CN106475061A - A kind of material for air purification and its preparation method and application - Google Patents
A kind of material for air purification and its preparation method and application Download PDFInfo
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- CN106475061A CN106475061A CN201611035010.4A CN201611035010A CN106475061A CN 106475061 A CN106475061 A CN 106475061A CN 201611035010 A CN201611035010 A CN 201611035010A CN 106475061 A CN106475061 A CN 106475061A
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- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
- B01J20/00—Solid sorbent compositions or filter aid compositions; Sorbents for chromatography; Processes for preparing, regenerating or reactivating thereof
- B01J20/22—Solid sorbent compositions or filter aid compositions; Sorbents for chromatography; Processes for preparing, regenerating or reactivating thereof comprising organic material
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- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01D—SEPARATION
- B01D53/00—Separation of gases or vapours; Recovering vapours of volatile solvents from gases; Chemical or biological purification of waste gases, e.g. engine exhaust gases, smoke, fumes, flue gases, aerosols
- B01D53/02—Separation of gases or vapours; Recovering vapours of volatile solvents from gases; Chemical or biological purification of waste gases, e.g. engine exhaust gases, smoke, fumes, flue gases, aerosols by adsorption, e.g. preparative gas chromatography
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- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
- B01J20/00—Solid sorbent compositions or filter aid compositions; Sorbents for chromatography; Processes for preparing, regenerating or reactivating thereof
- B01J20/02—Solid sorbent compositions or filter aid compositions; Sorbents for chromatography; Processes for preparing, regenerating or reactivating thereof comprising inorganic material
- B01J20/10—Solid sorbent compositions or filter aid compositions; Sorbents for chromatography; Processes for preparing, regenerating or reactivating thereof comprising inorganic material comprising silica or silicate
- B01J20/12—Naturally occurring clays or bleaching earth
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- Engineering & Computer Science (AREA)
- Life Sciences & Earth Sciences (AREA)
- Dispersion Chemistry (AREA)
- Geochemistry & Mineralogy (AREA)
- Inorganic Chemistry (AREA)
- Disinfection, Sterilisation Or Deodorisation Of Air (AREA)
- Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
- Solid-Sorbent Or Filter-Aiding Compositions (AREA)
Abstract
The invention discloses a kind of material for air purification and its preparation method and application, this material is made up of the following raw material according to weight portion:31 39 parts of Vermiculitum, 8 16 parts of naphthalene acetic acid, 3 11 parts of tea polyphenols, 59 parts of triethanolamine, 15 parts of guar gum.By Vermiculitum and tea polyphenols mixed grinding, add the stirring of triethanolamine solution heated sealed that mixture A is obtained;Guar gum is mixed heated sealed stirring with naphthalene acid solution and mixture B is obtained;Mixture A is mixed supersound process with mixture B, stirs to doing, calcining obtains final product.The material that the present invention is obtained, has great porosity, and makes it have an enhancing adsorption effect to the adsorptivity of poisonous and harmful substance, the light weight of material, using becoming convenient.The raw material that the present invention adopts is extremely simple, draws materials extensively, preparation technology is easy to operational control, and production cost is greatly lowered, and is suitable to industrialized production.
Description
Technical field
The present invention relates to environment-friendly materials technical field, specifically a kind of material for air purification and its preparation method and application.
Background technology
Atmospheric pollution is increasingly severe in recent years, cooking fume, steam, vehicle exhaust, industrial waste gas, building dust, altogether
Same-action forms the float of in the air, leads to PM2.5 concentration persistently to raise.PM2.5 refers to that in the air diameter is less than or equal to
2.5 μm of particulate matter, also referred to as inhalable particulate matter, the important impact to air quality.PM2.5 is as virus and antibacterial
Carrier, by virus and antibacterial bring in lung, be that the propagation of respiratory infectious disease is added fuel to the flames, serious is detrimental to health.
Being attached to skin makes skin produce various generation dermatosiss, and country quite payes attention to atmospheric environment and air quality, people itself
Urgently crave for pure air, the market of current air purifier is unprecedentedly wide, the air purifier species on market is various, purify
Single effect, clean-up effect is undesirable, typically main equipment, not only heavy be difficult to transport, and for air purification effect
Fruit is also unsatisfactory, studies carefully its underlying cause or the selection of material for air purification is not good, existing scavenging material is adopted in addition
Many with raw material, complicated process of preparation, high cost is it is impossible to meet the demand of people.
Content of the invention
It is an object of the invention to provide a kind of material for air purification and its preparation method and application, to solve above-mentioned background
The problem proposing in technology.
For achieving the above object, the present invention provides following technical scheme:
A kind of material for air purification, is made up of the following raw material according to weight portion:Vermiculitum 31-39 part, naphthalene acetic acid 8-16 part,
Tea polyphenols 3-11 part, triethanolamine 5-9 part, guar gum 1-5 part.
As the further scheme of the present invention:Described material for air purification, is made up of the following raw material according to weight portion:Trematodiasiss
Stone 33-37 part, naphthalene acetic acid 10-14 part, tea polyphenols 5-9 part, triethanolamine 6-8 part, guar gum 2-4 part.
As the further scheme of the present invention:Described material for air purification, is made up of the following raw material according to weight portion:Trematodiasiss
35 parts of stone, 12 parts of naphthalene acetic acid, 7 parts of tea polyphenols, 7 parts of triethanolamine, 3 parts of guar gum.
The present invention another object is that provides a kind of preparation method of material for air purification, comprises the steps of:
1) deionized water of 9.5 times of triethanolamine and its quality is mixed, prepared triethanolamine solution;By naphthalene acetic acid and its
The dehydrated alcohol mixing that 4.8 times of quality, prepared naphthalene acid solution;
2) by Vermiculitum and tea polyphenols mixed grinding, cross 120 mesh sieves, add triethanolamine solution, insert in reactor and
Stir process 1.8h, prepared mixture A is sealed at a temperature of 68 DEG C;
3) guar gum is mixed with naphthalene acid solution, at a temperature of 69 DEG C, seal stir process 55-60min, be obtained
Mixture B;
4) mixture A is mixed with mixture B, be warming up to 72 DEG C and supersound process 38min at such a temperature, ultrasonic power
For 700W, stir at a temperature of 88 DEG C to dry, then calcining 3.8h obtains final product material at a temperature of 365 DEG C.
The present invention another object is that offer application in air-treatment for the described material.
Compared with prior art, the invention has the beneficial effects as follows:
It is primary raw material that the present invention adopts Vermiculitum, mixes with tea polyphenols and mixes through triethanolamine, guar gum and naphthalene acetic acid
The material being obtained after calcining after process, has great porosity, and makes it to poisonous and harmful substance (escherichia coli, golden yellow
Glucose coccus, mycete, ammonia, hydrogen sulfide and formaldehyde etc.) adsorptivity have an enhancing adsorption effect, the light weight of material, use
Become convenient.The raw material that the present invention adopts is extremely simple, draws materials extensively, preparation technology is easy to operational control, production cost
It is greatly lowered, be suitable to industrialized production.
Specific embodiment
Below in conjunction with the embodiment of the present invention, the technical scheme in the embodiment of the present invention is clearly and completely described,
Obviously, described embodiment is only a part of embodiment of the present invention, rather than whole embodiments.Based in the present invention
Embodiment, the every other embodiment that those of ordinary skill in the art are obtained under the premise of not making creative work, all
Belong to the scope of protection of the invention.
Embodiment 1
In the embodiment of the present invention, a kind of material for air purification, it is made up of the following raw material according to weight portion:31 parts of Vermiculitum,
8 parts of naphthalene acetic acid, 3 parts of tea polyphenols, 5 parts of triethanolamine, 1 part of guar gum.
9.5 times of deionized water of triethanolamine and its quality is mixed, prepared triethanolamine solution;By naphthalene acetic acid and its matter
The dehydrated alcohol mixing of 4.8 times of amount, prepared naphthalene acid solution.By Vermiculitum and tea polyphenols mixed grinding, cross 120 mesh sieves, add three
Ethanolamine solutions, insert in reactor and seal stir process 1.8h, prepared mixture A at a temperature of 68 DEG C.By Guar beanss
Glue is mixed with naphthalene acid solution, seals stir process 55min, prepared mixture B at a temperature of 69 DEG C.By mixture A with mixed
Compound B mixes, and is warming up to 72 DEG C and supersound process 38min at such a temperature, and ultrasonic power is 700W, stirs at a temperature of 88 DEG C
Mix to dry, then calcining 3.8h obtains final product material at a temperature of 365 DEG C.
Embodiment 2
In the embodiment of the present invention, a kind of material for air purification, it is made up of the following raw material according to weight portion:39 parts of Vermiculitum,
16 parts of naphthalene acetic acid, 11 parts of tea polyphenols, 9 parts of triethanolamine, 5 parts of guar gum.
9.5 times of deionized water of triethanolamine and its quality is mixed, prepared triethanolamine solution;By naphthalene acetic acid and its matter
The dehydrated alcohol mixing of 4.8 times of amount, prepared naphthalene acid solution.By Vermiculitum and tea polyphenols mixed grinding, cross 120 mesh sieves, add three
Ethanolamine solutions, insert in reactor and seal stir process 1.8h, prepared mixture A at a temperature of 68 DEG C.By Guar beanss
Glue is mixed with naphthalene acid solution, seals stir process 60min, prepared mixture B at a temperature of 69 DEG C.By mixture A with mixed
Compound B mixes, and is warming up to 72 DEG C and supersound process 38min at such a temperature, and ultrasonic power is 700W, stirs at a temperature of 88 DEG C
Mix to dry, then calcining 3.8h obtains final product material at a temperature of 365 DEG C.
Embodiment 3
In the embodiment of the present invention, a kind of material for air purification, it is made up of the following raw material according to weight portion:33 parts of Vermiculitum,
10 parts of naphthalene acetic acid, 5 parts of tea polyphenols, 6 parts of triethanolamine, 2 parts of guar gum.
9.5 times of deionized water of triethanolamine and its quality is mixed, prepared triethanolamine solution;By naphthalene acetic acid and its matter
The dehydrated alcohol mixing of 4.8 times of amount, prepared naphthalene acid solution.By Vermiculitum and tea polyphenols mixed grinding, cross 120 mesh sieves, add three
Ethanolamine solutions, insert in reactor and seal stir process 1.8h, prepared mixture A at a temperature of 68 DEG C.By Guar beanss
Glue is mixed with naphthalene acid solution, seals stir process 58min, prepared mixture B at a temperature of 69 DEG C.By mixture A with mixed
Compound B mixes, and is warming up to 72 DEG C and supersound process 38min at such a temperature, and ultrasonic power is 700W, stirs at a temperature of 88 DEG C
Mix to dry, then calcining 3.8h obtains final product material at a temperature of 365 DEG C.
Embodiment 4
In the embodiment of the present invention, a kind of material for air purification, it is made up of the following raw material according to weight portion:37 parts of Vermiculitum,
14 parts of naphthalene acetic acid, 9 parts of tea polyphenols, 8 parts of triethanolamine, 4 parts of guar gum.
9.5 times of deionized water of triethanolamine and its quality is mixed, prepared triethanolamine solution;By naphthalene acetic acid and its matter
The dehydrated alcohol mixing of 4.8 times of amount, prepared naphthalene acid solution.By Vermiculitum and tea polyphenols mixed grinding, cross 120 mesh sieves, add three
Ethanolamine solutions, insert in reactor and seal stir process 1.8h, prepared mixture A at a temperature of 68 DEG C.By Guar beanss
Glue is mixed with naphthalene acid solution, seals stir process 58min, prepared mixture B at a temperature of 69 DEG C.By mixture A with mixed
Compound B mixes, and is warming up to 72 DEG C and supersound process 38min at such a temperature, and ultrasonic power is 700W, stirs at a temperature of 88 DEG C
Mix to dry, then calcining 3.8h obtains final product material at a temperature of 365 DEG C.
Embodiment 5
In the embodiment of the present invention, a kind of material for air purification, it is made up of the following raw material according to weight portion:35 parts of Vermiculitum,
12 parts of naphthalene acetic acid, 7 parts of tea polyphenols, 7 parts of triethanolamine, 3 parts of guar gum.
9.5 times of deionized water of triethanolamine and its quality is mixed, prepared triethanolamine solution;By naphthalene acetic acid and its matter
The dehydrated alcohol mixing of 4.8 times of amount, prepared naphthalene acid solution.By Vermiculitum and tea polyphenols mixed grinding, cross 120 mesh sieves, add three
Ethanolamine solutions, insert in reactor and seal stir process 1.8h, prepared mixture A at a temperature of 68 DEG C.By Guar beanss
Glue is mixed with naphthalene acid solution, seals stir process 58min, prepared mixture B at a temperature of 69 DEG C.By mixture A with mixed
Compound B mixes, and is warming up to 72 DEG C and supersound process 38min at such a temperature, and ultrasonic power is 700W, stirs at a temperature of 88 DEG C
Mix to dry, then calcining 3.8h obtains final product material at a temperature of 365 DEG C.
Comparative example 1
In addition to not containing triethanolamine, its material content and preparation process are consistent with embodiment 5.
Comparative example 2
In addition to not containing tea polyphenols, its material content and preparation process are consistent with embodiment 5.
Comparative example 3
In addition to not containing triethanolamine and tea polyphenols, its material content and preparation process are consistent with embodiment 5.
Embodiment 6
The material that embodiment 1-5 and comparative example 1-3 are obtained carries out the test of antibiotic property, abnormal flavour removal capacity.
GB21551.1-2008 is pressed in the detection of antibiotic rate《The antibacterial of household electrical appliances and similar applications electrical equipment, degerming, purification function lead to
Then》And JISZ2801:2000《The detection of antibacterial product anti-microbial property and evaluation》The method of testing of regulation is detected, test knot
Fruit is shown in Table 1.
GB/T18883-2002 is pressed in the detection of abnormal flavour clearance《Indoor Air Quality standards》The method of regulation is detected,
Testing time is 30 minutes, and test result is shown in Table 1.
The each embodiment of table 1 prepares product test result
Using raw material and the preparation method of the present invention, obtain various materials and there is excellent Air purification, can
Effectively escherichia coli, staphylococcus glucose coccus and mycete are killed in suppression.Harmful gass for air pollution:Ammonia, sulfur
Change hydrogen and formaldehyde etc. and also there is good adsorption effect.When not containing one of triethanolamine and tea polyphenols or two kinds, only
Change effect all not as good as the resultant effect of the material prepared containing triethanolamine and tea polyphenols, in contrast under each raw material common
When application, the effect killing antibacterial is especially prominent, has obtained greatly strengthening.
It is obvious to a person skilled in the art that the invention is not restricted to the details of above-mentioned one exemplary embodiment, Er Qie
In the case of the spirit or essential attributes of the present invention, the present invention can be realized in other specific forms.Therefore, no matter
From the point of view of which point, embodiment all should be regarded as exemplary, and be nonrestrictive, the scope of the present invention is by appended power
Profit requires rather than described above limits, it is intended that all in the implication and scope of the equivalency of claim by falling
Change is included in the present invention.
Moreover, it will be appreciated that although this specification is been described by according to embodiment, not each embodiment only wraps
Containing an independent technical scheme, only for clarity, those skilled in the art should for this narrating mode of description
Using description as an entirety, the technical scheme in each embodiment can also form those skilled in the art through appropriately combined
Understandable other embodiment.
Claims (5)
1. a kind of material for air purification is it is characterised in that be made up of the following raw material according to weight portion:Vermiculitum 31-39 part, naphthalene second
Sour 8-16 part, tea polyphenols 3-11 part, triethanolamine 5-9 part, guar gum 1-5 part.
2. material for air purification according to claim 1 is it is characterised in that be made up of the following raw material according to weight portion:
Vermiculitum 33-37 part, naphthalene acetic acid 10-14 part, tea polyphenols 5-9 part, triethanolamine 6-8 part, guar gum 2-4 part.
3. material for air purification according to claim 1 is it is characterised in that be made up of the following raw material according to weight portion:
35 parts of Vermiculitum, 12 parts of naphthalene acetic acid, 7 parts of tea polyphenols, 7 parts of triethanolamine, 3 parts of guar gum.
4. a kind of preparation method of described material for air purification as arbitrary in claim 1-3 is it is characterised in that by following steps
Composition:
1) deionized water of 9.5 times of triethanolamine and its quality is mixed, prepared triethanolamine solution;By naphthalene acetic acid and its quality
4.8 times of dehydrated alcohol mixing, prepared naphthalene acid solution;
2) by Vermiculitum and tea polyphenols mixed grinding, cross 120 mesh sieves, add triethanolamine solution, insert in reactor and at 68 DEG C
At a temperature of seal stir process 1.8h, prepared mixture A;
3) guar gum is mixed with naphthalene acid solution, at a temperature of 69 DEG C, seal stir process 55-60min, mixing is obtained
Thing B;
4) mixture A is mixed with mixture B, be warming up to 72 DEG C and supersound process 38min at such a temperature, ultrasonic power is
700W, stirs at a temperature of 88 DEG C to dry, then calcining 3.8h obtains final product material at a temperature of 365 DEG C.
5. application in air-treatment for the described material as arbitrary in claim 1-3.
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Cited By (2)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN107158923A (en) * | 2017-06-30 | 2017-09-15 | 应光森 | A kind of material for air purification and its preparation method and application |
CN108786731A (en) * | 2018-06-19 | 2018-11-13 | 杨秋林 | A kind of nanometer micropore material for air purification and preparation method thereof |
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US20060204559A1 (en) * | 2000-03-23 | 2006-09-14 | Bess William S | Fast dissolving orally consumable films containing an ion exchange resin as a taste masking agent |
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CN105567037A (en) * | 2014-10-08 | 2016-05-11 | 江苏瑞丰科技实业有限公司 | Efficient antibacterial formaldehyde-removing environmental protection coating material |
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2016
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Patent Citations (3)
Publication number | Priority date | Publication date | Assignee | Title |
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US20060204559A1 (en) * | 2000-03-23 | 2006-09-14 | Bess William S | Fast dissolving orally consumable films containing an ion exchange resin as a taste masking agent |
CN103623780A (en) * | 2013-12-11 | 2014-03-12 | 张旭东 | Purifying, adsorbing and sterilizing material and application thereof |
CN105567037A (en) * | 2014-10-08 | 2016-05-11 | 江苏瑞丰科技实业有限公司 | Efficient antibacterial formaldehyde-removing environmental protection coating material |
Non-Patent Citations (1)
Title |
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Cited By (2)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN107158923A (en) * | 2017-06-30 | 2017-09-15 | 应光森 | A kind of material for air purification and its preparation method and application |
CN108786731A (en) * | 2018-06-19 | 2018-11-13 | 杨秋林 | A kind of nanometer micropore material for air purification and preparation method thereof |
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