~6h is soaked;
C. heating extraction method:The mixture of Folium sophorae in step b and water is led to and is steam heated to 80~90 DEG C, circulation is carried 1.5~4h is taken, by extracting solution through coarse filtration, pump to receiver, during second extraction, water and Folium sophorae are mixed in 2~4 times of ratio Close, Extracting temperature and time are identical with first time;
D. concentrate drying method:By the extracting solution in step c, through membrane separation concentration adjustment, and membrance separation circulation is controlled Pump inlet pressure keeps 0.5MPa, 0.2~0.3MPa of outlet pressure, when concentrated solution density is 1.10~1.15g/mL, squeezes into true Empty pump;Spray-dried again to be prepared into finished product, when carrying out centrifugal spray drying, it is 160~180 DEG C to control inlet temperature, air-out 60~80 DEG C of temperature.
Above the above embodiments are only that the preferred embodiment of the present invention is described, not to the model of the present invention Enclose and be defined, on the premise of without departing from design spirit of the present invention, technical side of the those of ordinary skill in the art to the present invention Various modifications and improvement that case is made, all should fall in the protection domain of claims of the present invention determination.

Claims (9)

1. a kind of compound fragrant type environmental protection coating material, it is characterised in that including following components:It is Sophora japonica L. leaf extract, concrete of jasmine, thin Lotus oil, hydroxyethyl cellulose, titanium dioxide, calcium carbonate powder, acrylic emulsion, Semen phaseoli radiati powder, dehydrated alcohol and auxiliary agent.
2. such as the above-mentioned compound fragrant type environmental protection coating material of claim 1, it is characterised in that each component weight proportion is:Folium sophorae Extract 10-30 parts, concrete of jasmine 1-5 parts, Oleum menthae 1-6 parts, hydroxyethyl cellulose 5-10 parts, titanium dioxide 15-35 parts, carbonic acid Calcium powder 20-45 parts, acrylic emulsion 10-15 parts, Semen phaseoli radiati powder 5-15 parts, dehydrated alcohol 5-10 parts, auxiliary agent 1-10 parts.
3. such as the above-mentioned compound fragrant type environmental protection coating material of claim 2, it is characterised in that each component weight proportion is:Folium sophorae Extract 15-25 parts, concrete of jasmine 2-4 parts, Oleum menthae 2-5 parts, hydroxyethyl cellulose 5-8 parts, titanium dioxide 20-30 parts, carbonic acid Calcium powder 30-40 parts, acrylic emulsion 12-13 parts, Semen phaseoli radiati powder 8-10 parts, dehydrated alcohol 6-9 parts, auxiliary agent 3-5 parts.
4. such as the above-mentioned compound fragrant type environmental protection coating material of claim 1, it is characterised in that above-mentioned auxiliary agent be defoamer, wetting agent, Drier, suspending agent, levelling agent, flatting agent or UV absorbent or its mixing.
5. such as the above-mentioned compound fragrant type environmental protection coating material of claim 1, it is characterised in that the preparation side of above-mentioned Sophora japonica L. leaf extract Method is:A. pretreatment of raw material:The clean Folium sophorae of roguing is dried into process;B. pure water impregnation stage:By Folium sophorae and water According to 1:5~1:7 ratio mixing, is positioned over multi-function extractor, after stirring, soaks 2~6h;C. heating extraction:Will The mixture of Folium sophorae and water is logical in step b is steam heated to 80~90 DEG C, and 1.5~4h is extracted in circulation, by extracting solution through thick Filter, pump to receiver, during second extraction, water and Folium sophorae are mixed by 2~4 times of ratio, Extracting temperature and time and first time It is identical;D. concentrate drying stage:By the extracting solution in step c, adjust, and control membrance separation circulating pump to enter through membrane separation concentration Mouth pressure keeps 0.5MPa, 0.2~0.3MPa of outlet pressure, when concentrated solution density is 1.10~1.15g/mL, squeezes into vacuum pump; Spray-dried again to be prepared into finished product, when carrying out centrifugal spray drying, it is 160~180 DEG C to control inlet temperature, leaving air temp 60 ~80 DEG C.
6. such as the above-mentioned compound fragrant type environmental protection coating material of claim 1-5 any claim, it is characterised in that also including gas phase White carbon and silicon dioxide powder.
7. such as the above-mentioned compound fragrant type environmental protection coating material of claim 6, it is characterised in that above-mentioned gas-phase silica and silicon dioxide For 1-5 parts.
8. such as the above-mentioned compound fragrant type environmental protection coating material of claim 7, it is characterised in that above-mentioned gas-phase silica and silicon dioxide For 2-3 parts.
9. such as the above-mentioned compound fragrant type environmental protection coating material of claim 7 or 8, it is characterised in that above-mentioned gas-phase silica and dioxy The weight ratio of SiClx is 1:1-0.3.
CN201610886891.4A 2016-10-11 2016-10-11 Preparation method of composite fragrance type environment-friendly coating Pending CN106566333A (en)

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Application Number Priority Date Filing Date Title
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Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
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Publications (1)

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CN106566333A true CN106566333A (en) 2017-04-19

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Country Status (1)

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Citations (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN104530865A (en) * 2014-12-26 2015-04-22 青岛佳尚创意文化有限公司 Novel environment-friendly waterproof interior wall coating
CN104530866A (en) * 2014-12-26 2015-04-22 青岛佳尚创意文化有限公司 Novel environment-friendly anti-fouling coating
CN104861807A (en) * 2015-05-27 2015-08-26 湖州大周高分子材料有限公司 Interior wall coating and preparation method thereof

Patent Citations (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN104530865A (en) * 2014-12-26 2015-04-22 青岛佳尚创意文化有限公司 Novel environment-friendly waterproof interior wall coating
CN104530866A (en) * 2014-12-26 2015-04-22 青岛佳尚创意文化有限公司 Novel environment-friendly anti-fouling coating
CN104861807A (en) * 2015-05-27 2015-08-26 湖州大周高分子材料有限公司 Interior wall coating and preparation method thereof

Non-Patent Citations (1)

* Cited by examiner, † Cited by third party
Title
蔡辉益: "《饲料添加剂研究与应用新技术》", 31 January 2016 *

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