CN106496820A - A kind of rubber hose material and preparation method thereof - Google Patents

A kind of rubber hose material and preparation method thereof Download PDF

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Publication number
CN106496820A
CN106496820A CN201611054945.7A CN201611054945A CN106496820A CN 106496820 A CN106496820 A CN 106496820A CN 201611054945 A CN201611054945 A CN 201611054945A CN 106496820 A CN106496820 A CN 106496820A
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Prior art keywords
parts
raw material
rubber hose
rubber
hose material
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CN201611054945.7A
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杨雪梅
王维佳
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Anhui Mei Xiangsu Industry Co Ltd
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Anhui Mei Xiangsu Industry Co Ltd
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Priority to CN201611054945.7A priority Critical patent/CN106496820A/en
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    • CCHEMISTRY; METALLURGY
    • C08ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08LCOMPOSITIONS OF MACROMOLECULAR COMPOUNDS
    • C08L23/00Compositions of homopolymers or copolymers of unsaturated aliphatic hydrocarbons having only one carbon-to-carbon double bond; Compositions of derivatives of such polymers
    • C08L23/02Compositions of homopolymers or copolymers of unsaturated aliphatic hydrocarbons having only one carbon-to-carbon double bond; Compositions of derivatives of such polymers not modified by chemical after-treatment
    • C08L23/16Elastomeric ethene-propene or ethene-propene-diene copolymers, e.g. EPR and EPDM rubbers
    • CCHEMISTRY; METALLURGY
    • C08ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08LCOMPOSITIONS OF MACROMOLECULAR COMPOUNDS
    • C08L29/00Compositions of homopolymers or copolymers of compounds having one or more unsaturated aliphatic radicals, each having only one carbon-to-carbon double bond, and at least one being terminated by an alcohol, ether, aldehydo, ketonic, acetal or ketal radical; Compositions of hydrolysed polymers of esters of unsaturated alcohols with saturated carboxylic acids; Compositions of derivatives of such polymers
    • C08L29/10Homopolymers or copolymers of unsaturated ethers
    • CCHEMISTRY; METALLURGY
    • C08ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08KUse of inorganic or non-macromolecular organic substances as compounding ingredients
    • C08K2201/00Specific properties of additives
    • C08K2201/011Nanostructured additives
    • CCHEMISTRY; METALLURGY
    • C08ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08LCOMPOSITIONS OF MACROMOLECULAR COMPOUNDS
    • C08L2201/00Properties
    • C08L2201/08Stabilised against heat, light or radiation or oxydation
    • CCHEMISTRY; METALLURGY
    • C08ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08LCOMPOSITIONS OF MACROMOLECULAR COMPOUNDS
    • C08L2203/00Applications
    • C08L2203/18Applications used for pipes
    • CCHEMISTRY; METALLURGY
    • C08ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08LCOMPOSITIONS OF MACROMOLECULAR COMPOUNDS
    • C08L2205/00Polymer mixtures characterised by other features
    • C08L2205/02Polymer mixtures characterised by other features containing two or more polymers of the same C08L -group
    • CCHEMISTRY; METALLURGY
    • C08ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08LCOMPOSITIONS OF MACROMOLECULAR COMPOUNDS
    • C08L2205/00Polymer mixtures characterised by other features
    • C08L2205/03Polymer mixtures characterised by other features containing three or more polymers in a blend
    • C08L2205/035Polymer mixtures characterised by other features containing three or more polymers in a blend containing four or more polymers in a blend

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  • Chemical & Material Sciences (AREA)
  • Health & Medical Sciences (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Medicinal Chemistry (AREA)
  • Polymers & Plastics (AREA)
  • Organic Chemistry (AREA)
  • Compositions Of Macromolecular Compounds (AREA)

Abstract

The invention discloses a kind of rubber hose material and preparation method thereof, the rubber hose material is made up of the raw material of following weight portion:20 50 parts of ethylene propylene diene rubber, 20 50 parts of perfluoroelastomers, 3 10 parts of TCEP, 3 10 parts of dibenzoate, 8 16 parts of kaolin, 37 parts of activated magnesia, 4 12 parts of stearic acid, 26 parts of titanium dioxide, 15 parts of accelerator, 15 parts of inorganic active agent, 4 10 parts of zinc methacrylate, 26 parts of age resistor, 15 parts of nano zine oxide, 25 parts of hydrocarbon oil, 26 parts of vaseline, 27 parts of APP, 2.5 6 parts of coupling agent.Relative to prior art, the heat resistance and ageing-resistant performance of the rubber hose material in the present invention is more preferable, long service life.

Description

A kind of rubber hose material and preparation method thereof
Technical field
The invention belongs to technical field of rubber material, more particularly to a kind of rubber hose material and preparation method thereof.
Background technology
Rubber hose material is widely used in field of industrial production, and with its good heat-resisting, oil resistant, ozone resistance Approved by manufacturing enterprise.It is well known that automotive hose is exactly one of rubber hose material product, constitute in the part of automobile In, radiator hose is connected between the engine of automobile and radiator, plays conveying coolant to ensure the normal of engine The effect of work.Due to the heat-resisting, cold-resistant of engine radiator flexible pipe, oil resistant, the properties such as ageing-resistant restriction, thus lead Cause its Long-Time Service aging, be easily broken, and the safe operation to automobile brings huge potential safety hazard.
Content of the invention
It is an object of the invention to provide a kind of rubber hose material and preparation method thereof, which can be with effectively solving background technology In the technical problem that is previously mentioned.
For achieving the above object, the present invention provides following technical scheme:
A kind of rubber hose material, which is made up of the raw material of following weight portion:Ethylene propylene diene rubber 20-50 parts, perfluoroether Rubber 20-50 parts, TCEP 3-10 parts, dibenzoate 3-10 parts, kaolin 8-16 parts, activated magnesia 3-7 parts, Stearic acid 4-12 parts, titanium dioxide 2-6 parts, accelerator 1-5 parts, inorganic active agent 1-5 parts, zinc methacrylate 4-10 parts are prevented old Agent 2-6 parts, nano zine oxide 1-5 parts, hydrocarbon oil 2-5 parts, vaseline 2-6 parts, APP 2-7 parts, coupling agent 2.5-6 Part.
Preferably, described rubber hose material is made up of the raw material of following weight portion:50 parts of ethylene propylene diene rubber, perfluor 30 parts of ether rubber, 6 parts of TCEP, 6 parts of dibenzoate, 13 parts of kaolin, 4 parts of activated magnesia, 8 parts of stearic acid, 3.6 parts of titanium dioxide, 2.5 parts of accelerator, 3 parts of inorganic active agent, 7 parts of zinc methacrylate, 4 parts of age resistor, nano zine oxide 3 Part, 3 parts of hydrocarbon oil, 3 parts of vaseline, 6 parts of APP, 4 parts of coupling agent.
Preferably, described rubber hose material is made up of the raw material of following weight portion:40 parts of ethylene propylene diene rubber, perfluor 40 parts of ether rubber, 9 parts of TCEP, 9 parts of dibenzoate, 15 parts of kaolin, 6 parts of activated magnesia, 10 parts of stearic acid, 3.5 parts of titanium dioxide, 3 parts of accelerator, 2.5 parts of inorganic active agent, 7 parts of zinc methacrylate, 4.5 parts of age resistor, nano zine oxide 2.3 parts, 4 parts of hydrocarbon oil, 2 parts of vaseline, 5 parts of APP, 4 parts of coupling agent.
Preferably, described rubber hose material is made up of the raw material of following weight portion:48 parts of ethylene propylene diene rubber, perfluor 35 parts of ether rubber, 6 parts of TCEP, 8 parts of dibenzoate, 13 parts of kaolin, 5 parts of activated magnesia, 5 parts of stearic acid, 3 parts of titanium dioxide, 2 parts of accelerator, 3 parts of inorganic active agent, 7 parts of zinc methacrylate, 5 parts of age resistor, 5 parts of nano zine oxide, virtue 3 parts of fragrant hydrocarbon ils, 4 parts of vaseline, 6 parts of APP, 5 parts of coupling agent.
The preparation method of described rubber hose material, it is characterised in that comprise the following steps:
(1) each raw material components are weighed according to ratio of weight and number;
(2) mill is opened, mill temperature is adjusted to 50-55 DEG C, ethylene propylene diene rubber, perfluoroelastomers is added simultaneously Enter mill, the 20-24min that plasticates obtains broken-down rubber after being cooled to room temperature;
(3) temperature of banbury is adjusted to 130-138 DEG C, adds the broken-down rubber in step (2), after mixing 8-12min Add TCEP, dibenzoate, kaolin, activated magnesia, stearic acid, titanium dioxide, accelerator, inorganic active Agent, zinc methacrylate, age resistor, nano zine oxide, hydrocarbon oil, vaseline, APP and coupling agent, knead 22- After 26min, elastomeric compound is obtained;
(4) vulcanizing press is put into after the elastomeric compound in step (3) being loaded mould, in 14-16MPa, 158-165 DEG C of bar Heat-insulation pressure keeping 10-16min under part, is cooled to room temperature and obtains preparing raw material;
(5) the preparation raw material in step (4) are placed in an oven, 7-9h, cooling is incubated under the conditions of 106-112 DEG C The rubber hose material is obtained to room temperature.
Compared with prior art, the invention has the beneficial effects as follows:
Rubber hose material in the present invention in addition to primary raw material component ethylene propylene diene rubber, perfluoroelastomers are added with, It is additionally added the originals such as TCEP, kaolin, activated magnesia, titanium dioxide, inorganic active agent, age resistor and nano zine oxide Material, thus make its heat resistance and ageing-resistant performance more preferably, long service life.
Specific embodiment
Technical scheme is described in detail with reference to embodiment, but protection domain is not limited thereto.
Embodiment one:
A kind of rubber hose material is made up of the raw material of following weight portion:42 parts of ethylene propylene diene rubber, perfluoroelastomers 35 Part, 6 parts of TCEP, 5 parts of dibenzoate, 11 parts of kaolin, 6 parts of activated magnesia, 7 parts of stearic acid, titanium dioxide 3.8 Part, 2.6 parts of accelerator, 3 parts of inorganic active agent, 6 parts of zinc methacrylate, 4 parts of age resistor, 3 parts of nano zine oxide, hydrocarbon oil 2 parts, 3 parts of vaseline, 5 parts of APP, 3.5 parts of coupling agent.
The preparation method of described rubber hose material, comprises the following steps:
(1) each raw material components are weighed according to ratio of weight and number;
(2) mill is opened, mill temperature is adjusted to 50-55 DEG C, ethylene propylene diene rubber, perfluoroelastomers is added simultaneously Enter mill, the 20-24min that plasticates obtains broken-down rubber after being cooled to room temperature;
(3) temperature of banbury is adjusted to 130-138 DEG C, adds the broken-down rubber in step (2), after mixing 8-12min Add TCEP, dibenzoate, kaolin, activated magnesia, stearic acid, titanium dioxide, accelerator, inorganic active Agent, zinc methacrylate, age resistor, nano zine oxide, hydrocarbon oil, vaseline, APP and coupling agent, knead 22- After 26min, elastomeric compound is obtained;
(4) vulcanizing press is put into after the elastomeric compound in step (3) being loaded mould, in 14-16MPa, 158-165 DEG C of bar Heat-insulation pressure keeping 10-16min under part, is cooled to room temperature and obtains preparing raw material;
(5) the preparation raw material in step (4) are placed in an oven, 7-9h, cooling is incubated under the conditions of 106-112 DEG C The rubber hose material is obtained to room temperature.
Embodiment two:
A kind of rubber hose material is made up of the raw material of following weight portion:35 parts of ethylene propylene diene rubber, perfluoroelastomers 46 Part, 6 parts of TCEP, 7 parts of dibenzoate, 14 parts of kaolin, 6 parts of activated magnesia, 10 parts of stearic acid, titanium dioxide 4.8 parts, 3.6 parts of accelerator, 2.6 parts of inorganic active agent, 6 parts of zinc methacrylate, 5 parts of age resistor, 2 parts of nano zine oxide, virtue 2.5 parts of fragrant hydrocarbon ils, 3.4 parts of vaseline, 4.3 parts of APP, 5 parts of coupling agent.
The preparation method of described rubber hose material, comprises the following steps:
(1) each raw material components are weighed according to ratio of weight and number;
(2) mill is opened, mill temperature is adjusted to 50-55 DEG C, ethylene propylene diene rubber, perfluoroelastomers is added simultaneously Enter mill, the 20-24min that plasticates obtains broken-down rubber after being cooled to room temperature;
(3) temperature of banbury is adjusted to 130-138 DEG C, adds the broken-down rubber in step (2), after mixing 8-12min Add TCEP, dibenzoate, kaolin, activated magnesia, stearic acid, titanium dioxide, accelerator, inorganic active Agent, zinc methacrylate, age resistor, nano zine oxide, hydrocarbon oil, vaseline, APP and coupling agent, knead 22- After 26min, elastomeric compound is obtained;
(4) vulcanizing press is put into after the elastomeric compound in step (3) being loaded mould, in 14-16MPa, 158-165 DEG C of bar Heat-insulation pressure keeping 10-16min under part, is cooled to room temperature and obtains preparing raw material;
(5) the preparation raw material in step (4) are placed in an oven, 7-9h, cooling is incubated under the conditions of 106-112 DEG C The rubber hose material is obtained to room temperature.
Embodiment three:
A kind of rubber hose material is made up of the raw material of following weight portion:42 parts of ethylene propylene diene rubber, perfluoroelastomers 45 Part, 9 parts of TCEP, 7 parts of dibenzoate, 13 parts of kaolin, 5 parts of activated magnesia, 9 parts of stearic acid, titanium dioxide 5 Part, 4 parts of accelerator, 3 parts of inorganic active agent, 7 parts of zinc methacrylate, 5 parts of age resistor, 4 parts of nano zine oxide, hydrocarbon oil 3 Part, 5.5 parts of vaseline, 6 parts of APP, 5 parts of coupling agent.
The preparation method of described rubber hose material, comprises the following steps:
(1) each raw material components are weighed according to ratio of weight and number;
(2) mill is opened, mill temperature is adjusted to 50-55 DEG C, ethylene propylene diene rubber, perfluoroelastomers is added simultaneously Enter mill, the 20-24min that plasticates obtains broken-down rubber after being cooled to room temperature;
(3) temperature of banbury is adjusted to 130-138 DEG C, adds the broken-down rubber in step (2), after mixing 8-12min Add TCEP, dibenzoate, kaolin, activated magnesia, stearic acid, titanium dioxide, accelerator, inorganic active Agent, zinc methacrylate, age resistor, nano zine oxide, hydrocarbon oil, vaseline, APP and coupling agent, knead 22- After 26min, elastomeric compound is obtained;
(4) vulcanizing press is put into after the elastomeric compound in step (3) being loaded mould, in 14-16MPa, 158-165 DEG C of bar Heat-insulation pressure keeping 10-16min under part, is cooled to room temperature and obtains preparing raw material;
(5) the preparation raw material in step (4) are placed in an oven, 7-9h, cooling is incubated under the conditions of 106-112 DEG C The rubber hose material is obtained to room temperature.
Example IV:
A kind of rubber hose material is made up of the raw material of following weight portion:50 parts of ethylene propylene diene rubber, perfluoroelastomers 30 Part, 6 parts of TCEP, 6 parts of dibenzoate, 13 parts of kaolin, 4 parts of activated magnesia, 8 parts of stearic acid, titanium dioxide 3.6 Part, 2.5 parts of accelerator, 3 parts of inorganic active agent, 7 parts of zinc methacrylate, 4 parts of age resistor, 3 parts of nano zine oxide, hydrocarbon oil 3 parts, 3 parts of vaseline, 6 parts of APP, 4 parts of coupling agent.
The preparation method of described rubber hose material, comprises the following steps:
(1) each raw material components are weighed according to ratio of weight and number;
(2) mill is opened, mill temperature is adjusted to 50-55 DEG C, ethylene propylene diene rubber, perfluoroelastomers is added simultaneously Enter mill, the 20-24min that plasticates obtains broken-down rubber after being cooled to room temperature;
(3) temperature of banbury is adjusted to 130-138 DEG C, adds the broken-down rubber in step (2), after mixing 8-12min Add TCEP, dibenzoate, kaolin, activated magnesia, stearic acid, titanium dioxide, accelerator, inorganic active Agent, zinc methacrylate, age resistor, nano zine oxide, hydrocarbon oil, vaseline, APP and coupling agent, knead 22- After 26min, elastomeric compound is obtained;
(4) vulcanizing press is put into after the elastomeric compound in step (3) being loaded mould, in 14-16MPa, 158-165 DEG C of bar Heat-insulation pressure keeping 10-16min under part, is cooled to room temperature and obtains preparing raw material;
(5) the preparation raw material in step (4) are placed in an oven, 7-9h, cooling is incubated under the conditions of 106-112 DEG C The rubber hose material is obtained to room temperature.
Embodiment five:
A kind of rubber hose material is made up of the raw material of following weight portion:40 parts of ethylene propylene diene rubber, perfluoroelastomers 40 Part, 9 parts of TCEP, 9 parts of dibenzoate, 15 parts of kaolin, 6 parts of activated magnesia, 10 parts of stearic acid, titanium dioxide 3.5 parts, 3 parts of accelerator, 2.5 parts of inorganic active agent, 7 parts of zinc methacrylate, 4.5 parts of age resistor, 2.3 parts of nano zine oxide, 4 parts of hydrocarbon oil, 2 parts of vaseline, 5 parts of APP, 4 parts of coupling agent.
The preparation method of described rubber hose material, comprises the following steps:
(1) each raw material components are weighed according to ratio of weight and number;
(2) mill is opened, mill temperature is adjusted to 50-55 DEG C, ethylene propylene diene rubber, perfluoroelastomers is added simultaneously Enter mill, the 20-24min that plasticates obtains broken-down rubber after being cooled to room temperature;
(3) temperature of banbury is adjusted to 130-138 DEG C, adds the broken-down rubber in step (2), after mixing 8-12min Add TCEP, dibenzoate, kaolin, activated magnesia, stearic acid, titanium dioxide, accelerator, inorganic active Agent, zinc methacrylate, age resistor, nano zine oxide, hydrocarbon oil, vaseline, APP and coupling agent, knead 22- After 26min, elastomeric compound is obtained;
(4) vulcanizing press is put into after the elastomeric compound in step (3) being loaded mould, in 14-16MPa, 158-165 DEG C of bar Heat-insulation pressure keeping 10-16min under part, is cooled to room temperature and obtains preparing raw material;
(5) the preparation raw material in step (4) are placed in an oven, 7-9h, cooling is incubated under the conditions of 106-112 DEG C The rubber hose material is obtained to room temperature.
Embodiment six:
A kind of rubber hose material is made up of the raw material of following weight portion:48 parts of ethylene propylene diene rubber, perfluoroelastomers 35 Part, 6 parts of TCEP, 8 parts of dibenzoate, 13 parts of kaolin, 5 parts of activated magnesia, 5 parts of stearic acid, titanium dioxide 3 Part, 2 parts of accelerator, 3 parts of inorganic active agent, 7 parts of zinc methacrylate, 5 parts of age resistor, 5 parts of nano zine oxide, hydrocarbon oil 3 Part, 4 parts of vaseline, 6 parts of APP, 5 parts of coupling agent.
The preparation method of described rubber hose material, comprises the following steps:
(1) each raw material components are weighed according to ratio of weight and number;
(2) mill is opened, mill temperature is adjusted to 50-55 DEG C, ethylene propylene diene rubber, perfluoroelastomers is added simultaneously Enter mill, the 20-24min that plasticates obtains broken-down rubber after being cooled to room temperature;
(3) temperature of banbury is adjusted to 130-138 DEG C, adds the broken-down rubber in step (2), after mixing 8-12min Add TCEP, dibenzoate, kaolin, activated magnesia, stearic acid, titanium dioxide, accelerator, inorganic active Agent, zinc methacrylate, age resistor, nano zine oxide, hydrocarbon oil, vaseline, APP and coupling agent, knead 22- After 26min, elastomeric compound is obtained;
(4) vulcanizing press is put into after the elastomeric compound in step (3) being loaded mould, in 14-16MPa, 158-165 DEG C of bar Heat-insulation pressure keeping 10-16min under part, is cooled to room temperature and obtains preparing raw material;
(5) the preparation raw material in step (4) are placed in an oven, 7-9h, cooling is incubated under the conditions of 106-112 DEG C The rubber hose material is obtained to room temperature.
Finally illustrate, above example is only unrestricted in order to technical scheme to be described, although with reference to compared with Good embodiment has been described in detail to the present invention, it will be understood by those within the art that, can be to the skill of the present invention Art scheme is modified or equivalent, and without deviating from the objective and scope of the technical program, which all should be covered in the present invention Right in the middle of.

Claims (5)

1. a kind of rubber hose material, it is characterised in that be made up of the raw material of following weight portion:Ethylene propylene diene rubber 20-50 parts, Perfluoroelastomers 20-50 parts, TCEP 3-10 parts, dibenzoate 3-10 parts, kaolin 8-16 parts, activated magnesia 3-7 parts, stearic acid 4-12 parts, titanium dioxide 2-6 parts, accelerator 1-5 parts, inorganic active agent 1-5 parts, zinc methacrylate 4-10 Part, age resistor 2-6 parts, nano zine oxide 1-5 parts, hydrocarbon oil 2-5 parts, vaseline 2-6 parts, APP 2-7 parts, coupling agent 2.5-6 part.
2. rubber hose material according to claim 1, it is characterised in that be made up of the raw material of following weight portion:Ternary 50 parts of EP rubbers, 30 parts of perfluoroelastomers, 6 parts of TCEP, 6 parts of dibenzoate, 13 parts of kaolin, active oxidation 4 parts of magnesium, 8 parts of stearic acid, 3.6 parts of titanium dioxide, 2.5 parts of accelerator, 3 parts of inorganic active agent, 7 parts of zinc methacrylate, age resistor 4 Part, 3 parts of nano zine oxide, 3 parts of hydrocarbon oil, 3 parts of vaseline, 6 parts of APP, 4 parts of coupling agent.
3. rubber hose material according to claim 1, it is characterised in that be made up of the raw material of following weight portion:Ternary 40 parts of EP rubbers, 40 parts of perfluoroelastomers, 9 parts of TCEP, 9 parts of dibenzoate, 15 parts of kaolin, active oxidation 6 parts of magnesium, 10 parts of stearic acid, 3.5 parts of titanium dioxide, 3 parts of accelerator, 2.5 parts of inorganic active agent, 7 parts of zinc methacrylate, age resistor 4.5 parts, 2.3 parts of nano zine oxide, 4 parts of hydrocarbon oil, 2 parts of vaseline, 5 parts of APP, 4 parts of coupling agent.
4. rubber hose material according to claim 1, it is characterised in that be made up of the raw material of following weight portion:Ternary 48 parts of EP rubbers, 35 parts of perfluoroelastomers, 6 parts of TCEP, 8 parts of dibenzoate, 13 parts of kaolin, active oxidation 5 parts of magnesium, 5 parts of stearic acid, 3 parts of titanium dioxide, 2 parts of accelerator, 3 parts of inorganic active agent, 7 parts of zinc methacrylate, 5 parts of age resistor, 5 parts of nano zine oxide, 3 parts of hydrocarbon oil, 4 parts of vaseline, 6 parts of APP, 5 parts of coupling agent.
5. the preparation method of the rubber hose material according to any one of claim 1-4, it is characterised in that including following Step:
(1) each raw material components are weighed according to ratio of weight and number;
(2) mill is opened, and mill temperature is adjusted to 50-55 DEG C, ethylene propylene diene rubber, perfluoroelastomers are simultaneously introduced out Mill, the 20-24min that plasticates obtain broken-down rubber after being cooled to room temperature;
(3) temperature of banbury is adjusted to 130-138 DEG C, adds the broken-down rubber in step (2), add after mixing 8-12min TCEP, dibenzoate, kaolin, activated magnesia, stearic acid, titanium dioxide, accelerator, inorganic active agent, first Base zinc acrylate resin, age resistor, nano zine oxide, hydrocarbon oil, vaseline, APP and coupling agent, after mixing 22-26min, Obtain elastomeric compound;
(4) vulcanizing press is put into after the elastomeric compound in step (3) being loaded mould, under the conditions of 14-16MPa, 158-165 DEG C Heat-insulation pressure keeping 10-16min, is cooled to room temperature and obtains preparing raw material;
(5) the preparation raw material in step (4) are placed in an oven, 7-9h is incubated under the conditions of 106-112 DEG C, is cooled to room Temperature obtains the rubber hose material.
CN201611054945.7A 2016-11-25 2016-11-25 A kind of rubber hose material and preparation method thereof Pending CN106496820A (en)

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Cited By (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN109054344A (en) * 2018-07-18 2018-12-21 苏州环亚软管塑业有限公司 A kind of preparation method of high-strength ageing plastic flexible pipe material

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Publication number Priority date Publication date Assignee Title
CN104312010A (en) * 2014-09-23 2015-01-28 青岛美嘉隆包装机械有限公司 Vehicle rubber hose material
CN105273322A (en) * 2015-08-18 2016-01-27 苏州国泰科技发展有限公司 Automobile rubber hose modified rubber material and preparation method thereof
CN106046460A (en) * 2016-07-14 2016-10-26 吴明才 High-elasticity wear-resistant rubber shoe sole material and preparation method thereof

Patent Citations (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN104312010A (en) * 2014-09-23 2015-01-28 青岛美嘉隆包装机械有限公司 Vehicle rubber hose material
CN105273322A (en) * 2015-08-18 2016-01-27 苏州国泰科技发展有限公司 Automobile rubber hose modified rubber material and preparation method thereof
CN106046460A (en) * 2016-07-14 2016-10-26 吴明才 High-elasticity wear-resistant rubber shoe sole material and preparation method thereof

Non-Patent Citations (1)

* Cited by examiner, † Cited by third party
Title
韩永杰 等主编: "《工程实践》", 31 August 2012, 哈尔滨工程大学出版社 *

Cited By (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN109054344A (en) * 2018-07-18 2018-12-21 苏州环亚软管塑业有限公司 A kind of preparation method of high-strength ageing plastic flexible pipe material

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