CN106483164A - For testing test system and the method for oil sample close flash point - Google Patents
For testing test system and the method for oil sample close flash point Download PDFInfo
- Publication number
- CN106483164A CN106483164A CN201611012611.3A CN201611012611A CN106483164A CN 106483164 A CN106483164 A CN 106483164A CN 201611012611 A CN201611012611 A CN 201611012611A CN 106483164 A CN106483164 A CN 106483164A
- Authority
- CN
- China
- Prior art keywords
- oil sample
- flash
- point
- micro
- test system
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Pending
Links
Classifications
-
- G—PHYSICS
- G01—MEASURING; TESTING
- G01N—INVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES
- G01N25/00—Investigating or analyzing materials by the use of thermal means
- G01N25/50—Investigating or analyzing materials by the use of thermal means by investigating flash-point; by investigating explosibility
- G01N25/52—Investigating or analyzing materials by the use of thermal means by investigating flash-point; by investigating explosibility by determining flash-point of liquids
Landscapes
- Physics & Mathematics (AREA)
- Health & Medical Sciences (AREA)
- Life Sciences & Earth Sciences (AREA)
- Chemical & Material Sciences (AREA)
- Analytical Chemistry (AREA)
- Biochemistry (AREA)
- General Health & Medical Sciences (AREA)
- General Physics & Mathematics (AREA)
- Immunology (AREA)
- Pathology (AREA)
- Investigating Or Analyzing Materials Using Thermal Means (AREA)
Abstract
The present invention relates to a kind of test system for testing oil sample close flash point, wherein, the test system, including：Specimen cup, for accommodating the oil sample；Miniature heating furnace, for heating the oil sample in the specimen cup；The micro- electric arc of high frequency, for lighting a fire to the oil sample；With flash-point detection module, for detecting the flash-point of the oil sample.The invention further relates to a kind of method of testing for testing oil sample close flash point.
Description
Technical field
The invention belongs to field of analytic instrument, in particular it relates to for the test system and the side that test oil sample close flash point
Method.
Background technology
When liter high-temperature is heated, vapor concentration is also gradually increased liquid combustible, when removing, with outside burning things which may cause a fire disaster, the steam that ignites
During with the gaseous mixture of air, top occurs moment scintillation phenomenon, and now the temperature of liquid combustible is close flash point.Liquid
The danger classes of combustible is divided according to close flash point.The ratio of oil product composition can also be judged from the height of close flash point
Weight, identifies that oil product occurs the danger of fire.Close flash point is the very important physical characteristic of liquid combustible.However,
The close flash point instrument being widely used at present has the disadvantages that：Big using sample size, the testing time is long, and cooling velocity is slow.In order to
Overcome disadvantage mentioned above, it would be highly desirable to which exploitation is a kind of using sample size is little, test is fast, the fast cooling survey for testing oil sample close flash point
Test system.
Content of the invention
It is an object of the invention in order to solve the above problems, on the one hand, the present invention provides one kind and closes for testing oil sample
The test system of mouth flash-point, wherein, including：Specimen cup, for accommodating oil sample；Miniature heating furnace, for heating in specimen cup
The oil sample；The micro- electric arc of high frequency, for lighting a fire to oil sample；With flash-point detection module, for detecting the flash-point of oil sample.
According to an aspect of the present invention, miniature heating furnace includes fine air pump, temperature sensor and heater.
According to an aspect of the present invention, temperature sensor can be PT100 temperature sensor.
According to an aspect of the present invention, the micro- electric arc of high frequency is arranged at the outside of specimen cup, and flash-point detection module is light
Electric transducer, to determine the flash-point value of oil sample by the change of the flame light of the micro- electric arc of high frequency.
According to an aspect of the present invention, if the flame light duration is between 8s and 15s, it is determined that Current Temperatures are for dodging
Point.
According to an aspect of the present invention, the micro- electric arc of high frequency is arranged at the inside of specimen cup, and flash-point detection module is micro-
Pressure test device, to determine the flash-point value of oil sample by the air pressure change of the steam of the sample in specimen cup.
According to an aspect of the present invention, micro- pressure test device includes micro-pressure sensor.
On the other hand, the present invention also provides a kind of method of testing for testing oil sample close flash point, wherein, including following
Step：First operation, using the oil sample in miniature heating stove heat specimen cup, and supplements air with fine air pump；Second behaviour
Make, oil sample is lighted a fire using high frequency micro- electric arc；3rd operation, determines the flash-point value of oil sample using flash-point detection module, and
4th operation, records the flash-point value of oil sample using close flash point analysis module.
Compared with prior art, beneficial effects of the present invention：
(1) using the close flash point of the test system and test oil sample of the present invention, using sample size considerably less (1-2mL), both
Tested oil sample is saved, has saved cleaning solvent again, while the discharge of harmful substance is reduced, reduced the body to operating personnel
Body is damaged, and makes to be possibly realized the measurement of some micro rare oil sample close flash points；
(2) due to the volume very little of the test system of the present invention, save and taken up space and electric energy；With
(3) the test system and test speed of the present invention is fast, substantially increases operating efficiency, contributes to producing the quality of product
Control, is that society brings huge benefit.
Description of the drawings
Fig. 1 is the test system of test oil sample close flash point of flash-point detection module when being micro- pressure test device.
Fig. 2 is test system of the flash-point detection module for test oil sample close flash point during photoelectric sensor.
Specific embodiment
The present invention is described in further detail with specific embodiment below in conjunction with the accompanying drawings, described specific embodiment is only right
The present invention is explained, and is not limited to the present invention.
According to the embodiment of the present invention, the present invention provides a kind of such as Fig. 1 or as shown in Figure 2 and remains silent for testing oil sample
The test system of flash-point, which includes：Specimen cup 5, for accommodating oil sample 1；Miniature heating furnace 6, for heating the oil in specimen cup
Sample 1；The micro- electric arc 3 of high frequency, for lighting a fire to oil sample 1；With flash-point detection module, for detecting the flash-point of oil sample 1.
According to the embodiment of the present invention, miniature heating furnace includes fine air pump, temperature sensor and heater.
According to the embodiment of the present invention, temperature sensor can be PT100 temperature sensor.
According to the embodiment of the present invention, the micro- electric arc of high frequency is arranged at the outside of specimen cup, and flash-point detection module is
Photoelectric sensor 7 ', to determine the flash-point value of oil sample by the change of the flame light of the micro- electric arc of high frequency.
According to the embodiment of the present invention, if the flame light duration is between 8s and 15s, it is determined that Current Temperatures are
Flash-point.
According to the embodiment of the present invention, the micro- electric arc of high frequency is arranged at the inside of the specimen cup, and flash-point detection mould
Block is micro- pressure test device 7, to determine the flash-point value of oil sample by the air pressure change of the steam of the sample in specimen cup.
According to the embodiment of the present invention, micro- pressure test device includes micro-pressure sensor.
According to another implementation of the invention, the present invention also provides a kind of test for testing oil sample close flash point
Method, wherein, comprises the following steps：First operation, using the oil sample in miniature heating stove heat specimen cup, and uses fine air
Pump supplements air；Second operation, is lighted a fire to oil sample using the micro- electric arc of high frequency；3rd operation, true using flash-point detection module
The flash-point value of stand oil sample, and the 4th operation, record the flash-point value of oil sample using close flash point analysis module.
Operation principle for testing the test system of oil sample close flash point is as follows：
(1) when the micro- electric arc of high frequency is arranged at the outside of specimen cup, flash-point detection module is micro- pressure test device, test
The test system of oil sample close flash point such as Fig. 1, its Cleaning Principle is：Oil sample 1 is loaded in the specimen cup 5 of carry sample lid 2, cover
Sample lid 2, makes oil sample 1 in confined space, then provides air with fine air pump to the confined space；Use miniature heating
Stove 6 heats the oil sample 1 in confined space；When the temperature of oil sample 1 reaches the temperature for estimating 20 DEG C of below flash-point value, micro- with high frequency
Electric arc 3 is lighted a fire to the steam of 1 ullage of oil sample；During lighting a fire, 1 liquid of oil sample is detected with micro- pressure test device 7
The pressure change of the steam above face, when pressure has almost no change, continues heating oil sample, raises oil sample temperature, under wait
Once light a fire, when pressure becomes suddenly hour as the burning of steam consumes large quantity of air, then firing temperature is close flash point
Value.Said process is a complete test process, it is generally the case that the determination of flash-point value is needed from estimating below flash-point value 20
DEG C begin to test the flash-point value of oil sample, until obtaining flash-point value, this may need repeatedly to test.As described above, when flash-point is examined
When surveying module for micro- pressure test device, whole detection process is all carried out in confined space, need not open sample lid 2,
And detect that by micro- pressure test device 7 pressure change of steam of 1 ullage of oil sample, can determining the flash-point value of oil sample
Intuitively to find out temperature during pressure drop, i.e. flash-point value from corresponding computer software.Test process is simple and convenient, no
With atmosphere, it is prevented from catching fire etc. dangerous, because confined space itself is it is prevented that catch fire.
(2) when the micro- electric arc of high frequency is arranged at the inside of specimen cup, flash-point detection module is photoelectric sensor, tests oil sample
The test system of close flash point such as Fig. 2, its Cleaning Principle is：Oil sample 1 is loaded in the specimen cup 5 of carry sample lid 2, cover sample
Lid 2, makes oil sample 1 in confined space, then provides air with fine air pump to the confined space；With miniature heating furnace 6
Oil sample 1 in heating confined space；When the temperature of oil sample 1 reaches the temperature for estimating 20 DEG C of below flash-point value, by 2 dozens, sample lid
Open and the steam of 1 ullage of oil sample is streaked with the micro- electric arc 3 of high frequency and lighted a fire；During lighting a fire, with photoelectric sensor 7 '
The flame duration of the steam of detection 1 ullage of oil sample, when flame duration is less than 8s or is more than 15s, covers sample
Product lid 2, continues heating oil sample, raises oil sample temperature, wait and lighting a fire next time, when flame duration is between 8s and 15s,
Firing temperature is close flash point value.Said process is a complete test process, it is generally the case that the determination of flash-point value is needed
Will be from the flash-point value for estimating 20 DEG C of below flash-point value and begin to test oil sample, until obtaining flash-point value, this may need repeatedly to survey
Examination.As described above, when flash-point detection module is photoelectric sensor, streaking the steam of 1 ullage of oil sample with the micro- electric arc 3 of high frequency
And during being lighted a fire, sample lid 2 closelys follow the micro- electric arc 3 of high frequency, sample lid 2 can be covered in time, this can reduce high frequency
The time of contact of micro- electric arc 3, the steam of 1 ullage of oil sample and air, the danger that catches fire can be reduced, it is also possible to prevent oil sample
Burn in an atmosphere and discharge substantial amounts of pernicious gas.
Using the close flash point of the test system and test oil sample of the present invention, considerably less using sample size, both saved tested
Oil sample, saves cleaning solvent again, while reducing the discharge of harmful substance, reducing the physical impairment to operating personnel, making
Measurement to some micro rare oil sample close flash points is possibly realized.
Due to the volume very little of the test system of the present invention, save and taken up space and electric energy.
The test system and test speed of the present invention is fast, substantially increases operating efficiency, contributes to producing the quality control of product
System, is that society brings huge benefit.
Embodiments above is only used for that the present invention will be further described, it is impossible to be interpreted as to the scope of the present invention
Limit.Any engineers and technicians for being familiar with the field present invention is done according to foregoing invention content some nonessential change
Enter and adjust, should all be included within the scope of the present invention.
Claims (8)
1. a kind of test system for testing oil sample close flash point, wherein, including：
Specimen cup, for accommodating the oil sample；
Miniature heating furnace, for heating the oil sample in the specimen cup；
The micro- electric arc of high frequency, for lighting a fire to the oil sample；With
Flash-point detection module, for detecting the flash-point of the oil sample.
2. test system according to claim 1, wherein, the miniature heating furnace includes fine air pump, TEMP
Device and heater.
3. test system according to claim 1, wherein, the temperature sensor is PT100 temperature sensor.
4. test system according to claim 1, wherein, the micro- electric arc of the high frequency is arranged at the outside of the specimen cup,
And the flash-point detection module is photoelectric sensor, described to be determined by the change of the flame light of the micro- electric arc of the high frequency
The flash-point value of oil sample.
5. test system according to claim 4, wherein, if the flame light duration is between 8s and 15s,
Determine Current Temperatures for flash-point.
6. test system according to claim 1, wherein, the micro- electric arc of the high frequency is arranged at the inside of the specimen cup,
And the flash-point detection module is micro- pressure test device, with the air pressure of the steam by the sample in the specimen cup
The flash-point value for changing to determine the oil sample.
7. test system according to claim 6, wherein, micro- pressure test device includes micro-pressure sensor.
8. a kind of method of testing for testing oil sample close flash point, wherein, comprises the following steps：
First operation, using the oil sample in miniature heating stove heat specimen cup, and supplements air with fine air pump；
Second operation, is lighted a fire to the oil sample using the micro- electric arc of high frequency；
3rd operation, determines the flash-point value of the oil sample using flash-point detection module, and
4th operation, records the flash-point value of the oil sample using close flash point analysis module.
Applications Claiming Priority (4)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201610955646 | 2016-10-27 | ||
| CN2016109556464 | 2016-10-27 | ||
| CN201610927210 | 2016-10-31 | ||
| CN2016109272104 | 2016-10-31 |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| CN106483164A true CN106483164A (en) | 2017-03-08 |
Family
ID=58272496
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN201611012611.3A Pending CN106483164A (en) | 2016-10-27 | 2016-11-17 | For testing test system and the method for oil sample close flash point |
Country Status (1)
| Country | Link |
|---|---|
| CN (1) | CN106483164A (en) |
Cited By (5)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN109142439A (en) * | 2018-09-03 | 2019-01-04 | 管亮 | Distilling flask, oil product are without ignition type close flash point measuring method and system |
| US20200096198A1 (en) * | 2018-09-20 | 2020-03-26 | Anton Paar Provetec Gmbh | Electric Ignition for Flashpoint Tester |
| CN111537562A (en) * | 2020-04-30 | 2020-08-14 | 上海景颐自动化设备有限公司 | Flash point testing method for explosion-proof pressure detection |
| CN111766269A (en) * | 2020-08-11 | 2020-10-13 | 合肥国轩高科动力能源有限公司 | Automatic testing system and method for closed flash point of lithium ion battery electrolyte |
| CN114441596A (en) * | 2020-10-30 | 2022-05-06 | 中国石油天然气股份有限公司 | Diesel oil flash point testing device and diesel oil flash point testing method |
Citations (7)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| JP2006177976A (en) * | 2006-03-24 | 2006-07-06 | Sumitomo Chemical Co Ltd | Method for controlling mist explosion of flammable liquid |
| CN201170776Y (en) * | 2008-01-31 | 2008-12-24 | 中国人民解放军空军油料研究所 | Trace double-flash tester |
| CN201867385U (en) * | 2010-11-03 | 2011-06-15 | 淄博科通电气科技有限公司 | Stirring, uncapping and igniting integrated device for closed-cup flash point testing instrument |
| CN203101307U (en) * | 2012-12-26 | 2013-07-31 | 苏州市华安普电力工程有限公司 | Closed-cup flash point tester |
| US20140315764A1 (en) * | 2010-10-29 | 2014-10-23 | Racional Energy & Environment Company | Reclaimed Oil |
| CN104535614A (en) * | 2015-01-12 | 2015-04-22 | 国家电网公司 | Automatic measuring device and method for flash point of insulating oil special for electric power |
| CN204694665U (en) * | 2015-04-16 | 2015-10-07 | 中国人民解放军63963部队 | Flash-point pick-up unit |
-
2016
- 2016-11-17 CN CN201611012611.3A patent/CN106483164A/en active Pending
Patent Citations (7)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| JP2006177976A (en) * | 2006-03-24 | 2006-07-06 | Sumitomo Chemical Co Ltd | Method for controlling mist explosion of flammable liquid |
| CN201170776Y (en) * | 2008-01-31 | 2008-12-24 | 中国人民解放军空军油料研究所 | Trace double-flash tester |
| US20140315764A1 (en) * | 2010-10-29 | 2014-10-23 | Racional Energy & Environment Company | Reclaimed Oil |
| CN201867385U (en) * | 2010-11-03 | 2011-06-15 | 淄博科通电气科技有限公司 | Stirring, uncapping and igniting integrated device for closed-cup flash point testing instrument |
| CN203101307U (en) * | 2012-12-26 | 2013-07-31 | 苏州市华安普电力工程有限公司 | Closed-cup flash point tester |
| CN104535614A (en) * | 2015-01-12 | 2015-04-22 | 国家电网公司 | Automatic measuring device and method for flash point of insulating oil special for electric power |
| CN204694665U (en) * | 2015-04-16 | 2015-10-07 | 中国人民解放军63963部队 | Flash-point pick-up unit |
Non-Patent Citations (1)
| Title |
|---|
| 中国石油化工股份有限公司上海高桥分公司: "《中华人民共和国石油化工行业标准》", 10 October 2005 * |
Cited By (7)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN109142439A (en) * | 2018-09-03 | 2019-01-04 | 管亮 | Distilling flask, oil product are without ignition type close flash point measuring method and system |
| US20200096198A1 (en) * | 2018-09-20 | 2020-03-26 | Anton Paar Provetec Gmbh | Electric Ignition for Flashpoint Tester |
| US11635207B2 (en) * | 2018-09-20 | 2023-04-25 | Anton Paar Provetec Gmbh | Electric ignition for flashpoint tester |
| CN111537562A (en) * | 2020-04-30 | 2020-08-14 | 上海景颐自动化设备有限公司 | Flash point testing method for explosion-proof pressure detection |
| CN111766269A (en) * | 2020-08-11 | 2020-10-13 | 合肥国轩高科动力能源有限公司 | Automatic testing system and method for closed flash point of lithium ion battery electrolyte |
| CN114441596A (en) * | 2020-10-30 | 2022-05-06 | 中国石油天然气股份有限公司 | Diesel oil flash point testing device and diesel oil flash point testing method |
| CN114441596B (en) * | 2020-10-30 | 2024-01-30 | 中国石油天然气股份有限公司 | Diesel oil flash point testing device and diesel oil flash point testing method |
Similar Documents
| Publication | Publication Date | Title |
|---|---|---|
| CN106483164A (en) | For testing test system and the method for oil sample close flash point | |
| US9658146B2 (en) | Analysis of rechargeable batteries | |
| CN105489103A (en) | Experiment system for simulating cable burning under fire environment and method thereof | |
| CN201156037Y (en) | Pyrotechnic compound combustion and explosion performance detector | |
| CN201063028Y (en) | Flash point tester for minisize oil plants | |
| CN105092641B (en) | Gas or liquid self-ignition point test device and test method under high-pressure oxygen-enriched environment | |
| CN113791358A (en) | Multi-parameter lithium ion battery safety evaluation device and method | |
| CN101871901A (en) | System and method for detecting thermal protection performance of bunker clothing | |
| CN106769637A (en) | Explosive storage life assesses test system and detection method | |
| CN114217007B (en) | Outer flame ignition platform based on cone calorimeter | |
| CN111189959A (en) | Comprehensive experiment platform for testing powder pyrolysis and combustion characteristics and fire spreading characteristics | |
| CN112083040A (en) | Method for testing flash point of flammable liquid under high-pressure environment | |
| CN205920076U (en) | Full automatic testing device suitable for gaseous autoignition temperature | |
| CN105806880A (en) | Dust cloud ignition temperature testing device and method for determining ignition temperatures of dust cloud | |
| CN101726512A (en) | Method for rapidly testing shortest coal spontaneous combustion period by using external constant heating flow source | |
| CN205038183U (en) | Liquid self -ignition point survey device | |
| US6346420B1 (en) | Method of analyzing a gas mixture to determine its explosibility and system for implementing a method of this kind | |
| CN208109739U (en) | The micro full-automatic analyzer of close flash point | |
| CN110110443A (en) | It is a kind of for quickly examining the emulation mode of the flat combustion characteristics of single cable water | |
| CN114609186A (en) | Device and method for evaluating thermal runaway gas production explosion characteristics of lithium ion battery | |
| CN110895151A (en) | High-temperature performance verification system and method for engine blade tip sensor | |
| CN117693389A (en) | System and method for determining distillation characteristics of petroleum samples by partial distillation | |
| CN205280628U (en) | Visual test analytic system of power battery thermal runaway | |
| CN108918340B (en) | Device and method for testing air release amount of ablation-resistant phenolic resin in pyrolysis process | |
| CN112067659A (en) | Test device for testing high-pressure flash point of flammable liquid |
Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| C06 | Publication | ||
| PB01 | Publication | ||
| SE01 | Entry into force of request for substantive examination | ||
| SE01 | Entry into force of request for substantive examination | ||
| RJ01 | Rejection of invention patent application after publication |
Application publication date: 20170308 |
|
| RJ01 | Rejection of invention patent application after publication |