CN106521938A - Glossy polishing treating agent for synthetic leather and preparation method thereof - Google Patents

Glossy polishing treating agent for synthetic leather and preparation method thereof Download PDF

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Publication number
CN106521938A
CN106521938A CN201610963455.2A CN201610963455A CN106521938A CN 106521938 A CN106521938 A CN 106521938A CN 201610963455 A CN201610963455 A CN 201610963455A CN 106521938 A CN106521938 A CN 106521938A
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CN
China
Prior art keywords
mass parts
oil
synthetic leather
nitrocotton
polishing agent
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Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Pending
Application number
CN201610963455.2A
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Chinese (zh)
Inventor
陈勇刚
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Jiangsu Baoze Polymer Materials Co Ltd
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Jiangsu Baoze Polymer Materials Co Ltd
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Publication date
Application filed by Jiangsu Baoze Polymer Materials Co Ltd filed Critical Jiangsu Baoze Polymer Materials Co Ltd
Priority to CN201610963455.2A priority Critical patent/CN106521938A/en
Publication of CN106521938A publication Critical patent/CN106521938A/en
Pending legal-status Critical Current

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Classifications

    • D—TEXTILES; PAPER
    • D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
    • D06M—TREATMENT, NOT PROVIDED FOR ELSEWHERE IN CLASS D06, OF FIBRES, THREADS, YARNS, FABRICS, FEATHERS OR FIBROUS GOODS MADE FROM SUCH MATERIALS
    • D06M13/00—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with non-macromolecular organic compounds; Such treatment combined with mechanical treatment
    • D06M13/10—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with non-macromolecular organic compounds; Such treatment combined with mechanical treatment with compounds containing oxygen
    • D06M13/224—Esters of carboxylic acids; Esters of carbonic acid
    • D—TEXTILES; PAPER
    • D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
    • D06M—TREATMENT, NOT PROVIDED FOR ELSEWHERE IN CLASS D06, OF FIBRES, THREADS, YARNS, FABRICS, FEATHERS OR FIBROUS GOODS MADE FROM SUCH MATERIALS
    • D06M11/00—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with inorganic substances or complexes thereof; Such treatment combined with mechanical treatment, e.g. mercerising
    • D06M11/77—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with inorganic substances or complexes thereof; Such treatment combined with mechanical treatment, e.g. mercerising with silicon or compounds thereof
    • D06M11/79—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with inorganic substances or complexes thereof; Such treatment combined with mechanical treatment, e.g. mercerising with silicon or compounds thereof with silicon dioxide, silicic acids or their salts
    • D—TEXTILES; PAPER
    • D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
    • D06M—TREATMENT, NOT PROVIDED FOR ELSEWHERE IN CLASS D06, OF FIBRES, THREADS, YARNS, FABRICS, FEATHERS OR FIBROUS GOODS MADE FROM SUCH MATERIALS
    • D06M13/00—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with non-macromolecular organic compounds; Such treatment combined with mechanical treatment
    • D06M13/10—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with non-macromolecular organic compounds; Such treatment combined with mechanical treatment with compounds containing oxygen
    • D06M13/165—Ethers
    • D—TEXTILES; PAPER
    • D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
    • D06M—TREATMENT, NOT PROVIDED FOR ELSEWHERE IN CLASS D06, OF FIBRES, THREADS, YARNS, FABRICS, FEATHERS OR FIBROUS GOODS MADE FROM SUCH MATERIALS
    • D06M15/00—Treating fibres, threads, yarns, fabrics, or fibrous goods made from such materials, with macromolecular compounds; Such treatment combined with mechanical treatment
    • D06M15/01—Treating fibres, threads, yarns, fabrics, or fibrous goods made from such materials, with macromolecular compounds; Such treatment combined with mechanical treatment with natural macromolecular compounds or derivatives thereof
    • D06M15/03—Polysaccharides or derivatives thereof
    • D06M15/05—Cellulose or derivatives thereof
    • D06M15/07—Cellulose esters
    • D—TEXTILES; PAPER
    • D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
    • D06M—TREATMENT, NOT PROVIDED FOR ELSEWHERE IN CLASS D06, OF FIBRES, THREADS, YARNS, FABRICS, FEATHERS OR FIBROUS GOODS MADE FROM SUCH MATERIALS
    • D06M15/00—Treating fibres, threads, yarns, fabrics, or fibrous goods made from such materials, with macromolecular compounds; Such treatment combined with mechanical treatment
    • D06M15/19—Treating fibres, threads, yarns, fabrics, or fibrous goods made from such materials, with macromolecular compounds; Such treatment combined with mechanical treatment with synthetic macromolecular compounds
    • D06M15/37—Macromolecular compounds obtained otherwise than by reactions only involving carbon-to-carbon unsaturated bonds
    • D06M15/643—Macromolecular compounds obtained otherwise than by reactions only involving carbon-to-carbon unsaturated bonds containing silicon in the main chain
    • D—TEXTILES; PAPER
    • D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
    • D06M—TREATMENT, NOT PROVIDED FOR ELSEWHERE IN CLASS D06, OF FIBRES, THREADS, YARNS, FABRICS, FEATHERS OR FIBROUS GOODS MADE FROM SUCH MATERIALS
    • D06M2200/00—Functionality of the treatment composition and/or properties imparted to the textile material
    • D06M2200/50—Modified hand or grip properties; Softening compositions

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  • Engineering & Computer Science (AREA)
  • Textile Engineering (AREA)
  • Chemical & Material Sciences (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Treatment And Processing Of Natural Fur Or Leather (AREA)

Abstract

The invention relates to a glossy polishing treating agent for synthetic leather and a preparation method thereof. The glossy polishing treating agent for the synthetic leather is prepared from the following components: nitrocotton, butyl ether, ethyl ester, butyl ester, silicon dioxide matting powder, epoxidized soybean oil, methyl phenyl silicone oil and a dispersing agent. The components of the glossy polishing treating agent for the synthetic leather provided by the invention are coordinated mutually and acted jointly, a polished leather surface is high in layered sense and unique in hand feeling, and the leather treated through the treating agent is natural in gloss, and clear in color and lustre, and a leather surface is better in brilliance and crystalistic sense, cannot lose gloss through water kneading after being polished, and is excellent in comprehensive effect.

Description

A kind of use for synthetic leather oil polishing agent and preparation method thereof thoroughly
Technical field
The present invention relates to a kind of use for synthetic leather oil polishing agent thoroughly, is more particularly to applied to the conjunction of synthetic leather rear section technique Finished leather oil polishing agent thoroughly, while the invention also discloses the preparation method of the saturating polishing agent of use for synthetic leather oil.
Background technology
At present, leather surface stereovision after the saturating polishing agent polishing of existing use for synthetic leather oil, feel be not very good.Should With the synthetic leather of the saturating polishing agent of such oil, its gloss and color and luster are poor, and leather surface is gorgeous to spend, polishing after water poor with crystalistic sense Rub pool of being exposed to light accidentally.Accordingly, it would be desirable to a kind of improved oil polishing agent thoroughly.
The content of the invention
It is an object of the invention to provide a kind of use for synthetic leather oil polishing agent thoroughly.
Polishing agent is achieved through the following technical solutions the use for synthetic leather oil of the present invention thoroughly：
Use for synthetic leather oil polishing agent thoroughly disclosed in this invention, comprising following components：Nitrocotton, butyl ether, ethyl ester, fourth Ester, silicon dioxide flatting silica, epoxy soybean oil, methyl phenyl silicone oil and dispersant.
On the basis of the gross weight of resin, the proportioning of each component of the saturating polishing agent of use for synthetic leather oil that the present invention is provided Can be：20～22 mass parts of nitrocotton, 15～17 mass parts of butyl ether, 30～32 mass parts of ethyl ester, 15～17 mass parts of butyl ester, 4～6 mass parts of silicon dioxide flatting silica, 6～8 mass parts of epoxy soybean oil, 1～2 mass parts of methyl phenyl silicone oil, dispersant 0 ～1 mass parts.
In one embodiment of the invention, the proportioning of each component of the saturating polishing agent of use for synthetic leather oil is as follows：Nitrification 20 mass parts of cotton, 15 mass parts of butyl ether, 32 mass parts of ethyl ester, 17 mass parts of butyl ester, 6 mass parts of silicon dioxide flatting silica, epoxy 8 mass parts of soybean oil, 2 mass parts of methyl phenyl silicone oil, 0 mass parts of dispersant.
In another embodiment of the invention, the proportioning of each component of the saturating polishing agent of use for synthetic leather oil is as follows：Nitrification 22 mass parts of cotton, 17 mass parts of butyl ether, 30 mass parts of ethyl ester, 15 mass parts of butyl ester, 5 mass parts of silicon dioxide flatting silica, epoxy 8 mass parts of soybean oil, 2 mass parts of methyl phenyl silicone oil, 1 mass parts of dispersant.
In another embodiment of the invention, the proportioning of each component of the saturating polishing agent of use for synthetic leather oil is as follows：Nitrification 21 mass parts of cotton, 17 mass parts of butyl ether, 31 mass parts of ethyl ester, 17 mass parts of butyl ester, 5 mass parts of silicon dioxide flatting silica, epoxy 7 mass parts of soybean oil, 1 mass parts of methyl phenyl silicone oil, 1 mass parts of dispersant.
The present invention also provides a kind of preparation method of the saturating polishing agent of use for synthetic leather oil, comprises the steps of：
1) by a part of nitrocotton in formula, butyl ether, a part of ethyl ester, a part of butyl ester, silicon dioxide flatting silica, ring Grinding after the stirring of oxygen soybean oil, methyl phenyl silicone oil and dispersant is filtered；
2) in step 1) another part nitrocotton, another part ethyl ester, another part butyl ester are added in the mixture that obtains, Uniform stirring.
The proportioning of each component in the preparation method of the saturating polishing agent of use for synthetic leather oil of the present invention can be as follows：Nitrification 20～22 mass parts of cotton, 15～17 mass parts of butyl ether, 30～32 mass parts of ethyl ester, 15～17 mass parts of butyl ester, silicon dioxide disappear 4～6 mass parts of light powder, 6～8 mass parts of epoxy soybean oil, 1～2 mass parts of methyl phenyl silicone oil, 0～1 mass parts of dispersant.
Preferably, the proportioning of each component is as follows：20 mass parts of nitrocotton, 15 mass parts of butyl ether, 32 mass parts of ethyl ester, butyl ester 17 mass parts, 6 mass parts of silicon dioxide flatting silica, 8 mass parts of epoxy soybean oil, 2 mass parts of methyl phenyl silicone oil, dispersant 0 Mass parts.
It is highly preferred that the proportioning of each component is as follows：22 mass parts of nitrocotton, 17 mass parts of butyl ether, 30 mass parts of ethyl ester, fourth 15 mass parts of ester, 5 mass parts of silicon dioxide flatting silica, 8 mass parts of epoxy soybean oil, 2 mass parts of methyl phenyl silicone oil, dispersant 1 mass parts.
It is highly preferred that the proportioning of each component is as follows：21 mass parts of nitrocotton, 17 mass parts of butyl ether, 31 mass parts of ethyl ester, fourth 17 mass parts of ester, 5 mass parts of silicon dioxide flatting silica, 7 mass parts of epoxy soybean oil, 1 mass parts of methyl phenyl silicone oil, dispersant 1 mass parts.
As using above technical scheme, the present invention is had the advantage that compared with prior art：
1. each component of use for synthetic leather of the present invention oil polishing agent thoroughly is mutually coordinated, collective effect, after polishing Leather surface stereovision is strong, and feel is unique, the leather gloss nature made with this kind of inorganic agent, color clarification, the gorgeous degree of leather surface and crystalistic sense Good, after polishing, water is rubbed, and resultant effect is excellent；
2. on existing synthetic leather production line apply thoroughly by polishing agent for use for synthetic leather oil of the present invention, technique letter It is single, it is a kind of new material of back segment process, need not change production equipment increases cost；
3. the preparation method of the saturating polishing agent of use for synthetic leather oil of the present invention is simple, need not adopt complicated machinery Process, saved production cost, be suitable to industrialized production.
Specific embodiment
Below by embodiment, technical solution of the present invention is described in detail, but protection scope of the present invention not office It is limited to the embodiment.
Embodiment 1
Thoroughly polishing agent includes 20 mass parts nitrocottons to use for synthetic leather oil, 15 mass parts butyl ether, 32 mass parts ethyl esters, and 17 Mass parts butyl ester, 6 mass parts silicon dioxide flatting silicas, 8 mass parts epoxy soybean oils, 2 mass parts methyl phenyl silicone oils, 0 mass Part dispersant.
The preparation method of above-mentioned use for synthetic leather oil polishing agent thoroughly is：By 10 mass parts nitrocottons in formula, 15 matter Amount part butyl ether, 20 mass parts ethyl esters, 10 mass parts butyl esters, 6 mass parts silicon dioxide flatting silicas, 8 mass parts epoxy soybean oils, 2 Mass parts methyl phenyl silicone oil, grinding after the stirring of 0 mass parts dispersant are filtered；Then 10 mass are added in the mixture of gained Part nitrocotton, 12 mass parts ethyl esters and 7 mass parts butyl esters, obtain final product described use for synthetic leather oil polishing thoroughly after uniform stirring Agent.The performance indications of the resulting saturating polishing agent of use for synthetic leather oil are shown in Table 1.
The methods such as stirring, grinding, filtration employed in above-mentioned preparation process are customary way in the art.
Embodiment 2
Thoroughly polishing agent includes 22 mass parts nitrocottons to use for synthetic leather oil, 17 mass parts butyl ether, 30 mass parts ethyl esters, and 15 Mass parts butyl ester, 5 mass parts silicon dioxide flatting silicas, 8 mass parts epoxy soybean oils, 2 mass parts methyl phenyl silicone oils, 1 mass Part dispersant.
The preparation method of above-mentioned use for synthetic leather oil polishing agent thoroughly is：By 10 mass parts nitrocottons in formula, 17 matter Amount part butyl ether, 20 mass parts ethyl esters, 10 mass parts butyl esters, 5 mass parts silicon dioxide flatting silicas, 8 mass parts epoxy soybean oils, 2 Mass parts methyl phenyl silicone oil, grinding after the stirring of 1 mass parts dispersant are filtered；Then 12 mass are added in the mixture of gained Part nitrocotton, 10 mass parts ethyl esters and 5 mass parts butyl esters, obtain final product described use for synthetic leather oil polishing thoroughly after uniform stirring Agent.The performance indications of the resulting saturating polishing agent of use for synthetic leather oil are shown in Table 1.
The methods such as stirring, grinding, filtration employed in above-mentioned preparation process are customary way in the art.
Embodiment 3
Thoroughly polishing agent includes 21 mass parts nitrocottons to use for synthetic leather oil, 17 mass parts butyl ether, 31 mass parts ethyl esters, and 17 Mass parts butyl ester, 5 mass parts silicon dioxide flatting silicas, 7 mass parts epoxy soybean oils, 1 mass parts methyl phenyl silicone oil, 1 mass Part dispersant.
The preparation method of above-mentioned use for synthetic leather oil polishing agent thoroughly is：By 10 mass parts nitrocottons in formula, 17 matter Amount part butyl ether, 20 mass parts ethyl esters, 10 mass parts butyl esters, 5 mass parts silicon dioxide flatting silicas, 7 mass parts epoxy soybean oils, 1 Mass parts methyl phenyl silicone oil, grinding after the stirring of 1 mass parts dispersant are filtered；Then 11 mass are added in the mixture of gained Part nitrocotton, 11 mass parts ethyl esters and 7 mass parts butyl esters, obtain final product described use for synthetic leather oil polishing thoroughly after uniform stirring Agent.The performance indications of the resulting saturating polishing agent of use for synthetic leather oil are shown in Table 1.
The methods such as stirring, grinding, filtration employed in above-mentioned preparation process are customary way in the art.
Table 1
Embodiment 1 Embodiment 2 Embodiment 3
PH value 5 7 6
Outward appearance Micro- yellow thick liquid Micro- yellow thick liquid Micro- yellow thick liquid
Viscosity (cps/25 DEG C) 100 400 250
Stability Without precipitation Without precipitation Without precipitation
Dicyandiamide solution Ethyl ester, butyl ester Ethyl ester, butyl ester Ethyl ester, butyl ester
Solid content (%) 19 21 20
The foregoing is only presently preferred embodiments of the present invention, not for limit the present invention practical range；If do not taken off From the spirit and scope of the present invention, the present invention is modified or equivalent, all should be covered in the claims in the present invention In the middle of protection domain.

Claims (10)

1. a kind of use for synthetic leather oil polishing agent thoroughly, it is characterised in that comprising following components：Nitrocotton, butyl ether, ethyl ester, fourth Ester, silicon dioxide flatting silica, epoxy soybean oil, methyl phenyl silicone oil and dispersant.
2. use for synthetic leather according to claim 1 oil polishing agent thoroughly, it is characterised in that each component with such as Under：20～22 mass parts of nitrocotton, 15～17 mass parts of butyl ether, 30～32 mass parts of ethyl ester, 15～17 mass parts of butyl ester, dioxy 4～6 mass parts of SiClx flatting silica, 6～8 mass parts of epoxy soybean oil, 1～2 mass parts of methyl phenyl silicone oil, 0～1 matter of dispersant Amount part.
3. use for synthetic leather according to claim 2 oil polishing agent thoroughly, it is characterised in that each component with such as Under：20 mass parts of nitrocotton, 15 mass parts of butyl ether, 32 mass parts of ethyl ester, 17 mass parts of butyl ester, 6 mass of silicon dioxide flatting silica Part, 8 mass parts of epoxy soybean oil, 2 mass parts of methyl phenyl silicone oil, 0 mass parts of dispersant.
4. use for synthetic leather according to claim 2 oil polishing agent thoroughly, it is characterised in that each component with such as Under：22 mass parts of nitrocotton, 17 mass parts of butyl ether, 30 mass parts of ethyl ester, 15 mass parts of butyl ester, 5 mass of silicon dioxide flatting silica Part, 8 mass parts of epoxy soybean oil, 2 mass parts of methyl phenyl silicone oil, 1 mass parts of dispersant.
5. use for synthetic leather according to claim 2 oil polishing agent thoroughly, it is characterised in that each component with such as Under：21 mass parts of nitrocotton, 17 mass parts of butyl ether, 31 mass parts of ethyl ester, 17 mass parts of butyl ester, 5 mass of silicon dioxide flatting silica Part, 7 mass parts of epoxy soybean oil, 1 mass parts of methyl phenyl silicone oil, 1 mass parts of dispersant.
6. the preparation method of the oily polishing agent thoroughly of use for synthetic leather described in claim 1, it is characterised in that comprising following step Suddenly：
1) will be a part of nitrocotton in formula, butyl ether, a part of ethyl ester, a part of butyl ester, silicon dioxide flatting silica, epoxy big Grinding after the stirring of Oleum Glycines, methyl phenyl silicone oil and dispersant is filtered；
2) in step 1) another part nitrocotton, another part ethyl ester, another part butyl ester are added in the mixture that obtains, uniformly Stirring.
7. the preparation method of use for synthetic leather according to claim 6 oil polishing agent thoroughly, it is characterised in that each component Proportioning is as follows：20～22 mass parts of nitrocotton, 15～17 mass parts of butyl ether, 30～32 mass parts of ethyl ester, 15～17 mass of butyl ester Part, 4～6 mass parts of silicon dioxide flatting silica, 6～8 mass parts of epoxy soybean oil, 1～2 mass parts of methyl phenyl silicone oil, dispersion 0～1 mass parts of agent.
8. the preparation method of use for synthetic leather according to claim 7 oil polishing agent thoroughly, it is characterised in that each component Proportioning is as follows：20 mass parts of nitrocotton, 15 mass parts of butyl ether, 32 mass parts of ethyl ester, 17 mass parts of butyl ester, silicon dioxide flatting silica 6 mass parts, 8 mass parts of epoxy soybean oil, 2 mass parts of methyl phenyl silicone oil, 0 mass parts of dispersant.
9. the preparation method of use for synthetic leather according to claim 7 oil polishing agent thoroughly, it is characterised in that each component Proportioning is as follows：22 mass parts of nitrocotton, 17 mass parts of butyl ether, 30 mass parts of ethyl ester, 15 mass parts of butyl ester, silicon dioxide flatting silica 5 mass parts, 8 mass parts of epoxy soybean oil, 2 mass parts of methyl phenyl silicone oil, 1 mass parts of dispersant.
10. the preparation method of use for synthetic leather according to claim 7 oil polishing agent thoroughly, it is characterised in that each component Proportioning it is as follows：21 mass parts of nitrocotton, 17 mass parts of butyl ether, 31 mass parts of ethyl ester, 17 mass parts of butyl ester, silicon dioxide delustring 5 mass parts of powder, 7 mass parts of epoxy soybean oil, 1 mass parts of methyl phenyl silicone oil, 1 mass parts of dispersant.
CN201610963455.2A 2016-10-28 2016-10-28 Glossy polishing treating agent for synthetic leather and preparation method thereof Pending CN106521938A (en)

Priority Applications (1)

Application Number Priority Date Filing Date Title
CN201610963455.2A CN106521938A (en) 2016-10-28 2016-10-28 Glossy polishing treating agent for synthetic leather and preparation method thereof

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Application Number Priority Date Filing Date Title
CN201610963455.2A CN106521938A (en) 2016-10-28 2016-10-28 Glossy polishing treating agent for synthetic leather and preparation method thereof

Publications (1)

Publication Number Publication Date
CN106521938A true CN106521938A (en) 2017-03-22

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Citations (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN105200774A (en) * 2015-11-10 2015-12-30 江苏宝泽高分子材料股份有限公司 Oil-wax polishing treatment agent for synthetic leather and preparation method thereof

Patent Citations (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN105200774A (en) * 2015-11-10 2015-12-30 江苏宝泽高分子材料股份有限公司 Oil-wax polishing treatment agent for synthetic leather and preparation method thereof

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Application publication date: 20170322