CN106509988A - HEPA (high-efficiency particulate air) cigarette harm reducing particles as well as preparation method and application thereof - Google Patents
HEPA (high-efficiency particulate air) cigarette harm reducing particles as well as preparation method and application thereof Download PDFInfo
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- CN106509988A CN106509988A CN201611072486.5A CN201611072486A CN106509988A CN 106509988 A CN106509988 A CN 106509988A CN 201611072486 A CN201611072486 A CN 201611072486A CN 106509988 A CN106509988 A CN 106509988A
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- hepa
- granule
- cigarette
- cigarettes
- evil
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Links
- 235000019504 cigarettes Nutrition 0.000 title claims abstract description 82
- 238000002360 preparation method Methods 0.000 title claims abstract description 11
- 239000002245 particle Substances 0.000 title abstract description 7
- 239000008187 granular material Substances 0.000 claims abstract description 68
- 239000000835 fiber Substances 0.000 claims abstract description 34
- 239000002131 composite material Substances 0.000 claims abstract description 23
- 239000000843 powder Substances 0.000 claims abstract description 13
- 238000003756 stirring Methods 0.000 claims abstract description 9
- 229920002301 cellulose acetate Polymers 0.000 claims abstract description 8
- 238000001035 drying Methods 0.000 claims abstract description 8
- 238000000034 method Methods 0.000 claims abstract description 7
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims abstract description 6
- 239000002994 raw material Substances 0.000 claims abstract description 3
- DNIAPMSPPWPWGF-UHFFFAOYSA-N Propylene glycol Chemical compound CC(O)CO DNIAPMSPPWPWGF-UHFFFAOYSA-N 0.000 claims description 15
- 239000005020 polyethylene terephthalate Substances 0.000 claims description 12
- 229920004933 Terylene® Polymers 0.000 claims description 6
- 239000004745 nonwoven fabric Substances 0.000 claims description 6
- 229920000139 polyethylene terephthalate Polymers 0.000 claims description 6
- 230000015572 biosynthetic process Effects 0.000 claims description 5
- 239000003365 glass fiber Substances 0.000 claims description 5
- 150000001875 compounds Chemical class 0.000 claims description 4
- LFQSCWFLJHTTHZ-UHFFFAOYSA-N Ethanol Chemical compound CCO LFQSCWFLJHTTHZ-UHFFFAOYSA-N 0.000 claims 1
- PEDCQBHIVMGVHV-UHFFFAOYSA-N Glycerine Chemical compound OCC(O)CO PEDCQBHIVMGVHV-UHFFFAOYSA-N 0.000 abstract description 10
- SNICXCGAKADSCV-JTQLQIEISA-N (-)-Nicotine Chemical compound CN1CCC[C@H]1C1=CC=CN=C1 SNICXCGAKADSCV-JTQLQIEISA-N 0.000 abstract description 4
- 241000208125 Nicotiana Species 0.000 abstract description 4
- 235000002637 Nicotiana tabacum Nutrition 0.000 abstract description 4
- 238000005469 granulation Methods 0.000 abstract description 4
- 230000003179 granulation Effects 0.000 abstract description 4
- 229960002715 nicotine Drugs 0.000 abstract description 4
- SNICXCGAKADSCV-UHFFFAOYSA-N nicotine Natural products CN1CCCC1C1=CC=CN=C1 SNICXCGAKADSCV-UHFFFAOYSA-N 0.000 abstract description 4
- 230000000391 smoking effect Effects 0.000 abstract description 3
- 239000003205 fragrance Substances 0.000 abstract description 2
- 206010013911 Dysgeusia Diseases 0.000 abstract 1
- 238000001816 cooling Methods 0.000 abstract 1
- 235000011187 glycerol Nutrition 0.000 abstract 1
- 235000012907 honey Nutrition 0.000 abstract 1
- 238000000465 moulding Methods 0.000 abstract 1
- ULWHHBHJGPPBCO-UHFFFAOYSA-N propane-1,1-diol Chemical compound CCC(O)O ULWHHBHJGPPBCO-UHFFFAOYSA-N 0.000 abstract 1
- 238000007873 sieving Methods 0.000 abstract 1
- 239000004743 Polypropylene Substances 0.000 description 10
- 235000021419 vinegar Nutrition 0.000 description 6
- 239000000052 vinegar Substances 0.000 description 6
- 239000011269 tar Substances 0.000 description 4
- 238000012360 testing method Methods 0.000 description 4
- 230000000694 effects Effects 0.000 description 3
- 239000003546 flue gas Substances 0.000 description 3
- 239000000463 material Substances 0.000 description 3
- 238000011160 research Methods 0.000 description 3
- UGFAIRIUMAVXCW-UHFFFAOYSA-N Carbon monoxide Chemical compound [O+]#[C-] UGFAIRIUMAVXCW-UHFFFAOYSA-N 0.000 description 2
- 239000002671 adjuvant Substances 0.000 description 2
- 239000011280 coal tar Substances 0.000 description 2
- 239000000203 mixture Substances 0.000 description 2
- -1 polypropylene Polymers 0.000 description 2
- 229920001155 polypropylene Polymers 0.000 description 2
- 239000000779 smoke Substances 0.000 description 2
- XSTXAVWGXDQKEL-UHFFFAOYSA-N Trichloroethylene Chemical compound ClC=C(Cl)Cl XSTXAVWGXDQKEL-UHFFFAOYSA-N 0.000 description 1
- 230000007812 deficiency Effects 0.000 description 1
- 238000001514 detection method Methods 0.000 description 1
- 238000005516 engineering process Methods 0.000 description 1
- 238000011156 evaluation Methods 0.000 description 1
- 238000002474 experimental method Methods 0.000 description 1
- 239000004744 fabric Substances 0.000 description 1
- 239000000796 flavoring agent Substances 0.000 description 1
- 235000019634 flavors Nutrition 0.000 description 1
- 238000009472 formulation Methods 0.000 description 1
- 238000007689 inspection Methods 0.000 description 1
- 229920000728 polyester Polymers 0.000 description 1
- 238000012216 screening Methods 0.000 description 1
- 239000000126 substance Substances 0.000 description 1
- 235000019505 tobacco product Nutrition 0.000 description 1
Classifications
-
- A—HUMAN NECESSITIES
- A24—TOBACCO; CIGARS; CIGARETTES; SIMULATED SMOKING DEVICES; SMOKERS' REQUISITES
- A24D—CIGARS; CIGARETTES; TOBACCO SMOKE FILTERS; MOUTHPIECES FOR CIGARS OR CIGARETTES; MANUFACTURE OF TOBACCO SMOKE FILTERS OR MOUTHPIECES
- A24D3/00—Tobacco smoke filters, e.g. filter-tips, filtering inserts; Filters specially adapted for simulated smoking devices; Mouthpieces for cigars or cigarettes
- A24D3/06—Use of materials for tobacco smoke filters
- A24D3/08—Use of materials for tobacco smoke filters of organic materials as carrier or major constituent
- A24D3/10—Use of materials for tobacco smoke filters of organic materials as carrier or major constituent of cellulose or cellulose derivatives
Landscapes
- Chemical & Material Sciences (AREA)
- Engineering & Computer Science (AREA)
- Materials Engineering (AREA)
- Cigarettes, Filters, And Manufacturing Of Filters (AREA)
Abstract
The invention provides HEPA (high-efficiency particulate air) cigarette harm reducing particles as well as a preparation method and an application thereof. The HEPA cigarette harm reducing particles are prepared by the following steps: uniformly stirring HEPA fiber powder, propanediol, propanetriol, honey and pure water which serve as raw materials until agglomerated granules are obtained; conducting granulation by virtue of a granulator; and drying and cooling prepared granules, and sieving the granules so as to obtain the HEPA granules of 20-80 mesh. In a filter stick molding process, the HEPA cigarette harm reducing particles, which account for 5-20% in terms of the weight of a filter stick, are uniformly sprinkled on tows of the filter stick, so that the prepared filter stick contains the HEPA cigarette harm reducing particles; the filter stick, when combined with a conventional cellulose acetate filter stick, can be prepared into a composite filter tip, and the filter tip, together with cut tobacco sticks, can be prepared into a cigarette; and the cigarette is excellent in harm reducing performance, and tar and nicotine in the cigarette are reduced. In addition, instead of affecting the smoking quality of the cigarette, the fragrance of the cigarette is reduced, so that the cigarette becomes mild in taste and is more comfortable and cleaner in aftertaste.
Description
Technical field
The invention belongs to cigarette filter rod technical field, and in particular to a kind of to be made using high efficiency air atom filter element (HEPA)
Standby HEPA cigarettes drop evil granule and its preparation method and application.
Background technology
With《The Framework Convention on Tobacco Control》Signing, the harmful components such as cigarette mainstream flue gas are coal-tar middle oil, CO, HCN are extremely
Concern, the Less harmful cigarette for researching and developing high-quality and safety have become the developing direction of international Medicated cigarette.Wherein, with the new of drop evil function
Filter stick material has been the emphasis that each cigarette enterprise is broken through, and becomes the focus of Medicated cigarette worker research.High efficiency air atom
Filter element (High-Efficiency Particulate Air), the i.e. sub- drainage screen of high efficiency air atom, abbreviation HEPA, are states
The best filter material that exceeds is generally acknowledged on border, mainly including glass fibre, PP fibers, PP and PET composite fibres, terylene non-woven fabric, melt-blown
Long fibre.HEPA drainage screens have complete classification, retain thick effect filter screen, middle effect filter screen, sub- efficient filter and ultra high efficiency filter screen.Filter
The standard of net is set by USDOE, and to particle diameter in 0.3 μm of particle, filter effect is about more than DOP99.97%.Generally
The efficient filter for using can reach 99.99% intercepting efficiency.Meet HEPA standards filter have many uses it is general, from medical treatment
Equipment, automobile, aircraft and household can be applied.But so far, without the research that it is used for cigarette harm-reducing field.
The content of the invention
For the above-mentioned deficiency of prior art, the technical problem to be solved in the present invention is to provide a kind of using high efficiency air
HEPA cigarettes drop evil granule that particulate filter element (HEPA) material is prepared from and its preparation method and application, cigarette drop evil granule
Rod can reduce flue gas harmful substance, and affect less to Medicated cigarette reviewing prnciple.
The present invention provide technical scheme be：A kind of HEPA cigarettes drop evil granule, it is characterised in that specifically include with
The raw material of lower weight portion：
Wherein described HEPA fiber powders be by PP fibers, PP/PET composite fibres, glass fibre, terylene non-woven fabric wherein
A kind of chopped fiber of the length made by after crushing for 0.8-10mm；
A kind of HEPA cigarettes that the present invention is provided preparation method of drop evil granule, comprises the following steps that：
(1) HEPA fibers are crushed and chopped fiber of the length for 0.8-10mm is obtained as HEPA fiber powders；The HEPA is fine
One of which in dimension PP fibers, PP/PET composite fibres, glass fibre, terylene non-woven fabric；
(2) the HEPA fiber powders obtained by 20-75 part steps 1 are weighed by weight, add 5-10 part Propylene Glycol, 0-10 parts third
Triol, the Mel and 10-30 part pure water of 10-30 parts, after stirring, presents into bulk granule；
(3) granule of gained in step 2 is stood into 30-60 minutes under the conditions of 4-40 DEG C, is then made with comminutor
Grain, and the granule made is put in drying baker, 8-12h is dried under conditions of 25-80 DEG C, and which is entered in dry run
Row is stirred；
(4) after being dried in step (3), granule is cooled to room temperature, then with the sieved through sieve of different meshes, obtains 20-80
Purpose HEPA granule is HEPA cigarettes drop evil granule.
The present invention preferably technical scheme：Stir per hour once during being dried in step (3), stir the time every time
For 2-5min.
A kind of application of the HEPA cigarettes that the present invention is provided with drop evil granule, it is characterised in that：During filter stick formation, will
Above-mentioned HEPA cigarettes drop evil granule is added on tow, is prepared into the filter stick for dropping evil granule containing HEPA cigarettes, wherein, described
5%-20% of the addition of HEPA drop evil granules for filter stick gross weight；Then will containing HEPA cigarettes with drop evil granule filter stick with
Conventional cellulose acetate filter rod makes HEPA cigarettes drop evil composite tip stick using existing mouth rod complex method is compound.
Preferably application process of the invention is：The HEPA cigarettes drop evil composite tip stick is contained by 5mm vinegar fibre filter stick, 15mm
The Three-element composite filter core that the filter stick and 5mm cellulose acetate filter rods for having HEPA cigarettes drop evil granule is composited, or contained by 15mm
The binary compound filter candle for having the filter stick of HEPA cigarettes drop evil granule to be composited with the cellulose acetate filter rod of 10mm.
Cigarette prepared by the present invention is added in filter stick with drop evil granule, and makes Medicated cigarette with tobacco rod, detects cigarette smoke
Its TPM maximum reduction rate 30.1%；Tar maximum reduction rate 37.63%.With excellent drop evil performance, can reduce
Medicated cigarette is coal-tar middle oil, nicotine.And the judging parameter of Medicated cigarette is not interfered with, and can make that the fragrance of Medicated cigarette is thin out on the contrary, mouthfeel becomes
Gently, pleasant impression is more liked comfortable clean.
Specific embodiment
Below the specific embodiment and its relevant technical problem of the present invention are described in further detail.
Embodiment 1, preparation method of a kind of HEPA cigarettes with drop evil granule, it is characterised in that comprise the following steps that：
(1) PP (polypropylene) fiber is crushed and chopped fiber of the length for 1mm is obtained as HEPA fiber powders；
(2) weigh the HEPA fiber powders obtained by 20 parts of steps (1) by weight, add 5 parts of Propylene Glycol, 1 part of glycerol, 10
The Mel and 10 parts of pure water of part, after stirring, presents pockets of granule；
(3) granule obtained by step (2) is stood into 60 minutes under the conditions of 4 DEG C, then with granulator granulation, and will be made
Granule be put in drying baker, be dried 12h in 25 DEG C of degree, period is stirred once per hour, each 5min；
(4) dried granule in step (3) is cooled to into room temperature, and with the sieved through sieve of different meshes, obtains 20 mesh
HEPA granules are described HEPA drop evil cigarette granule A.
During filter stick formation, the 5% of filter stick weight HEPA drop evil cigarette granule A are uniformly sprinkling upon into filter stick tow
On, the filter stick for dropping evil cigarette granule A containing HEPA is made, and the filter stick of evil cigarette granule A will be dropped containing HEPA in conventional vinegar
Sour fibrous filter candle is obtained two-part composite filter A using existing mouth rod complex technique.
Embodiment 2, preparation method of a kind of HEPA cigarettes with drop evil granule, it is characterised in that comprise the following steps that：
(1) PP is crushed the chopped fiber work that length is obtained for 5mm with PET composite fibres (polypropylene and polyester complex fiber)
For HEPA fiber powders；
(2) weigh the HEPA fiber powders obtained by 50 parts of steps (1) by weight, add 7 parts of Propylene Glycol, 5 parts of glycerol, 15
The Mel and 15 parts of pure water of part, after stirring, presents pockets of granule；
(3) granule obtained by step (2) is stood into 40 minutes at 20 DEG C, and with granulator granulation after, be put in drying baker
It is interior, 10h is dried in 60 DEG C of degree, period is stirred once per hour, each 3min；Room temperature is cooled to after drying, with different meshes
Sieved through sieve, obtains 60 mesh HEPA granules and is described HEPA drop evil cigarette granule B.
During filter stick formation, the 10% of filter stick weight HEPA drop evil cigarette granule B are uniformly sprinkling upon into filter stick tow
On, the filter stick for dropping evil cigarette granule B containing HEPA is made, and the filter stick of evil cigarette granule B will be dropped containing HEPA in conventional vinegar
Sour fibrous filter candle makes three-stage composite filter B using existing mouth rod complex technique.
Embodiment 3, preparation method of a kind of HEPA cigarettes with drop evil granule, it is characterised in that comprise the following steps that：
(1) terylene non-woven fabric is crushed and chopped fiber of the length for 10mm is obtained as HEPA fiber powders；
(2) weigh the HEPA fiber powders obtained by 75 parts of steps (1) by weight, add 10 parts of Propylene Glycol, 10 parts of glycerol,
30 parts of Mel and 30 parts of pure water, after stirring, present pockets of granule；
(3) granule obtained by step (2) is stood into 30 minutes at 40 DEG C, with granulator granulation after, be put in drying baker,
8h is dried in 80 DEG C of degree, period is stirred once per hour, each 2min；Room temperature is cooled to after drying, with the screen cloth of different meshes
Screening, obtains 80 mesh HEPA granules and is described HEPA drop evil cigarette granule C.
During filter stick formation, the 20% of filter stick weight HEPA drop evil cigarette granule C are uniformly sprinkling upon into filter stick tow
On, the filter stick for dropping evil cigarette granule C containing HEPA is made, and the filter stick of evil cigarette granule C will be dropped containing HEPA in conventional vinegar
Sour fibrous filter candle is obtained into three-stage composite filter C using existing mouth rod complex technique.
Applicant has done following research experiment to new drop evil application of the filter stick in Medicated cigarette prepared in three embodiments：
(1), the drop evil performance of new drop evil filter stick
In the case where cigarette tobacco leaf formulation and other adjuvants are constant, will containing HEPA drop the filter stick of evil cigarette granule with it is identical
The blank vinegar fibre filter stick of specification is fabricated to the flue gases such as Medicated cigarette, the TPM (TPM) of detection cigarette smoke, tar, moisture, nicotine
Index, is as a result listed in table 1.
The drop evil Performance comparision of 1 new drop of table evil composite filter
1 testing result of table shows, in the case where cigarette composition and other adjuvants are constant, with respect to blank Medicated cigarette,
HINH can reduce tar, nicotine.Wherein, TPM maximum reduction rate 30.1%；Tar maximum reduction rate 37.63%.This
Illustrating, the Medicated cigarette for composite filter being done harm to added with new drop has excellent drop evil performance.
(2), new drop does harm to the evaluation of smokeing panel test of composite filter
For further determining that the cigarette potentiality for doing harm to composite filter containing new drop, the present inventor's commission Hubei Province's tobacco product matter
Cigarette committee member is commented in amount supervision and inspection station tissue Hubei Province, by the regulation of GB5606.4-1996, to containing new drop evil composite filter volume
The cigarette and blank cigarette of system has carried out contrast and has smoked panel test.Smoking result is shown in Table 2.
2 new drop of table does harm to the Medicated cigarette smoking result of composite filter
4 result of table shows that the score of smokeing panel test containing new drop evil composite filter and blank vinegar fibre filter stick is substantially close to total body constitution
Amount level and product style no significant difference.Comparatively, the evil composite filter cigarette flavor containing new drop is slightly light, but mouthfeel becomes
Obtain gently, pleasant impression is comfortably clean.
Claims (5)
1. a kind of HEPA cigarettes are used and drop evil granule, it is characterised in that specifically include the raw material of following weight portion：
Wherein described HEPA fiber powders are by one of which in PP fibers, PP/PET composite fibres, glass fibre, terylene non-woven fabric
Chopped fiber of the length made by after crushing for 0.8-10mm.
2. a kind of preparation method of drop evil granule of the HEPA cigarettes described in claim 1, comprises the following steps that：
(1) HEPA fibers are crushed and chopped fiber of the length for 0.8-10mm is obtained as HEPA fiber powders；The HEPA fibers PP
One of which in fiber, PP/PET composite fibres, glass fibre, terylene non-woven fabric；
(2) weigh the HEPA fiber powders obtained by 20-75 part steps 1 by weight, add 5-10 part Propylene Glycol, 0-10 parts the third three
Alcohol, the Mel and 10-30 part pure water of 10-30 parts, after stirring, presents into bulk granule；
(3) granule of gained in step 2 is stood into 30-60 minutes under the conditions of 4-40 DEG C, then pelletize is carried out with comminutor, and
The granule made is put in drying baker, 8-12h is dried under conditions of 25-80 DEG C, and which is turned in dry run
It is dynamic；
(4) after being dried in step (3), granule is cooled to room temperature, then with the sieved through sieve of different meshes, obtains 20-80 mesh
HEPA granules be HEPA cigarettes drop evil granule.
3. a kind of HEPA cigarettes use drop according to claim 2 does harm to the preparation method of granule, it is characterised in that：The step
(3) stir per hour once during being dried in, the time is stirred every time for 2-5min.
4. application of the HEPA cigarettes described in a kind of claim 1 or 2 with drop evil granule, it is characterised in that：In filter stick formation mistake
Cheng Zhong, above-mentioned HEPA cigarettes drop evil granule is added on tow, the filter stick for dropping evil granule containing HEPA cigarettes is prepared into, its
In, the addition of the HEPA drops evil granule is the 5%-20% of filter stick gross weight；Then will be containing HEPA cigarettes drop evil granule
Filter stick make the harmful composite tip stick of HEPA cigarettes drop with conventional cellulose acetate filter rod using existing mouth rod complex method is compound.
5. application of the HEPA cigarettes according to claim 4 with drop evil granule, it is characterised in that：The HEPA cigarettes are multiple with drop evil
It is that the filter stick and 5mm cellulose acetate filter rods for containing HEPA cigarettes drop evil granule by 5mm cellulose acetate filter rods, 15mm is combined to close mouth rod
Three-element composite filter core, or contained by 15mm filter stick and the 10mm of HEPA cigarettes drop evil granule cellulose acetate filter rod it is multiple
The binary compound filter candle for closing.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201611072486.5A CN106509988A (en) | 2016-11-29 | 2016-11-29 | HEPA (high-efficiency particulate air) cigarette harm reducing particles as well as preparation method and application thereof |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201611072486.5A CN106509988A (en) | 2016-11-29 | 2016-11-29 | HEPA (high-efficiency particulate air) cigarette harm reducing particles as well as preparation method and application thereof |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| CN106509988A true CN106509988A (en) | 2017-03-22 |
Family
ID=58355210
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN201611072486.5A Pending CN106509988A (en) | 2016-11-29 | 2016-11-29 | HEPA (high-efficiency particulate air) cigarette harm reducing particles as well as preparation method and application thereof |
Country Status (1)
| Country | Link |
|---|---|
| CN (1) | CN106509988A (en) |
Citations (5)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN1771846A (en) * | 2005-10-26 | 2006-05-17 | 常德卷烟厂 | Non-woven fabric water filter tip for reducing tar and harmful matter of cigareffe effectively |
| CN201536617U (en) * | 2009-09-29 | 2010-08-04 | 菲尔创纳国际有限公司 | Filter tip bar used for smoking tobacco |
| CN101822425A (en) * | 2010-04-16 | 2010-09-08 | 云南正邦生物技术有限公司 | Preparation method of cigarette absorption type flavor compensation material |
| CN102178350A (en) * | 2011-04-07 | 2011-09-14 | 红云红河烟草(集团)有限责任公司 | Silk protein compound filter tip and preparing method thereof |
| CN105533794A (en) * | 2016-01-15 | 2016-05-04 | 红云红河烟草(集团)有限责任公司 | Method for preparing honey-fragrant cigarette fragrance line through longan nectar |
-
2016
- 2016-11-29 CN CN201611072486.5A patent/CN106509988A/en active Pending
Patent Citations (5)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN1771846A (en) * | 2005-10-26 | 2006-05-17 | 常德卷烟厂 | Non-woven fabric water filter tip for reducing tar and harmful matter of cigareffe effectively |
| CN201536617U (en) * | 2009-09-29 | 2010-08-04 | 菲尔创纳国际有限公司 | Filter tip bar used for smoking tobacco |
| CN101822425A (en) * | 2010-04-16 | 2010-09-08 | 云南正邦生物技术有限公司 | Preparation method of cigarette absorption type flavor compensation material |
| CN102178350A (en) * | 2011-04-07 | 2011-09-14 | 红云红河烟草(集团)有限责任公司 | Silk protein compound filter tip and preparing method thereof |
| CN105533794A (en) * | 2016-01-15 | 2016-05-04 | 红云红河烟草(集团)有限责任公司 | Method for preparing honey-fragrant cigarette fragrance line through longan nectar |
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Application publication date: 20170322 |