CN106490571A - A kind of microcapsule embedded acidity regulator and preparation method thereof - Google Patents

A kind of microcapsule embedded acidity regulator and preparation method thereof Download PDF

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Publication number
CN106490571A
CN106490571A CN201610967580.0A CN201610967580A CN106490571A CN 106490571 A CN106490571 A CN 106490571A CN 201610967580 A CN201610967580 A CN 201610967580A CN 106490571 A CN106490571 A CN 106490571A
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CN
China
Prior art keywords
acidity regulator
parts
wall material
microcapsule embedded
core
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Pending
Application number
CN201610967580.0A
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Chinese (zh)
Inventor
何贝
何松
苏子良
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GUANGDONG GUANGYI TECHNOLOGY Co Ltd
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GUANGDONG GUANGYI TECHNOLOGY Co Ltd
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Priority to CN201610967580.0A priority Critical patent/CN106490571A/en
Publication of CN106490571A publication Critical patent/CN106490571A/en
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Abstract

The present invention relates to technical field of food additives, and in particular to a kind of microcapsule embedded acidity regulator and preparation method thereof, it is by wall material and acidity regulator core with weight than 1 30:Leavening agent core is embedded by 31 compositions, wall material;The wall material is at least one in Distilled glycerin monostearate, sorbitan mono-oleic acid ester, hydrogenated vegetable oil, single glycerol monolaurate, diacetyl tartarate list double glyceride, polyglyceryl fatty acid ester, stearoylketene sodium lactate and stearoylketene calcium lactate;The acidity regulator core is at least one in glucono-delta-lactone, malic acid, citric acid and fumaric acid.The microcapsule embedded acidity regulator of the present invention can Controlled acidity conditioning agent release under certain condition speed, reacted with other materials in advance so as to reduce acidity regulator in some environments;And the acidity regulator after embedding, moisture-sensitive, is not easy to store and transports.

Description

A kind of microcapsule embedded acidity regulator and preparation method thereof
Technical field
The present invention relates to technical field of food additives, and in particular to a kind of microcapsule embedded acidity regulator and its preparation Method.
Background technology
Used as the main additive of food tart flavour, which can improve a poor appetite acid, can adjust the pH value of food again, with When can also be beneficial to preservative and play more preferable fresh-keeping effect.If but acid runs into carbonate etc. and easily produces carbon dioxide gas Body, makes leavening agent play a role ahead of time, and anaphase effect can then weaken.In addition, some acids such as citric acid, lactone Deng its hygroscopicity is stronger, when normal temperature is stored, it is easy to caking occurs and affects the use of product.
Content of the invention
In order to overcome shortcoming and defect present in prior art, it is an object of the invention to provide a kind of microcapsule embedded Acidity regulator, the microcapsule embedded acidity regulator can under certain condition Controlled acidity conditioning agent release speed, from And reduce acidity regulator and react with other materials in advance in some environments;And the acidity regulator after embedding, no Moisture-sensitive, is easy to store and transports.
Another object of the present invention is to providing a kind of preparation method of microcapsule embedded acidity regulator, the preparation method Acidity regulator is embedded by microcapsule embedded technology, can under certain condition Controlled acidity conditioning agent release speed Degree, is reacted with other materials in some environments in advance so as to reduce acidity regulator.
The purpose of the present invention is achieved through the following technical solutions:A kind of microcapsule embedded acidity regulator, it by wall material and Acidity regulator core compares 1-30 with weight:3-1 is constituted, and leavening agent core is embedded by wall material;
The wall material be Distilled glycerin monostearate, sorbitan mono-oleic acid ester, hydrogenated vegetable oil, single glycerol monolaurate, At least one in diacetyl tartarate list double glyceride, polyglyceryl fatty acid ester, stearoylketene sodium lactate and stearoylketene calcium lactate;
The acidity regulator core is at least one in glucono-δ-lactone, malic acid, citric acid and fumaric acid.
Because most preservative only has in acid condition, its antiseptic effect could be preferably played.After embedding Acidity regulator do not interfere with dough, without worrying to destroy gluten structure because of too sour, and acidity can also be played simultaneously Synergistic effect of the conditioning agent to preservative.The microcapsule embedded acidity regulator of the present invention can Controlled acidity under certain condition The speed of conditioning agent release, is reacted with other materials in some environments in advance so as to reduce acidity regulator;And embed Later acidity regulator, moisture-sensitive, is not easy to store and transports.
Preferably, the wall material is Distilled glycerin monostearate.Distilled glycerin monostearate be through monoglyceride again Secondary purification, its purity can typically reach more than 95%, also been removed some impurity of monoglyceride.The present invention is by using steaming Glycerin monostearate is evaporated as wall material, can play improves baked product(It is primarily directed to bread or cake)The effect of tissue Really;And wall material belongs to oil soluble material, it is not easy to react in water, and protect acidity adjustment soluble in water well The using effect of agent core.
Preferably, the wall material includes the raw material of following weight portion:Distilled glycerin monostearate 30-80 parts and hydrogenation are planted Thing oil 10-70 parts.The present invention is by being used as wall material using Distilled glycerin monostearate and hydrogenated vegetable oil, and controls its weight Than for 30-80:10-70, can play improves the effect of baked product tissue.
Preferably, the wall material also includes sorbitan mono-oleic acid ester 1-10 parts.The present invention is by single stearic using distillation Acid glyceride, hydrogenated vegetable oil and sorbitan mono-oleic acid ester are used as wall material, and control its weight ratio for 30-80:10-70:1- 10, can play improves the effect of baked product tissue.
Preferably, the wall material also includes stearoylketene sodium lactate 1-10 parts.The present invention is by sweet using distillation monostearate Grease, hydrogenated vegetable oil, sorbitan mono-oleic acid ester and stearoylketene sodium lactate are used as wall material, and control its weight ratio for 30-80: 10-70:1-10:1-10, can play improves the effect of baked product tissue.
Preferably, the acidity regulator core includes the raw material of following weight portion:Glucono-δ-lactone 10-80 parts With citric acid 1-10 parts.The present invention is used as acidity regulator compounding use by adopting glucono-δ-lactone and citric acid, and Its weight ratio is controlled for 10-80:1-10, can adjust the pH value of dough.
The acidity regulator of embedding can apply to the product of a lot of compoundings, individually can also make in addition to auxiliary anticorrosion With.Lactone easily makes albuminous degeneration, so be applied directly in cake act on auxiliary anticorrosion well, but which easily makes egg Leucismus and occur tissue caking phenomenon.The contact of lactone and cake slurries can be just avoided using the lactone for embedding, The phenomenon of cake tissue caking is avoided, while also having played the effect of good auxiliary anticorrosion synergy.
The easy moisture absorption of the acidity regulator that do not embed and conglomeration, cause not allow easy to maintain.Acidity regulator after embedding is kept away The problem is exempted from, has solved the problems, such as transport and carry out compounding conglomeration with other materials.
It is more highly preferred to, the acidity regulator core includes the raw material of following weight portion:Glucono-δ-lactone 30- 50 parts and citric acid 3-8 parts.
It is more highly preferred to, the acidity regulator core includes the raw material of following weight portion:45 parts of glucono-δ-lactone With 5 parts of citric acid.
Preferably, the acidity regulator core also includes filler 1-10 parts, and the filler is wheat flour and/or jade Rice starch., by adopting above-mentioned filler, its filling effect is good for the present invention.It is more highly preferred to, the filler is cornstarch.
A kind of preparation method of microcapsule embedded acidity regulator, after first melt wall material at a temperature of 70-150 DEG C, throws The acidity regulator core for entering mixed material stirs, and carries out spray congealing granulation by centrifugal spray tower, and microcapsules bag is obtained Bury acidity regulator.
The beneficial effects of the present invention is:The microcapsule embedded acidity regulator of the present invention can Controlled acidity under certain condition The speed of conditioning agent release, is reacted with other materials in some environments in advance so as to reduce acidity regulator;And embed Later acidity regulator, moisture-sensitive, is not easy to store and transports.
The preparation method of the present invention is embedded to acidity regulator by microcapsule embedded technology, can be in certain condition The speed of lower Controlled acidity conditioning agent release, is occurred instead with other materials in some environments in advance so as to reduce acidity regulator Should;Step is simple, convenient operation and control, steady quality, and production efficiency is high, and low production cost can large-scale industrial production.
Specific embodiment
For the ease of the understanding of those skilled in the art, with reference to embodiment, the present invention is further illustrated, real The content that the mode of applying is referred to not limitation of the invention.
Embodiment 1
A kind of microcapsule embedded acidity regulator, it compare 1 by wall material and acidity regulator core with weight:3 compositions, wall material will be swollen Loose agent core embedding;
The wall material includes the raw material of following weight portion:40 parts of 55 parts of Distilled glycerin monostearate and hydrogenated vegetable oil;
The wall material is glucono-δ-lactone.
A kind of preparation method of microcapsule embedded acidity regulator, after first melt wall material at a temperature of 70 DEG C, input is mixed The acidity regulator core of honest material stirs, and carries out spray congealing granulation by centrifugal spray tower, and microcapsule embedded acid is obtained Degree conditioning agent.
Embodiment 2
A kind of microcapsule embedded acidity regulator, it compare 10 by wall material and acidity regulator core with weight:2.5 compositions, wall material Leavening agent core is embedded;
The wall material includes the raw material of following weight portion:30 parts of Distilled glycerin monostearate, 10 parts of hydrogenated vegetable oil and sorb 1 part of alcohol acid anhydride monoleate;
The acidity regulator core includes the raw material of following weight portion:10 parts of glucono-δ-lactone, 1 part of citric acid and jade 1 part of rice starch.
A kind of preparation method of microcapsule embedded acidity regulator, after first melt wall material at a temperature of 90 DEG C, input is mixed The acidity regulator core of honest material stirs, and carries out spray congealing granulation by centrifugal spray tower, and microcapsule embedded acid is obtained Degree conditioning agent.
Embodiment 3
A kind of microcapsule embedded acidity regulator, it compare 15 by wall material and acidity regulator core with weight:2 compositions, wall material will Leavening agent core is embedded;
The wall material includes the raw material of following weight portion:55 parts of Distilled glycerin monostearate, 40 parts of hydrogenated vegetable oil and sorb 5 parts of alcohol acid anhydride monoleate;
The acidity regulator core includes the raw material of following weight portion:45 parts of glucono-δ-lactone, 5 parts of citric acid and jade 5 parts of rice starch.
A kind of preparation method of microcapsule embedded acidity regulator, after first melt wall material at a temperature of 110 DEG C, input is mixed The acidity regulator core of honest material stirs, and carries out spray congealing granulation by centrifugal spray tower, and microcapsule embedded acid is obtained Degree conditioning agent.
Embodiment 4
A kind of microcapsule embedded acidity regulator, it compare 20 by wall material and acidity regulator core with weight:1.5 compositions, wall material Leavening agent core is embedded;
The wall material includes the raw material of following weight portion:80 parts of Distilled glycerin monostearate, 70 parts of hydrogenated vegetable oil and sorb 10 parts of alcohol acid anhydride monoleate;
The acidity regulator core includes the raw material of following weight portion:80 parts of glucono-δ-lactone, 10 parts of citric acid and jade 10 parts of rice starch.
A kind of preparation method of microcapsule embedded acidity regulator, after first melt wall material at a temperature of 130 DEG C, input is mixed The acidity regulator core of honest material stirs, and carries out spray congealing granulation by centrifugal spray tower, and microcapsule embedded acid is obtained Degree conditioning agent.
Embodiment 5
A kind of microcapsule embedded acidity regulator, it compare 30 by wall material and acidity regulator core with weight:1 composition, wall material will Leavening agent core is embedded;
The wall material is sorbitan mono-oleic acid ester, single glycerol monolaurate, diacetyl tartarate list double glyceride, polyglycerol ester Fat acid esters, stearoylketene sodium lactate or stearoylketene calcium lactate;
The acidity regulator core is malic acid, citric acid or fumaric acid.
A kind of preparation method of microcapsule embedded acidity regulator, after first melt wall material at a temperature of 150 DEG C, input is mixed The acidity regulator core of honest material stirs, and carries out spray congealing granulation by centrifugal spray tower, and microcapsule embedded acid is obtained Degree conditioning agent.
Above-described embodiment is the present invention preferably implementation, and in addition, the present invention can be realized with alternate manner, On the premise of without departing from present inventive concept, any obvious replacement is within protection scope of the present invention.

Claims (10)

1. a kind of microcapsule embedded acidity regulator, it is characterised in that:It compares 1- by wall material and acidity regulator core with weight 30:3-1 is constituted, and leavening agent core is embedded by wall material;
The wall material be Distilled glycerin monostearate, sorbitan mono-oleic acid ester, hydrogenated vegetable oil, single glycerol monolaurate, At least one in diacetyl tartarate list double glyceride, polyglyceryl fatty acid ester, stearoylketene sodium lactate and stearoylketene calcium lactate;
The acidity regulator core is at least one in glucono-δ-lactone, malic acid, citric acid and fumaric acid.
2. a kind of microcapsule embedded acidity regulator according to claim 1, it is characterised in that:The wall material is single for distillation Tristerin.
3. a kind of microcapsule embedded acidity regulator according to claim 2, it is characterised in that:The wall material includes as follows The raw material of weight portion:Distilled glycerin monostearate 30-80 parts and hydrogenated vegetable oil 10-70 parts.
4. a kind of microcapsule embedded acidity regulator according to claim 3, it is characterised in that:The wall material also includes mountain Pears alcohol acid anhydride monoleate 1-10 parts.
5. a kind of microcapsule embedded acidity regulator according to claim 4, it is characterised in that:The wall material also includes firmly Ester acyl lactylate 1-10 parts.
6. a kind of microcapsule embedded acidity regulator according to claim 1, it is characterised in that:The acidity regulator core Material includes the raw material of following weight portion:Glucono-δ-lactone 10-80 parts and citric acid 1-10 parts.
7. a kind of microcapsule embedded acidity regulator according to claim 6, it is characterised in that:The acidity regulator core Material includes the raw material of following weight portion:Glucono-δ-lactone 30-50 parts and citric acid 3-8 parts.
8. a kind of microcapsule embedded acidity regulator according to claim 7, it is characterised in that:The acidity regulator core Material includes the raw material of following weight portion:5 parts of 45 parts of glucono-δ-lactone and citric acid.
9. a kind of microcapsule embedded acidity regulator according to claim 6, it is characterised in that:The acidity regulator core Material also includes filler 1-10 parts, and the filler is wheat flour and/or cornstarch.
10. the preparation method of a kind of microcapsule embedded acidity regulator as described in any one of claim 1-9, its feature exist In:After first melt wall material at a temperature of 70-150 DEG C, the acidity regulator core for putting into mixed material stirs, by centrifugation Spray tower carries out spray congealing granulation, and microcapsule embedded acidity regulator is obtained.
CN201610967580.0A 2016-10-31 2016-10-31 A kind of microcapsule embedded acidity regulator and preparation method thereof Pending CN106490571A (en)

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Cited By (10)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN108740971A (en) * 2018-05-14 2018-11-06 中玺(天津)枣业技术工程中心 Green mustard jujube western-style food garnishes and production method
CN109699997A (en) * 2018-12-18 2019-05-03 嘉益食品科技(昆山)有限公司 A kind of production method of the without phosphorus edible compounding leavening agent of no aluminium
CN110150615A (en) * 2019-05-18 2019-08-23 上海早苗食品有限公司 A kind of compounding acidity regulator and preparation method thereof
CN110800978A (en) * 2019-11-20 2020-02-18 义乌市嘉奇食品有限公司 Embedding method of sour agent
US10617617B1 (en) 2018-12-04 2020-04-14 Momentive Performance Materials Inc. Polycarboxylic acid compounds for the treatment of fibrious amino acid based substrates, especially hair
WO2020117516A1 (en) 2018-12-04 2020-06-11 Momentive Performance Materials Inc. Use of polycarboxylic acid compounds for the treatment of fibrous amino acid based substrates, especially hair
CN111685256A (en) * 2020-06-22 2020-09-22 禾川(泉州)生物科技有限责任公司 Natural compound antiseptic emulsifying preservative
CN113508835A (en) * 2021-07-01 2021-10-19 大连果真鲜供应链管理有限公司 Composite microcapsule fruit and vegetable fresh-keeping coating agent and preparation method thereof
US11179312B2 (en) 2017-06-05 2021-11-23 Momentive Performance Materials Inc. Aqueous compositions for the treatment of hair
CN114600931A (en) * 2022-04-22 2022-06-10 福建达利食品科技有限公司 Method for adjusting acidity of cake

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Cited By (12)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US11179312B2 (en) 2017-06-05 2021-11-23 Momentive Performance Materials Inc. Aqueous compositions for the treatment of hair
CN108740971A (en) * 2018-05-14 2018-11-06 中玺(天津)枣业技术工程中心 Green mustard jujube western-style food garnishes and production method
US10617617B1 (en) 2018-12-04 2020-04-14 Momentive Performance Materials Inc. Polycarboxylic acid compounds for the treatment of fibrious amino acid based substrates, especially hair
WO2020117509A1 (en) 2018-12-04 2020-06-11 Momentive Performance Materials Inc. Polycarboxylic acid compounds for the treatment of fibrous amino acid based substrates, especially hair
WO2020117516A1 (en) 2018-12-04 2020-06-11 Momentive Performance Materials Inc. Use of polycarboxylic acid compounds for the treatment of fibrous amino acid based substrates, especially hair
US11090255B2 (en) 2018-12-04 2021-08-17 Momentive Performance Materials Inc. Use of polycarboxylic acid compounds for the treatment of fibrious amino acid based substrates, especially hair
CN109699997A (en) * 2018-12-18 2019-05-03 嘉益食品科技(昆山)有限公司 A kind of production method of the without phosphorus edible compounding leavening agent of no aluminium
CN110150615A (en) * 2019-05-18 2019-08-23 上海早苗食品有限公司 A kind of compounding acidity regulator and preparation method thereof
CN110800978A (en) * 2019-11-20 2020-02-18 义乌市嘉奇食品有限公司 Embedding method of sour agent
CN111685256A (en) * 2020-06-22 2020-09-22 禾川(泉州)生物科技有限责任公司 Natural compound antiseptic emulsifying preservative
CN113508835A (en) * 2021-07-01 2021-10-19 大连果真鲜供应链管理有限公司 Composite microcapsule fruit and vegetable fresh-keeping coating agent and preparation method thereof
CN114600931A (en) * 2022-04-22 2022-06-10 福建达利食品科技有限公司 Method for adjusting acidity of cake

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