CN106498544A - A kind of flame-retardant water-repellent refuses oily woven cloth and preparation method thereof - Google Patents
A kind of flame-retardant water-repellent refuses oily woven cloth and preparation method thereof Download PDFInfo
- Publication number
- CN106498544A CN106498544A CN201611236026.1A CN201611236026A CN106498544A CN 106498544 A CN106498544 A CN 106498544A CN 201611236026 A CN201611236026 A CN 201611236026A CN 106498544 A CN106498544 A CN 106498544A
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- Prior art keywords
- flame
- repellent
- retardant
- oily
- water
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Classifications
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- D—TEXTILES; PAPER
- D01—NATURAL OR MAN-MADE THREADS OR FIBRES; SPINNING
- D01F—CHEMICAL FEATURES IN THE MANUFACTURE OF ARTIFICIAL FILAMENTS, THREADS, FIBRES, BRISTLES OR RIBBONS; APPARATUS SPECIALLY ADAPTED FOR THE MANUFACTURE OF CARBON FILAMENTS
- D01F6/00—Monocomponent artificial filaments or the like of synthetic polymers; Manufacture thereof
- D01F6/88—Monocomponent artificial filaments or the like of synthetic polymers; Manufacture thereof from mixtures of polycondensation products as major constituent with other polymers or low-molecular-weight compounds
- D01F6/92—Monocomponent artificial filaments or the like of synthetic polymers; Manufacture thereof from mixtures of polycondensation products as major constituent with other polymers or low-molecular-weight compounds of polyesters
-
- D—TEXTILES; PAPER
- D01—NATURAL OR MAN-MADE THREADS OR FIBRES; SPINNING
- D01F—CHEMICAL FEATURES IN THE MANUFACTURE OF ARTIFICIAL FILAMENTS, THREADS, FIBRES, BRISTLES OR RIBBONS; APPARATUS SPECIALLY ADAPTED FOR THE MANUFACTURE OF CARBON FILAMENTS
- D01F1/00—General methods for the manufacture of artificial filaments or the like
- D01F1/02—Addition of substances to the spinning solution or to the melt
- D01F1/07—Addition of substances to the spinning solution or to the melt for making fire- or flame-proof filaments
-
- D—TEXTILES; PAPER
- D04—BRAIDING; LACE-MAKING; KNITTING; TRIMMINGS; NON-WOVEN FABRICS
- D04C—BRAIDING OR MANUFACTURE OF LACE, INCLUDING BOBBIN-NET OR CARBONISED LACE; BRAIDING MACHINES; BRAID; LACE
- D04C1/00—Braid or lace, e.g. pillow-lace; Processes for the manufacture thereof
- D04C1/02—Braid or lace, e.g. pillow-lace; Processes for the manufacture thereof made from particular materials
-
- D—TEXTILES; PAPER
- D04—BRAIDING; LACE-MAKING; KNITTING; TRIMMINGS; NON-WOVEN FABRICS
- D04C—BRAIDING OR MANUFACTURE OF LACE, INCLUDING BOBBIN-NET OR CARBONISED LACE; BRAIDING MACHINES; BRAID; LACE
- D04C1/00—Braid or lace, e.g. pillow-lace; Processes for the manufacture thereof
- D04C1/06—Braid or lace serving particular purposes
-
- D—TEXTILES; PAPER
- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06M—TREATMENT, NOT PROVIDED FOR ELSEWHERE IN CLASS D06, OF FIBRES, THREADS, YARNS, FABRICS, FEATHERS OR FIBROUS GOODS MADE FROM SUCH MATERIALS
- D06M15/00—Treating fibres, threads, yarns, fabrics, or fibrous goods made from such materials, with macromolecular compounds; Such treatment combined with mechanical treatment
- D06M15/19—Treating fibres, threads, yarns, fabrics, or fibrous goods made from such materials, with macromolecular compounds; Such treatment combined with mechanical treatment with synthetic macromolecular compounds
- D06M15/21—Macromolecular compounds obtained by reactions only involving carbon-to-carbon unsaturated bonds
- D06M15/263—Macromolecular compounds obtained by reactions only involving carbon-to-carbon unsaturated bonds of unsaturated carboxylic acids; Salts or esters thereof
- D06M15/277—Macromolecular compounds obtained by reactions only involving carbon-to-carbon unsaturated bonds of unsaturated carboxylic acids; Salts or esters thereof containing fluorine
-
- D—TEXTILES; PAPER
- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06M—TREATMENT, NOT PROVIDED FOR ELSEWHERE IN CLASS D06, OF FIBRES, THREADS, YARNS, FABRICS, FEATHERS OR FIBROUS GOODS MADE FROM SUCH MATERIALS
- D06M2101/00—Chemical constitution of the fibres, threads, yarns, fabrics or fibrous goods made from such materials, to be treated
- D06M2101/16—Synthetic fibres, other than mineral fibres
- D06M2101/30—Synthetic polymers consisting of macromolecular compounds obtained otherwise than by reactions only involving carbon-to-carbon unsaturated bonds
- D06M2101/32—Polyesters
-
- D—TEXTILES; PAPER
- D10—INDEXING SCHEME ASSOCIATED WITH SUBLASSES OF SECTION D, RELATING TO TEXTILES
- D10B—INDEXING SCHEME ASSOCIATED WITH SUBLASSES OF SECTION D, RELATING TO TEXTILES
- D10B2331/00—Fibres made from polymers obtained otherwise than by reactions only involving carbon-to-carbon unsaturated bonds, e.g. polycondensation products
- D10B2331/04—Fibres made from polymers obtained otherwise than by reactions only involving carbon-to-carbon unsaturated bonds, e.g. polycondensation products polyesters, e.g. polyethylene terephthalate [PET]
-
- D—TEXTILES; PAPER
- D10—INDEXING SCHEME ASSOCIATED WITH SUBLASSES OF SECTION D, RELATING TO TEXTILES
- D10B—INDEXING SCHEME ASSOCIATED WITH SUBLASSES OF SECTION D, RELATING TO TEXTILES
- D10B2401/00—Physical properties
- D10B2401/02—Moisture-responsive characteristics
- D10B2401/021—Moisture-responsive characteristics hydrophobic
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- Engineering & Computer Science (AREA)
- Textile Engineering (AREA)
- Chemical & Material Sciences (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Manufacturing & Machinery (AREA)
- General Chemical & Material Sciences (AREA)
- Treatments For Attaching Organic Compounds To Fibrous Goods (AREA)
Abstract
In order to solve above-mentioned technical problem, the present invention provides another flame-retardant water-repellent and refuses oily woven cloth and preparation method thereof.Its technical scheme is：A kind of flame-retardant water-repellent refuses oily woven cloth, and its component by mass percentage is：Low elastic polyester filament 60～75%, phosphorus flame retardant 20～65%, six carbon fluoroacrylic resins 10～35%.The invention also discloses a kind of flame-retardant water-repellent refuses the preparation method of oily woven cloth, comprise the steps：Step 1, prepares low elastic polyester filament standby；Step 2, prepares the working solution of six carbon fluoroacrylic resin mixture；Step 3, by the working solution pH value modulation in step 2 to 5.8～6.7；Step 4, the low elastic polyester filament that step 1 is obtained is put in the working solution in step 3, pads infiltration 1min～5h, and step 5, prebaking, step 6 are baked；Step 7, is woven into flame-retardant water-repellent using the mode of interlacing and refuses oily woven cloth.Flame-retardant water-repellent of the present invention refuses oil, is applied to outer package braiding screen cloth.
Description
Technical field
The invention belongs to woven cloth technical field, is related to preservation of fishery technology, specially a kind of flame-retardant water-repellent refuses oily volume
Weave cotton cloth and preparation method thereof.
Background technology
Electric wire is conventional articles for use in actual life, and a lot, great majority all have the species of existing electric wire
There is certain anti-flammability, but the outer woven cloth fire protecting performance in wire rod field is poor at present, there is no water repellent, refuse oily function.
Content of the invention
In order to solve above-mentioned technical problem, the present invention provides another flame-retardant water-repellent and refuses oily woven cloth and its preparation side
Method.
Its technical scheme for adopting is：
A kind of flame-retardant water-repellent refuses oily woven cloth, and its component by mass percentage is：
Low elastic polyester filament 60～75%,
Phosphorus flame retardant 20～65%,
Six carbon fluoroacrylic resins 10～35%；
The phosphorus flame retardant is phosphate ester, phosphite ester, one or more combination in organic phosphate, the phosphorous flame-retardant
Agent PPM >=6300.
Preferably, the low elastic polyester filament is the monofilament of 0.10～0.40mm or for a kind of multifilament in 50D ~ 900D.
A kind of flame-retardant water-repellent refuses the preparation method of oily woven cloth, comprises the steps：
Step 1, prepares low elastic polyester filament, adds phosphorus flame retardant in low elastic polyester filament filamentation；Preparation reaches 0.10～
A kind of multifilament in the monofilament or 50D ~ 900D of 0.40mm；Totally standby with clean water；
Step 2, prepares six carbon fluoroacrylic resin mixture, by six carbon fluoroacrylic resins with water according to 30～50g/L
Disperseed, be modulated into the working solution of six carbon fluoroacrylic resin mixture；
Step 3, by the working solution pH value modulation in step 2 to 5.8～6.7；
Step 4, the low elastic polyester filament that step 1 is obtained is put in the working solution in step 3, pads infiltration 1min～5h,
Step 5, prebaking, baking temperature are 100 °～120 °/1min ~ 1h；
Carrying out baking after step 6, step 5 and then obtain flame-retardant water-repellent and refuse oily braided wires, baking temperature is 150 °～175 °/1 ~
30min；
The flame-retardant water-repellent that step 6 is obtained is refused oily braided wires and is wrapped on reel by step 7, and reel is placed on Revolving ingot braiding
On machine, flame-retardant water-repellent is woven into using the mode of interlacing and refuses oily woven cloth.
Preferably, the flame-retardant water-repellent that step 7 is obtained refuses oily woven cloth thread count for 1 ~ 100 mesh number, and nonwoven fabric layer thickness is
0.1~10mm.
The invention has the advantages that：Fire-retardant purpose is reached by adding phosphorus flame retardant in the present invention, due to phosphorus
On the one hand flame retardant forms phosphoric acid as dehydrant, and facilitates charcoal, and the generation of charcoal is can be reduced from flame to condensed phase
Conduction of heat, on the other hand, phosphoric acid absorbs heat, and reduces heating process, while phosphorus flame retardant is matched somebody with somebody with six carbon fluoroacrylic resins
Close use to reach to form one layer of waterproof membrane, reach the purpose of water and oil repellant.
Specific embodiment
With reference to embodiment, the present invention is further illustrated, but the foundation for being not intended as limiting the present invention.
Embodiment 1：
A kind of flame-retardant water-repellent refuses the preparation method of oily woven cloth, comprises the steps：
Step 1, prepares low elastic polyester filament, adds phosphorus flame retardant in low elastic polyester filament filamentation；Preparation reaches 0.10～
A kind of multifilament in the monofilament or 50D ~ 900D of 0.40mm；Totally standby with clean water；
Wherein low elastic polyester filament 60%, phosphorus flame retardant 20%；
Step 2, prepares six carbon fluoroacrylic resin mixture, six carbon fluoroacrylic resins and water is carried out according to 30g/L
Dispersion, is modulated into the working solution of six carbon fluoroacrylic resin mixture；
Step 3, by the working solution pH value modulation in step 2 to 5.8；
Step 4, the low elastic polyester filament that step 1 is obtained is put in the working solution in step 3, pads infiltration 15min,
Step 5, prebaking, baking temperature are 110 °/2h；
Carry out baking after step 6, step 5 and then obtain flame-retardant water-repellent and refuse oily braided wires, baking temperature is 160 °/30min；
The flame-retardant water-repellent that step 6 is obtained is refused oily braided wires and is wrapped on reel, reel is placed on 16 Revolving ingots by step 7
On seam loop, flame-retardant water-repellent is woven into using the mode of interlacing and refuses oily woven cloth.
The flame-retardant water-repellent that step 7 is obtained refuses oily woven cloth thread count for 28 mesh numbers（Note：Mesh number is referred in every 25.4mm
Crossover node quantity）, nonwoven fabric layer thickness be 0.5mm, fire-retardant rank >=V-1 levels, water repellent grade >=8 are marked with GBT19977-2005
Quasi- test, without immersion oil phenomenon in 30s.
Embodiment 2：
A kind of flame-retardant water-repellent refuses the preparation method of oily woven cloth, comprises the steps：
Step 1, prepares low elastic polyester filament, adds phosphorus flame retardant in low elastic polyester filament filamentation；Preparation reaches 0.10～
A kind of multifilament in the monofilament or 50D ~ 900D of 0.40mm；Totally standby with clean water；
Wherein low elastic polyester filament 75%, phosphorus flame retardant 65%；
Step 2, prepares six carbon fluoroacrylic resin mixture, six carbon fluoroacrylic resins and water is carried out according to 50g/L
Dispersion, is modulated into the working solution of six carbon fluoroacrylic resin mixture；
Step 3, by the working solution pH value modulation in step 2 to 6.7；
Step 4, the low elastic polyester filament that step 1 is obtained is put in the working solution in step 3, pads infiltration 5h,
Step 5, prebaking, baking temperature are 120 °/60min；
Carry out baking after step 6, step 5 and then obtain flame-retardant water-repellent and refuse oily braided wires, baking temperature is 170 °/5min；
The flame-retardant water-repellent that step 6 is obtained is refused oily braided wires and is wrapped on reel, reel is placed on 24 Revolving ingots by step 7
On seam loop, flame-retardant water-repellent is woven into using the mode of interlacing and refuses oily woven cloth.
The flame-retardant water-repellent that step 7 is obtained refuses oily woven cloth thread count for 18 mesh numbers（Note：Mesh number is referred in every 25.4mm
Crossover node quantity）, nonwoven fabric layer thickness be 0.1 ~ 10mm, fire-retardant rank >=V-1 levels, GBT19977- is used in water repellent grade >=10
Without immersion oil phenomenon in 2005 standard testings, 30s.
Embodiment 3：
A kind of flame-retardant water-repellent refuses the preparation method of oily woven cloth, comprises the steps：
Step 1, prepares low elastic polyester filament, adds phosphorus flame retardant in low elastic polyester filament filamentation；Preparation reaches 0.10～
A kind of multifilament in the monofilament or 50D ~ 900D of 0.40mm；Totally standby with clean water；
Wherein low elastic polyester filament 50%, phosphorus flame retardant 45%；
Step 2, prepares six carbon fluoroacrylic resin mixture, six carbon fluoroacrylic resins and water is carried out according to 40g/L
Dispersion, is modulated into the working solution of six carbon fluoroacrylic resin mixture；
Step 3, by the working solution pH value modulation in step 2 to 6.0；
Step 4, the low elastic polyester filament that step 1 is obtained is put in the working solution in step 3, pads infiltration 24h,
Step 5, prebaking, baking temperature are 105 °/1h；
Carry out baking after step 6, step 5 and then obtain flame-retardant water-repellent and refuse oily braided wires, baking temperature is 175 °/30min；
The flame-retardant water-repellent that step 6 is obtained is refused oily braided wires and is wrapped on reel, reel is placed on 24 Revolving ingots by step 7
On seam loop, flame-retardant water-repellent is woven into using the mode of interlacing and refuses oily woven cloth.
The flame-retardant water-repellent that step 7 is obtained refuses oily woven cloth thread count for 1 ~ 100 mesh number（Note：Mesh number refers to every 25.4mm
Interior crossover node quantity）, nonwoven fabric layer thickness be 0.1 ~ 10mm, fire-retardant rank >=V-1 levels, water repellent grade >=9, use
Without immersion oil phenomenon in GBT19977-2005 standard testings, 30s.
Above-described embodiment can be read a book, and embodiment 2 is the preferred embodiments of the present invention, by adding the resistance of phosphorus system in the present invention
Fire agent to reach fire-retardant purpose, as on the one hand phosphorus flame retardant forms phosphoric acid as dehydrant, and facilitate charcoal, the generation of charcoal
The conduction of heat from flame to condensed phase is can be reduced, on the other hand, phosphoric acid absorbs heat, and reduces heating process, while the resistance of phosphorus system
Combustion agent reaches the purpose of water and oil repellant with six carbon fluoroacrylic resins with the use of reaching to form one layer of waterproof membrane.
The preferred embodiments of the present invention are had been described in detail above, but the present invention is not limited to these embodiments, in the present invention
Application range in can carry out various changes.Although simply illustrating the preferred embodiments of the present invention above, institute
Category those skilled in the art will be apparent that substantially without departing from the present invention novelty and advantage in the range of, can be to showing
Example property embodiment carries out various modifications.
Claims (4)
1. a kind of flame-retardant water-repellent refuses oily woven cloth, it is characterised in that its component by mass percentage is：
Low elastic polyester filament 60～75%,
Phosphorus flame retardant 20～65%,
Six carbon fluoroacrylic resins 10～35%；
The phosphorus flame retardant is phosphate ester, phosphite ester, one or more combination in organic phosphate, the phosphorous flame-retardant
Agent PPM >=6300.
2. flame-retardant water-repellent according to claim 1 refuses oily woven cloth, it is characterised in that the low elastic polyester filament be 0.10～
The monofilament of 0.40mm or for a kind of multifilament in 50D ~ 900D.
3. a kind of flame-retardant water-repellent refuses the preparation method of oily woven cloth, it is characterised in that comprise the steps：
Step 1, prepares low elastic polyester filament, adds phosphorus flame retardant in low elastic polyester filament filamentation；Preparation reaches 0.10～
A kind of multifilament in the monofilament or 50D ~ 900D of 0.40mm；Totally standby with clean water；
Step 2, prepares six carbon fluoroacrylic resin mixture, by six carbon fluoroacrylic resins with water according to 30～50g/L
Disperseed, be modulated into the working solution of six carbon fluoroacrylic resin mixture；
Step 3, by the working solution pH value modulation in step 2 to 5.8～6.7；
Step 4, the low elastic polyester filament that step 1 is obtained is put in the working solution in step 3, pads infiltration 1min～5h,
Step 5, prebaking, baking temperature are 100 °～120 °/1min ~ 1h；
Carrying out baking after step 6, step 5 and then obtain flame-retardant water-repellent and refuse oily braided wires, baking temperature is 150 °～180 °/1 ~
30min；
The flame-retardant water-repellent that step 6 is obtained is refused oily braided wires and is wrapped on reel by step 7, and reel is placed on Revolving ingot braiding
On machine, flame-retardant water-repellent is woven into using the mode of interlacing and refuses oily woven cloth.
4. method according to claim 3, it is characterised in that the flame-retardant water-repellent that step 7 is obtained refuses oily woven cloth weft density
Spend for 1 ~ 100 mesh number, nonwoven fabric layer thickness is 0.1 ~ 10mm.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201611236026.1A CN106498544A (en) | 2016-12-28 | 2016-12-28 | A kind of flame-retardant water-repellent refuses oily woven cloth and preparation method thereof |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201611236026.1A CN106498544A (en) | 2016-12-28 | 2016-12-28 | A kind of flame-retardant water-repellent refuses oily woven cloth and preparation method thereof |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| CN106498544A true CN106498544A (en) | 2017-03-15 |
Family
ID=58334578
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN201611236026.1A Pending CN106498544A (en) | 2016-12-28 | 2016-12-28 | A kind of flame-retardant water-repellent refuses oily woven cloth and preparation method thereof |
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Cited By (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN113152087A (en) * | 2021-04-07 | 2021-07-23 | 伊科纳米科技(苏州)有限公司 | Waterproof flame-retardant finishing agent and finishing process of polyester fabric by using same |
| CN114214843A (en) * | 2021-12-21 | 2022-03-22 | 绍兴兆丰绒织品有限公司 | Finishing process of flame-retardant polyester |
Citations (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| JPH06136666A (en) * | 1992-10-26 | 1994-05-17 | Teijin Ltd | Antifouling flame retardant polyester textile product and its production |
| CN101709547A (en) * | 2009-12-08 | 2010-05-19 | 苏州双轮化纤有限公司 | Flame-retardant finishing process for polyester-cotton blended fabric |
| CN102704277A (en) * | 2012-06-07 | 2012-10-03 | 浙江真北纺织新材料研究院有限公司 | Manufacturing method of multifunctional outdoor protective fabric |
-
2016
- 2016-12-28 CN CN201611236026.1A patent/CN106498544A/en active Pending
Patent Citations (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| JPH06136666A (en) * | 1992-10-26 | 1994-05-17 | Teijin Ltd | Antifouling flame retardant polyester textile product and its production |
| CN101709547A (en) * | 2009-12-08 | 2010-05-19 | 苏州双轮化纤有限公司 | Flame-retardant finishing process for polyester-cotton blended fabric |
| CN102704277A (en) * | 2012-06-07 | 2012-10-03 | 浙江真北纺织新材料研究院有限公司 | Manufacturing method of multifunctional outdoor protective fabric |
Cited By (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN113152087A (en) * | 2021-04-07 | 2021-07-23 | 伊科纳米科技(苏州)有限公司 | Waterproof flame-retardant finishing agent and finishing process of polyester fabric by using same |
| CN113152087B (en) * | 2021-04-07 | 2023-08-04 | 伊科纳米科技(苏州)有限公司 | Waterproof flame-retardant finishing agent and finishing process for polyester fabric by using same |
| CN114214843A (en) * | 2021-12-21 | 2022-03-22 | 绍兴兆丰绒织品有限公司 | Finishing process of flame-retardant polyester |
| CN114214843B (en) * | 2021-12-21 | 2024-01-30 | 绍兴兆丰绒织品有限公司 | Finishing process of flame-retardant polyester |
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Application publication date: 20170315 |