CN106552439A - A kind of recovery system of Herba Rosmarini Officinalis extract Extraction solvent - Google Patents
A kind of recovery system of Herba Rosmarini Officinalis extract Extraction solvent Download PDFInfo
- Publication number
- CN106552439A CN106552439A CN201710064086.8A CN201710064086A CN106552439A CN 106552439 A CN106552439 A CN 106552439A CN 201710064086 A CN201710064086 A CN 201710064086A CN 106552439 A CN106552439 A CN 106552439A
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- CN
- China
- Prior art keywords
- rectifying column
- extraction solvent
- pipeline
- officinalis extract
- herba rosmarini
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
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- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01D—SEPARATION
- B01D3/00—Distillation or related exchange processes in which liquids are contacted with gaseous media, e.g. stripping
- B01D3/14—Fractional distillation or use of a fractionation or rectification column
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01D—SEPARATION
- B01D11/00—Solvent extraction
- B01D11/02—Solvent extraction of solids
- B01D11/0292—Treatment of the solvent
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01D—SEPARATION
- B01D3/00—Distillation or related exchange processes in which liquids are contacted with gaseous media, e.g. stripping
- B01D3/14—Fractional distillation or use of a fractionation or rectification column
- B01D3/32—Other features of fractionating columns ; Constructional details of fractionating columns not provided for in groups B01D3/16 - B01D3/30
- B01D3/322—Reboiler specifications
-
- Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
- Y02—TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
- Y02P—CLIMATE CHANGE MITIGATION TECHNOLOGIES IN THE PRODUCTION OR PROCESSING OF GOODS
- Y02P70/00—Climate change mitigation technologies in the production process for final industrial or consumer products
- Y02P70/10—Greenhouse gas [GHG] capture, material saving, heat recovery or other energy efficient measures, e.g. motor control, characterised by manufacturing processes, e.g. for rolling metal or metal working
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- Chemical & Material Sciences (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Vaporization, Distillation, Condensation, Sublimation, And Cold Traps (AREA)
Abstract
The present invention relates to the rapidly and efficiently low consumption of this practical design Herba Rosmarini Officinalis extract Extraction solvent is reclaimed，It is specifically related to a kind of recovery system of Herba Rosmarini Officinalis extract Extraction solvent，Including reboiler，The reboiler gas outlet is connected with hypergravity rectifying column air inlet by the first pipeline，Feed pipe is connected with hypergravity rectifying column，Hypergravity rectifying column liquid outlet is connected with reboiler inlet by second pipe，Hypergravity rectifying column gas outlet is connected with condenser inlet by the 3rd pipeline，Condensator outlet is connected with collecting tank entrance by the 4th pipeline，Collecting tank outlet is connected with reflux pump，Reflux pump is connected with hypergravity rectifying column inlet by the 5th pipeline，The recovery system of the Herba Rosmarini Officinalis extract Extraction solvent of the present invention can substitute traditional old-fashioned distillation system，It is rationally distributed efficient，Greatly increase Extraction solvent organic efficiency，Reducing energy consumption，Energy-saving and emission-reduction.
Description
Technical field
The present invention relates to the rapidly and efficiently low consumption of Herba Rosmarini Officinalis extract Extraction solvent is reclaimed, a kind of Herba Rosmarini Officinalis is specifically related to
The recovery system of extract Extraction solvent.
Background technology
Solvent still with the value for recycling, is such as directly discharged after practicality by Herba Rosmarini Officinalis extract Extraction solvent, right
Environment etc. can affect, and equally affect economic worth, the practical rectifying column of previous solvent recovery to take up an area space
Greatly, invest high, power consumption is high, organic efficiency is relatively low, and separating power is poor, waste discharge pollution is larger, is not suitable for large-scale production.
The content of the invention
To solve problem of the prior art, the invention provides a kind of recovery system of Herba Rosmarini Officinalis extract Extraction solvent.
In order to achieve the above object, the present invention is employed the following technical solutions：A kind of Herba Rosmarini Officinalis extract Extraction solvent return
Receipts system, including reboiler, the reboiler gas outlet are connected with hypergravity rectifying column air inlet by the first pipeline, feed pipe
Connect with hypergravity rectifying column, hypergravity rectifying column liquid outlet is connected with reboiler inlet by second pipe, hypergravity rectification
Tower gas outlet is connected with condenser inlet by the 3rd pipeline, and condensator outlet is connected with collecting tank entrance by the 4th pipeline,
Collecting tank outlet is connected with reflux pump, and reflux pump is connected with hypergravity rectifying column inlet by the 5th pipeline.
Preferred described feed pipe one end is connected with preheater, and preheater is connected with filter, filter and storage tank phase
Even, first flowmeter is provided between storage tank and filter.
Second flowmeter is provided with preferred 3rd pipeline.
Temperature sensor is provided with the preferred hypergravity rectifying column, temperature sensor connection controller, controller connect
Stirring motor is connect, in hypergravity rectifying column, nitrogen is passed through.
Thermometer is provided with preferred first pipeline.
Surge tank is provided between the condensator outlet and collecting tank entrance preferably, nitrogen in surge tank, is passed through.
Pressure gauge is provided with preferred 5th pipeline.
Preferred reflux pump upper end pipeline is provided with outlet.
The recovery system of the Herba Rosmarini Officinalis extract Extraction solvent of the present invention can substitute traditional old-fashioned distillation system, layout
It is new reasonable efficiently to greatly increase Extraction solvent organic efficiency, reducing energy consumption, energy-saving and emission-reduction.
Description of the drawings
Fig. 1 is schematic diagram of the present invention.
Specific embodiment
The present invention is described in further details below by embodiment, embodiment is only used for illustrating the present invention, does not limit
The scope of the present invention processed.
A kind of such as recovery systems of Herba Rosmarini Officinalis extract Extraction solvent of Fig. 1, including reboiler 1, reboiler 1 is using energy source capsule
2 heat supplies, are electric energy or gas heating, and 1 bottom of reboiler is provided with drain pipe 3, and 1 gas outlet of the reboiler passes through the first pipeline 5
It is connected with 7 air inlet of hypergravity rectifying column, 1 gas outlet of reboiler is located at 1 top of reboiler, feed pipe 18 and hypergravity rectifying column
Connect in the middle part of 7 sides, 7 liquid outlet of hypergravity rectifying column is connected with 1 inlet of reboiler by second pipe 4, hypergravity rectifying column 7
Liquid outlet is located at 7 bottom of hypergravity rectifying column, and 1 inlet of reboiler is located at 1 lower end of reboiler, 7 gas outlet of hypergravity rectifying column
It is connected with 9 import of condenser by the 3rd pipeline 8,7 gas outlet of hypergravity rectifying column is located at 7 top of hypergravity rectifying column, condensation
The outlet of device 9 is connected with 11 entrance of collecting tank by the 4th pipeline 25, and collecting tank 11 is exported and is connected with reflux pump 13, and reflux pump 13 leads to
Cross the 5th pipeline 12 to be connected with hypergravity rectifying column inlet 26,18 one end of feed pipe is connected with preheater 19, to carrying out
Preheating, improves the efficiency of hypergravity rectifying column 7, and preheater 19 is connected with filter 21, and filter 21 is connected with storage tank 22, storage
First flowmeter 20 is provided between batch can 22 and filter 21, second flowmeter 17 is provided with the 3rd pipeline 8, further detection control
Flow in tubing giving sufficient strength, is provided with temperature sensor 16, the connection controller 23 of temperature sensor 16, controller in hypergravity rectifying column 7
23 connection stirring motors 24, can interrupt stirring electricity by controller in time when temperature exceedes setting value in hypergravity rectifying column
Machine 24 is moved, and is passed through nitrogen and ensures there is antioxygenic property in rectifying column 7 in hypergravity rectifying column 7, raising rectification efficiency, and first
Thermometer 6 is provided with pipeline 5, gas temperature is monitored, condenser 9 is exported and surge tank 10 is provided with and 11 entrance of collecting tank between, delay
The pressure oscillation that tank 10 is mainly used in buffer system in various systems is rushed, nitrogen is passed through and system oxidation resistance is improved, make
System work is safer steady, is provided with pressure gauge 14, monitoring pressure in real time, it is ensured that production pressure is in qualified in the 5th pipeline 12
State, 13 upper end pipeline of reflux pump are provided with outlet 15, are material outlet.
Extract liquor to be heated to after boiling temperature entering hypergravity rectifying column by pipeline into preheater by pipeline
It is interior, by the reverse and air-flow shearing splitting of the high speed rotation of row into micron to nanometer in baffling runner between rotor and stator
The liquid film of level, brin and drop, so as to greatly enhance the heat transfer between vehicle repair major, mass transport process, make mass-transfer efficiency significantly
Increase, Herba Rosmarini Officinalis extract Extraction solvent is delivered to reboiler tower reactor, described by thermal source（Steam, electricity）By pipeline in tower reactor
Herba Rosmarini Officinalis extract Extraction solvent carry out being heated to Extraction solvent boiling point, carried out into hypergravity rectifying column by pipeline overweight
Vapour-liquid high-speed separation in the field of force, the liquid film brin drop after the separation enter condenser by pipeline（Sheet frame exchanges heat）Carry out cold
Gas-liquid separator separates are entered after solidifying, the quality of recycling design after the separation, can be detected by sample valve, the finished product leads to
Condenser cooling is crossed, collecting tank is delivered to by pump, the below standard solvent goes successively to hypergravity by pipeline by reflux pump
Rectification is carried out in rectifying column, the process control back-flow velocity, temperature, concentration change, the waste liquid Jing after system is reclaimed pass through tower
Waste discharge after kettle heat exchange.
The common structure that the structure that the present invention is not pointed out should be known for those skilled in the art, what the present invention was not pointed out
The conventional connected mode that connected mode should be known for those skilled in the art.
The above, is only presently preferred embodiments of the present invention, is not the restriction for making other forms to the present invention, is appointed
What those skilled in the art possibly also with the disclosure above technology contents changed or be modified as equivalent variations etc.
Effect embodiment.But it is every without departing from technical solution of the present invention content, according to the technical spirit of the present invention to above example institute
Any simple modification, equivalent variations and the remodeling made, still falls within the protection domain of technical solution of the present invention.
Claims (8)
1. a kind of recovery system of Herba Rosmarini Officinalis extract Extraction solvent, including reboiler（1）, it is characterised in that：The reboiler
（1）Gas outlet passes through the first pipeline（5）With hypergravity rectifying column（7）Air inlet is connected, feed pipe（18）With hypergravity rectifying column
（7）Even, hypergravity rectifying column（7）Liquid outlet passes through second pipe（4）With reboiler（1）Inlet is connected, hypergravity rectifying column
（7）Gas outlet passes through the 3rd pipeline（8）With condenser（9）Import is connected, condenser（9）Outlet is by the 4th pipeline（25）With receipts
Collection groove（11）Entrance is connected, collecting tank（11）Outlet and reflux pump（13）It is connected, reflux pump（13）By the 5th pipeline（12）With
Hypergravity rectifying column inlet（26）Connection.
2. the recovery system of Herba Rosmarini Officinalis extract Extraction solvent according to claim 1, it is characterised in that：The feed pipe
（18）One end and preheater（19）It is connected, preheater（19）With filter（21）It is connected, filter（21）With storage tank（22）Phase
Even, storage tank（22）And filter（21）Between be provided with first flowmeter（20）.
3. the recovery system of Herba Rosmarini Officinalis extract Extraction solvent according to claim 1, it is characterised in that：3rd pipe
Road（8）Second flowmeter is provided with inside（17）.
4. the recovery system of Herba Rosmarini Officinalis extract Extraction solvent according to claim 1, it is characterised in that：The hypergravity
Rectifying column（7）Temperature sensor is provided with inside（16）, temperature sensor（16）Connection controller（23）, controller（23）Connection stirring
Motor（24）, hypergravity rectifying column（7）Nitrogen is passed through inside.
5. the recovery system of Herba Rosmarini Officinalis extract Extraction solvent according to claim 1, it is characterised in that：The first pipe
Road（5）Thermometer is provided with inside（6）.
6. the recovery system of Herba Rosmarini Officinalis extract Extraction solvent according to claim 1, it is characterised in that：The condenser
（9）Outlet and collecting tank（11）Surge tank is provided between entrance（10）, surge tank（10）Nitrogen is passed through inside.
7. the recovery system of Herba Rosmarini Officinalis extract Extraction solvent according to claim 1, it is characterised in that：5th pipe
Road（12）Pressure gauge is provided with inside（14）.
8. the recovery system of Herba Rosmarini Officinalis extract Extraction solvent according to claim 1, it is characterised in that：The reflux pump
（13）Upper end pipeline is provided with outlet（15）.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201710064086.8A CN106552439A (en) | 2017-02-04 | 2017-02-04 | A kind of recovery system of Herba Rosmarini Officinalis extract Extraction solvent |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201710064086.8A CN106552439A (en) | 2017-02-04 | 2017-02-04 | A kind of recovery system of Herba Rosmarini Officinalis extract Extraction solvent |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| CN106552439A true CN106552439A (en) | 2017-04-05 |
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ID=58445664
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN201710064086.8A Pending CN106552439A (en) | 2017-02-04 | 2017-02-04 | A kind of recovery system of Herba Rosmarini Officinalis extract Extraction solvent |
Country Status (1)
| Country | Link |
|---|---|
| CN (1) | CN106552439A (en) |
Cited By (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN108410566A (en) * | 2017-11-20 | 2018-08-17 | 杭州创屹机电科技有限公司 | A kind of camellia oil production method of low trans fatty acid content |
| CN111905404A (en) * | 2020-09-02 | 2020-11-10 | 上海复旦复华药业有限公司 | Method for removing residual ethanol from tripterygium wilfordii alcohol extraction residues |
| CN115777981A (en) * | 2022-11-08 | 2023-03-14 | 湖北中烟工业有限责任公司 | Production method and device of reconstituted tobacco raw material extracting solution |
Citations (5)
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|---|---|---|---|---|
| JPH0631107A (en) * | 1992-07-14 | 1994-02-08 | Juki Corp | Solvent extraction/solvent recovery apparatus |
| CN203220773U (en) * | 2013-04-15 | 2013-10-02 | 襄阳楚天源化工有限公司 | Methanol distillation equipment |
| CN103394210A (en) * | 2013-08-12 | 2013-11-20 | 北京化工大学 | Supergravity device for reduced pressure distillation and application method |
| CN203989931U (en) * | 2014-07-11 | 2014-12-10 | 江苏华泰重工装备有限公司 | High-efficient energy-saving alcohol recovery tower |
| CN206444221U (en) * | 2017-02-04 | 2017-08-29 | 河南佳尚农业科技发展有限公司 | A kind of recovery system of Rosmarinus officinalis extract Extraction solvent |
-
2017
- 2017-02-04 CN CN201710064086.8A patent/CN106552439A/en active Pending
Patent Citations (5)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| JPH0631107A (en) * | 1992-07-14 | 1994-02-08 | Juki Corp | Solvent extraction/solvent recovery apparatus |
| CN203220773U (en) * | 2013-04-15 | 2013-10-02 | 襄阳楚天源化工有限公司 | Methanol distillation equipment |
| CN103394210A (en) * | 2013-08-12 | 2013-11-20 | 北京化工大学 | Supergravity device for reduced pressure distillation and application method |
| CN203989931U (en) * | 2014-07-11 | 2014-12-10 | 江苏华泰重工装备有限公司 | High-efficient energy-saving alcohol recovery tower |
| CN206444221U (en) * | 2017-02-04 | 2017-08-29 | 河南佳尚农业科技发展有限公司 | A kind of recovery system of Rosmarinus officinalis extract Extraction solvent |
Non-Patent Citations (1)
| Title |
|---|
| 刘有智: "《超重力化工过程与技术》", 31 January 2009 * |
Cited By (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN108410566A (en) * | 2017-11-20 | 2018-08-17 | 杭州创屹机电科技有限公司 | A kind of camellia oil production method of low trans fatty acid content |
| CN111905404A (en) * | 2020-09-02 | 2020-11-10 | 上海复旦复华药业有限公司 | Method for removing residual ethanol from tripterygium wilfordii alcohol extraction residues |
| CN115777981A (en) * | 2022-11-08 | 2023-03-14 | 湖北中烟工业有限责任公司 | Production method and device of reconstituted tobacco raw material extracting solution |
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| RJ01 | Rejection of invention patent application after publication |
Application publication date: 20170405 |
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| RJ01 | Rejection of invention patent application after publication |