CN1064471A - Method for manufacturing black porcelain granite slab - Google Patents

Method for manufacturing black porcelain granite slab Download PDF

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Publication number
CN1064471A
CN1064471A CN 91106346 CN91106346A CN1064471A CN 1064471 A CN1064471 A CN 1064471A CN 91106346 CN91106346 CN 91106346 CN 91106346 A CN91106346 A CN 91106346A CN 1064471 A CN1064471 A CN 1064471A
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China
Prior art keywords
slag
granite slab
black porcelain
additive
ore
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Pending
Application number
CN 91106346
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Chinese (zh)
Inventor
曹树梁
吕伟
杜毅
许建华
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Shandong Inst Of New Material
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Shandong Inst Of New Material
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Publication date
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Priority to CN 91106346 priority Critical patent/CN1064471A/en
Publication of CN1064471A publication Critical patent/CN1064471A/en
Pending legal-status Critical Current

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Abstract

The invention provides a kind of manufacture method of black porcelain granite slab, the common wet ball mill of tailings in vanadium extraction and clay, press filtration are become pug or powder process granulation, add mineral substance or trade waste additive, with half-dried pressure, roll extrusion, extrude, conventional industrial means such as slip casting are shaped to tabular, drying is after 1100-1120 ℃ of high-temperature calcination, make black porcelain granite slab through grinding and polishing again, can carry out large-scale industrial production with granule and decorative pattern attractive in appearance.

Description

Method for manufacturing black porcelain granite slab
The present invention relates to the manufacture method of the inorganic black granite slab of a kind of synthetical, specifically be with the tailings in vanadium extraction main raw material add the method that portions additive is made inorganic black granite slab again and again.
It is that one of raw material is made black porcelain goods and made the method that black ceramic polishes decorative sheet with conventional industrial means with the tailings in vanadium extraction that Chinese patent CN85102464 has narrated.The black ceramic polishing decorative sheet of producing is even black, and polished face has mirror effect, and the physical and chemical index of this sheet material is better than the natural black granite in slab.
The lithotome that natural granite is made up of feldspar, quartz, mica etc. is because of its polished face of difference of itself structure construction spot and multiple decorative pattern attractive in appearance in pelletized form.
The objective of the invention is in above-mentioned black ceramic polishing decorative sheet production process, to add portions additive,, be called black porcelain granite slab to produce artificial black granite slab with natural granite particulate state spot and decorative pattern attractive in appearance.
The production process of black ceramic polishing decorative sheet is: with tailings in vanadium extraction and the common wet ball mill of clay, press filtration becomes pug or powder process granulation, use conventional industrial means moulding then, as half-dried pressure, roll extrusion, extrude, slip casting etc. becomes tabular, drying is after 1100-1120 ℃ of high-temperature calcination can make black ceramic polishing decorative sheet through grinding and polishing again.
The present invention adds additive before being achieved in that drying in above-mentioned production process, and then can make black porcelain granite slab through high-temperature calcination and grinding and polishing.Wherein its granularity of the additive of Jia Ruing is 0.1-5mm, and add-on is the 1-50%(weight percent).The additive that adds can be mineral substance or trade waste.Mineral substance can be transparency materials such as optical calcite, corundum, also can be vitrinas such as mica, quartz, feldspar, frit, barite, can also be opaque materials such as fluorite, rhombspar, calcite, iron ore, talcum, natural sand, magnesite, malachite, mine tailing, zeolite, triphane, zircon, clay.Additive can also be a trade waste, as: blast-furnace slag, granulated blast-furnace slag, ferromanganese ore slag, phosphorus slag, slag, iron-tion slag, aluminium ore slag, pyrite slag, lead ore residue, electric furnace chromium slag, cobalt slag etc.
Be exemplified below:
1, with 65 parts of tailings in vanadium extraction, 35 parts of clays add the suitable quantity of water ball milling, and to become fineness be 200 purpose mud, with spray drying device powder process granulation, the adding granularity is the mica 1% about 2mm in powder, compression moulding is tabular through pressing machine again, after 1100 ℃ of calcinings, promptly make black porcelain granite slab with the shredder grinding and polishing.
2, with 65 parts of tailings in vanadium extraction, 35 parts of clays add the suitable quantity of water ball milling and become 200 purpose mud, add granularity in the mud and be the quartz 4% about 0.1mm, mica 2%, unnecessary moisture content is removed in press filtration then, obtains mud cake, mud cake is after stirring, by the roller head machine roll forming is tabular, dry after 1100 ℃ burn till, again through the shredder grinding and polishing.
3, with 60 parts of tailings in vanadium extraction, 40 parts of clays add the suitable quantity of water ball milling, and to become fineness be 180 purpose mud, add granularity in the mud and be the electric furnace chromium slag 2% about 1mm, triphane 2%, excessive moisture is removed in press filtration then, makes moisture about 20% mud cake, mud cake is after stirring, be shaped to by extrusion shaping machine tabular, dry after 1120 ℃ burn till, get final product through the shredder grinding and polishing again.
4, with 65 parts of tailings in vanadium extraction, 35 parts of clays add the suitable quantity of water ball milling, and to become fineness be 200 purpose mud, and adding granularity in the mud is the optical calcite 3% of 1-2mm, fluorite 2%, stir the back be shaped to gypsum mold tabular, dry after 1100 ℃ burn till, get final product through the shredder grinding and polishing again.
5, with 50 parts of tailings in vanadium extraction, 50 parts of clays add the suitable quantity of water ball milling, and to become fineness be 200 order mud, adding fineness in the mud is the quartz 5% of 1-2mm, blast furnace granulated slag 4% zircon 4%, excessive moisture is removed in press filtration then, obtains mud cake, after the mud cake stirring, be shaped to tabularly through roller head machine, burn till through 1100 ℃, grinding and polishing gets final product.
6, with 85 parts of tailings in vanadium extraction, 15 parts of clays add the suitable quantity of water ball milling, and to become fineness be 150 purpose mud, remove excessive moisture through press filtration, with the oven dry of gained mud cake, use the powder beater granulation then, the adding granularity is the frit 45% about 5mm in granulation process, corundum 5%, be tabular through pressing machine compression moulding again, 1100 ℃ are burnt till, and the shredder grinding and polishing can make black porcelain granite slab.
The black porcelain granite slab that is made by the present invention, its burnishing surface visible particulate spot and merocrystalline or fine and close cryptocrystalline decorative pattern attractive in appearance, extremely approximate with natural output granite polishing sheet material, because manufacturing process is easy, the primary raw material cost is low, its cost is natural product granite in slab 1/2-1/4, main physical and chemical index quite or surpass natural granite, rupture strength is granitic 4 times, resistance to compression is that granitic finished product thickness is thinner than granite more than 2 times, and glossiness is higher than natural granite, acidproof, alkaline-resisting, the indexs such as hardness are suitable with granite, can carry out large-scale industrial production.

Claims (3)

1, the common wet ball mill of tailings in vanadium extraction and clay, press filtration are become pug or powder process granulation, become tabular with conventional industrial means moulding then, drying is after 1100-1120 ℃ of high-temperature calcination, make the method for black porcelain granite slab again through grinding and polishing, it is characterized in that adding granularity before dry is 0.1-5mm, add-on is the 1-50%[weight percent] mineral substance or trade waste additive.
2; the manufacture method of black porcelain granite slab according to claim 1; it is characterized in that being meant optical calcite at described mineral additive; transparency materials such as corundum; it also can be mica; quartzy; feldspar; frit; vitrinas such as barite; it can also be fluorite; rhombspar; calcite; iron ore; talcum; natural sand; magnesite; malachite; mine tailing; zeolite; triphane; zircon; opaque material such as clay; described trade waste additive is meant the State of Blast Furnace slag; granulated blast-furnace slag; ferromanganese ore slag; phosphorus slag; slag; iron-tion slag; the aluminium ore slag; the copper mine slag; pyrite slag, lead ore residue; electric furnace chromium slag; cobalt slag etc.
3, the manufacture method of black porcelain granite slab according to claim 1 is characterized in that described mineral substance or trade waste additive can add a kind of, two kinds or multiple common adding wherein.
CN 91106346 1991-03-05 1991-03-05 Method for manufacturing black porcelain granite slab Pending CN1064471A (en)

Priority Applications (1)

Application Number Priority Date Filing Date Title
CN 91106346 CN1064471A (en) 1991-03-05 1991-03-05 Method for manufacturing black porcelain granite slab

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
CN 91106346 CN1064471A (en) 1991-03-05 1991-03-05 Method for manufacturing black porcelain granite slab

Publications (1)

Publication Number Publication Date
CN1064471A true CN1064471A (en) 1992-09-16

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Family Applications (1)

Application Number Title Priority Date Filing Date
CN 91106346 Pending CN1064471A (en) 1991-03-05 1991-03-05 Method for manufacturing black porcelain granite slab

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CN (1) CN1064471A (en)

Cited By (8)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN1091755C (en) * 1995-09-29 2002-10-02 杨德宁 Stereo ceramic granite and marble
CN102910892A (en) * 2012-09-28 2013-02-06 新嘉理(江苏)陶瓷有限公司 Black ceramic plate prepared by natural minerals and extracted vanadium tailings and preparation method of black ceramic plate
CN103435330A (en) * 2013-08-19 2013-12-11 佛山市亮剑陶瓷有限公司 Anti-static ceramic material manufactured by vanadium slags and manufacturing method thereof,
CN103553579A (en) * 2012-12-05 2014-02-05 佛山市唯格瓷砖有限责任公司 Environment-friendly full body porcelain brick having characteristic of natural granite, and preparation method thereof
CN106431458A (en) * 2016-09-18 2017-02-22 攀枝花学院 Method for preparing porous ceramics from vanadium extraction tailings
US10248903B2 (en) * 2016-05-25 2019-04-02 American Express Travel Related Services Company, Inc. Method for creating ceramic-containing transaction cards
US10607125B2 (en) * 2015-02-06 2020-03-31 American Express Travel Related Services Company, Inc. Method of making ceramic-containing transaction cards
CN112939567A (en) * 2019-12-11 2021-06-11 辽宁省轻工科学研究院有限公司 Black ceramic tile prepared by using vanadium extraction tailings and preparation method thereof

Cited By (12)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN1091755C (en) * 1995-09-29 2002-10-02 杨德宁 Stereo ceramic granite and marble
CN102910892A (en) * 2012-09-28 2013-02-06 新嘉理(江苏)陶瓷有限公司 Black ceramic plate prepared by natural minerals and extracted vanadium tailings and preparation method of black ceramic plate
CN103553579A (en) * 2012-12-05 2014-02-05 佛山市唯格瓷砖有限责任公司 Environment-friendly full body porcelain brick having characteristic of natural granite, and preparation method thereof
CN103435330A (en) * 2013-08-19 2013-12-11 佛山市亮剑陶瓷有限公司 Anti-static ceramic material manufactured by vanadium slags and manufacturing method thereof,
CN103435330B (en) * 2013-08-19 2016-03-30 佛山市亮剑陶瓷有限公司 A kind of with the anti-electrostatic ceramic material of vanadium slag production and manufacture method thereof
US10607125B2 (en) * 2015-02-06 2020-03-31 American Express Travel Related Services Company, Inc. Method of making ceramic-containing transaction cards
US11227201B1 (en) 2015-02-06 2022-01-18 American Express Travel Related Services Company, Inc Ceramic transaction cards
US11915075B1 (en) 2015-02-06 2024-02-27 American Express Travel Related Services Company, Inc. Ceramic transaction cards
US10248903B2 (en) * 2016-05-25 2019-04-02 American Express Travel Related Services Company, Inc. Method for creating ceramic-containing transaction cards
CN106431458A (en) * 2016-09-18 2017-02-22 攀枝花学院 Method for preparing porous ceramics from vanadium extraction tailings
CN106431458B (en) * 2016-09-18 2019-05-28 攀枝花学院 The method that tailings in vanadium extraction prepares porous ceramics
CN112939567A (en) * 2019-12-11 2021-06-11 辽宁省轻工科学研究院有限公司 Black ceramic tile prepared by using vanadium extraction tailings and preparation method thereof

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