CN106511463A - Production process of compound radix salviae miltiorrhizae decoction pieces - Google Patents
Production process of compound radix salviae miltiorrhizae decoction pieces Download PDFInfo
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- CN106511463A CN106511463A CN201611184713.3A CN201611184713A CN106511463A CN 106511463 A CN106511463 A CN 106511463A CN 201611184713 A CN201611184713 A CN 201611184713A CN 106511463 A CN106511463 A CN 106511463A
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- salviae miltiorrhizae
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K36/00—Medicinal preparations of undetermined constitution containing material from algae, lichens, fungi or plants, or derivatives thereof, e.g. traditional herbal medicines
- A61K36/18—Magnoliophyta (angiosperms)
- A61K36/185—Magnoliopsida (dicotyledons)
- A61K36/53—Lamiaceae or Labiatae (Mint family), e.g. thyme, rosemary or lavender
- A61K36/537—Salvia (sage)
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K36/00—Medicinal preparations of undetermined constitution containing material from algae, lichens, fungi or plants, or derivatives thereof, e.g. traditional herbal medicines
- A61K36/06—Fungi, e.g. yeasts
- A61K36/062—Ascomycota
- A61K36/066—Clavicipitaceae
- A61K36/068—Cordyceps
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K9/00—Medicinal preparations characterised by special physical form
- A61K9/20—Pills, tablets, discs, rods
- A61K9/2004—Excipients; Inactive ingredients
- A61K9/2022—Organic macromolecular compounds
- A61K9/205—Polysaccharides, e.g. alginate, gums; Cyclodextrin
- A61K9/2059—Starch, including chemically or physically modified derivatives; Amylose; Amylopectin; Dextrin
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K2236/00—Isolation or extraction methods of medicinal preparations of undetermined constitution containing material from algae, lichens, fungi or plants, or derivatives thereof, e.g. traditional herbal medicine
- A61K2236/10—Preparation or pretreatment of starting material
- A61K2236/13—Preparation or pretreatment of starting material involving cleaning, e.g. washing or peeling
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K2236/00—Isolation or extraction methods of medicinal preparations of undetermined constitution containing material from algae, lichens, fungi or plants, or derivatives thereof, e.g. traditional herbal medicine
- A61K2236/10—Preparation or pretreatment of starting material
- A61K2236/15—Preparation or pretreatment of starting material involving mechanical treatment, e.g. chopping up, cutting or grinding
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K2236/00—Isolation or extraction methods of medicinal preparations of undetermined constitution containing material from algae, lichens, fungi or plants, or derivatives thereof, e.g. traditional herbal medicine
- A61K2236/10—Preparation or pretreatment of starting material
- A61K2236/17—Preparation or pretreatment of starting material involving drying, e.g. sun-drying or wilting
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Abstract
The invention provides a production process of compound radix salviae miltiorrhizae decoction pieces. The compound radix salviae miltiorrhizae decoction pieces are prepared by conducting medicinal material treatment, primary sterilization, sterilizing test, mixing as well as blending and tabletting. By virtue of a way of conducting wall-breaking and crushing on cordyceps militaris and the radix salviae miltiorrhizae, essence of the cordyceps militaris and the radix salviae miltiorrhizae can be released from cell walls, and moreover, in a mode of mutually stirring and mixing the essence, each decoction piece is uniform in content distribution; by conducting ultrasonic cleaning, dirt can be removed without the application of any detergents; in addition, microwave sterilization is adopted as a sterilizing mode, so as to rapidly and effectively kill microorganisms and to protect medicinal components from being damaged; and one tablet (the decoction piece) can achieve double functions, so that the practical value of the tablet is developed to the greatest extent under equal resource conditions.
Description
Technical field
The present invention relates to technical field of traditional Chinese medicine preparation, and in particular to a kind of production technology of compound Salviae Miltiorrhizae decoction pieces.
Background technology
Radix Salviae Miltiorrhizae, the effect of with blood circulation promoting and blood stasis dispelling, inducing menstruation to relieve menalgia, relieving restlessness that clears away heart-fire, cool blood to disappear carbuncle.For obstruction of qi in the chest and cardialgia, gastral cavity abdomen
Hypochondriac pain, the accumulation of abdominal mass abdominal mass, hot numbness pain, dysphoria and insomnia, menoxenia, dysmenorrhea amenorrhea, sore swell and ache curative.
Cordyceps militaris (L.) Link., also referred to as Cordyceps militaris, by Stroma(I.e. careless part, also known as sporophore)With sclerotium(That is the corpse portion of insecticide
Point)Complex dimerous.The pupa of many infection lepidopteran insects.The traditional Chinese medical science thinks that cordycepic acid (Mannitol) enters lung kidney two warp,
Can tonifying the lung it is cloudy, and can kidney-replenishing, cure mainly kidney deficiency, impotence and seminal emission, soreness of waist and knee joint, eak after being ill, chronic cough are weak, phthisical cough expectorant blood,
Spontaneous sweating etc., be it is unique it is a kind of can be while balancing, adjusting the Chinese medicine of negative and positive.
Cardiovascular disease is suffered from as the crowd using Radix Salviae Miltiorrhizae is most, which inevitably results in body during long-term illness
Body function declines so that body produces the yin and yang imbalance of traditional Chinese medical science description, therefore simple reference Radix Salviae Miltiorrhizae is only capable for the treatment of and adjusts the heart
Angiopathy, can not refigure body equilibrium between yin and yang, and in prior art also occur can either treat cardiovascular
Disease can adjust the FUFANG DANSHEN PIAN of equilibrium between yin and yang again, even and if also can not as conventional preparation method is merged
Elite therein is discharged completely, human body is absorbed, and immersion could be by its drug effect for a long time to there are needs
Into analyzing in the solution, it is not convenient to use and absorption, it is therefore desirable to a kind of to realize treating the effect for adjusting, again can
Realization is quickly used and is easy to the decoction pieces for absorbing.
The content of the invention
In view of this, the purpose that the present invention is provided is for the deficiencies in the prior art, there is provided a kind of compound Salviae Miltiorrhizae decoction pieces
Production technology.
To solve above-mentioned technical problem, the technical solution used in the present invention is:
A kind of production technology of compound Salviae Miltiorrhizae decoction pieces, comprises the steps:
A. medical material is processed:Cleaned during ultrasonic cleaner is put into after Radix Salviae Miltiorrhizae Tabellae is selected, then using microwave after cutting
The mode of heating is dried, and carries out high speed breaking cellular wall using breaking cellular wall regulation machine, and obtains Radix Salviae Miltiorrhizae fine powder by 200 mesh sieves;
Cordyceps militaris (L.) Link. is selected to be put in ultrasonic cleaner after mud and is cleaned, drenched dry rear cutting and adopting ultrasonic Wave heating
Mode be dried, being then placed in breaking cellular wall regulation machine carries out high speed breaking cellular wall, and obtains Cordyceps militaris (L.) Link. fine powder by 200 mesh sieves;
B. it is preliminary to sterilize:By Radix Salviae Miltiorrhizae coarse powder and Cordyceps militaris (L.) Link. coarse powder after processing of step A, carried out soon by instantaneous ultrahigh-temperature sterilization machine
Speed sterilizing, is then placed within aseptic interior;
C. sterilizing test:The Radix Salviae Miltiorrhizae fine powder and Cordyceps militaris (L.) Link. fine powder obtained to step B carries out observation 1-3d, and is sampled and tests bacterium,
Downstream is carried out if after qualified, if unqualified, repeat step B;
D. mix:The Radix Salviae Miltiorrhizae fine powder of system and Cordyceps militaris (L.) Link. fine powder are passed through into blender according to 5:1~5:4 mass ratio is carried out fully
Mixing 10-20min, the amylum pregelatinisatum for then adding 0.1 ~ 0.15 times of Radix Salviae Miltiorrhizae coarse powder parts by weight carry out mixing 20-
40min;
E. piece is made in modulation:The mixed material of the acquisition in step D is added into the seasoning that mixed material mass fraction is 0.6-1.2 times
Agent, is made soft material, and makes decoction pieces by comminutor, and dried using microwave applicator, make compound Salviae Miltiorrhizae decoction pieces.
Preferably, the flavoring agent is the xylitol solution that concentration is 0.2% ~ 0.5%.
Preferably, the Radix Salviae Miltiorrhizae fine powder and the addition mass fraction ratio of the Cordyceps militaris (L.) Link. fine powder are 5:2.
Preferably, the sterilizing of 20-30S is carried out by the way of microwave sterilizating in step B.
Preferably, the microwave of 50-70GHz is adopted in step B.
The Radix Salviae Miltiorrhizae for collecting and Cordyceps militaris (L.) Link. are carried out preliminary sorting by the present invention, and remove the dirt for easily removing, then
Cleaned in putting it into ultrasonic washing unit, it is mutual that the sound wave for sending high frequency by ultrasonic washing unit causes hydrone to occur
Vibration, and then the dirt being difficult to clean off on Radix Salviae Miltiorrhizae and Cordyceps militaris (L.) Link. is removed, can carry out the quality for ensureing cleaning is cleaned multiple times, subtract
The phenomenon of few enrichment for thoroughly not caused sand and dust due to cleaning, is cut off after cleaning up, and passes through micro-wave drying, and energy
Enough play a part of primary sterilization, after drying is finished, high-speed stirred breaking cellular wall is directly carried out by breaking cellular wall cooking machine, and then will be thin
The nutrient substance of intracellular is directly discharged from cell wall, so as to be easier to allow absorption of human body, obtains thick after high speed breaking cellular wall
Powder is screened using 200 mesh sieves, so as to by unbroken particle screen selecting out, so as to obtain the fine powder rich in essential ingredient,
Then sterilization treatment is carried out to fine powder, does not then directly use after sterilization, but place it in gnotobasiss, stood
Observe within 1-3 days, be then sampled analysis, so as to obtain the raw material for meeting national microbial standard, then put it into stirring
It is sufficiently stirred in machine, after stirring one end time, is added thereto to amylum pregelatinisatum and proceeds stirring mixing, so as to obtain
The mixed dry material that must be stirred, then adds flavoring agent and makes soft material, and be directly prepared into decoction pieces by comminutor, and adopt
Microwave applicator is dried, and then obtains the product of the present invention.
Cordyceps militaris (L.) Link. and Radix Salviae Miltiorrhizae are carried out the present invention mode of wall breaking pulverization, can not only be by respective elite from cell wall
In discharge, and by way of mutually stirring mixing so that the content distribution of each decoction pieces is uniform, and adopts ultrasound wave
The mode of cleaning can by dirt and without any cleaning agent, and adopt sterilizing also for microwave sterilizating can be rapidly and efficiently kill
Dead microorganism, also avoids active ingredient from being destroyed, and can be capable of achieving double effects by a tablet, in equal resources supplIes
Under played its practical value to greatest extent.
Specific embodiment
To make purpose, technical scheme and the advantage of the embodiment of the present invention clearer, below in conjunction with the embodiment of the present invention,
The technical scheme of the embodiment of the present invention is clearly and completely described.Obviously, described embodiment is of the present invention
Divide embodiment, rather than the embodiment of whole.Based on described embodiments of the invention, those of ordinary skill in the art are obtained
The every other embodiment for obtaining, belongs to the scope of protection of the invention.
Embodiment one
A kind of production technology of compound Salviae Miltiorrhizae decoction pieces, comprises the steps:
A. medical material is processed:Cleaned during ultrasonic cleaner is put into after Radix Salviae Miltiorrhizae Tabellae is selected, then using microwave after cutting
The mode of heating is dried, and carries out high speed breaking cellular wall using breaking cellular wall regulation machine, and obtains Radix Salviae Miltiorrhizae fine powder by 200 mesh sieves;
Cordyceps militaris (L.) Link. is selected to be put in ultrasonic cleaner after mud and is cleaned, drenched dry rear cutting and adopting ultrasonic Wave heating
Mode be dried, being then placed in breaking cellular wall regulation machine carries out high speed breaking cellular wall, and obtains Cordyceps militaris (L.) Link. fine powder by 200 mesh sieves;
B. it is preliminary to sterilize:By Radix Salviae Miltiorrhizae coarse powder and Cordyceps militaris (L.) Link. coarse powder after processing of step A, carried out soon by instantaneous ultrahigh-temperature sterilization machine
Speed sterilizing, is then placed within aseptic interior;
C. sterilizing test:The Radix Salviae Miltiorrhizae fine powder and Cordyceps militaris (L.) Link. fine powder obtained to step B carries out observation 1d, and is sampled and tests bacterium, closes
Downstream is carried out after lattice then;
D. mix:The Radix Salviae Miltiorrhizae fine powder of system and Cordyceps militaris (L.) Link. fine powder are passed through into blender according to 5:1 mass ratio is sufficiently mixed
10min, the amylum pregelatinisatum for then adding 0.1 times of Radix Salviae Miltiorrhizae coarse powder parts by weight carry out mixing 20min;
E. piece is made in modulation:The mixed material of the acquisition in step D is added into the flavoring agent that mixed material mass fraction is 0.6 times,
Soft material is made, and decoction pieces are made by comminutor, and dried using microwave applicator, make compound Salviae Miltiorrhizae decoction pieces.
The flavoring agent is xylitol solution that concentration is 0.2%.
In step B by the way of microwave sterilizating, the sterilizing of 20S is carried out.
The microwave of 50GHz is adopted in step B.
The decoction pieces of the embodiment are in 10 glasss of 300ml and temperature is present on a small quantity to be dissolved into bottom in 50 DEG C of water in 1min
The slightly cloudy solution of deposition, and mouthfeel is gently beneficial to absorption.
Embodiment two
A kind of production technology of compound Salviae Miltiorrhizae decoction pieces, comprises the steps:
A. medical material is processed:Cleaned during ultrasonic cleaner is put into after Radix Salviae Miltiorrhizae Tabellae is selected, then using microwave after cutting
The mode of heating is dried, and carries out high speed breaking cellular wall using breaking cellular wall regulation machine, and obtains Radix Salviae Miltiorrhizae fine powder by 200 mesh sieves;
Cordyceps militaris (L.) Link. is selected to be put in ultrasonic cleaner after mud and is cleaned, drenched dry rear cutting and adopting ultrasonic Wave heating
Mode be dried, being then placed in breaking cellular wall regulation machine carries out high speed breaking cellular wall, and obtains Cordyceps militaris (L.) Link. fine powder by 200 mesh sieves;
B. it is preliminary to sterilize:By Radix Salviae Miltiorrhizae coarse powder and Cordyceps militaris (L.) Link. coarse powder after processing of step A, carried out soon by instantaneous ultrahigh-temperature sterilization machine
Speed sterilizing, is then placed within aseptic interior;
C. sterilizing test:The Radix Salviae Miltiorrhizae fine powder and Cordyceps militaris (L.) Link. fine powder obtained to step B carries out observation 2d, and is sampled and tests bacterium, no
It is qualified, then repeat step B;
D. sterilizing test:The Radix Salviae Miltiorrhizae fine powder and Cordyceps militaris (L.) Link. fine powder obtained to step B carries out observation 2d, and is sampled and tests bacterium, closes
Downstream is carried out after lattice then;
E. mix:The Radix Salviae Miltiorrhizae fine powder of system and Cordyceps militaris (L.) Link. fine powder are passed through into blender according to 5:2 mass ratio is sufficiently mixed
15min, the amylum pregelatinisatum for then adding 0.12 times of Radix Salviae Miltiorrhizae coarse powder parts by weight carry out mixing 30min;
F. piece is made in modulation:The mixed material of the acquisition in step D is added into the flavoring agent that mixed material mass fraction is 0.9 times,
Soft material is made, and decoction pieces are made by comminutor, and dried using microwave applicator, make compound Salviae Miltiorrhizae decoction pieces.
The flavoring agent is xylitol solution that concentration is 0.3%.
In step B by the way of microwave sterilizating, the sterilizing of 25S is carried out.
The microwave of 50-70GHz is adopted in step B.
The decoction pieces of the embodiment are averagely dissolved into bottom in 08 seconds in 1min in 10 glasss of 300ml and during temperature is 50 DEG C of water
There is the slightly cloudy solution of a small amount of deposition, and mouthfeel gently beneficial to absorption in portion.
Embodiment three
A kind of production technology of compound Salviae Miltiorrhizae decoction pieces, comprises the steps:
A. medical material is processed:Cleaned during ultrasonic cleaner is put into after Radix Salviae Miltiorrhizae Tabellae is selected, then using microwave after cutting
The mode of heating is dried, and carries out high speed breaking cellular wall using breaking cellular wall regulation machine, and obtains Radix Salviae Miltiorrhizae fine powder by 200 mesh sieves;
Cordyceps militaris (L.) Link. is selected to be put in ultrasonic cleaner after mud and is cleaned, drenched dry rear cutting and adopting ultrasonic Wave heating
Mode be dried, being then placed in breaking cellular wall regulation machine carries out high speed breaking cellular wall, and obtains Cordyceps militaris (L.) Link. fine powder by 200 mesh sieves;
B. it is preliminary to sterilize:By Radix Salviae Miltiorrhizae coarse powder and Cordyceps militaris (L.) Link. coarse powder after processing of step A, carried out soon by instantaneous ultrahigh-temperature sterilization machine
Speed sterilizing, is then placed within aseptic interior;
C. sterilizing test:The Radix Salviae Miltiorrhizae fine powder and Cordyceps militaris (L.) Link. fine powder obtained to step B carries out observation 3d, and is sampled and tests bacterium, closes
Downstream is carried out after lattice then;
D. mix:The Radix Salviae Miltiorrhizae fine powder of system and Cordyceps militaris (L.) Link. fine powder are passed through into blender according to 5:1 mass ratio is sufficiently mixed
20min, the amylum pregelatinisatum for then adding 0.1 times of Radix Salviae Miltiorrhizae coarse powder parts by weight carry out mixing 40min;
E. piece is made in modulation:The mixed material of the acquisition in step D is added into the flavoring agent that mixed material mass fraction is 1.2 times,
Soft material is made, and decoction pieces are made by comminutor, and dried using microwave applicator, make compound Salviae Miltiorrhizae decoction pieces.
The flavoring agent is xylitol solution that concentration is 0.5%.
In step B by the way of microwave sterilizating, the sterilizing of 30S is carried out.
The microwave of 70GHz is adopted in step B.
The decoction pieces of the embodiment in 10 glasss of 300ml and temperature be 50 DEG C of water in, be averagely dissolved into bottom in 48 seconds and deposit
It is easy to drink and absorption in the slightly cloudy solution of a small amount of deposition, and the gentle sweetness of mouthfeel.
The above is the preferred embodiment of the present invention, it is noted that for those skilled in the art
For, on the premise of without departing from principle of the present invention, some improvements and modifications can also be made, these improvements and modifications
Should be regarded as protection scope of the present invention.
Claims (5)
1. a kind of production technology of compound Salviae Miltiorrhizae decoction pieces, comprises the steps:
A. medical material is processed:Cleaned during ultrasonic cleaner is put into after Radix Salviae Miltiorrhizae Tabellae is selected, then using microwave after cutting
The mode of heating is dried, and carries out high speed breaking cellular wall using breaking cellular wall regulation machine, and obtains Radix Salviae Miltiorrhizae fine powder by 200 mesh sieves;
Cordyceps militaris (L.) Link. is selected to be put in ultrasonic cleaner after mud and is cleaned, drenched dry rear cutting and adopting ultrasonic Wave heating
Mode be dried, being then placed in breaking cellular wall regulation machine carries out high speed breaking cellular wall, and obtains Cordyceps militaris (L.) Link. fine powder by 200 mesh sieves;
B. it is preliminary to sterilize:By Radix Salviae Miltiorrhizae coarse powder and Cordyceps militaris (L.) Link. coarse powder after processing of step A, carried out soon by instantaneous ultrahigh-temperature sterilization machine
Speed sterilizing, is then placed within aseptic interior;
C. sterilizing test:The Radix Salviae Miltiorrhizae fine powder and Cordyceps militaris (L.) Link. fine powder obtained to step B carries out observation 1-3d, and is sampled and tests bacterium,
Downstream is carried out if after qualified, if unqualified, repeat step B;
D. mix:The Radix Salviae Miltiorrhizae fine powder of system and Cordyceps militaris (L.) Link. fine powder are passed through into blender according to 5:1~5:4 mass ratio is carried out fully
Mixing 10-20min, the amylum pregelatinisatum for then adding 0.1 ~ 0.15 times of Radix Salviae Miltiorrhizae coarse powder parts by weight carry out mixing 20-
40min;
E. piece is made in modulation:The mixed material of the acquisition in step D is added into the seasoning that mixed material mass fraction is 0.6-1.2 times
Agent, is made soft material, and makes decoction pieces by comminutor, and dried using microwave applicator, make compound Salviae Miltiorrhizae decoction pieces.
2. the production technology of compound Salviae Miltiorrhizae decoction pieces as claimed in claim 1, it is characterised in that:The flavoring agent for concentration is
0.2% ~ 0.5% xylitol solution.
3. the production technology of compound Salviae Miltiorrhizae decoction pieces as claimed in claim 1, it is characterised in that:The Radix Salviae Miltiorrhizae fine powder and the pupa
The addition mass fraction ratio of Cordycepses fine powder is 5:2.
4. the production technology of compound Salviae Miltiorrhizae decoction pieces as claimed in claim 1, it is characterised in that:Microwave is adopted in step B
The mode of sterilizing, carries out the sterilizing of 20-30S.
5. the production technology of compound Salviae Miltiorrhizae decoction pieces as claimed in claim 1, it is characterised in that:50- is adopted in step B
The microwave of 70GHz.
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Citations (3)
Publication number | Priority date | Publication date | Assignee | Title |
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CN103393896A (en) * | 2013-07-11 | 2013-11-20 | 浙江磐谷药源有限公司 | Traditional Chinese medicine formulation paris polyphylla direct-oral decoction piece for preventing and treating tumors |
CN105997895A (en) * | 2016-08-08 | 2016-10-12 | 湖南盟合投资管理有限公司 | Preparation method of wall-broken decoction piece |
CN106038689A (en) * | 2016-08-08 | 2016-10-26 | 湖南盟合投资管理有限公司 | Preparation method of radix salviae miltiorrhizae cellwall-broken decoction piece |
-
2016
- 2016-12-20 CN CN201611184713.3A patent/CN106511463A/en active Pending
Patent Citations (3)
Publication number | Priority date | Publication date | Assignee | Title |
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CN103393896A (en) * | 2013-07-11 | 2013-11-20 | 浙江磐谷药源有限公司 | Traditional Chinese medicine formulation paris polyphylla direct-oral decoction piece for preventing and treating tumors |
CN105997895A (en) * | 2016-08-08 | 2016-10-12 | 湖南盟合投资管理有限公司 | Preparation method of wall-broken decoction piece |
CN106038689A (en) * | 2016-08-08 | 2016-10-26 | 湖南盟合投资管理有限公司 | Preparation method of radix salviae miltiorrhizae cellwall-broken decoction piece |
Non-Patent Citations (1)
Title |
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牛超,等: "新型中药饮片研究进展", 《药学研究》 * |
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Application publication date: 20170322 |