CN106507708B - A kind of graphite crucible of manufacture C/SiC ceramic matric composite brake discs - Google Patents

A kind of graphite crucible of manufacture C/SiC ceramic matric composite brake discs

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Publication number
CN106507708B
CN106507708B CN200610056327.6A CN200610056327A CN106507708B CN 106507708 B CN106507708 B CN 106507708B CN 200610056327 A CN200610056327 A CN 200610056327A CN 106507708 B CN106507708 B CN 106507708B
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CN
China
Prior art keywords
graphite crucible
graphite
manufacture
ceramic matric
brake discs
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Active
Application number
CN200610056327.6A
Other languages
Chinese (zh)
Other versions
CN106507708C (en
Inventor
徐永东
张立同
成来飞
王东
刘小瀛
涂建勇
陈旭
付志强
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Northwestern Polytechnical University
Original Assignee
Northwestern Polytechnical University
Filing date
Publication date
Application filed by Northwestern Polytechnical University filed Critical Northwestern Polytechnical University
Priority to CN200610056327.6A priority Critical patent/CN106507708C/en
Priority claimed from CN200610056327.6A external-priority patent/CN106507708C/en
Application granted granted Critical
Publication of CN106507708B publication Critical patent/CN106507708B/en
Publication of CN106507708C publication Critical patent/CN106507708C/en
Active legal-status Critical Current
Anticipated expiration legal-status Critical

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Abstract

The present invention relates to a kind of graphite crucible of manufacture C/SiC ceramic matric composite brake discs.Described graphite crucible includes graphite crucible body, offers equally distributed aperture on graphite crucible body, is coated with boron nitride (BN) coating, is equipped with graphite paper in boron nitride (BN) coating in graphite crucible body on wall.The graphite crucible long service life of the present invention, and material is easily cleared up in use, and high-temperature vacuum in-furnace temperature uniformity can be made good.The graphite crucible of the present invention can be also used for reaction melt method of impregnation and prepare other ceramic matric composites.

Description

A kind of graphite crucible of manufacture C/SiC ceramic matric composite brake discs
Technical field
The present invention relates to a kind of graphite crucible, more particularly to a kind of manufacture C/SiC ceramic matric composites The graphite crucible of brake disc.
Background technology
The manufacture method of carbon/carbon/silicon carbide ceramic matrix composite (C/SiC) brake disc is to adopt chemical vapor infiltration Saturating method (CVI) association reaction molten liquid forming (RMI).Initially with chemical vapor infiltration (CVI) in three-dimensional Pyrolytic carbon (C) boundary layer is deposited on needled carbon (C) fiber preform, then adjustment propylene and carrier gas The flow-rate ratio of body and depositing temperature, realize CVI fast depositions, make carbon/carbon (C/C) porous and are combined Material;Siliconising is melted in vacuum high temperature furnace finally by reaction melt method of impregnation (RMI) obtains carbon/carbonization Silicon (C/SiC) friction material.At present, in RMI technical process, using traditional graphite crucible, Be easily caused raw material and graphite crucible to react, the serious service life for reducing crucible, the manufacturing cost that increases, Material is difficult to the problems such as clearing up;Meanwhile, because graphite crucible and raw material thermal capacity are big, and heater element is produced The channel of raw energy transmission is limited so that in-furnace temperature uniformity is poor, it is impossible to meet brake disc batch The requirement of production.
Content of the invention
The technical problem to be solved is to provide a kind of manufacture C/SiC ceramic matric composites brake The graphite crucible of disk, the graphite crucible long service life, and material is easily cleared up in use, can make height Warm the temp. in vacuum furnace uniformity is good.
For solving above-mentioned technical problem, a kind of manufacture C/SiC ceramic matric composites that the present invention is provided are stopped The graphite crucible of hull, it include that graphite crucible body, described graphite crucible body top offer a circle Equally distributed aperture, in graphite crucible body, surface is coated with BN coatings, is equipped with graphite in BN coatings Paper.
The thickness of above-mentioned BN coatings is generally 0.3~0.5mm, and the thickness of graphite paper is 0.3~0.4mm.
It is an advantage of the invention that:(1) open up equally distributed aperture on graphite crucible to improve in burner hearth The uniformity of temperature, lengthens uniform temperature zone, processes ceramic matric composite so as to quantitatively improve equipment The ability of brake disc;(2) coat in graphite crucible boron nitride (BN) coating can prevent graphite paper with Crucible adhesion, while preventing which from entering in graphite in material accident seepage, improves service life;(3) After the graphite paper that lays in boron nitride (BN) coating, material not with graphite crucible directly contact, can make Material is easily separated with crucible, is convenient to clean, and further extends the service life of graphite crucible, while contracting The cycle of short RMI techniques.
The graphite crucible of the present invention can be also used for reaction melt method of impregnation and prepare other ceramic base composite woods Material.
Description of the drawings
Below in conjunction with the accompanying drawings the present invention is elaborated.
Fig. 1 is the sectional view of graphite crucible of the present invention.
Fig. 2 is the top view of graphite crucible of the present invention.
In figure, 1- graphite crucible bodies, 2- boron nitride (BN) coating, 3- graphite papers, 4- apertures.
Specific embodiment
Referring to Fig. 1 and Fig. 2, manufacture carbon/carborundum (C/SiC) ceramic matric composite of the present invention is stopped The graphite crucible of hull, it includes graphite crucible body 1, described 1 top of graphite crucible body offers- Equally distributed aperture 4 is enclosed, the diameter of aperture 4 is generally 16~20mm, and surface applies in graphite crucible body BN coatings 2 are covered with, and the thickness of coating 2 is generally 0.3~0.5mm, and graphite paper is laid in BN coatings 3, the thickness of graphite paper is generally 0.3~0.4mm.

Claims (2)

1. a kind of graphite crucible of manufacture C/SiC ceramic matric composite brake discs, it includes graphite crucible Body (1), it is characterised in that:It is equally distributed little that graphite crucible body (1) top offers a circle Hole (4), graphite crucible body (1) inner surface are coated with boron nitride coating (2), boron nitride coating upper berth It is provided with graphite paper (3);A diameter of 16~20mm of aperture (4).
2. the graphite earthenware of manufacture C/SiC ceramic matric composite brake discs according to claim 1 Crucible, it is characterised in that:The thickness of boron nitride coating (2) is 0.3~0.5mm, and the thickness of graphite paper is 0.3~0.4mm.
CN200610056327.6A 2006-06-22 2006-06-22 A kind of graphite crucible for manufacturing C/SiC ceramic matrix composite brake disc Active CN106507708C (en)

Priority Applications (1)

Application Number Priority Date Filing Date Title
CN200610056327.6A CN106507708C (en) 2006-06-22 2006-06-22 A kind of graphite crucible for manufacturing C/SiC ceramic matrix composite brake disc

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
CN200610056327.6A CN106507708C (en) 2006-06-22 2006-06-22 A kind of graphite crucible for manufacturing C/SiC ceramic matrix composite brake disc

Publications (2)

Publication Number Publication Date
CN106507708B true CN106507708B (en) 2010-03-10
CN106507708C CN106507708C (en) 2010-03-10

Family

ID=58264251

Family Applications (1)

Application Number Title Priority Date Filing Date
CN200610056327.6A Active CN106507708C (en) 2006-06-22 2006-06-22 A kind of graphite crucible for manufacturing C/SiC ceramic matrix composite brake disc

Country Status (1)

Country Link
CN (1) CN106507708C (en)

Cited By (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN107244943A (en) * 2017-07-10 2017-10-13 巩义市泛锐熠辉复合材料有限公司 A kind of reaction melt method of impregnation prepares the preparation method of C/C SiC ceramic matrix composite material graphite crucible face coats
CN112341213A (en) * 2020-11-26 2021-02-09 西安鑫垚陶瓷复合材料有限公司 Method for carrying out melt siliconizing on small-size circular-section ceramic matrix composite component
CN114455965B (en) * 2021-12-30 2023-09-05 西安超码科技有限公司 A composition containing alpha-Al 2 O 3 Coated C/SiC composite crucible

Cited By (4)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN107244943A (en) * 2017-07-10 2017-10-13 巩义市泛锐熠辉复合材料有限公司 A kind of reaction melt method of impregnation prepares the preparation method of C/C SiC ceramic matrix composite material graphite crucible face coats
CN112341213A (en) * 2020-11-26 2021-02-09 西安鑫垚陶瓷复合材料有限公司 Method for carrying out melt siliconizing on small-size circular-section ceramic matrix composite component
CN112341213B (en) * 2020-11-26 2022-05-13 西安鑫垚陶瓷复合材料有限公司 Method for carrying out melt siliconizing on small-size circular-section ceramic matrix composite component
CN114455965B (en) * 2021-12-30 2023-09-05 西安超码科技有限公司 A composition containing alpha-Al 2 O 3 Coated C/SiC composite crucible

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