CN106521155B - A kind of anti-block apparatus for titanium sponge distillation passageway - Google Patents

A kind of anti-block apparatus for titanium sponge distillation passageway Download PDF

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Publication number
CN106521155B
CN106521155B CN201611196332.7A CN201611196332A CN106521155B CN 106521155 B CN106521155 B CN 106521155B CN 201611196332 A CN201611196332 A CN 201611196332A CN 106521155 B CN106521155 B CN 106521155B
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China
Prior art keywords
passageway
tube
titanium alloy
vertical tube
block apparatus
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CN201611196332.7A
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Chinese (zh)
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CN106521155A (en
Inventor
穆贤明
郭有刚
李金泽
李斗良
罗建平
梁强
李刚
田维梅
陈强
岑春铁
盛远禄
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Zunyi Titanium Industry Co Ltd
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Zunyi Titanium Industry Co Ltd
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    • CCHEMISTRY; METALLURGY
    • C22METALLURGY; FERROUS OR NON-FERROUS ALLOYS; TREATMENT OF ALLOYS OR NON-FERROUS METALS
    • C22BPRODUCTION AND REFINING OF METALS; PRETREATMENT OF RAW MATERIALS
    • C22B5/00General methods of reducing to metals
    • C22B5/02Dry methods smelting of sulfides or formation of mattes
    • C22B5/04Dry methods smelting of sulfides or formation of mattes by aluminium, other metals or silicon
    • CCHEMISTRY; METALLURGY
    • C22METALLURGY; FERROUS OR NON-FERROUS ALLOYS; TREATMENT OF ALLOYS OR NON-FERROUS METALS
    • C22BPRODUCTION AND REFINING OF METALS; PRETREATMENT OF RAW MATERIALS
    • C22B34/00Obtaining refractory metals
    • C22B34/10Obtaining titanium, zirconium or hafnium
    • C22B34/12Obtaining titanium or titanium compounds from ores or scrap by metallurgical processing; preparation of titanium compounds from other titanium compounds see C01G23/00 - C01G23/08

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  • Engineering & Computer Science (AREA)
  • Chemical & Material Sciences (AREA)
  • Metallurgy (AREA)
  • Manufacturing & Machinery (AREA)
  • Materials Engineering (AREA)
  • Mechanical Engineering (AREA)
  • Organic Chemistry (AREA)
  • Geology (AREA)
  • General Life Sciences & Earth Sciences (AREA)
  • Environmental & Geological Engineering (AREA)
  • Life Sciences & Earth Sciences (AREA)
  • Manufacture And Refinement Of Metals (AREA)
  • Vaporization, Distillation, Condensation, Sublimation, And Cold Traps (AREA)

Abstract

The invention discloses a kind of anti-block apparatus for titanium sponge distillation passageway, the passageway vertical tube mainly set by condenser and thereon forms, the lower end of passageway vertical tube is bell-mouth structure of air, titanium alloy tube is equipped with the vertical tube of passageway, the lower end of titanium alloy tube is equipped with titanium alloy nozzle, top flange and connection flexible pipe of the upper end of titanium alloy tube through passageway vertical tube, the other end connection pneumatic high vacuum flapper valve of hose, pneumatic high vacuum flapper valve is connected with tunger tube, valve is equipped with tunger tube, the continuity of distillation process can be realized using the present apparatus, it is not required to dismantle pipe-dredging repeatedly, greatly reduce hand labor intensity, shorten distillation time, reduce energy consumption, improve product quality.

Description

A kind of anti-block apparatus for titanium sponge distillation passageway
Technical field
It is more particularly to a kind of for the anti-blocking of titanium sponge distillation passageway the present invention relates to titanium sponge production equipment technical field Device.
Background technology
During existing magnesium reduction produces titanium sponge, vacuum distillation process is master operation in titanium sponge production, Technology content is higher, complex production process, and process time length, external advanced titanium sponge production can ensure that in vacuum distillation Occur without plugging phenomenon.And there is vacuum distillation process plugging for a long time in titanium sponge production for the country(Mainly condenser mistake The horn mouth position of road vertical tube)Often the problem of, though employing the measures such as passageway heating, interior heating, do not obtain thoroughly always Solve, domestic existing enterprise is average per stove siphunculus 5,6 times in distillation process, and average plugging about 2 times, is carrying out siphunculus and plugging During processing, not only labor intensity is big, influences the normal operation and product quality of production, and easily leads to product energy consumption increase, unfavorable In cost control.
The content of the invention
To solve problems of the prior art, invention proposes providing a kind of for the anti-of titanium sponge distillation passageway Block apparatus, the continuity of distillation process can be realized using the present apparatus, be not required to dismantle pipe-dredging repeatedly, greatly reduce artificial labor Fatigue resistance, shortens distillation time, reduces energy consumption, improves product quality.
Technical scheme is as described below:
A kind of anti-block apparatus for titanium sponge distillation passageway, the passageway vertical tube group mainly set by condenser and thereon Into the lower end of passageway vertical tube is bell-mouth structure of air, and titanium alloy tube is equipped with the vertical tube of passageway, and the lower end of titanium alloy tube is closed equipped with titanium Golden nozzle, the upper end of titanium alloy tube pass through the top flange and connection flexible pipe of passageway vertical tube, and the other end connection of hose is pneumatic high Vacuum flapper valve, pneumatic high vacuum flapper valve are connected with tunger tube, and valve is equipped with tunger tube.
The anti-block apparatus is connected with automatic control system, it can be achieved that automatically controlling argon filling operation.
In the present invention by rushing argon gas to the horn mouth position self-timing of condenser passageway vertical tube, come reach prevent magnesium and Magnesium chloride puts up a bridge in condensation process and blocked road junction purpose.
The advantages of the present invention mainly have:
The continuity of distillation process can be realized using the present apparatus, is not required to dismantle pipe-dredging repeatedly, is greatly reduced manually Labor intensity, shortens distillation time, reduces energy consumption, improves product quality.
Brief description of the drawings
Fig. 1 is the anti-block apparatus schematic diagram of the present invention;
In figure:1- tunger tubes, 2- valves, 3- pneumatic high vacuums flapper valve, 4- hoses, 5- titanium alloy tubes, the spray of 6- titanium alloys Head, 7- condensers, 8- passageways vertical tube.
Embodiment
The present invention is described in further detail below in conjunction with attached drawing, but not theme of the present invention should not be interpreted as with regard to this Scope is only limitted to following embodiment, without departing from the idea case in the present invention described above, all according to ordinary skill Various modifications, replacement and the change that knowledge and customary means are made, are included within the scope of the present invention.
Embodiment one
As shown in Figure 1, a kind of anti-block apparatus for titanium sponge distillation passageway, mainly set by condenser 7 and thereon Passageway vertical tube 8 forms, and the lower end of passageway vertical tube 8 is bell-mouth structure of air, and titanium alloy tube 5, titanium alloy tube are equipped with vertical tube 8 in passageway 5 lower end is equipped with titanium alloy nozzle 6, and the upper end of titanium alloy tube 5 passes through the top flange and connection flexible pipe 4 of passageway vertical tube 8, soft The other end connection pneumatic high vacuum flapper valve 3 of pipe 4, pneumatic high vacuum flapper valve 3 is connected with tunger tube 1, is set on tunger tube 1 There is valve 2.
The anti-block apparatus is connected with automatic control system, it can be achieved that automatically controlling argon filling operation.

Claims (2)

  1. A kind of 1. anti-block apparatus for titanium sponge distillation passageway, mainly by condenser(7)And the passageway vertical tube set thereon (8) form, the lower end of passageway vertical tube (8) is bell-mouth structure of air, it is characterised in that be equipped with titanium alloy tube in vertical tube (8) in passageway (5), titanium alloy tube(5)Lower end be equipped with titanium alloy nozzle(6), titanium alloy tube(5)Upper end pass through passageway vertical tube (8) top Portion's flange and connection flexible pipe(4), hose(4)The other end connection pneumatic high vacuum flapper valve(3), pneumatic high vacuum flapper valve (3)With tunger tube(1)Connection, in tunger tube(1)It is equipped with valve(2).
  2. 2. a kind of anti-block apparatus for titanium sponge distillation passageway according to claim 1, it is characterised in that described is anti- Block apparatus is connected with automatic control system.
CN201611196332.7A 2016-12-22 2016-12-22 A kind of anti-block apparatus for titanium sponge distillation passageway Active CN106521155B (en)

Priority Applications (1)

Application Number Priority Date Filing Date Title
CN201611196332.7A CN106521155B (en) 2016-12-22 2016-12-22 A kind of anti-block apparatus for titanium sponge distillation passageway

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
CN201611196332.7A CN106521155B (en) 2016-12-22 2016-12-22 A kind of anti-block apparatus for titanium sponge distillation passageway

Publications (2)

Publication Number Publication Date
CN106521155A CN106521155A (en) 2017-03-22
CN106521155B true CN106521155B (en) 2018-05-04

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Families Citing this family (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN110241312A (en) * 2019-07-26 2019-09-17 攀钢集团钛业有限责任公司 Thin blocking method for titanium sponge " I " type retort production process channel
CN110904345A (en) * 2020-01-08 2020-03-24 遵义钛业股份有限公司 Large cover with heat-preservation and heating function for titanium sponge distillation production
CN116607021A (en) * 2022-02-09 2023-08-18 遵义钛业股份有限公司 Low-valence object cleaning and recycling device for titanium in reduction production of titanium sponge

Citations (6)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN2830416Y (en) * 2005-10-11 2006-10-25 遵义钛业股份有限公司 Still pipeline on reactor cover for preparing sponge Ti and heater thereof
JP2010013686A (en) * 2008-07-02 2010-01-21 Osaka Titanium Technologies Co Ltd Method for producing sponge titanium
CN201942731U (en) * 2010-12-31 2011-08-24 遵义钛业股份有限公司 Big cover for producing titanium sponge by distillation
CN205275670U (en) * 2015-11-30 2016-06-01 金川集团股份有限公司 A prevent blockking up upper cover for reactor
CN205329137U (en) * 2015-11-30 2016-06-22 金川集团股份有限公司 Upper cover of reactor for producing titanium sponge
CN206298626U (en) * 2016-12-22 2017-07-04 遵义钛业股份有限公司 A kind of anti-block apparatus that passageway is distilled for titanium sponge

Patent Citations (6)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN2830416Y (en) * 2005-10-11 2006-10-25 遵义钛业股份有限公司 Still pipeline on reactor cover for preparing sponge Ti and heater thereof
JP2010013686A (en) * 2008-07-02 2010-01-21 Osaka Titanium Technologies Co Ltd Method for producing sponge titanium
CN201942731U (en) * 2010-12-31 2011-08-24 遵义钛业股份有限公司 Big cover for producing titanium sponge by distillation
CN205275670U (en) * 2015-11-30 2016-06-01 金川集团股份有限公司 A prevent blockking up upper cover for reactor
CN205329137U (en) * 2015-11-30 2016-06-22 金川集团股份有限公司 Upper cover of reactor for producing titanium sponge
CN206298626U (en) * 2016-12-22 2017-07-04 遵义钛业股份有限公司 A kind of anti-block apparatus that passageway is distilled for titanium sponge

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