CN106507791B - A kind of priming production line of the completely man-machine isolation of serialization automatization and application - Google Patents

Abstract

The present invention relates to a kind of priming serialization automatic production line、Key device、Technological process arrangement，The through arrangement of all fronts homonymy straight line is invented，Insertion is realized by the steel pass-through box of controlled switch between adjacent antiknock room、Transmission、Closing、Anti- biography fire、The function of anti-propagation of explosion，Using equipped with antistatic、The double-layer trolley of sparkproof material wheel loads initiating explosive tray and realizes priming geo-stationary、Without friction、Without the safety transmission that clashes into，The completely man-machine isolation automation mechanized operation of dangerous operation，Reduce the operational motion of priming production process，Reduce operation frequency，Improve the intrinsic safety of priming production line and production process，The production capacity that class produces 150kg primings is reached，Three carbohydrazide of perchloric acid can be met and close zinc (GTX)、Three carbohydrazide of perchloric acid closes cadmium (GTG)、Nickel hydrazine nitrate (NHN)、The serialization automated production of the primings such as dextrin lead azide (LA) is used.

Description

A kind of serialization automation priming production line of man-machine isolation and application completely

Technical field

The present invention relates to a kind of production technology arrangement that priming is produced with serialization, automation mode, the technology relate to Priming production process operator and manufacturing machine is completely isolated, automation mechanized operation production-line arrangement mode, priming dispensing, The critical processes such as chemical combination, portioning filtering and washing, automation water-bath vacuum drying box, automatic transmission, automatic sieving mounted box vanning are set Standby arrangement.

The present invention is directed to priming serialization automatic production line, it is proposed that the through arrangement of homonymy straight line in completely, each adjacent anti- Insertion, transmission, closing, the anti-function of passing fiery, anti-propagation of explosion, priming are realized by the steel pass-through box of controlled switch between shot room Serialization, automation, the preferred arrangement scheme of complete man-machine isolation production line and process unit；Emphasis, which is solved, continuously to be produced Process automation is closed, the automatic production technology device arrangement for curing, crystallizing automatically, automatic portioning, automatic suction filtration, automatic washers The arrangement of skill equipment, automatic water-bath vacuum drying box, automatic drying vehicle, dry in the air medicine frame and automatic medicine of a cold nature frame, automatic mistake automatically The arrangement of the priming production process key equipment such as sieve, mounted box, boxing apparatus；Propose serialization automatic production process Procedural order：Raw material are weighed and pure water metering, dispensing, suction filtration, feed liquid storage, feed liquid metering, charging, chemical combination, ripe Change, crystallization, portioning, suction filtration, washing, dehydration, fall disk, entrucking, the medicine that dries in the air, drying, the medicine of a cold nature, pass disk, fall medicine, sieving, The operation logic process of each step such as mounted box, vanning.

The production line and technology arrangement mode of serialization automated manufacturing priming proposed by the present invention are applied to have similar production work The production of the various primings of skill process, such as：The carbohydrazide of perchloric acid three close zinc (GTX), the carbohydrazide of perchloric acid three close cadmium (GTG), Nickel hydrazine nitrate (NHN), lead azide (LA), lead styphnate (LS), potassium picrate (KP), this base of a fruit phenolic acid potassium (KS) etc. Priming.Point of the compatible dinitrodiazophenol (DDNP) of the serialization automatic production line technology arrangement mode, key equipment Disk, the medicine that dries in the air, drying, the medicine of a cold nature, medicine, sieving, mounted box, the serialization automated production of binning process.

Background technology

Priming is that all military priming systems and the initial of industrial explosive material originate the energy, is the core powder charge of firer's device, Principal item have DDNP, GTX, GTG, NHN, LA, LS, basic lead picrate and lead azide double salt (KD), Lead azide is co-precipitated primings such as (DS) with lead styphnate.Because priming has sensitivity high, dangerous big, easily Hot fried the characteristics of, easily cause accidental explosion accident in production process.Therefore, priming is national defense industry and civil blast device One of most dangerous explosive that material production field must be used, the production-line arrangement and production technology of priming are national defence works One of key technology of industry industrial explosive material production field.

Transmission between in-process and process is all artificial directly facing face manual operations, and danger is greatly.Such production-line arrangement With technology mode although it is simple to operate, be easy to grasp, but operating personnel spirit in high-pressure state, be easily caused unexpected combustion Burn and explosion accident occurs, cause casualties.At present, production and using priming enterprise use mostly it is this fall Production line and production technology.The main deficiency that current production line and the mode of production are present is as follows：

(1) intermittent feeds, chemical combination, discharging technology, the production cycle are long, manually operate, labor intensity is big, security is poor.

(2) all it is straight by workman in the multiple working procedure such as priming chemical combination, discharging, point disk, transmission, drying, medicine taking box, vanning The manual operations of junction opposite, easily occurs accidental explosion accident, causes casualties.

(3) in priming baking operation, some enterprises use drying room drying mode, deposit that dose is big, drying efficiency is low, operative employee People, which frequently passes in and out storage, has the room of a large amount of primings, precarious position duration long, dangerous high, production environment condition Very severe.

In order to solve the safety issue of priming production line and production process, countries in the world are in the automatic metaplasia of priming serialization Production technical field has all carried out substantial amounts of research work in succession, and Germany have developed lead azide (LA) in 1970s The continuous production technology of priming, uses the glass reactor of straight barrel, and sodium azide feed liquid and plumbi nitras feed liquid connect It is continuous to be added in combination apparatus, stirring is realized by air-blowing bubble, two kinds of feed liquid reaction generation lead azide primings work as priming Crystal grain is grown up to after certain size, is gradually deposited to the bottom of combination apparatus, by the alternation switch of two choke valves, is made Generation lead azide priming outflow combination apparatus, into filtering and washing procedure.But, this technology has certain office It is sex-limited, lead azide priming this kind is only used for, and be required in the early stage produced every time carrying out substantial amounts of work Skill parameter adjustment, the lead azide product qualified until producing could put into continuous production, cause in this process big The loss of material of amount, the stability of product quality is poor, and production capacity is small.Therefore, the technological principle, method and apparatus do not have It is expanded to be applied in the production of other primings.

The priming flexible automation life of 804 factories carried out by the research of China North Industries Group Corporation technological equipment and 121 factory's development and designs Producing line, 204 factories have also built two similar priming automatic production lines on this basis, but this four production lines are present Following something in common：

(1) batch production mode：Dispensing, chemical combination, drying overall process be all connect a collection ofly, batch (-type) carry out, The serialization automated production of priming can not be realized.

(2) equipment capacity is low：Due to the danger of priming, the place capacity of design is small, a collection of inventory in theory only 4kg priming products can be produced, production capacity is low, it is impossible to meet high-volume use requirement.

(3) all fronts low production efficiency：Because the technology uses single box thermal current top blast to draw dry technology with, in every batch of product mistake The built-in about 2kg priming products of medicine box after filter, manipulator, which is sent under top blast, to be drawn after Drying station, above pipeline drying hot blast, Priming could be dried to qualified level by vacuum suction traction below, drying time for 2h~4h.The critical process took It is long, cause whole production line production efficiency low, daily production capacity is less than 10kg, it is impossible to which meeting large-scale industrial production makes With requiring.

(4) it is discontinuous between each operation, it is provided between machinery, is transmitted using 180 ° of revolutions of manipulator between adjacent process Quick-fried medicine box, production process substep is separated, it is impossible to realize continuous production, it is impossible to meet priming high-volume, big production Fertile use requirement.

With the continuous improvement of China's scientific and technological level, the kind of priming, the species of military priming system and explosive and Demand also increasingly increases, and is badly in need of solving the high-volume of priming, the technical barrier of safety in production.Because priming is dangerous Property it is big, using serialization, automatic production line and technical process difficulty greatly, universal process units and equipment can not The fire-proof and explosion-proof use requirement of priming is met, and special equipment and device do not obtain due development, some techniques and set Apply poor with equipment dependability, therefore priming serialization automatic producing technology never has and solved well, forms system The about bottleneck of the dual-use priming system art progress of China.

According to the military priming system of China and the growth requirement of industrial explosive material, design and manufacture meet China's priming it is wide in variety, Yield is high, consumption is big priming serialization automatic production line, technology mode, technical process and technology, for carrying Automaticity, intrinsic safety and the production efficiency of high China's priming production process, reduction on-line operation personnel amount, The safety of operating personnel of reducing labor intensity, ensure has important practical significance.

Therefore, the present invention proposes the production line and technology arrangement technology of a kind of various primings of serialization automated manufacturing, leads to The innovative design of optimization design to production line, the preferred arrangement of technical process, production equipment and device is crossed, has been realized The complete man-machine isolated operation of quick-fried medicine production overall process, dangerous process are unattended, operating personnel are not directly contacted with priming Important safety function, improves the intrinsic safety of priming production line, improves production capacity and production efficiency, disclosure satisfy that Various priming production and application requirements.

The content of the invention

The present invention relates to the production line of priming production overall process and technology arrangement, the arrangement of crucial production equipment and device, danger Key project technical problem of the dangerous post without serialization automated production primings such as operation, the man-machine isolation in all fronts.

Priming serialization automatic production line of the present invention and technology arrangement mode are：The through cloth of all fronts homonymy straight line Put, insertion, transmission, closing, anti-fiery, the anti-propagation of explosion of biography are realized by the steel pass-through box of controlled switch between each adjacent antiknock room Function, the priming between each operation is by equipped with being loaded on antistatic, the double-deck transfering small vehicle of sparkproof material wheel Papery or wooden or aluminum batch pan equipped with priming realize the transmission without friction, without shock, priming geo-stationary, Corresponding process units and equipment realize automation function by ecp, and production overall process is transmitted automatically, the full mistake of production line Journey danger post and process all realize complete mechanical isolation, scene without human users.

According to the technology arrangement mode of foregoing invention, the key issue of the safety transmission of priming is solved, priming is reduced The operational motion and operating frequency of production process, the security for improving production process, improve production capacity and production efficiency, The automation journey and essential safety level of priming production process are improved, the need for meeting a variety of priming production processes.

According to the Design of Production Line principle of the present invention, it is proposed that the arrangement and building of production line scheme of priming production line, Production-line arrangement, technical process arrangement, the scheme of key equipment arrangement are proposed, foring one kind can realize that priming connects Continuousization automated production, whole man-machine isolation, production process essential safety, production efficiency is high, operating personnel are few, work is strong The low priming production line technology of degree.

The serialization automation priming production-line arrangement and production technology arrangement embodiment of the present invention is as follows：

According to the technical requirements of the typical priming production process of China, the requirement of safe general rule, worker-house construction of structures design rule Model requirement, the present invention propose the production-line arrangement mode of serialization automated production priming, technical process arrangement and Process unit arrangement, which goes for the various priming production and applications with similar production process, only Need corresponding technological parameter being adjusted.

In terms of serialization automatic production line arrangement, each operational sequence of priming production process is successively close to arrangement, " completely Between the through arrangement of homonymy straight line, each adjacent antiknock room by the steel pass-through box of controlled switch realize insertion, transmission, closing, Priming between the anti-function of passing fiery, anti-propagation of explosion, each operation is by the bilayer equipped with antistatic, sparkproof material wheel Papery or wooden or aluminum batch pan equipped with priming is loaded on transfering small vehicle to realize without friction, without shock, detonation medicine phases To static transmission " design philosophy be embodied in following implementation process：

Starting end is：1) priming produces mechanical admixture in the reaction material liquid preparation needed, acid-base value regulation, feed liquid and crosses elimination Remove, the standby, chemical combination of filtered fluid collection is measured with feed liquid, priming combination reaction.

Critical process is the chemical combination process of priming, and the process is relevant with the kind of priming, Operating parameters are according to detonation The kind of medicine is determined：A kind of reaction material liquid is first put into combination apparatus first and makees bottom liquid, be heated to reaction temperature, then will be another Plant feed liquid to be gradually added in the bottom liquid in combination apparatus with certain flow velocity, now two kinds of feed liquids are stirred in uniform temperature, necessarily Chemical reaction generation priming occurs under the conditions of mixing, the crystallization with certain size is formed.Second of feed liquid filling is finished, will Reaction mixture insulation curing, make reaction carry out completely, make priming crystallization gradually grow up.Again by reaction mixture by reacting Temperature cooling close to room temperature, the priming of generation is crystallized out as much as possible, obtain bulky grain priming, raising yield, Improve the free-running property of priming.

Follow-up technical process is the general production process of all primings, and the kind with priming is unrelated.Of all kinds Quick-fried medicine is carried out using identical processing step and identical technological parameter：The reaction mixture after cooling is passed through first Filter realizes the separation between priming crystallization and reaction mother liquor, and priming Crystallization Separation is come out, retained in the filter. In the process, the reaction mixture of outflow can be automatically separated into aliquot collect priming product, also can will be big after filtering Amount priming product is separated into aliquot and carries out follow-up drying process, and the purpose is to the same.But, this two mode was operated The safe coefficient of journey is different.The design of the present invention is the filtering of the reaction mixture automatic shunt that just flows out to capacity about 1kg In bucket, priming product is collected in aliquot mode, the subsequent operation security of this mode is good, the priming of aliquot is placed Shakeout in a paper disc (or treucher or aluminium dish), harrow uniform；The plate that will be equipped with priming is put into a special racks On dry in the air a period of time, as often as possible by moisture content and dehydrating agent volatilization, the load to mitigate vacuum drying process；It will dry in the air again Initiating explosive tray is transferred in vacuum drying box, and the regular hour is dried under certain vacuum degree, uniform temperature, is made in priming Moisture content reach qualified degree, then eliminate vacuum, baking oven opened to door cooling a period of time；The detonation that vacuum drying is crossed Medicine drying vehicle is transferred on the shelf of an andron and places cool a period of time, the temperature of priming is down into room temperature, with true Protect the safe operation of subsequent process；Just batch pan is transferred on the machine of falling medicine, priming is wandered onto screen cloth, in jitter conditions Under make medicament by screen cloth, by fallen under guide housing collect medicine box in；Medicine box will be collected to take out, wipe the floating of removing surface Medicine, rotate to fortune medicine-chest in；After fortune medicine-chest is filled to quantitatively, medicine-chest is delivered into priming storehouse.

According to above-mentioned process sequences, it is possible to safely produce the priming product of required kind.It is above-mentioned in order to meet Technical process, the present invention proposes the production-line arrangement scheme of two kinds of serialization automated manufacturing primings.

Brief description of the drawings

The priming serialization automatic production process of accompanying drawing 1 and production-line arrangement：The first plan arranges schematic diagram

The priming serialization automatic production process of accompanying drawing 2 and production-line arrangement：The first scheme part elevation arranges schematic diagram

The priming serialization automatic production process of accompanying drawing 3 and production-line arrangement：Second scheme horizontal layout schematic diagram

The priming serialization automatic production process of accompanying drawing 4 and production-line arrangement：Second scheme part elevation arranges schematic diagram

The floor map of first arrangement and local elevational schematic view such as Fig. 1 and Fig. 2, the plane signal of the second arrangement Figure and local elevational schematic view are as shown in 3 and Fig. 4.Function, purposes and the setting in each label room are described as follows in figure：

1 --- weighing area, table scale, measuring tank, dosage bunker, lautertuns, feed liquid collecting tank, material are placed with the operation room Liquid measuring tank, with the main devices such as acid tank, type washing sink, equipment and facility, it is main to complete priming production and uses all former materials The preparation of material, weighing, the metering of various dispensing pure water, the heating of various dispensing pure water, various solid materials Dissolving, heating, filtering, filtrate collection, acid-base value regulation, feed liquid storage, the metering of combination reaction feed liquid.The room For normal operations room, all production works are completed by operator's auxiliary.

The priming of different cultivars, the main distinction of its production process be exactly variety of raw material, inventory, the acid-base value of feed liquid, Preparing process parameter, all these production processes differed from one another are mainly reflected in the operation in the room, and this room is someone Work intervention operation, raw material by various primings species, ingredient proportion carry out preparation feed liquid, realize the different product of production The priming planted, the room that the present invention is designed is universal, therefore the priming production line disclosure satisfy that different cultivars is detonated The production and application requirement of medicine.

2 --- between chemical combination, two kinds of feed liquids are chemically reacted under condition of heating and stirring in the room, chemical combination production priming Product, and form the crystalline solid with certain granules degree, the room is provided with the danger of priming, therefore by the room design For structure between antiknock.Capital equipment is the combination apparatus with chuck, can be by flowing through temperature and the flow control of hot water in chuck The temperature of reaction solution in inhibition and generation clutch, makes two kinds of feed liquids react generation priming under the conditions of temperature controllable.Two kinds of feed liquids add Material is finished, and the reaction mixture of generation will all be released by the way that the controllable frictionless valve door in combination apparatus bottom is disposable, downwards It is transferred in ager.

3 --- curing room, the insulation, under agitation of the above-mentioned reaction mixture passed over is mainly completed in the room Sustained response certain time, make generation priming combination reaction carry out completely, make priming crystal growth, in the room Material has explosion hazard, therefore the room design is structure between antiknock.Capital equipment is that the insulation with chuck is cured Combination apparatus, can control the temperature of reaction solution in combination apparatus, reaction mixture by flowing through the temperature and flow of hot water in chuck The insulation curing certain time under the conditions of temperature controllable, after slaking reaction time as defined in is incubated, reaction mixture will All release, be passed down in cooler crystallizer by the way that the controllable frictionless valve door in combination apparatus bottom is disposable.

4 --- between crystallisation by cooling, the cooling of the above-mentioned reaction mixture passed over is mainly completed in the room, is made higher At a temperature of the priming crystal growth that dissolves in reaction solution, while making priming crystallize out as much as possible, improve priming Production yield.Material in the room has very strong explosion hazard, therefore the room is structure between antiknock.Mainly Equipment is the crystallisation by cooling combination apparatus with chuck, can be by flowing through 10 DEG C or so of cooling flow and water flowing time in chuck The temperature of reaction mixture in cooler crystallizer is controlled, when mixeding liquid temperature is reached below 30 DEG C, mixed liquor will pass through chemical combination The controllable frictionless valve door in device bottom is disposable all to release, and is passed down in portioning filtration washing device.

Above-mentioned 2 to No. 4 processes are only so be divided into three rooms, when being because of being broken down in production process or being unexpected, often Individual operating unit is all independent, and operating personnel, which relatively safe can be entered in room, to fix a breakdown, resumes production；If three When accidental explosion occurs in any one in individual process, due to the separation in room, loss can be made to be reduced to bottom line.

According to the requirement of related construction specification and antiknock ability, 2 to No. 4 processes can also be placed on to one has equivalent resist In the big antiknock of ability, such arrangement can save land area and construction cost to greatest extent, therefore in scheme two Employ the design of " Trinity ".

All be to carry out identical operation for all primings in follow-up all operation rooms, with the kind of priming without Close, be universal design.

5 --- portioning, filtering, washing, dehydration, cross pan transmission, cross pan, stand batch pan, batch pan transmission between.The room Between be a comprehensive function at most, most complicated room, in the room complete reaction mixture in priming crystallization and mother liquor Separation, priming deposit dose at most, dangerous most imperial palace, therefore the room is this production line has the room of maximum antiknock ability Between between antiknock structure.

The capital equipment deposited in the room has：Portioning device, guiding gutter, priming cross pan, cross pan loading disk, wash Wash water injector plus absolute ethyl alcohol device, priming cross pan transfer robots, stand batch pan manipulator, batch pan transmission machinery Hand, initiating explosive tray transmission track, mother liquor surge tank, mother liquor collecting tank, mother liquor destroy charging system, destroy mother liquor stillpot, Pure water storage tank, anhydrous acetic acid storage tank, destruction nitric acid storage tank etc..

The technological process completed in the room is：Mixed liquor in cooler crystallizer is rubbed by the controllable nothing in combination apparatus bottom Wipe that valve is disposably all released, the upper top that flow to portioning air deflector, mixed liquor have substantially been divided evenly into 9 streams Road, each it flow to the priming of bottom along guiding gutter and crosses in pan, crosses that pan bottom is vacuumized, mother liquor is under vacuum suction effect Entered by the filter bag crossed in pan in mother liquor collector, entered along pipeline in mother liquor dashpot, priming crystallization is detained Cross in pan the separation for realizing that mother liquor and priming are crystallized, then pure water, pure water are sprayed by the top of air deflector and equally lead to Cross guiding gutter to flow in pan, priming washing by soaking is removed mother liquor, washings in vacuum suction effect lower edge by pure water Pipeline is entered in buffer, secondary with pure water washing successively, then in the same way with absolute ethanol washing once, lead to Cross to vacuumize and fully drain the priming crossed in pan, after end is drained, vacuum system emptying recovers normal pressure, buffering Mother liquor and cleaning solution in groove automatically inject mother liquor in the presence of drop and collected in destruction groove.Complete portioning, filtering, Washing, dewatering process process.

Then, the priming after medicine taking box machinery drains adjacent nearest one equipped with washing cross pan pick up, remove it is solid Positioning, which put, this is crossed to pan delivers to the top of fall box stand disk device, manipulator along 180 ° of central shaft rotation, by the detonation in box Medicine down to made on the guider above batch pan, by vibration priming result in pan the clean, manipulator turn round, Retraction, by it is empty cross pan be back on the position of pickup, manipulator retraction, 40 ° of turntable rotation for loading medicine box, by another Pan of crossing equipped with priming crystallization is delivered on the adjacent nearest position of the manipulator, repeats aforesaid operations.

The priming crystallization fallen down along guider by the batch pan immediately below relatively evenly dropping down onto down, push-plate manipulator by batch pan to The preceding distance for promoting a batch pan, rake medicine manipulator fall, pull rake teeth to shakeout the priming crystallization in disk, push-plate machinery Hand promotes batch pan the distance of one batch pan, drug delivery disk manipulator lift the batch pan, deliver in pass-through box further along, machinery Hand retraction, transmission close, are sequentially completed all 9 and cross the fetching and delivering of pans, the transmission of batch pan.Follow-up work is weighed successively It is multiple to carry out.

6 --- it is antiknock compartment between entrucking.The operation room by the initiating explosive tray spread out automatically transmission be loaded on drying vehicle, Car be divided into above and below two layers, every time place 3 disks, a car load 6 disks.Capital equipment has the manipulator, automatic for picking and placeing batch pan Drying vehicle, rotary rail, main guide rail, drying vehicle transmission track etc..

The operating process completed in the room is：Taking plate manipulator taken out from pass-through box one equipped with priming batch pan, Return back to drying vehicle upper strata number one position, initiating explosive tray put down, the signal such as manipulator is returned back to before pass-through box, when Pass-through box is intraoral when having initiating explosive tray, window is opened, taking plate manipulator takes out the initiating explosive tray from pass-through box again, return Go to the position of drying vehicle upper strata second, put down initiating explosive tray, be sequentially completed the loading that third place is put.Then, then from No. four position of lower floor starts to load, retracts to original position until installing 6 initiating explosive trays, taking plate manipulator and await orders. Drying vehicle equipped with initiating explosive tray fix in orbit, the track turn round 90 °, by entrucking track and main orbit pair along cantilevered axle Be in line together, between now entrucking between the medicine that dries in the air between transmission window open, push-and-pull transfer robots by priming drying vehicle to Front transfer, entered between the medicine that dries in the air by transmitting window.

7 --- it is antiknock compartment between No. second medicine that dries in the air.Temperature control in the room is more than 40 DEG C, and major function is by disk The moisture content that middle priming contains volatilizees, dried as much as possible, to mitigate the live load of follow-up drying course.In order to improve life The utilization rate of efficiency and room, once dries two car primings in the room.Main device has：Two priming drying vehicles, Two groups of parallel connections and the drying vehicle frame that can be moved in parallel, main orbit.

8 --- number one dries in the air between medicine, is antiknock compartment.The function in the room is identical with No. 7 room, between parallel two are dried, Mainly for improving the relationship between productivity between production capacity and production efficiency, balance chemical combination and drying.Equally, the indoor temperature Degree control more than 40 DEG C, major function be the moisture content that will contain in priming after point disk volatilize as much as possible, it is follow-up to mitigate The live load of drying course.In order to improve the utilization rate of the rate of coming into force and room, two car primings are once dried in the room. Main device has：Two priming drying vehicles, two groups of the drying vehicle frames in parallel that can steadily move, main orbits.

9 --- it is antiknock compartment between No. four vacuum drying.Be placed with the room water-bath type vacuum drying chamber, main orbit, Transfer robots.Specific operation process is：Priming drying vehicle dries the defined time between the medicine that dries in the air or runs to transmission During program, the medicine mounted track that dries in the air is alignd with main orbit, the transmission window between the medicine that dries in the air between dry house is opened, push-and-pull transmission machinery Priming drying vehicle is entered dry house by hand to front transfer, by transmitting window, and now, the movable end of vacuum drying oven is in The position removed, baking oven inner orbit are in empty state, and after priming drying vehicle is delivered in baking oven, drying vehicle will be consolidated It is scheduled on the track in baking oven, the movable end of vacuum drying oven is sealed in by push-and-pull to reach, with fixing end fastening, by drying vehicle In baking oven, now open vacuum-pumping valve, be evacuated in baking oven, vacuum reaches -0.08MPa vacuum.Meanwhile, The chuck of baking oven starts to be passed through more than 90 DEG C of hot water, the temperature in baking oven is increased to more than 60 DEG C, maintains the vacuum With under temperature conditionss, by priming drying more than 40min, below 60min time, priming is oven-dried, contained moisture content Reach qualified level.Vacuum-pumping valve is closed, emptying valve is opened, the vacuum in baking oven is reached normal pressure, baking The fixing end of case and mobile terminal unclamp, the movable end of baking oven removed, by the cool about 2min in situ of the priming on drying vehicle. Now, transmission window between dry house and the medicine of a cold nature is opened, and push-and-pull transfer robots are by priming drying vehicle to front transfer, logical Transmission window is crossed to enter on the medicine of a cold nature frame between the medicine of a cold nature.

10 --- it is antiknock compartment between No. three vacuum drying.The function in the room and No. 9 room, setting, operating process It is identical.

11 --- it is antiknock compartment between No. second vacuum drying.The function in the room and No. 9 room, setting, operating process It is identical.

12 --- it is antiknock compartment between number one vacuum drying.The function in the room and No. 9 room, setting, operating process It is identical.

Only so repeating configuration 9,10,11, No. 12 dry houses, main balance drying course needs time length, needed with changing The contradiction of process compatible is closed, the production capacity of production line is improved.

13 --- it is antiknock compartment between No. second medicine of a cold nature.Temperature control in the room below 10 DEG C, major function be by The priming in the condition of high temperature is cooled to room temperature after drying, to ensure subsequent operation safety.In order to improve the rate of coming into force and room Utilization rate, two car primings are once dried in the room.Main device has：Two priming drying vehicles, two groups of parallel connections The drying vehicle frame that can steadily move, main orbit.

14 --- it is antiknock compartment between the number one medicine of a cold nature.The function in the room, setting, operating process are identical with No. 14 room It is identical.Between parallel two medicine of a cold natures, mainly for improving the production capacity between production capacity and production efficiency, balance chemical combination and drying Relation.

15 --- passage room, is antiknock compartment.This major function is to remove the initiating explosive tray for cooling normal temperature, be delivered to Pass-through box between the sieving of falling medicine mounted box is intraoral.

Capital equipment has：Priming drying vehicle, rotation main orbit, taking plate manipulator, drying vehicle transfer robots.

Primary operational process：Taking plate manipulator returns back to drying vehicle upper strata number one position, initiating explosive tray has been taken, machinery Hand returns back to before pass-through box and waits signal, is empty when pass-through box is intraoral, opens transmission window, taking plate manipulator by batch pan It is placed on the shelf for holding medicine in pass-through box, bounces back, transmitting close, machinery rotation to the position of drying vehicle upper strata second will Initiating explosive tray has taken, turned round before transmission window, opened transmission window, initiating explosive tray is placed into the intraoral shelf for holding medicine of pass-through box On room, retraction, shelf for holding medicine replace, manipulator protracts again, taken first in window empty batch pan, retraction, pass-through box Mouth is closed, manipulator puts back to empty batch pan on a number room of drying vehicle.It is repeated in 6 disk primings being all sent to transmission In window on shelf for holding medicine.6 empty batch pans are mounted with after the transmission of 6 disk primings is completed, on drying vehicle, the revolution of track road is carried 90 ° alignd with exit track, drying vehicle empty wagons transmission window is opened, empty drying vehicle and empty batch pan are delivered to the corridor in worker-house On pick up on frame.

16 --- fall between medicine, sieving, mounted box, vanning, be antiknock compartment.

Major function be by the priming after drying by screen cloth, by the priming of bulk tremble it is broken, by the priming knot after sieving Crystalline substance is attached in priming medicinal box special, is attached to the medicine box for filling priming in fortune medicine-chest.

Main device has：Pick and place batch pan manipulator, sieve basket, screen cloth, pick and place medicine box manipulator, the powder charge punch-out equipment in pass-through box Structure.

Primary operational process：Disc-taking machine tool hand is taken initiating explosive tray from the shelf for holding medicine in pass-through box, the transmission window that bounces back out, Close pass-through box, manipulator to be turned back to above priming sieve basket, be rotated by 90 ° along manipulator central shaft, by dried detonation Medicine is poured into sieve basket, and manipulator turns round, sends back to empty initiating explosive tray on the frame in pass-through box along original track, and bounce back out biography Pass window, close pass-through box, etc. next time fetch the instruction of batch pan.Make on the screen cloth that priming is poured into sieve basket, in vibrations Being crystallized to be trembled by screen cloth, big medicament block and the bolus in basket with lower priming broken by screen cloth, the crystallization of bulk and can not tremble Broken medicine block, which is trapped on screen cloth, to be separated, is fallen on along screen cloth inclined-plane guide groove in recycling box.Pass through the detonation after screen cloth The residence that sieve basket bottom is fallen under medicine crystallization is fallen in two detonation medicine boxs respectively into groove, by gathering sill, and a disk priming is just One group of two detonation medicine box of bottom are filled well, and the two connect medicine box and are placed in medicine box transfer robots.The disk priming is sieved After complete, medicine box transfer robots fall, turned round, extension, and two detonation medicine boxs of the group are sent on the intraoral medicine-chest frame of pass-through box Priming pass box in, medicine box transfer robots retraction, medicine-chest add by priming pass box turn round 180 °, make in pass box Empty medicine box to medicine box transfer robots, medicine box transfer robots extension, the empty detonation medicine boxs of one group two taken out in case, Manipulator bounces back, turned round, protracting again, upper lift, at the lower part outlet that empty medicine box is placed into sieving basket.Repeat aforesaid operations Process, you can complete the operation of next disk priming.

17 --- between medicine fetching case.There is fortune medicine work auxiliary operation in the room, when the green beacon lamp of transmission window is lighted, operate Work presses start button, and transmission window is opened, the medicine-chest for filling priming put forward, while will be equipped with the medicine-chest of sky medicine box It is placed on medicine-chest frame, presses button by close, the medicine-chest for filling priming is weighed up after gross mass, record, by behaviour Make code and detonation medicine-chest is delivered into detonation Drug Storage.

18 --- between arrangement.The empty drying vehicle and empty batch pan for being passed out production line automatically by underworker are pushed into the room, Floating medicine on cleaning drying vehicle, by the priming crystallization adhered on drying vehicle clean it up, clear disk of applying medicinal lotion or ointment, by packing paper and batch pan Clean it up, will after 6 sub- clean it ups of blank panel pile get up, be put on drying vehicle.It is pushed into the pass-through box on the outside of No. 5 room Before mouthful, start button is pressed, empty batch pan is placed on shelf for holding medicine, is got down empty batch pan in disk by programme-control is automatic； Docked before the transmission window that empty drying vehicle is pushed into outside No. 6 room and with alignment pin, press start button, will be by program control System is automatic to pull in empty drying vehicle in entrucking.The clear waste water containing priming produced of wiping is flowed in collecting vessel, logical daily Cross vacuum washes is transferred in mother liquor tank, concentration is destroyed.Capital equipment and device in this room：Pure water Storage tank, kitchen sink, wastewater collection pond.

19 --- between cooling water prepares.The major function in the room：Prepare the recirculated water of cooling for crystallisation by cooling combination apparatus, By Automatic-cooling system, by the running water in cooling water tank be cooled to less than 10 DEG C it is standby.Capital equipment：Cold medium compressor, Cooling water tank, storage water tank, pipeline pump, ventilation blower.

20 --- between drying vehicle storage.The major function in the room：Store empty drying vehicle.Capital equipment and device：Drying Car track frame, drying vehicle, can store 16 drying vehicles.

21 --- between switch board.The major function in the room：Serialization is automated into all control nodes on priming production line Weak electric signal, communication signal, power switch, air circuit breaker all concentrate in the switch board in the room, realize that flame proof is prevented Quick-fried purpose.

22 --- central control room.The major function in the room：Monitoring, control, on duty of operating personnel, by video, Audio surveillance completely the course of work of each operation room, monitoring indicating fault situation, to assign the life fixed a breakdown, straighforward operation each Station.It is main to set and device：Televimonitor, hard disc recorder, central processing computer.

23 --- pure water treatment room.The major function in the room is to meet the pure water of use requirement completely to prepare and providing, Aquifer yield is in more than 0.3t/h.Capital equipment：Pellicle purifier, middle water storage tank, pure water storage tank, automatic water pipeline pump.

24 --- between raw material storage.Alkali solid material required for main storage priming production.

25 --- total switchgear house.Major function：The power that priming production line distributes 220V and 380V is automated for serialization Electricity.Capital equipment：Power distribution cabinet, ventilation unit.

26 --- between air compressor or between gas tank.Major function：Pressure is provided for serialization automation priming production line Power is below 0.8MPa compressed air, and the energy is provided for all pneumatic function elements.Capital equipment：Air compressor, storage Gas tank, or gas tank is only set, for storing the compressed air that central supply station is sent.

27 --- between vavuum pump.Major function：The room for placing vavuum pump is concentrated, is serialization automation priming production line Vacuum power is provided, suction filtration feed liquid, lifting feed liquid, suction filtration priming product, vacuum drying chamber are vacuumized.Capital equipment： The water-ring vacuum pump of motor driving.

28 --- heat exchange powerhouse.Major function：Heating power, more than 90 DEG C are provided for serialization automation priming production line Hot water supplies vacuum drying box hot bath, and 80 DEG C or so of hot water is for measurer, liquid tank, combination apparatus, ager, dry in the air medicine Room heating is used.Capital equipment：Tubular heat exchanger, hot water storgae, electric heating constant temperature tank, hot water pipeline pump.

By taking second of arrangement as an example, the operation logic process description of all fronts is as follows：

1 feed liquid process for preparation：Human assistance is operated, raw material, dispensing water as required for the priming kind produced Amount by technological procedure requirements weighing and measure, be added in dosage bunker, heat temperature raising, by dissolution of raw material in water, put to filtering Solid impurity is filtered to remove in storage tank, filtrate is collected, is lifted feed liquid into storage tank, with constant volume measurement measuring of groove with vacuum Feed liquid required for unification batch priming.In the case of one, the feed liquid required for production 20kg~40kg priming products is once prepared.

The metering of 2 feed liquids, charging, chemical combination process：The first feed liquid is disposably all put into chemical combination and makees bottom liquid, be heated to Between 50 DEG C~80 DEG C of reaction temperature；Second of feed liquid follow procedure control is added in combination apparatus again, general control feed time Between 15min~25min；After second of feed liquid is added, continue to react 1min.Then, discharge valve is opened, will be reacted All reaction mixtures in device are disposably all transferred in insulation curing combination apparatus, and blowing process lasts about 1min.Blowing is complete Finish, close discharge valve, repeat aforesaid operations, the process repeats the operating process always, until the whole for completing on duty is raw Production process.

3 curing crystallization process：Continue to stir anti-between whole mixed liquors that transfer comes above-mentioned 2) are maintained into 50 DEG C~80 DEG C 20min should be crystallized with curing.Then, the reaction mixture is disposably all transferred in crystallisation by cooling combination apparatus, blowing mistake Journey holds renewed treaty 1min.Blowing finishes, closes discharge valve, repeats aforesaid operations, and the process repeats the operating process always, Until completing overall production process on duty.

4 crystallisation by cooling processes：By above-mentioned whole mixed liquors for coming of 3) transfer decrease temperature crystalline, crystallisation by cooling reaction under agitation 10 DEG C or so of cooling water is passed through in device chuck, when reaction solution stirring is cooled to less than 30 DEG C or stirring reaction reaches 20min Afterwards, the reaction mixture is disposably all put into portioning filter, blowing process lasts about 1min.Blowing is finished, closed Discharge valve, repeats aforesaid operations, and the process repeats the operating process always, until completing overall production process on duty.

5 portionings, filtering, washing, dehydration：The guiding gutter one that the above-mentioned whole mixed liquors 3) released are passed through into current divider Secondary whole is put into 9 filter tunnels, bottom is evacuated in vacuum buffer groove with vacuum suction 2min, by reaction mother liquor, put automatically Into mother liquor collecting tank.From the top of portioning device spray pure water, pan was flowed to by guiding gutter in soaked detonation in pan Medicine crystallization, bottom are evacuated in vacuum buffer groove with vacuum suction 1min, by cleaning solution, put automatically into mother liquor collecting tank；Again from The top of portioning device sprays pure water, the priming crystallization soaked in pan, bottom vacuum was flowed in pan by guiding gutter 1min is aspirated, cleaning solution is evacuated in vacuum buffer groove, put automatically into mother liquor collecting tank；Anhydrous second is sprayed from the top of portioning device Alcohol, flowed in pan by guiding gutter the priming crystallization soaked in pan, bottom and be sucked by vacuum 2min, by cleaning solution It is evacuated in vacuum buffer groove, puts automatically into mother liquor collecting tank.

6 took pan, transmission, fall medicine, stand disk, rake, pass disk：Took pan box machinery to be equipped with adjacent one to wash Wash the priming drained and cross pan and pick up, remove fixed position, this is crossed to pan delivering to the top of fall box stand disk device, machinery edge Central shaft rotates 180 °, the priming crossed in pan is poured on the guider above batch pan, manipulator retraction, by empty medicine Box is back on the position of pickup, manipulator bounces back, load 40 ° of the turntable rotation of medicine box, another is equipped with into what priming was crystallized Medicine box is delivered on the adjacent position of the manipulator, repeats aforesaid operations, and the process is with 1min time.The priming fallen down Crystallize in the batch pan for relatively evenly dropping down onto bottom along guider, batch pan is pushed ahead the distance of a batch pan, harrowed by push-plate manipulator Medicine manipulator falls, pulls rake teeth by the priming crystallization in disk is shakeout, push-plate manipulator promotes batch pan one batch pan further along Distance, drug delivery disk manipulator the batch pan is lifted, delivered in pass-through box, manipulator retraction.All 9 filterings are completed with this The the fetching and delivering of medicine box, the transmission of batch pan.

7 initiating explosive tray entruckings：Taking plate manipulator takes out a plate equipped with priming from pass-through box, returns back to drying Car upper strata number one position, initiating explosive tray put down, the signal such as manipulator is returned back to before pass-through box, when having had in window During quick-fried medicine, window is opened, taking plate manipulator takes out the plate of the priming from pass-through box again, return back to drying vehicle upper strata the No. two positions, be sequentially completed the loading that third place is put, then, then since No. four position of lower floor rotation, up to installing 6 Disk priming, taking plate manipulator retract to original position and awaited orders.Dolly equipped with priming fixes in orbit, the track edge The axle of cantilever turn round 90 °, by carry track road alignd with main orbit be in line, between now entrucking between the medicine that dries in the air between transmission window beat Open, push-and-pull manipulator enters priming drying vehicle between the medicine that dries in the air to front transfer, by transmitting window.

8 dry in the air medicine process

8.1 align drying vehicle with main orbit, and push-and-pull manipulator will be loaded with the drying vehicle of priming to front transfer.

8.2 initial programs：The later all stations of this medicine that dries in the air all are empty, each transmission windows all in open mode, manipulator By the first car priming is directly delivered to the number one vacuum drying box of rearmost end, dry in the air medicine 15min in this position.Then, into certainly Dynamic drying procedure.

8.3 now, and the station between medicine and No. second baking oven that dries in the air all is empty, transmission window all in open mode, manipulator By the second car priming is directly delivered to No. second vacuum drying box of rearmost end, dry in the air medicine 15min in this position.Then, baking oven from It is dynamic to close, vacuumize, leading to heating water, keeping temperature drying 45min.

8.4 now, and the station between medicine and No. three baking oven that dries in the air all is empty, transmission window all in open mode, manipulator By the 3rd car priming is directly delivered to No. three vacuum drying box of rearmost end, dry in the air medicine 15min in this position.Then, baking oven from It is dynamic to close, vacuumize, leading to heating water, keeping temperature drying 45min.

8.5 now, and the station between medicine and No. four baking oven that dries in the air all is empty, transmission window all in open mode, manipulator By the 4th car priming is directly delivered to No. four vacuum drying box of rearmost end, dry in the air medicine 15min in this position.Then, baking oven from It is dynamic to close, vacuumize, leading to heating water, keeping temperature drying 45min.

8.6 now, and the transmission window of four dry houses is all in closed state, and the 5th car priming is transferred between No. 1 medicine that dries in the air On No. 1 track, dried in the air medicine state in room temperature；The medicine track that dries in the air is conjugated；

8.7 the 6th car primings produced are transferred between No. 1 medicine that dries in the air on No. 2 track, are dried in the air medicine state in room temperature；

8.8 the 7th car primings produced are transferred between No. 2 medicine that dries in the air on No. 1 track, are dried in the air medicine state in room temperature；

8.9 the 8th car primings produced are transferred between No. 2 medicine that dries in the air on No. 2 track, are dried in the air medicine state in room temperature；

8.10 now, and all with completely between the medicine that dries in the air, until being shifted to drying baker, this four cars medicine has all reached the requirement of flash-off time .The 8th car priming produced is stored on the track between entrucking.

8.11 follow-up medicine programs of drying in the air：Into after follow-up work program, it is above-mentioned be stored in the four drying vehicle medicines dried in the air on medicine frame will once It is fully transferred in four drying bakers below, all framves that dry all are available, continues to receive follow-up by 8.6 to 8.9 program The priming drying vehicle produced enters medicine program of drying in the air.

9 automation drying processes

9.1 number one drying vehicles are in the position of number one baking oven, after 15min is dried, baking oven closes, vacuumizes automatically, Logical heating water, keeping temperature drying 40min~50min.After the completion of baking oven automatic buckling, beginning vacuumizing and drying, continuous drying, Baking oven eliminates negative pressure state automatically, automatically turn on baking oven, baking oven mobile terminal automatically pushes open, drying vehicle is exposed to room temperature condition Under, drying vehicle medicine of a cold nature 2min in the original location.Then, passage room, medicine of a cold nature 10min in orbit are automatically passed to, subsequently into rise Quick-fried batch pan transmission procedure.Now, opened between number one baking oven between the number one medicine of a cold nature and by insertion, transmission window.

9.2 No. second drying vehicles are in the position of No. second baking oven, after 15min is dried, baking oven closes, vacuumizes automatically, Logical heating water, keeping temperature drying 40min~50min.After the completion of baking oven automatic buckling, beginning vacuumizing and drying, continuous drying, Baking oven eliminates negative pressure state automatically, automatically turn on baking oven, baking oven mobile terminal automatically pushes open, drying vehicle is exposed to room temperature condition Under, drying vehicle medicine of a cold nature 2min in the original location.Then, it is automatic by between number one dry house and No. second medicine of a cold nature, drying vehicle is transmitted On to the number one medicine of a cold nature frame between the number one medicine of a cold nature on track, medicine of a cold nature 10min at ambient temperature.Then, the letter of passage room is waited Number, drying vehicle is delivered to passage room, into initiating explosive tray transmission procedure again.Now, to the number one medicine of a cold nature between No. second baking oven Between between and pass through insertion, transmission window open.

9.3 No. three drying vehicles are in the position of No. three baking oven, after 15min is dried, baking oven closes, vacuumizes automatically, Logical heating water, keeping temperature drying 40min~50min.After the completion of baking oven automatic buckling, beginning vacuumizing and drying, continuous drying, Baking oven eliminates negative pressure state automatically, automatically turn on baking oven, baking oven mobile terminal automatically pushes open, drying vehicle is exposed to room temperature condition Under, drying vehicle medicine of a cold nature 2min in the original location.Then, automatically by between No. second dry house and No. second medicine of a cold nature, drying vehicle is transmitted On to No. second medicine of a cold nature frame between the number one medicine of a cold nature on track, at ambient temperature between medicine of a cold nature 10min, the number one medicine of a cold nature with second Close between number medicine of a cold nature.Then, wait passage room signal, again by drying vehicle be delivered to passage room, into initiating explosive tray pass Pass program.Now, being opened by insertion, transmission window between No. second medicine of a cold nature between No. three baking oven.

9.4 No. four drying vehicles are in the position of No. four baking oven, after 15min is dried, baking oven closes, vacuumizes automatically, Logical heating water, keeping temperature drying 40min~50min.After the completion of baking oven automatic buckling, beginning vacuumizing and drying, continuous drying, Baking oven eliminates negative pressure state automatically, automatically turn on baking oven, baking oven mobile terminal automatically pushes open, drying vehicle is exposed to room temperature condition Under, drying vehicle medicine of a cold nature 2min in the original location.Then, automatically by No. three dry house and between No. second medicine of a cold nature, by drying vehicle Be delivered on the number one medicine of a cold nature frame between No. second medicine of a cold nature on track, medicine of a cold nature 10min at ambient temperature.The now number one medicine of a cold nature Between track it is entirely empty, opened between the number one medicine of a cold nature with the transmission window of passage room.Then, the signal of passage room is waited, again by the 3rd Drying vehicle is delivered to passage room, into initiating explosive tray transmission procedure.Now, between number one dry house between No. four baking oven Opened by insertion, transmission window.

9.5 follow-up drying procedures：Now, the medicine car in number one to No. four priming car dry house all drying, the medicine of a cold nature, And be delivered between the medicine of a cold nature, No. four to the full insertion of transmission channels between number one drying baker, transmission window be both powered on.

5th drying vehicle is directly delivered to number one drying baker, is directly entered drying procedure by 9.6；6th drying vehicle is directly transmitted To No. second drying baker, it is directly entered drying procedure；7th drying vehicle is directly delivered to No. three drying baker, is directly entered drying Program；8th drying vehicle is directly delivered to No. four drying baker, is directly entered drying procedure.Repeat, completed all according to this Drying course.

9.7 are repeated in 9.1 to 9.4 program, complete whole drying courses.

10 medicine of a cold nature processes

10.1 every drying vehicles are in baking oven medicine of a cold nature 2min in situ.

10.2 No. 1 drying vehicles are directly delivered to passage room medicine of a cold nature 10min again.Then, into transmission batch pan program.

10.3 No. 2 drying vehicles are delivered between No. 1 medicine of a cold nature on No. 1 medicine of a cold nature frame, and medicine of a cold nature frame becomes track, No. 2 track alignments and passed Pass main orbit.Make No. 2 drying vehicle in this medicine of a cold nature 10min.Then, into transmission batch pan program.

10.4 No. 3 drying vehicles are delivered between No. 1 medicine of a cold nature on No. 2 medicine of a cold nature frame, medicine of a cold nature 10min.Then, the medicine of a cold nature frame displacement, Make No. 2 drying vehicle alignment main orbit, then, into transmission batch pan program.

10.5 No. 4 drying vehicles are delivered between No. 2 medicine of a cold natures on No. 1 medicine of a cold nature frame, alignment main orbit, medicine of a cold nature 10min then, Into transmission batch pan program.

10.6 follow-up medicine of a cold nature processes repeat 10.2 to 10.5 operation.Whole production processes are completed according to this.

The automatic transmittance process of 11 initiating explosive trays

11.1 passage rooms transmit track of changing trains or buses and alignd with main orbit.

11.2 No. 1 drying vehicles are directly delivered to passage room and changed trains or buses track, after medicine of a cold nature 10min, and transmission batch pan manipulator starts to take By number one batch pan, it is fed directly to the upper empty frame between sieving in pass-through box, manipulator retraction, transmits close, manipulator Go to drying vehicle and fetch No. second batch pan.

11.3 deliver to the upper empty frame position between sieving in pass-through box, manipulator retraction, decline displacement, fetch out shelf for holding medicine in pass-through box On empty batch pan, manipulator retraction, transmission close, manipulator go to drying vehicle, empty batch pan be placed into the of drying vehicle On a number position, conjugate, fetch No. three batch pan.

11.4 deliver to the upper empty frame position between sieving in pass-through box, manipulator retraction, decline displacement, fetch out shelf for holding medicine in pass-through box On empty batch pan, manipulator retraction, transmission close, manipulator go to drying vehicle, empty batch pan be placed into the of drying vehicle On No. two positions, conjugate, fetch No. four batch pan.

11.5 deliver to the upper empty frame position between sieving in pass-through box, manipulator retraction, decline displacement, fetch out shelf for holding medicine in pass-through box On empty batch pan, manipulator retraction, transmission close, manipulator go to drying vehicle, empty batch pan be placed into the of drying vehicle On third place, conjugate, fetch No. five batch pan.

11.6 deliver to the upper empty frame position between sieving in pass-through box, manipulator retraction, decline displacement, fetch out shelf for holding medicine in pass-through box On empty batch pan, manipulator retraction, transmission close, manipulator go to drying vehicle, empty batch pan be placed into the of drying vehicle On No. four positions, conjugate, fetch No. six batch pan.

11.7 deliver to the upper empty frame position between sieving in pass-through box, manipulator retraction, decline displacement, fetch out shelf for holding medicine in pass-through box On empty batch pan, manipulator retraction, transmission close, manipulator go to drying vehicle, empty batch pan be placed into the of drying vehicle On No. five positions.

11.8 manipulators return to transmission window, decline displacement, fetch out empty batch pan in pass-through box on shelf for holding medicine, manipulator retraction, Transmission close, manipulator go to drying vehicle, are placed into empty batch pan on No. six position of drying vehicle.

11.9 this enter, the room does not have priming, without danger, change trains or buses track when rotation, with main orbit it is in 90 °, with to unofficial biography The drying vehicle for sending the track alignment of drying vehicle, transmission window to open, be loaded with sky batch pan automatically passes out passage room, reaches worker-house Picking up on frame on corridor, provide instruction modulating signal, auxiliary operation work car is connect into away arrangement.

After 11.10 drying vehicles are passed out when changing trains or buses track, track convolution of changing trains or buses is alignd with main orbit, empty drying vehicle transmission close, The drying vehicle transmission window for carrying priming is opened, and next drying vehicle is automatically passed to change trains or buses on track.

11.11 repeat 11.1 to 11.10 operating process, until completing whole production tasks.

12 fall medicine, sieving, mounted box, case, pick and place medicine-chest process

12.1 batch pans transmission window is opened, taking plate manipulator reaches support in window, pick up be equipped with priming batch pan, time Contracting, transmission close.

12.2 taking plate manipulators return to above sieving basket, are rotated by 90 ° along itself axle, under shock effect by the detonation in batch pan Medicine is all poured on the screen cloth in sieve basket.

12.3 taking plate manipulators turn round into horizontal state, move ahead, transmission window is opened, the support room that is put into batch pan in window, Retraction, transmission close, etc. a disk to be removed signal.

12.4 two detonation medicine boxs are taken by medicine taking box machinery to be placed on the medicine outlet of sieve basket bottom, in shock effect lower screen cloth On priming crystallization by by sieve aperture, fall on the sieve basket of bottom, along basket wall flow to detonate medicine box in, can not be by sieve aperture Big medicine block rolls down to big medicine block along screen cloth and received in box.

12.5 box taking machine tool hands fill two in the medicine-chest that priming declines, turns round, is sent in dress pass-through box, manipulator is disclosed, Retraction, 180 ° of medicine-chest revolution, two empty medicine boxs to manipulator, manipulator extension, by two empty kit of parts to picking up, being turned back to Basket bottom, upper lift and medicine outlet are sieved to tight.

12.6 repeat 12.4 operating process.

12.7 two fill priming decline, turn round, be sent to dress pass-through box in medicine-chest in, manipulator disclose, bounce back, medicine-chest Fill, pass-through box is closed, indicator lamp is bright on the outside of pass-through box.

12.8 fortune medicine works press between getting it filled take case button, pass-through box open, fortune medicine work by fill priming medicine-chest take out, will The medicine-chest for filling sky medicine box is placed on vanning frame, closes pass-through box.

12.9 repeat 12.1 to 12.8 operation automatically again, until completing overall production process.

The medicine-chest of the dress priming of taking-up is placed on table scale by 12.10 fortune medicine works together to be weighed gross mass, writes label, has been sent to Quick-fried Drug Storage.

12.11 repeat above-mentioned work, until completing whole production tasks.

Repeat 1 to 12 all operationss, complete whole production tasks.

13 drying vehicles are arranged

13.1 carry out manual operations by auxiliary operation work

13.2 when indicator lamp is green between sieving, and operative employee initially enters sieving, arranges the bulk medicine on screen cloth, is arranged Enter to reclaim in medicine box.When recovery medicine, which is closed, is bordering on full box, empty medicine box is removed by hand, an empty medicine box is changed again.By bulk medicine Box, which is concentrated, to be placed, and is prepared recrystallization recovery and is used.The floating medicine clean it up on basket will be sieved again, it is a large amount of on the packing paper of basket bottom by sieving Spread pesticides and be put on the pallet of falling medicine, by ground floating medicine clean it up.Walk out between sieving, room door is shut.

13.3 hand-guideds, the medicine on pallet is poured into sieve basket, medicine box, medicine box vanning is put into.

13.4 operative employees again by the drying vehicle on passage room outside corridor and empty batch pan push-and-pull between wash paper, will be on packing paper it is floating Medicine clean out and hang up dry, the floating medicine on batch pan is cleaned out and pads clean dry packing paper, the floating medicine cleaning on drying vehicle Totally and the batch pan for having padded paper is set.

13.5 operative employees open door between sieving mounted box antiknock, enter in room the scattered medicine and floating medicine observed and clear up under sieve basket, take The sampling box of priming is housed on lower sieve basket, and changes an empty sampling box.

13.6 push to the drying vehicle put in order at the transmission window on the outside of No. 6 room and with steady pin to connecting, pressing certainly Dynamic transmission button, the next circulation of startup.

13.7 will complete packing paper on car have batch pan pile, the pass-through box being placed on the outside of No. 5 room intraoral, shuts transmission outside window Side transfer gate, presses automatic transmission button, starts next circulation.

The present invention key technology be：

1) serialization automation priming production line and technical process arrangement

Serialization automation priming production-line technique arrangement must assure that production line can be reliably achieved production process, it is complete The antiknock explosion-proof security of process, operating process are most short, satisfaction produces required equipment and the installation of device and use requirement, each work Orthofunction between sequence is with matching, the matching of mass transport process, the matching of security process.Therefore, technology arrangement side of the invention The key technology of formula and technical process starts from raw material preparation, feed liquid filtering, feed liquid storage, feed liquid metering, material by priming Liquid adds combination apparatus, priming chemical combination, priming curing, priming crystallization, priming discharging, priming filtering, priming Water washing, the washing of priming ethanol, the stand of falling disk disk, batch pan dress drying vehicle, the medicine that dries in the air, automatic vacuum drying, the medicine of a cold nature, batch pan are passed Pass, medicine, sieving, mounted box, each operation to the priming production process including terminating of casing all have been included in the present invention's Among design, serialization automated production mode and production process to each in-process have carried out detailed design, pass through machine The operation of tool hand, realizes man-machine isolation completely, and scene improves the essential safety of priming production process without human users Property.

Above-mentioned each operation is all arranged in the same side in worker-house, the adjacent straight line insertion arrangement of each operation, each danger since chemical combination process Dangerous section's sequence is all in interior between respective antiknock, and priming drying vehicle is the antiknock by separating adjacent inter process between each operation What the antiknock window opened up on wall by design requirement was transmitted automatically, it is not necessary to which artificial stroller is transmitted from transport corridor, is realized Priming produces the complete man-machine isolation of overall process, it is ensured that the security of production process.

Therefore, priming charging of the present invention, chemical combination, curing, crystallization and discharge process use explosion-proof type serialization certainly Dynamicization is operated, and the chemical combination of priming manufacturing process, curing, three continuous processes of crystallization are respectively placed in different reactors Complete, realize every crowd of production 6kg to the small lots of 10kg primings, the serialization side that each operation is connected, the operating time is parallel Formula, realizes that split run production priming reaches 150kg production capacity, improves production efficiency.

2) drying vehicle of priming is transported

In order to realize the automation transmission of initiating explosive tray, improve the transmission capacity and drying amount of single, the present invention proposes a kind of double-deck knot Structure, bottom are equipped with without friction, collisionless, the drying vehicle for not producing spark wheel, still contain a certain amount of moisture content after suction filtration dehydration Priming crystallization be just placed in the batch pan for be lined with paper be loaded on drying vehicle, complete with making priming geo-stationary entrucking process, Dry in the air medicine process, drying course, medicine of a cold nature process and the transmittance process respectively walked.The batch pan used be papery, wooden or aluminum product, Brown paper is lined with batch pan, initiating explosive tray is placed into the upper and lower of drying vehicle, proposition of the invention automatically by manipulator Be to place 6 disk primings altogether in two layers up and down each 3 disks, a car placed.

3) initiating explosive tray automatic loading and wagon shaker hand and operation sequence

The mode that proposition of the present invention once loads 6 disk primings with drying vehicle is transmitted and dried, and improves operating efficiency, drop Low operational danger, the safety transmission for realizing priming.Therefore, initiating explosive tray automatic loading and wagon shaker hand and operation Program is just into one of key technology of the present invention.

First, the priming for draining point disk is attached on drying vehicle.In the entrucking, by taking plate loading manipulator from pass-through box It is middle to take out the initiating explosive tray shakeout, it is turned back to before drying vehicle, the first disk priming is put into a position of the last layer of drying vehicle On.Same mode, the second disk priming is put on No. two positions of the last layer of drying vehicle, the 3rd disk priming is put into The third place of the last layer of drying vehicle is put.Then, the 4th disk priming is put on a position of next floor of drying vehicle, 5th disk priming is put on No. two positions of next floor of drying vehicle, the 6th disk priming is put into next layer of drying vehicle Third place is put.Drying vehicle is loaded with after 6 initiating explosive trays, drying vehicle transmission track frame rotates, is in line with main orbit, Between entrucking between the medicine that dries in the air between antiknock transmission window open, drying vehicle is sent to by pushing machinery hand in the antiknock of medicine process of drying in the air.

Finally, the cool initiating explosive tray to room temperature after drying is unloaded down and is sent to sieving mounted box process.In passage room of unloading, by unloading Car manipulator first takes out initiating explosive tray from number position of next floor of drying vehicle, delivered on the empty shelf for holding medicine between sieving in pass-through box； Manipulator returns drying vehicle, the initiating explosive tray taken on No. two position of next floor of drying vehicle, delivered in the pass-through box between sieving On empty shelf for holding medicine, while the empty batch pan retract, conjugate, taking out on shelf for holding medicine, sends back on number position of the next floor of drying vehicle； Initiating explosive tray that one layer of third place put is removed again, delivered on the blank panel frame in the pass-through box between sieving, meanwhile, take out shelf for holding medicine On empty batch pan, send back on No. two position of the next floor of drying vehicle；The initiating explosive tray on number position of floor one by one is taken again, delivered to On blank panel frame in pass-through box between sieve, meanwhile, the empty batch pan on shelf for holding medicine is taken out, next layer of third place of drying vehicle is sent back to and puts On；The initiating explosive tray on No. two positions of last layer is taken again, delivered on the blank panel frame in the pass-through box between sieving, meanwhile, take out medicine Empty batch pan on plate rail, sends back on number position of drying vehicle last layer；Initiating explosive tray that last layer third place puts is taken again, sent On the blank panel frame in pass-through box between sieving, meanwhile, the empty batch pan on shelf for holding medicine is taken out, drying vehicle last layer two is sent back to On position；It is back to inside and outside the pass-through box between sieving, waits the empty batch pan on shelf for holding medicine to be removed, send back to drying vehicle last layer three On number position.

Then, drying vehicle is loaded with after 6 blank panels, by the rotation of drying vehicle transmission track frame, with sending out track alignment, passage room Pass-through box between corridor is opened, and is passed out to drying vehicle on corridor by pushing machinery hand.

4) priming automated production transfer mode and transmission operation sequence

The priming drying vehicle of the present invention, slides along " [" and "] " track in the way of the present invention and advances.When drying vehicle fills 6 After disk, the rotation of entrucking track frame is in line with main orbit, and the transmission window between two antiknock division walls is opened, by pushing machinery hand Drying vehicle is sent in the antiknock of medicine process of drying in the air, makes priming interior completion about 20min here dry process.Then, dry Between steel antiknock window follow procedure on antiknock wall open, the automatic vacuum drying baker for being sent into drying vehicle in dry house by pushing machinery hand It is interior.

It is put between the medicine that dries in the air and the procedure stipulation of drying baker is：First drying vehicle on duty produced, will be directly delivered to number one baking On the support of dry case, first dry 20min, then fasten again drying baker, vacuumize, heating, drying 40min, in the original location the medicine of a cold nature drop Warm 2min, then it is delivered to passage room preparation sieving mounted box.

During this period, the second drying vehicle produced, will be directly delivered on the support of No. second drying baker, first dries 20min, Then fasten again drying baker, vacuumize, heating, drying 40min, in the original location the medicine of a cold nature cooling 2min.Now, the master of drying vehicle transmission Track upstream end has been blocked, and sending out end does not have obstacle all the way smoothly, then be delivered to passage room preparation transmission batch pan.

During this period, the 3rd drying vehicle produced, will be directly delivered on the support of No. three drying baker, first dries 20min, Then fasten again drying baker, vacuumize, heating, drying 40min, in the original location the medicine of a cold nature cooling 10min.Now, drying vehicle is transmitted Main orbit upstream end has been blocked, and sending out end does not have obstacle all the way smoothly, then be delivered between the medicine of a cold nature 2min that cools, and waits passage room The instruction being available, is then delivered to passage room and prepares transmission batch pan again.

During this period, the 4th drying vehicle produced, will be directly delivered on the support of No. four drying baker, first dries 20min, Then fasten again drying baker, vacuumize, heating, drying 40min, in the original location the medicine of a cold nature cooling 2min.Now, the master of drying vehicle transmission Track upstream end has been blocked, and sending out end does not have obstacle smoothly, drying vehicle can be delivered to between the medicine of a cold nature 10min that cools again all the way, etc. The instruction that passage room is available is treated, passage room is then delivered to again and prepares transmission batch pan.

During this period, the 5th to the 8th drying vehicle priming produced, by be respectively passed to number one and second dry in the air between medicine four Dry, await orders on the individual medicine frame that dries in the air.After until the priming after being dried in No. four drying baker passes out, main orbit now is complete Line insertion.No. five car is sent to number one drying baker and is directly entered vacuum drying program, No. six car is sent to No. second drying baker Vacuum drying program is directly entered, No. seven car is sent into No. three drying baker is directly entered vacuum drying program, and No. eight car is sent Vacuum drying program is directly entered to No. four drying baker.Priming in each drying baker all dries 40min, all medicine of a cold nature in the original location 2min.Then, No. five drying vehicle is directly delivered in passage room, starts transmission batch pan after the medicine 5min that dries in the air again, performs sieving dress On box-packed case program, the number one medicine of a cold nature frame that No. six drying vehicle is directly delivered between first medicine of a cold nature, No. seven drying vehicle directly transmit On to No. second medicine of a cold nature frame between the number one medicine of a cold nature, No. eight drying vehicle be directly delivered on the number one medicine of a cold nature frame between second medicine of a cold nature, And stand ready be delivered to passage room carry out transmission batch pan program.Subsequent production process all repeats this working procedure.

5) serialization automation priming production transmission track

Because priming proposed by the present invention is placed on papery or wooden or aluminum packing paper batch pan, is put on drying vehicle, passes through again Manipulator is come what is transmitted, and all transmittance process all without manually operation and are intervened.It is therefore desirable to transmittance process must steadily, can Lean on, accurately, in place.In order to realize this target, the present invention is proposed makees rail body by aluminium section bar, particularly with " [" type and "] " section bar material constitutes one group of track, and the wheel on drying vehicle is clipped in the centre of " [" type and "] " section bar, it is ensured that drying vehicle is being passed Do not produced during passing derailing, overturn, it is crooked, block the unexpected phenomenon such as can not advance.Simultaneously as have multigroup wheel on drying vehicle, When drying vehicle first advances to track breakpoint, other wheels are still fixed in the middle of profiled rail, it is ensured that drying vehicle traveling process Steadily.

In view of picking and placeing batch pan technique, entrucking, transmission, between the priming point disk entrucking, priming take disk fall medicine filtering between, One end of track is fixed in rotating shaft, and the other end is free end, can be needed the action with procedure stipulation according to technique, be made the part 90 degree of orbit rotation, 180 degree, with meet drying vehicle transmission, pick and place batch pan the need for.

The machinery coupling sliding block that the transmission power of drying vehicle in orbit comes from Rodless cylinder fixed on track, the cylinder is being pressed Slided along its length by regulated procedure in the presence of contracting air, fixed mechanical shifting fork will promote drying vehicle forward on the sliding block Advance, stroke is length and program by setting to meet delivery request.

6) the automatic portioning filtering and washing technology mode of priming

Priming chemical combination curing crystallization process is finished, and the priming crystallization of formation is mixed with reaction mother liquor, it is necessary to used The method of filter crystallizes priming mother liquor and the adhesion that separates and will be sticked to pure water on priming crystalline particle with mother liquor Thing washing is removed, and finally absolute ethyl alcohol as far as possible removes moisture content again.Because the number of operations of this process is more, process length, technique Complexity is high, realizes that the difficulty of automation is very big.Solution proposed by the present invention：

Disposable to be all released in production filter, the priming structure and mother liquor mixture of outflow are more uniform by its by distributor Ground scatter, flowed to along the guiding gutter on distributor in 9 filter tunnels of dispenser bottom, the mistake that mother liquor passes through funnel bottom Filter screen is extracted into mother liquor surge tank, and priming crystalline solid is stayed in distributor and filter tunnel, and the dose in every funnel is about 1kg. Then, pure water is sprayed by the shower nozzle above distributor, priming crystallizing and washing is drained, washs secondary with this, same Mode once, is drained with absolute ethanol washing, is then sent to stand disk process.

Pass through said process, you can complete the separation of priming crystallization, washing, dehydration, quantitatively divide disk process.

7) priming serialization automation stoving process mode

The present invention proposes two kinds of schemes using drying vehicle first drying 6kg primings：Scheme (1) uses normal pressure drying road type water Drying baker is bathed, drying casing is placed on support, wherein side is light explosion relief structure, guide rail built in baking oven is used to dry with outside The fixation guide rail of dry trolley travelling connects, and the oven door of termination both sides can be opened and closed freely, the turnover of convenient drying dolly. Oven temperature is automatically controlled by heating water bath, is heated evenly, and is had a safety feature, and drying efficiency is high, is easy to implement priming production Automation.Scheme (2) uses water-bath automatic vacuum drying mode, and vacuum drying casing is the mode being divided into two, by removable Fixation lid two parts of dynamic casing and belt track frame are constituted.When needing drying vehicle sending into baking oven, will dry casing automatically first can Movable part is outwards pushed open, and track frame is exposed, transfer robots will be equipped with initiating explosive tray drying vehicle be sent to drying baker consolidate In fixed track frame, casing moveable part then will be dried again to lira, makes movable part and fixes cover buckle altogether, then lead to Cross control system automatic opening to vacuumize, drying baker movable part is sucked automatically with fixed lid, then in drying baker crustless sandwich is led to More than 90 DEG C of hot water is crossed, passes through flash baking under the heating of heat radiation, thermal convection current and heat exchange pattern and vacuumized conditions.

8) priming sieves mounted box vanning technology automatically

In the present invention using manipulator by after drying batch pan send into pass-through box in, the automatic taking plate of taking plate, return to sieve basket above, Axle rotation 180 degree by initiating explosive tray along manipulator was poured into ethmoidal infundibulum, accelerated priming particle to lead to automatically by air-flow vibrations Screen cloth is crossed, is flowed into by the guide cylinder of device in medicine box, it is impossible in the recovery medicine box that bottom is flowed to by the bulky grain of screen cloth. Two boxes will be divided into by sieving the guide cylinder of basket by a disk medicament, per box about 0.5kg.The medicine box for installing medicine is filled by manipulator from sieving Bottom set is moved down, turned round again in the medicine-chest being sent in pass-through box.

Compared with existing priming production line and process unit arrangement, serialization automation priming production line of the invention and The major advantage of process unit placement technique is：

(1) priming automatic production line of the present invention and technology arrangement mode are all in the homonymy, formula that is in line arrangement, adjacent Inter process is connected with the explosion-proof pass-through box of antiknock, realizes the dangerous unmanned execute-in-place of process of priming production overall process institute, The complete man-machine isolation in the dangerous post of priming production process is realized, the intrinsic safety of priming production line is improved.

(2) priming automatic production process mode and technical process of the present invention are sufficiently used the priming production of transmission The custom of operating unit and technical process, takes further innovation and develops, meet the automatic metaplasia of serialization in principle The use requirement of production process.

(3) priming automatic production process mode and technical process of the present invention can realize split run production priming 150kg Ability, drastically increase the production capacity of wall scroll priming production line, improve production efficiency.Reduce the number of priming production line Amount, reduces the dangerous matter sources in enterprise, is conducive to improving the safe coefficient of whole enterprise.

(4) priming automatic production process mode and technical process of the present invention are power source using compressed air with device, Manipulator completes the operating process of multistation, and stability of the production process is good, meets priming serialization automated production mode Use requirement, automated procedures are high, dramatically reduce labor intensity.

The serialization of the present invention automates priming production line and the particularly suitable priming kind of technology arrangement mode：GTX、 The primings such as GTG, NHN, LA, LS, KP, KS.The production technology mode has serialization, automation, man-machine isolation Technical characteristic.

The common implementing operating process description of the individual character production process for the different cultivars priming being applicable firstly, for this production line is such as Under：

1) two kinds of reaction material liquids, 2 are prepared) it is filtered to remove mechanical admixture, unreacted reactant, undissolved thing, 3) collect filtrate, adjust Save acid-base value, 4) measure chemical combination reduction of feed volume, 5) a kind of reaction solution is first put into combination apparatus and makees bottom liquid, be heated to reaction Temperature, 6) another feed liquid is gradually added in combination apparatus under conditions of coutroi velocity again, two kinds of feed liquid reaction generation institutes The priming kind needed, 7) reaction solution is incubated, cured, crystallizes and gradually grows up, 8) reaction solution is cooled down by reaction temperature All crystallized out as far as possible close to room temperature, by priming, obtain big priming particle, improve yield.It is above-mentioned 1) to 8) Processing step, as the different of priming kind, technological parameter slightly have difference, but the above-mentioned production process of these primings It is identical, with common point, equipment and process unit have versatility.

Then, the identical implementation operating process of the general character production process for the various primings being applicable for this production line is described as follows：

9) reaction mixture after cooling is filtered to isolate into priming crystalline product, 10) a large amount of primings after filtering are divided into Aliquot, 11) priming of aliquot is placed in the plate of a safety and shakeouts, harrow uniform, 12) it will be equipped with the disk of priming Dried in the air on the shelf for being put into an andron a period of time, as far as possible by moisture content and dehydrating agent volatilization, to mitigate vacuum drying process Load, 13) initiating explosive tray dried in the air is transferred in vacuum drying box, dried necessarily under certain vacuum degree, uniform temperature Time, eliminate again vacuum, by baking oven open door cooling a period of time, 14) initiating explosive tray that vacuum drying is crossed is transferred to one Cool a period of time is placed on the shelf of andron, the temperature of priming is down to room temperature, the safe operation to ensure subsequent process, 15) just batch pan is transferred on the machine of falling medicine, priming is wandered onto screen cloth, makes medicament by screen cloth under jitter conditions, leads to Cross and fallen under guide housing in collection medicine box, 17) medicine box taking-up will be collected, the floating medicine on removing surface is wiped, rotates in fortune medicine-chest, 18) after fortune medicine-chest is filled to quantitatively, medicine-chest is delivered into priming storehouse.It is above-mentioned 9) to processing step 18), for various The production process of quick-fried medicine kind, technological parameter are just as, with the phase same sex, and equipment and process unit are all general.

Embodiment is arranged as with the production line and process unit required for GTX primings to be described in detail as follows, but the production line and work Process and equipment placement technique is not only limited to the production of GTX primings.

1) carbohydrazide feed liquid is prepared：Using pure water as solvent, by the pure water of amount of calculation (described pure water herein：Refer to lead to Ion-exchange method, pellicle mode, electrodialysis mode etc. are crossed by the metal ion in running water, acid ion, mechanical solid The electric conductivity value that obtains is not more than 3.3 μ s/cm pure water after impurity is removed) water is put into dosage bunker, stirs, heats, weigh The carbohydrazide solid of amount of calculation is added in dosage bunker, stirring and dissolving, forms the clear solution of water white transparency, adjusts acid-base value. The blending process can once complete the dispensing of 20kg~40kg GTX primings, and Primary batching system is available for multiple chemical combination to use.

The solution of preparation is removed into mechanical admixture, filtrate by vacuum filter to be collected in storagetank in.

Filtrate is sent into constant volume measurement groove by pipeline, the feed liquid required for measuring a collection of priming of chemical combination is standby.It is connected to behaviour After instructing, charging switch is opened, and feed liquid is disposably all added in combination apparatus.

2) zinc perchlorate feed liquid is prepared：Using pure water as solvent, the water of amount of calculation is put into dosage bunker, stirring, heating, amount Take the pure perchloric acid of analysis of amount of calculation to be added in dosage bunker, then weigh the zinc oxide solid of amount of calculation and be added in dosage bunker, Stirring reaction, until perchloric acid reaction is complete, reaction solution shows that the zinc oxide that adds is excessive and by perchloric acid into muddy shape Consumption is complete.The blending process can once complete the dispensing of 20kg~80kg GTX primings, and Primary batching system is available for repeatedly Chemical combination is used.

The solution of preparation is removed into mechanical admixture, filtrate by vacuum filter to be collected in storagetank in.

Filtrate is sent into constant volume measurement groove by pipeline, the feed liquid required for measuring a collection of priming of chemical combination is standby.It is connected to behaviour After instructing, charging switch is opened, and feed liquid is added in combination apparatus by the flow velocity of setting.

3) chemical combination process：

The phosphinylidyne hydrazine solution measured is put into priming combination apparatus by the feeding tube on charging spout, stirred with constant speed Mix, feed liquid is heated between 50 DEG C~80 DEG C with hot water by combination apparatus chuck.

When phosphinylidyne hydrazine solution reaches combination reaction temperature, the zinc perchlorate solution measured is passed through into the feeding tube on charging spout It is added under conditions of control flow in priming combination apparatus, now phosphinylidyne hydrazine solution and zinc perchlorate solution reaction generation GTX Priming crystal.The charging process is completed about in the range of 20min~50min.It is connected to after control instruction, passes through combination apparatus bottom Without friction blowing switch release mixed liquor, once by reaction mixture all be put into curing crystallizer in.Repeat according to this, It is continuously finished the task of this process.

4) curing crystallization：3) mixed liquor that reaction is produced disposably all is put by combination apparatus bottom without friction blowing switch Enter into curing crystallizer, under constant speed stirring, the insulation reaction between 50 DEG C~80 DEG C, cure 10min~30min. It is connected to after control instruction, mixed liquor is released by curing being switched without friction blowing for crystalliser feet, it is once that mixed liquor is whole It is put into cooler crystallizer.Repeat according to this, be continuously finished the task of this process.

5) crystallisation by cooling：4) mixed liquor of curing crystallization generation is disposable complete without friction blowing switch by combination apparatus bottom Portion is put into cooler crystallizer, under constant speed stirring, by having cooled to 10 DEG C or so in the chuck of cooler crystallizer Running water, within 10min~40min time control mixed liquor be cooled to less than 30 DEG C from 50 DEG C~80 DEG C, make mixed liquor The big priming crystal of the priming sufficient crystallising of middle dissolving, acquisition, reduction solution loss, raising yield.When crystallization clutch When the temperature of interior feed liquid drops to less than 30 DEG C, mixed liquor is released without friction blowing switch by combination apparatus bottom, once all It is put into portioning filter progress.Repeat according to this, be continuously finished the task of this process.

6) portioning, filter, wash, draining：The process mainly completes product by the way of filtering and separated with mother liquor.According to making Filtering separation device is different, and specific mode of operation is also incomplete same.

5) feed liquid of generation is disposably all released in product filter, priming crystallization and the mother liquor mixture of outflow lead to Cross distributor it relatively evenly scatter, it is female in 9 filter tunnels for flowing to dispenser bottom along the guiding gutter on distributor Liquid is extracted into mother liquor surge tank by the screen pack of funnel bottom, and priming crystalline solid is stayed in distributor and filter tunnel, often Dose in individual funnel is about 1kg.Then, pure water is sprayed by the shower nozzle above distributor, by rising for being adhered on distributor Quick-fried medicine crystallization, mother liquor etc. wash in filter tunnel, priming crystallizing and washing, vacuum are drained together.With this operating method weight After backwashing washs 2 times, in the same way with absolute ethanol washing 1 time, drains, then by manipulator by the funnel drained together with Quick-fried medicine is carried to box point disk process, the stand of falling medicine disk together.Manipulator often operates the detonation medicine box completed on a station, suction filtration point Disk machine just one station of stepping forward.Repeat according to this, be continuously finished the task of this process.

7) medicine that falls is raked stand disk：6) priming drained in step is crossed pan and carried to the station of falling box by manipulator, in the upper of batch pan Side rotates 180 ° around the central shaft of manipulator, the priming drained is poured into beneath batch pan and sky is crossed into pan after turning round and returned Return on point disk suction filtration machine.Now, manipulator of raking, which takes off the priming heap in batch pan, to scatter, harrows into uniform thin layer medicine layer. The batch pan taken off after putting down is carried by drug delivery disk manipulator and is sent in pass-through box, the operation of a filtering medicine box is completed.Repeat according to this Operation, is continuously finished the task of this process.

8) taking plate dress drying vehicle：In entrucking antiknock, the detonation shakeout is taken out from pass-through box by taking plate loading manipulator Batch pan, is turned back to before drying vehicle, on the fixed position that the batch pan is put into the first layer of drying vehicle.Repeat, until will dry Untill dry turning fills 6 initiating explosive trays.After drying vehicle fills 6 car, the rotation of drying vehicle transmission track frame and main orbit Cheng Zhi Line, between entrucking between the medicine that dries in the air between antiknock transmission window open, drying vehicle is sent to the antiknock for medicine process of drying in the air by pushing machinery hand In.Repeat according to this, be continuously finished the task of this process.

9) dry in the air medicine：Drying vehicle equipped with initiating explosive tray is sent in the main transmission track frame between drying, is delivered to dries on frame again, To dry frame to the left (or right side) displacement, make lower second dry frame position dock with main orbit, with this repeatedly reception second Drying vehicle restocking, dry medicine.Temperature control in the room is dried condition more than 40 DEG C, and with good ventilation.Dry in the air medicine Time control makes the moisture content and ethanol of priming crystallization adhesion volatilize as far as possible removing, to reduce priming in 15min~25min The moisture content amount carried in crystallization, reduces follow-up drying work load.In the room can with parallel arranged two groups or three groups dry rail Road, to improve the overall efficiency of production line.Repeat according to this, be continuously finished the task of this process.

10) priming drying process：The process is to be dried priming by indirect modes such as heat radiation, thermal convection current and heat transfer. The baking oven must be water proof heating bath, prohibit the use of electric heating bath of liquid or electric hot-air dry heat.

First way is boulton process, is dried according to 9) process after the defined time, and the drying vehicle equipped with priming leads to Main orbit transfer robots are crossed by drying vehicle to front transfer, the antiknock transmission window between the medicine that dries in the air between dry house is opened, until will Drying vehicle is sent in vacuum drying box.The fixing end of drying baker and mobile terminal arrange with main orbit into vertical direction, drying baker After fixing end is closed with mobile terminal, opening vacuum switch makes the negative pressure of formation -0.08MPa in drying baker, is then turned on heating water and opens Close, by heating jacket of more than 95 DEG C of the hot water by drying baker, the temperature in case is risen to more than 60 DEG C, maintenance 40min~60min, it is qualified to moisture content that priming is dried.Then, the atmospheric valve on vacuum line is opened, will be negative in drying baker Pressure is eliminated, and mobile terminal is removed, drying vehicle is exposed under room temperature environment, and then drying vehicle is transferred to cool by medicine of a cold nature 5min again Between medicine.Repeat according to this, be continuously finished the task of this process.

Second way atmosphere pressure desiccation：By the length of drying baker to should be parallel with main orbit and ride on main orbit.By front end Wind blocking door is lifted, and priming drying vehicle is pushed into drying baker, then the wind blocking door of front end is put down into closing, makes rising on drying vehicle The flash baking under the heating of heat radiation, thermal convection current and heat exchange pattern of quick-fried medicine.All the time more than 95 DEG C are led in drying baker crustless sandwich Hot water, it is not necessary to vacuumize, it is only necessary to keep micro- ventilation by air inducing pipeline, makes the temperature in case rise to more than 70 DEG C, maintenance 40min~60min, it is qualified to moisture content that priming is dried.Then, the wind blocking door of drying baker front and back end is lifted, made in case Drying vehicle push-and-pull is gone out drying baker, is transferred between the medicine of a cold nature by temperature drop, manipulator.Repeat according to this, be continuously finished this process Task.

11) medicine of a cold nature：After condition drying of the priming on drying vehicle as described in 10), the drying vehicle that will be equipped with initiating explosive tray leads to Transfer robots are crossed to push in the main transmission track frame between the medicine of a cold nature, be delivered to again on medicine of a cold nature frame, medicine of a cold nature frame is (or right to the left Side) shift, lower second medicine of a cold nature frame is docked with main orbit, repeat to receive second drying vehicle restocking, the medicine of a cold nature with this.The room Between there is good ventilation to dry condition, room temperature is controlled below 20 DEG C, and dry in the air medicine 10min~20min.Make in higher temperature Priming is cooled to room temperature, in order to safe operation.Repeat according to this, be continuously finished the task of this process.

12) batch pan transmission, the medicine that falls：Pushed away by above-mentioned 11) the cool drying vehicle to room temperature, equipped with initiating explosive tray by transfer robots Deliver between transfer, a batch pan is taken from the drying vehicle equipped with initiating explosive tray by Disc-taking machine tool hand, pass-through box between sieving is delivered in revolution It is interior, carry batch pan manipulator the batch pan has been carried, turn round be delivered to priming sieve basket above, be rotated by 90 ° along manipulator central shaft, will Dried priming is poured into sieving basket, manipulator revolution, along original track empty initiating explosive tray is sent back into pass-through box when, Disc-taking machine tool hand is extended the blank panel is taken out in pass-through box again, and revolution is returned, and empty batch pan is put back into position original on drying vehicle. Meanwhile, manipulator is shifted one's position, then takes a disk that the batch pan that priming is crystallized is housed, and repeats above-mentioned action, until by 6 disk on car Priming is all repeated according to this, is continuously finished the task of this process.

Now, 90 ° of the main orbit revolution equipped with 6 empty batch pan drying vehicles, by track and the contraposition of drying vehicle outflow track, will detonate Medicine drying vehicle and empty batch pan are handed on worker-house corridor by the pass-through box oral instructions between the antiknock, provide signal, should by arranging workman Car is handled between moving to arrangement.

13) sieving, mounted box, vanning：By 12) the step of, taking plate manipulator is above priming sieve basket along manipulator center Axle is rotated by 90 °, and dried priming is poured into sieving basket, and priming crystallization passes through the screen cloth of vibrations, big medicament group in basket Block is trembled broken be trapped in by screen cloth, the crystallization of bulk with crispy rice on screen cloth and shares out, fallen on back along sieve basket inclined-plane guide groove Receive in box.Connecing in medicine box for sieve basket bottom is fallen under being crystallized by the priming after sieve, a disk priming just fills the one of bottom Two medicine boxs of group, the two connect medicine box and are placed in medicine box transfer robots.After the disk medicine has been sieved, medicine box transfer robots are treated down Fall, turn round, protract, by the box initiating explosive feeding of group two into priming pass box, medicine box transfer robots retraction, priming are passed Case is passed to turn round 180 °, make empty medicine box in case to medicine box transfer robots, medicine box transfer robots extension, take out in case one Two medicine boxs of group, manipulator bounces back, turned round, protracting again, upper lift, at the lower part outlet that empty medicine box is placed into sieving basket.According to This is repeated, and is continuously finished the task of this process.

After priming pass box fills 4 box priming, workplace indicator lamp is lighted, and pass-through box is opened by submitting medicine operating personnel, The medicine-chest for filling priming is taken out, rotates to another priming pass box that two groups 4 empty medicine boxs are housed on fixed position, The medicine-chest of portable full priming is sent to detonation Drug Storage.Repeat according to this, be continuously finished task on duty.

14) drying vehicle and batch pan arrange passback：Priming drying vehicle and empty batch pan have been shown on worker-house corridor when priming is produced After the information passed out, by operator will spread out of the drying vehicle for being loaded with sky batch pan come, to move to arrangement interior, by car and batch pan Wipe clearly, remove floating medicine, cleaning drying packing paper, empty batch pan is put on the fixed position of drying vehicle, then after this is arranged Drying after and empty the batch pan incoming transmission window of drying vehicle and the incoming pass-through box of empty batch pan that are sent to along worker-house one skilled in the art corridor between entrucking Mouthful, by the alignment pin in empty wagons alignment windows, empty batch pan is piled up and transmits window in batch pan, will be by manipulator by start button Follow procedure is automatic to be delivered to empty batch pan, drying vehicle indoor between antiknock, starts next automatic cycle.Repeat according to this, even It is continuous to complete task on duty.

Claims (8)

1. a kind of serialization, automation, the production-line arrangement mode of man-machine isolation priming completely, it is characterised in that including dispensing with pure Water measuring tank, reaction dosage bunker, feed liquid lautertuns, Promoting Layered Buffer hopper, feed liquid metered charge groove, chuck heating water bath Clutch, the heat aging device of chuck water-bath, chuck water-bath cooler crystallizer, automatic portioning and filtering and washing device, automatic water jetting Sink, it is automatic took pan fall medicine point disk device, automatically a point disk share equally device, automatic batch pan shipment medicine drying vehicle device, Two-layer equation fortune medicine drying vehicle, the automatic transmission system of drying vehicle, rotary rail device, automatic multi-row dry in the air medicine frame, automatic switch water Bathe vacuum drying box, automatic multi-row medicine of a cold nature frame, unload drying vehicle taking plate device, automatic medicine pouring, automatic vibration sieving dress automatically Put, box-packed medicine case apparatus of getting it filled automatically, by the combination of above-mentioned automation equipment, realize priming production process automation, Serialization, man-machine isolation completely；Priming production from expect priming vanning outward transport it is various be related to dangerous material operation wholes During, all logistics all design the same side that worker-house is produced in priming, and linear formula is arranged, and between each operation mutually Insertion, papery or wooden or aluminum batch pan double-deck transfering small vehicle equipped with priming are transmitted track by double rail type and transported, Realize priming geo-stationary, without friction, the transmission without shock, pass through steel antiknock pass-through box between each adjacent process and realize It is interconnected and isolates, the steel antiknock window between each operation antiknock room is realized by programme-control opens and closes function, So as to realize that isolation between each operation, insertion, transmission, closing, anti-biography be fiery, anti-propagation of explosion function.

2. serialization according to claim 1, automation, the production-line arrangement mode of complete man-machine isolation priming, produce work The deionization pure water of skill needs, heating water, cooling water, cooling air, negative pressure of vacuum, atmospheric compression air, 220V / 380V commercial power, the light current of position switch input and output are all arranged in priming automatic production line by code requirement In same worker-house.

3. serialization according to claim 1, automation, the production-line arrangement mode of complete man-machine isolation priming, its feature It with feed liquid, the equipment of priming solid contact and device is all to be not less than the stainless of 1Cr18Ni9Ti by corrosion resistance to be What steel matter made, each equipment is arranged between the corresponding antiknock of each operation indoor by function, is to use UPVC between equipment Plastic conduit is come the feed liquid that conveys, it is ensured that its corrosion resistance and security.

4. serialization according to claim 1, automation, the production-line arrangement mode of complete man-machine isolation priming, with pressure Be power source for 0.1MPa-0.8MPa compressed air, by weak electric signal observing and controlling, by PLC, bus system and on Bit machine realizes automatically controlling for completely each equipment and device, includes：The dispensing liquid level up and down of pure water measuring tank and true Air switch closes control, reacts the stirring start and stop, speed of agitator regulation, heating and temperature control of dosage bunker, and feed liquid lautertuns vacuum is opened Close control and liquid level warning, the control of Promoting Layered Buffer hopper vacuum switch and liquid level warning, feed liquid metered charge groove vacuum switch control System, liquid level warning and discharging switch control, combination apparatus chuck heating pump start and stop, speed of agitator regulation, chemical combination outlet valve Start-up and shut-down control is switched, the start and stop of ager chuck heating pump, speed of agitator are adjusted, the switch start-up and shut-down control of chemical combination outlet valve, Crystallizer chuck cooling water pump start and stop, speed of agitator regulation, the switch start-up and shut-down control of chemical combination outlet valve, suction filtration vavuum pump are opened Dynamic and stopping is controlled, and washing is controlled with deionization pure water tank liquid level and vacuum switch, is washed and is used absolute ethyl alcohol tank liquor position and true Air switch closes control, and automatic portioning and filtering and washing device, which are rotated, starts and stop control, takes pan to fall medicine point disk device automatically Advance, gripping, lifting, rotation, retrogressing, upset and return to control, automatic point of disk share equally the vibrations of device, advance, Retreat lifting control, the advance of automatic batch pan shipment medicine drying vehicle device, gripping, lifting, rotate, put down, retreat and return Return control, the advance of two-layer equation fortune medicine drying vehicle, stop control, the lifting of the automatic transmission system of drying vehicle, advance, return, Landing control, the startup of rotary rail device, positioning, stoppings, retracting controls, automatic multi-row dry in the air medicine frame it is spacing, shift, Contraposition control, the unlatching of automatic switch water-bath vacuum drying box, fortune medicine car positions, closed, vacuumizing, heat temperature raising, added Hot time timing, temperature survey, vacuum measurement, eliminate vacuum control automatically, automatic multi-row medicine of a cold nature frame is spacing, displacement, Contraposition control, unloads the advance of drying vehicle taking plate device, gripping, lifting, rotates, puts down, retreats and return control automatically, The gripping of automatic medicine pouring device, displacement, upset, rollback, sale at reduced prices, return process control, the shake of automatic vibration sieving equipment It is dynamic to start and stop control, box-packed medicine case apparatus advance of getting it filled automatically, gripping, lifting, rotate, put down, retreat and return Control.

5. serialization according to claim 1, automation, the production-line arrangement mode of complete man-machine isolation priming, priming It is to be contained in papery, in wooden, aluminum batch pan, is reloading with bilayer transmission drying vehicle, equipped with anti-on transmission drying vehicle Multigroup wheel of electrostatic, sparkproof material, the design ensure transmission drying vehicle can smoothly through track gap, pass Pass drying vehicle smoothly to transmit on default track between each operation, realize priming in overall production process without friction, nothing Shock, the transmission of geo-stationary, with this technology arrangement mode and the transfer mode of priming, it is possible to decrease priming was produced The operational motion and operating frequency of journey, the security for improving production process, improve production capacity and production efficiency, meet detonation The production process of medicine needs.

6. serialization according to claim 1, automation, the production-line arrangement mode of complete man-machine isolation priming, each work Track realization is transmitted between sequence by double rail type to be coupled to each other, the track is by pass-through box, vacuum drying box, revolution During joint, track all disconnects corresponding length, to ensure that transmission window is closed, vacuum drying casing is closed, revolution pair Connect place's rotation and align；A pair of tracks that double rail type transmission track is made up of " [" shape section bar and "] " shape section bar, The wheel of transmission drying vehicle is limited in " in the structure of [" shape, it is ensured that transmission drying vehicle is not in derailing, card wheel event Barrier.

7. serialization according to claim 1, automation, the production-line arrangement mode of complete man-machine isolation priming, it is special It is to be provided between the more than one medicine that dries in the air to levy, and the drying transmission of 2 to 4 can be deposited on the medicine frame that dries in the air between the medicine that each dries in the air Car；A transmission drying vehicle can only be deposited by setting 2 to 6 water-bath vacuum drying box, each drying baker；Set one Between the medicine of a cold nature above, the drying transmission car of 2 to 4 can be deposited on the medicine of a cold nature frame between each medicine of a cold nature, to ensure to produce energy Power and production efficiency.

8. serialization according to claim 1, automation, the production line of complete man-machine isolation priming, it is characterised in that should For with similar production process the carbohydrazide of perchloric acid three close zinc (GTX), the carbohydrazide of perchloric acid three close cadmium (GTG), Nickel hydrazine nitrate (NHN), lead azide (LA), lead styphnate (LS), potassium picrate (KP), this base of a fruit phenolic acid potassium (KS) The serialization of priming, automation, man-machine isolation production.