CN106430990B - A kind of the tcughened glass insulator and its manufacturing method of multilayer gluing - Google Patents

A kind of the tcughened glass insulator and its manufacturing method of multilayer gluing Download PDF

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CN106430990B
CN106430990B CN201610678027.5A CN201610678027A CN106430990B CN 106430990 B CN106430990 B CN 106430990B CN 201610678027 A CN201610678027 A CN 201610678027A CN 106430990 B CN106430990 B CN 106430990B
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CN106430990A (en
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何苗
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Jiangsu Shifeng Enterprise Management Consulting Co.,Ltd.
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Ningbo High Technology Consulting Services Co Ltd
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    • CCHEMISTRY; METALLURGY
    • C03GLASS; MINERAL OR SLAG WOOL
    • C03CCHEMICAL COMPOSITION OF GLASSES, GLAZES OR VITREOUS ENAMELS; SURFACE TREATMENT OF GLASS; SURFACE TREATMENT OF FIBRES OR FILAMENTS MADE FROM GLASS, MINERALS OR SLAGS; JOINING GLASS TO GLASS OR OTHER MATERIALS
    • C03C14/00Glass compositions containing a non-glass component, e.g. compositions containing fibres, filaments, whiskers, platelets, or the like, dispersed in a glass matrix
    • C03C14/004Glass compositions containing a non-glass component, e.g. compositions containing fibres, filaments, whiskers, platelets, or the like, dispersed in a glass matrix the non-glass component being in the form of particles or flakes
    • CCHEMISTRY; METALLURGY
    • C09DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
    • C09JADHESIVES; NON-MECHANICAL ASPECTS OF ADHESIVE PROCESSES IN GENERAL; ADHESIVE PROCESSES NOT PROVIDED FOR ELSEWHERE; USE OF MATERIALS AS ADHESIVES
    • C09J1/00Adhesives based on inorganic constituents
    • C09J1/02Adhesives based on inorganic constituents containing water-soluble alkali silicates
    • HELECTRICITY
    • H01ELECTRIC ELEMENTS
    • H01BCABLES; CONDUCTORS; INSULATORS; SELECTION OF MATERIALS FOR THEIR CONDUCTIVE, INSULATING OR DIELECTRIC PROPERTIES
    • H01B17/00Insulators or insulating bodies characterised by their form
    • H01B17/38Fittings, e.g. caps; Fastenings therefor
    • HELECTRICITY
    • H01ELECTRIC ELEMENTS
    • H01BCABLES; CONDUCTORS; INSULATORS; SELECTION OF MATERIALS FOR THEIR CONDUCTIVE, INSULATING OR DIELECTRIC PROPERTIES
    • H01B19/00Apparatus or processes specially adapted for manufacturing insulators or insulating bodies

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  • Engineering & Computer Science (AREA)
  • Organic Chemistry (AREA)
  • Dispersion Chemistry (AREA)
  • Life Sciences & Earth Sciences (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • General Chemical & Material Sciences (AREA)
  • Geochemistry & Mineralogy (AREA)
  • Materials Engineering (AREA)
  • Ceramic Engineering (AREA)
  • Inorganic Chemistry (AREA)
  • Insulators (AREA)
  • Insulating Bodies (AREA)

Abstract

The invention discloses the tcughened glass insulator and its manufacturing method of a kind of multilayer gluing, which at least can anti lightning abrupt slope peak value 5000kV/s;- 50 DEG C~500 DEG C iterative cycles impacts can be born in normal loading;Still sustainable normal loading after zero degree self-destruction;Bearing stress is not less than 300Mpa;U-shaped notch impact strength is not less than 25J/cm2;Light transmittance is not less than 80%;By way of repeatedly thickening-cooling down, make the insulator of finished product that there is multilayer buffering and support construction, the ballistic work of multi-angle, high frequency time can be born, high-temperature plastic mixture is added in layer structure, is on the one hand convenient to use, on the other hand also increases impact resistance;The tcughened glass insulator good economy performance of multilayer gluing of the invention, impact resistance, fracture toughness is high, comprehensive mechanical performance is good, long service life.

Description

A kind of the tcughened glass insulator and its manufacturing method of multilayer gluing
Technical field
The present invention relates to the tcughened glass insulators and its manufacturer of field of electrical components more particularly to a kind of multilayer gluing Method.
Background technique
Insulator is a kind of special insulation control, can be played an important role in overhead transmission lines.
Insulator is chiefly used in electric pole between one's early years, and the one end for being slowly developed in high type high-tension bus-bar connection tower has hung many disks The insulator of shape, it is usually made of glass or ceramics to increase creepage distance, is just insulator.Insulator is in frame Two basic roles are played in empty transmission line of electricity, i.e., the two effects must be guaranteed support conducting wire with returning with electric current is prevented; Meanwhile insulator should have enough electrical insulation strengths, moisture-resistance and high temperature resistance.
In the related patents applied at home, patent " a kind of glass insulator " (application number: 201210349297.3, Publication date: 2013~01~16), disclosing a kind of composition formula of glass insulator that stability is good, but due to after being powder processed Sintering, brittleness is larger and binding force is poor, can not still retain basic working performance after zero degree self-destruction, and due to powder weight Melt and destroy glass and be quickly cooled down bring tempering effect and bearing stress, mechanical performance is poor and short (the surface of service life Compression can significantly improve service life), on the other hand, there is no toughening and shock resistance processing is carried out, make the glass insulator It is damaged vulnerable to physical impact or cold cycling;Patent " composite glass fiber reinforced insulator " (application number: 201210470969.6, it is public It opens day: 2014~06~04), disclosing a kind of glass insulator of housing pellosil, but since glass body does not carry out intensity Improved treatment, the insulator comprehensive performance is poor, in the invention preferred black pellosil due to light transmittance it is poor, destroy glass Insulator relative to the maximum advantage of porcelain insulator one by one defect as it can be seen that make maintenance replacement it is more difficult, even if insulator Have occurred zero degree self-destruction be also not easy find and handle, on the other hand, due to the invention be not directed to glass insulator ontology into The improvement of row electric property, electric property are poor.
Summary of the invention
To solve drawbacks described above existing in the prior art, the present invention is intended to provide a kind of good economy performance, impact resistance, fracture The tcughened glass insulator and its manufacturing method of toughness height, good, the with long service life multilayer gluing of comprehensive mechanical performance.
To achieve the goals above, the invention adopts the following technical scheme: a kind of tcughened glass insulator of multilayer gluing Manufacturing method, comprising the following steps:
1) raw material prepare
1. glass body raw material comprise the following components in parts by weight: 70~80 parts of silica, 8~10 parts of calcium oxide, 10~15 parts of sodium carbonate and 3~5 parts of magnesia powder, 3~5 parts of straight iron powder, 1~2 part of phosphorus powder, 1~2 part of carbon dust;
2. adhesive raw material comprise the following components in parts by weight: 50~60 parts of sodium metasilicate, 3-5 parts of acetic acid, silicone 10-15 Part, 30-35 parts of pure water;
3. technique auxiliary material includes: enough release agents, enough nitrogen;
4. technological equipment includes: central metal mould and the screw-like structure one of the bottom centre equipped with screw-like structure Austenite stainless steel long bolt, the inner surface of sample thread shape are coated with coating metal mould and the surface layer of WC base wear-resistant coating The matched vibration device of metal mold;
2) melting and reinforcing of glass
1. 1) 1. silica, calcium oxide, sodium carbonate and magnesia powder that step in is prepared are uniformly mixed, then use Electric melting furnace carry out melt process, 1300 DEG C~1400 DEG C of melting temperature, the melting time be reach assigned temperature after keep the temperature 30min~ 40min obtains original glass melt flow stream;
2. step 1. after the completion of, be passed through enough nitrogen, then add straight iron powder, phosphorus powder and carbon dust that in 1) 1. step prepares, It stirs evenly, keeps the temperature 5min~10min, obtain stand-by strengthened glass melt flow stream;
3) center portion insulator forms
1. spraying enough release agents in central metal mould inner surface, it is passed through enough nitrogen, then heats central metal mould To 650 DEG C~700 DEG C, then by part 2) in the stand-by strengthened glass melt flow stream that 2. obtains of step inject central metal mould, until Until central metal mould fills up;
1. 2. step is passed through nitrogen after the completion with the pressure of 5bar~8bar, until central metal mould is cooled to room temperature molding, Insulation subcenter blank is obtained after demoulding;
4) layer structure forms
1. sodium metasilicate, acetic acid, silicone, pure water that step in 1) 2. prepares are mixed and stirred under room temperature environment It is even, obtain stand-by glued liquid;
2. preparing canister, it is passed through enough nitrogen, canister is then heated to 1000 DEG C~1100 DEG C, injection unit Divide the stand-by strengthened glass melt flow stream that in 2) 2. step obtains, is placed in 1000 DEG C~1100 DEG C temperature, nitrogen protection always Environment in, obtain stand-by insulator blank liquid;
3. the austenitic stainless steel screw rod and insulation subcenter blank intermediate thread section structure are connected and through the screw thread Through-hole forms removable insulation subcenter blank;
4. 3. removable insulation subcenter blank that step is obtained is placed in air to being cooled to room temperature, pass through control Austenitic stainless steel screw rod is moved in 1. stand-by glued liquid that step obtains, is then taken out to glued liquid and is solidified;Then may be used Mobile insulation subcenter blank is moved in stand-by insulator blank liquid local environment, is slowly put into after keeping the temperature 20min-30min In stand-by insulator blank liquid, then takes out and be placed in air to being cooled to room temperature;
5. 4. repeating step is less than coating metal model cavity three-dimensional to removable insulation subcenter blank three-D profile size Overall size 5mm-8mm, layer structure insulator blank needed for obtaining;
5) insulator forms
It is coated with enough release agents 1. 4) 5. layer structure insulator blank that step in obtains is placed in and is heated to In 650 DEG C~700 DEG C of coating metal mould, the stand-by strengthened glass melt flow stream that step in 2) 2. obtains then is added, until table Layer metal pattern chamber is filled full, and is started with the matched vibration device of coating metal mould, duration 10min~15min;
1. 2. step is passed through nitrogen after the completion with the pressure of 5bar~8bar, until coating metal mould is cooled to room temperature molding, Insulator blank is obtained after demoulding;
3. carrying out vibrator deburring to 2. insulator blank that step obtains using diamond abrasive vibrator deburring equipment And polishing treatment, that is, insulator needed for obtaining.
A kind of tcughened glass insulator of the multilayer gluing according to manufactured by above-mentioned manufacturing method, the insulator include one The one compound glass layer and multiple glued layers, center portion staggeredly interted is made of glass.
The insulator at least can anti lightning abrupt slope peak value 5000kV/s;- 50 DEG C~500 can be born in normal loading The impact of DEG C iterative cycles;Still sustainable normal loading after zero degree self-destruction;Bearing stress is not less than 300Mpa;U-shaped notch shock Intensity is not less than 25J/cm2;Light transmittance is not less than 80%.
Compared with prior art, the invention has the following advantages that due to being utilized well by managing formula preparation entirely Melt temperature and invalid temperature are higher than 1300 DEG C again after glued liquid out is dry and hard, be successfully realized glass replace with gluing liquid it is cold But, completely new multilayer gluing tcughened glass structure has been prepared;It has mentioned a kind of complete glass formula and its has strengthened ingredient, also Detailed process flow and intensifying method, process is clear, definite principle, is easily achieved;Since profiled insulation has multilayer tempering Glass structure, multilayer tempering glass structure centre is there are also increase binding force and with the adhesive of powerful pooling feature, as branch It supports, pull, stress conduction, in addition every layer of glass structure of glass insulator of the invention all coolings are quickly, that is, using There is very huge pressing stress on steel process, glass insulator surface layer, can offset part foreign impacts power, and there is very high tension in inside, can support Anti- external world's part of impact force, therefore this glass insulator strong shock resistance, have since adhesive also plays every layer of glass structure The effect pullled and fixed, in addition tempered glass zero point self-destruction after will not peel off naturally, still retain significant proportion binding force and Mechanical strength, even if so that this glass insulator have occurred zero point self-destruction, can also continue to complete basic function, until maintenance when it is saturating It is replaced after crossing the high vitreum of light transmittance and can be visually seen crackle, it is easy to use;According to correlative study, iron-phosphorus-carbon system tempering Glass good-toughness, its ontology toughness obtains considerable raising after glass insulator of the invention has dissolved in toughening element, in addition, this Invention has selected optimal procedure parameters during the sintering process, the thermal stress and structural stress of itself insulator remnants is all lower, It joined vibration processes again in later period polishing treatment, homogenize internal stress, improve the uniformity of overall performance, reduce scarce Mouthful sensibility, and the major reason that impact flexibility of the present invention is high, impact flexibility be four times of conventional tempering glass with On, ten times or more of porcelain insulator;Due to using steel process (making flow-like glass metal rapid cooling), glass of the invention is exhausted Center portion is also uncolled when edge sublist layer cools down, and forms oneself however the tensile stress of uniform bearing stress layer and center portion, surface layer Compression can obviously increase fatigue life, and part of impact force is offset when by foreign impacts, the tensile stress of center portion can also Extraneous impact force can be resisted, under comprehensive use, long service life of the invention, comprehensive mechanical performance are good;It is refined due to strengthening Process carries out under nitrogen protection entirely, participates in without impurity, and hot tearing is inclined in process for technical maturity, method of the invention To low, micro-crack is few, therefore the light transmittance of final finished is high, excellent electrical properties.
Detailed description of the invention
Fig. 1 is structural schematic diagram of the invention.
Specific embodiment
Embodiment 1:
A kind of tcughened glass insulator of multilayer gluing, the insulator include staggeredly interspersed compound glass layer and more one by one Layer cementing layer, center portion are made of glass;
The manufacturing method of the tcughened glass insulator of the multilayer gluing the following steps are included:
1) raw material prepare
1. glass body raw material comprise the following components in parts by weight: 70 parts of silica, 8 parts of calcium oxide, sodium carbonate 10 Part and 3 parts of magnesia powder, 3 parts of straight iron powder, 1 part of phosphorus powder, 1 part of carbon dust;
2. adhesive raw material comprise the following components in parts by weight: 50 parts of sodium metasilicate, 3 parts of acetic acid, 10 parts of silicone, pure water 30 parts;
3. technique auxiliary material includes: enough release agents, enough nitrogen;
4. technological equipment includes: central metal mould and the screw-like structure one of the bottom centre equipped with screw-like structure Austenite stainless steel long bolt, the inner surface of sample thread shape are coated with coating metal mould and the surface layer of WC base wear-resistant coating The matched vibration device of metal mold;
2) melting and reinforcing of glass
1. 1) 1. silica, calcium oxide, sodium carbonate and magnesia powder that step in is prepared are uniformly mixed, then use Electric melting furnace carries out melt process, and 1300 DEG C of melting temperature, the melting time is to keep the temperature 30min after reaching assigned temperature, obtains original Glass melting fluid;
2. step 1. after the completion of, be passed through enough nitrogen, then add straight iron powder, phosphorus powder and carbon dust that in 1) 1. step prepares, It stirs evenly, keeps the temperature 5min, obtain stand-by strengthened glass melt flow stream;
3) center portion insulator forms
1. spraying enough release agents in central metal mould inner surface, it is passed through enough nitrogen, then heats central metal mould To 650 DEG C, then by part 2) in the stand-by strengthened glass melt flow stream that 2. obtains of step inject central metal mould, until central metal Until mould fills up;
2. 1. step is passed through nitrogen after the completion with the pressure of 5bar, until central metal mould is cooled to room temperature molding, after demoulding Obtain insulation subcenter blank;
4) layer structure forms
1. sodium metasilicate, acetic acid, silicone, pure water that step in 1) 2. prepares are mixed and stirred under room temperature environment It is even, obtain stand-by glued liquid;
2. preparing canister, be passed through enough nitrogen, canister be then heated to 1000 DEG C, inject part 2) in step Suddenly the stand-by strengthened glass melt flow stream that 2. obtains, is placed in always 1000 DEG C of temperature, in the environment of nitrogen protection, obtains stand-by Insulator blank liquid;
3. the austenitic stainless steel screw rod and insulation subcenter blank intermediate thread section structure are connected and through the screw thread Through-hole forms removable insulation subcenter blank;
4. 3. removable insulation subcenter blank that step is obtained is placed in air to being cooled to room temperature, pass through control Austenitic stainless steel screw rod is moved in 1. stand-by glued liquid that step obtains, is then taken out to glued liquid and is solidified;Then may be used Mobile insulation subcenter blank is moved in stand-by insulator blank liquid local environment, is slowly put into for use absolutely after keeping the temperature 20min In edge blank liquid, then takes out and be placed in air to being cooled to room temperature;
5. 4. repeating step is less than coating metal model cavity three-dimensional to removable insulation subcenter blank three-D profile size Overall size 5mm, layer structure insulator blank needed for obtaining;
5) insulator forms
It is coated with enough release agents 1. 4) 5. layer structure insulator blank that step in obtains is placed in and is heated to In 650 DEG C of coating metal mould, the stand-by strengthened glass melt flow stream that step in 2) 2. obtains then is added, until coating metal mould Type chamber is filled full, and is started with the matched vibration device of coating metal mould, duration 10min;
2. 1. step is passed through nitrogen after the completion with the pressure of 5bar, until coating metal mould is cooled to room temperature molding, after demoulding Obtain insulator blank;
3. carrying out vibrator deburring to 2. insulator blank that step obtains using diamond abrasive vibrator deburring equipment And polishing treatment, that is, insulator needed for obtaining.
It, can anti lightning abrupt slope peak value by the tcughened glass insulation subsample for the multilayer gluing that the present embodiment is produced 6300kV/s;- 50 DEG C~500 DEG C iterative cycles impacts can be born in normal loading;Still sustainable mark after zero degree self-destruction Quasi- load;Bearing stress 380Mpa;U-shaped notch impact strength 33J/cm2;Light transmittance 87%.
Embodiment 2:
A kind of tcughened glass insulator of multilayer gluing, the insulator include staggeredly interspersed compound glass layer and more one by one Layer cementing layer, center portion are made of glass;
The manufacturing method of the tcughened glass insulator of the multilayer gluing the following steps are included:
1) raw material prepare
1. glass body raw material comprise the following components in parts by weight: 80 parts of silica, 10 parts of calcium oxide, sodium carbonate 15 Part and 5 parts of magnesia powder, 5 parts of straight iron powder, 2 parts of phosphorus powder, 2 parts of carbon dust;
2. adhesive raw material comprise the following components in parts by weight: 60 parts of sodium metasilicate, 5 parts of acetic acid, 15 parts of silicone, pure water 35 parts;
3. technique auxiliary material includes: enough release agents, enough nitrogen;
4. technological equipment includes: central metal mould and the screw-like structure one of the bottom centre equipped with screw-like structure Austenite stainless steel long bolt, the inner surface of sample thread shape are coated with coating metal mould and the surface layer of WC base wear-resistant coating The matched vibration device of metal mold;
2) melting and reinforcing of glass
1. 1) 1. silica, calcium oxide, sodium carbonate and magnesia powder that step in is prepared are uniformly mixed, then use Electric melting furnace carries out melt process, and 1400 DEG C of melting temperature, the melting time is to keep the temperature 40min after reaching assigned temperature, obtains original Glass melting fluid;
2. step 1. after the completion of, be passed through enough nitrogen, then add straight iron powder, phosphorus powder and carbon dust that in 1) 1. step prepares, It stirs evenly, keeps the temperature 10min, obtain stand-by strengthened glass melt flow stream;
3) center portion insulator forms
1. spraying enough release agents in central metal mould inner surface, it is passed through enough nitrogen, then heats central metal mould To 700 DEG C, then by part 2) in the stand-by strengthened glass melt flow stream that 2. obtains of step inject central metal mould, until central metal Until mould fills up;
2. 1. step is passed through nitrogen after the completion with the pressure of 8bar, until central metal mould is cooled to room temperature molding, after demoulding Obtain insulation subcenter blank;
4) layer structure forms
1. sodium metasilicate, acetic acid, silicone, pure water that step in 1) 2. prepares are mixed and stirred under room temperature environment It is even, obtain stand-by glued liquid;
2. preparing canister, be passed through enough nitrogen, canister be then heated to 1100 DEG C, inject part 2) in step Suddenly the stand-by strengthened glass melt flow stream that 2. obtains, is placed in always 1100 DEG C of temperature, in the environment of nitrogen protection, obtains stand-by Insulator blank liquid;
3. the austenitic stainless steel screw rod and insulation subcenter blank intermediate thread section structure are connected and through the screw thread Through-hole forms removable insulation subcenter blank;
4. 3. removable insulation subcenter blank that step is obtained is placed in air to being cooled to room temperature, pass through control Austenitic stainless steel screw rod is moved in 1. stand-by glued liquid that step obtains, is then taken out to glued liquid and is solidified;Then may be used Mobile insulation subcenter blank is moved in stand-by insulator blank liquid local environment, is slowly put into for use absolutely after keeping the temperature 30min In edge blank liquid, then takes out and be placed in air to being cooled to room temperature;
5. 4. repeating step is less than coating metal model cavity three-dimensional to removable insulation subcenter blank three-D profile size Overall size 8mm, layer structure insulator blank needed for obtaining;
5) insulator forms
It is coated with enough release agents 1. 4) 5. layer structure insulator blank that step in obtains is placed in and is heated to In 700 DEG C of coating metal mould, the stand-by strengthened glass melt flow stream that step in 2) 2. obtains then is added, until coating metal mould Type chamber is filled full, and is started with the matched vibration device of coating metal mould, duration 15min;
2. 1. step is passed through nitrogen after the completion with the pressure of 8bar, until coating metal mould is cooled to room temperature molding, after demoulding Obtain insulator blank;
3. carrying out vibrator deburring to 2. insulator blank that step obtains using diamond abrasive vibrator deburring equipment And polishing treatment, that is, insulator needed for obtaining.
It, can anti lightning abrupt slope peak value by the tcughened glass insulation subsample for the multilayer gluing that the present embodiment is produced 6600kV/s;- 50 DEG C~500 DEG C iterative cycles impacts can be born in normal loading;Still sustainable mark after zero degree self-destruction Quasi- load;Bearing stress 410Mpa;U-shaped notch impact strength 36J/cm2;Light transmittance 83%.
The foregoing description of the disclosed embodiments, only for can be realized professional and technical personnel in the field or use this Invention.Various modifications to these embodiments will be readily apparent to those skilled in the art, institute herein The General Principle of definition can be realized in other embodiments without departing from the spirit or scope of the present invention.Therefore, The present invention will not be limited to the embodiments shown herein, and is to fit to special with principles disclosed herein and novelty The consistent widest scope of point.

Claims (2)

1. a kind of manufacturing method of the tcughened glass insulator of multilayer gluing, it is characterised in that the following steps are included:
1) raw material prepare
1. glass body raw material comprise the following components in parts by weight: 70~80 parts of silica, 8~10 parts of calcium oxide, carbonic acid 10~15 parts of sodium and 3~5 parts of magnesia powder, 3~5 parts of straight iron powder, 1~2 part of phosphorus powder, 1~2 part of carbon dust;
2. adhesive raw material comprise the following components in parts by weight: 50~60 parts of sodium metasilicate, 3-5 parts of acetic acid, 10-15 parts of silicone, 30-35 parts of pure water;
3. technique auxiliary material includes: enough release agents, enough nitrogen;
4. technological equipment includes: central metal mould, the spiral shell as the screw-like structure that bottom centre is equipped with screw-like structure Austenite stainless steel long bolt, the inner surface of line shape are coated with the coating metal mould and coating metal of WC base wear-resistant coating The matched vibration device of mould;
2) melting and reinforcing of glass
1. 1) 1. silica, calcium oxide, sodium carbonate and magnesia powder that step in is prepared are uniformly mixed, electric smelting is then used Kiln carry out melt process, 1300 DEG C~1400 DEG C of melting temperature, the melting time be reach assigned temperature after keep the temperature 30min~ 40min obtains original glass melt flow stream;
2. step 1. after the completion of, be passed through enough nitrogen, then add straight iron powder, phosphorus powder and carbon dust that in 1) 1. step prepares, stir Uniformly, 5min~10min is kept the temperature, stand-by strengthened glass melt flow stream is obtained;
3) center portion insulator forms
1. spraying enough release agents in central metal mould inner surface, it is passed through enough nitrogen, central metal mould is then heated to 650 DEG C~700 DEG C, then by part 2) in the stand-by strengthened glass melt flow stream that 2. obtains of step inject central metal mould, until center is golden Until category mould fills up;
1. 2. step is passed through nitrogen after the completion with the pressure of 5bar~8bar, until central metal mould is cooled to room temperature molding, demoulding Insulation subcenter blank is obtained afterwards;
4) layer structure forms
1. sodium metasilicate, acetic acid, silicone, pure water that step in 1) 2. prepares are mixed and stirred for uniformly, obtaining under room temperature environment Obtain glued liquid for use;
2. preparing canister, it is passed through enough nitrogen, canister is then heated to 1000 DEG C~1100 DEG C, injects part 2) 2. stand-by strengthened glass melt flow stream that middle step obtains is placed in always 1000 DEG C~1100 DEG C temperature, the ring of nitrogen protection In border, stand-by insulator blank liquid is obtained;
3. the austenitic stainless steel screw rod and insulation subcenter blank intermediate thread section structure are connected and through the tapped through hole, Form removable insulation subcenter blank;
4. 3. removable insulation subcenter blank that step is obtained is placed in air to being cooled to room temperature, by controlling Ovshinsky Body stainless steel screw rod is moved in 1. stand-by glued liquid that step obtains, is then taken out to glued liquid and is solidified;Then it will move Insulation subcenter blank is moved in stand-by insulator blank liquid local environment, is slowly put into for use after keeping the temperature 20min-30min In insulator blank liquid, then takes out and be placed in air to being cooled to room temperature;
5. 4. repeating step is less than coating metal model cavity three-D profile to removable insulation subcenter blank three-D profile size Size 5mm-8mm, layer structure insulator blank needed for obtaining;
5) insulator forms
It is coated with enough release agents 1. 4) 5. layer structure insulator blank that step in obtains is placed in and is heated to 650 DEG C In~700 DEG C of coating metal mould, the stand-by strengthened glass melt flow stream that step in 2) 2. obtains then is added, until coating metal Model cavity is filled full, and is started with the matched vibration device of coating metal mould, duration 10min~15min;
1. 2. step is passed through nitrogen after the completion with the pressure of 5bar~8bar, until coating metal mould is cooled to room temperature molding, demoulding Insulator blank is obtained afterwards;
3. carrying out vibrator deburring and throwing to 2. insulator blank that step obtains using diamond abrasive vibrator deburring equipment Light processing, that is, insulator needed for obtaining.
2. a kind of tcughened glass insulator of multilayer gluing manufactured by manufacturing method according to claim 1, feature Be: the insulator includes that the compound glass layer and multiple glued layers, center portion staggeredly interted one by one is made of glass.
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CN101409119A (en) * 2008-11-18 2009-04-15 上海玻璃机器制造厂有限公司 Laminated toughened glass insulator and preparation method thereof
CN103420609A (en) * 2013-07-24 2013-12-04 浙江大学 Low-loss glass formula and method for manufacturing of DC glass insulator
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