CN106423019A - Insert tube type titanium solution hydrolysis stirring apparatus - Google Patents
Insert tube type titanium solution hydrolysis stirring apparatus Download PDFInfo
- Publication number
- CN106423019A CN106423019A CN201611050893.6A CN201611050893A CN106423019A CN 106423019 A CN106423019 A CN 106423019A CN 201611050893 A CN201611050893 A CN 201611050893A CN 106423019 A CN106423019 A CN 106423019A
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- China
- Prior art keywords
- intubation
- steam
- stirring
- pot
- type titanium
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- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
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Classifications
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- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
- B01J19/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
- B01J19/18—Stationary reactors having moving elements inside
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01F—MIXING, e.g. DISSOLVING, EMULSIFYING OR DISPERSING
- B01F27/00—Mixers with rotary stirring devices in fixed receptacles; Kneaders
- B01F27/80—Mixers with rotary stirring devices in fixed receptacles; Kneaders with stirrers rotating about a substantially vertical axis
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01F—MIXING, e.g. DISSOLVING, EMULSIFYING OR DISPERSING
- B01F35/00—Accessories for mixers; Auxiliary operations or auxiliary devices; Parts or details of general application
- B01F35/90—Heating or cooling systems
- B01F35/91—Heating or cooling systems using gas or liquid injected into the material, e.g. using liquefied carbon dioxide or steam
-
- C—CHEMISTRY; METALLURGY
- C01—INORGANIC CHEMISTRY
- C01G—COMPOUNDS CONTAINING METALS NOT COVERED BY SUBCLASSES C01D OR C01F
- C01G23/00—Compounds of titanium
- C01G23/04—Oxides; Hydroxides
- C01G23/047—Titanium dioxide
- C01G23/053—Producing by wet processes, e.g. hydrolysing titanium salts
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01F—MIXING, e.g. DISSOLVING, EMULSIFYING OR DISPERSING
- B01F35/00—Accessories for mixers; Auxiliary operations or auxiliary devices; Parts or details of general application
- B01F35/90—Heating or cooling systems
- B01F2035/99—Heating
Abstract
The invention discloses an insert tube type titanium solution hydrolysis stirring apparatus and belongs to the technical field of titanium dioxide production. The insert tube type titanium solution hydrolysis stirring apparatus comprises a pot and a steam insert tube, the steam insert tube is perpendicular to and runs through the bottom of the pot, the top end of the steam insert tube is provided with a positioning pin and a first air hole, and an inner cavity of the steam insert tube is communicated with the outside through the first air hole; the apparatus also comprises a stirring shaft, the stirring shaft comprises a stirring tube and blades, the top end of the inner cavity of the stirring tube is provided with a positioning hole mating with the positioning pin, the bottom end of the stirring tube is provided with a second air hole whereby an inner cavity of the stirring tube is communicated with the outside, the bottom end of the stirring tube is provided with a receiving hole, the steam insert tube is inserted into the inner cavity of the stirring tube through the receiving hole, a gap is provided between the outer wall of the steam insert tube and the sidewall of the inner cavity of the stirring tube, and the stirring tube may rotate by centering on the axis of the steam insert tube. The insert tube type titanium solution hydrolysis stirring apparatus enables titanium solution to be mixed and stirred during hydrolysis, and the hydrolysis of the titanium solution is more sufficient.
Description
Technical field
The present invention relates to titanium white production technical field, especially a kind of cannula type titanium hydrolysis agitating device.
Background technology
Domestic production titanium dioxide mainly leans on sulphuric acid legal system titanium dioxide at present, and wherein hydrolytic process is sulfuric acid method titanium pigment life
Produce a vital step, predominantly titanium dioxide from liquid phase be solid phase metatitanic acid, thus miscellaneous with the solubility in mother solution
Matter separates, to extract pure titanium dioxide.
Existing way is that several steam pipes are directly inserted into the bottom of hydrolyzer, using steam ascension heating upwards, but
It is that this way is not high to the utilization ratio of steam, and poor to liquid agitation mixed effect, affect final solid phase metatitanic acid life
Become.
Content of the invention
The technical problem to be solved is：There is provided a kind of cannula type titanium hydrolysis agitating device so that hydrolyzed
The titanium liquid of Cheng Dangzhong is mixedly more abundant, and hydrolysis is more thorough.
The technical solution adopted for the present invention to solve the technical problems is：A kind of cannula type titanium hydrolysis agitating device, bag
Include pot and steam intubation, described steam intubation is vertical and bottom that run through described pot, and the bottom of described steam intubation
It is connected with the outfan of the vapour system being arranged at outside pot, the top of described steam intubation is disposed with from top to bottom determines
Position pin and the first air port, described alignment pin is coaxial with described steam intubation, and described first air port is arranged at described steam intubation
Side wall on and the inner chamber of described steam intubation is connected with the external world；Also include by motor-driven shaft, described stir
Mix axle and include being arranged at described steam intubation periphery and the stirring pipe that is coaxial therewith and being arranged on described stirring pipe lateral wall
Blade, be provided with stirring tube cavity in described stirring pipe, the top of described stirring tube cavity is provided with and described alignment pin phase
The location hole of adaptation, the side wall of described stirring pipe bottom is provided with the second air port making stirring tube cavity be connected with the external world,
Described stirring pipe bottom offers the socket that diameter is adapted with described steam cannula diameter, and described steam intubation is passed through socket and inserted
Enter in described stirring tube cavity, described alignment pin and location hole mutually rotate connection, described steam intubation lateral wall with described
It is provided with gap, described stirring pipe can be rotated centered on the axis of described steam intubation between stirring pipe intracavity sidewall；Also wrap
Include the cantilever being arranged above pot, described cantilever is provided with decelerator and motor, the top of described shaft and setting
The outfan of the decelerator above pot is connected, and the input of described decelerator is connected with motor.
Further, the bottom of described pot is additionally provided with pulley.
Further, also include lifting platform, described lifting platform includes base, lifting plate and lowering or hoisting gear, described
Lifting plate is slidably connected with described pulley by the track being arranged on its top surface, and described base is arranged at the lower section of lifting plate,
Described lifting plate is moved up and down by the lowering or hoisting gear being arranged between described lifting plate and described base；Described lifting plate is permissible
The distance moving up and down is more than vertical dimension h on the top of described alignment pin to described bottom of pot body.
Further, the position in described first air port is higher than the rim of a cup position of described pot.
Further, described lowering or hoisting gear is hydraulic cylinder.
Further, described track is provided with limited block, the position of described limited block and described location hole and positioning
The position of pin axis is adapted.
Further, described steam intubation adopts metal material to make.
The invention has the beneficial effects as follows：Using intubation steam pipe and stirring pipe, titanium liquid is made to be mixed stirring in hydrolysis,
Titanium hydrolysis are more abundant.
Brief description
Fig. 1 is the structural representation of pot and shaft in cannula type titanium hydrolysis agitating device of the present invention.
Fig. 2 is the sectional view in A-A face in cannula type titanium hydrolysis agitating device Fig. 1 of the present invention.
Fig. 3 is the structural representation of stirring pipe in cannula type titanium hydrolysis agitating device of the present invention.
Fig. 4 is the structural representation of cannula type hydrolytic agitator of the present invention.
Fig. 5 is the top view of lifting plate in cannula type hydrolytic agitator of the present invention.
【Concrete symbol description】
1- pot, 2- steam intubation, 3- alignment pin, 4- first air port, 5- shaft, 6- stirring pipe, 7- blade, 8- stirs
Tube cavity, 9- location hole, 10- second air port, 11- socket, 12- cantilever, 13- decelerator, 14- motor, 15- pulley, 16- bottom
Seat, 17- lifting plate, 18- lowering or hoisting gear, 19- track, 20- limited block.
Specific embodiment
The present invention is further described with reference to the accompanying drawings and examples.
As Figure 1-5, a kind of cannula type titanium hydrolysis agitating device, including pot 1 and steam intubation 2, described steaming
Vapour intubation 2 is vertical and bottom that run through described pot 1, and the bottom of described steam intubation 2 and the steam system being arranged at outside pot 1
The outfan of system (in figure is not drawn into) is connected, the top of described steam intubation 2 be disposed with from top to bottom alignment pin 3 and
First air port 4, described alignment pin 3 is coaxial with described steam intubation 2, and described first air port 4 is arranged at the side of described steam intubation 2
On wall and the inner chamber of described steam intubation 2 is connected with the external world；Also include the shaft 5 being driven by motor 14, described stir
Mix axle 5 and include being arranged at described steam intubation 2 periphery and the stirring pipe 6 that is coaxial therewith and being arranged at outside described stirring pipe 6
Blade 7 on wall, be provided with described stirring pipe 6 stirring tube cavity 8, described stirring tube cavity 8 top be provided with described
The location hole 9 that alignment pin 3 is adapted, the side wall of described stirring pipe 6 bottom is provided with makes stirring tube cavity 8 be connected with the external world
The second air port 10, described stirring pipe bottom offers the socket 11 that diameter is adapted, described steaming with described steam intubation 2 diameter
Vapour intubation 2 is inserted in described stirring tube cavity 8 by described socket 11, described alignment pin 3 and the location hole 9 mutually company of rotation
Connect, be provided with gap between described steam intubation 2 lateral wall and described stirring tube cavity 8 side wall, described stirring pipe 6 can be with described
Rotate centered on the axis of steam intubation 2；Also include being arranged at the cantilever 12 of pot 1 top, described cantilever 12 is provided with and subtracts
Fast device 13 and motor 14, the top of described shaft 5 is connected with the outfan of the decelerator 13 being arranged at pot 1 top,
The input of described decelerator 13 is connected with motor 14.
Such scheme is main scheme for implementing said method, and its know-why is：As shown in Fig. 1, Fig. 3, Fig. 4, Implanted Titanium in pot 1
Liquid, the meaning that wherein socket 11 diameter is adapted with steam intubation 2 diameter is that steam intubation can be inserted in socket 11.Steam intubation
2 pass through in socket 11 insertion stirring tube cavity 8, and alignment pin 3 is be combined with each other with location hole 9, starts motor 14, is driven by motor 14
Stirring pipe 6 rotated centered on the axis of described steam intubation 2, the blade 7 on its lateral wall starts titanium liquid is stirred
Mixing.As shown in Fig. 2 the vapour system (in figure is not drawn into) being arranged at outside pot 1 conveys the inner chamber that steam enters steam intubation 2
Interior, steam flows out inner chamber by the first air port 4, then is flowed into the seam that steam intubation 2 lateral wall and stirring tube cavity 8 medial wall are formed
Between gap.Steam presses through liquid, makes titanium liquid discharge stirring pipe 6, steam finally flows out the second air port 10 to the titanium being stored in pot 1
Liquid is heated.While titanium liquid is heated, shaft 6 has carried out mix and blend to titanium liquid, makes the hydrolyzed of titanium liquid
Cheng Gengwei is abundant.
Further, the bottom of described pot 1 is additionally provided with pulley 15, so that pot 1 can be moved.
Further, also include lifting platform, described lifting platform includes base 16, lifting plate 17 and lowering or hoisting gear
18, described lifting plate 17 is slidably connected with described pulley 15 by the track 19 being arranged on its top surface, and described base 16 is arranged
In the lower section of lifting plate 17, described lifting plate 17 is by being arranged at the lowering or hoisting gear between described lifting plate 17 and described base 16
18 move up and down；The distance that described lifting plate 17 can move up and down is more than top to described pot 1 bottom of described alignment pin 3
Vertical dimension h.As Figure 1 and Figure 4, wherein, when the distance of lifting plate 17 movement is more than apart from h, steam intubation 2 is passed through
Move up and down lifting plate 17 and can achieve and separate with shaft 5 or combine.When steam intubation 2 is separated with shaft 5, pot
1 can be can move freely by track 19 and pulley 15.
Further, the position in described first air port 4 is higher than the rim of a cup position of described pot 1.As shown in figure 1, in order to anti-
Only the first air port 4 position is too low leads to titanium liquid to pour in down a chimney in steam intubation 2, so making the position in the first air port 4 be higher than described pot
The rim of a cup position of body 1.
Further, described lowering or hoisting gear 18 is hydraulic cylinder.Hydraulic cylinder, as lowering or hoisting gear 18, has stable movement, goes out
The features such as power is big.
Further, described track 19 is provided with limited block 20, the position of described limited block 20 and described location hole 9 with
And the position of alignment pin 3 axis is adapted.As shown in figure 5, when pot 1 is moved on lifting plate 17 by track 19, spacing
Block 20 blocks pulley 15, pot 1 is carried out spacing.Wherein, the position of the position of described limited block 20 and described steam intubation 2 axis
Put to be adapted and refer to limited block 20 and enable steam intubation 2 to move to the lower section of shaft 5 with pot 1, make location hole 9 with fixed
Position pin 3 coaxial line, after opening lifting plate 17, location hole 9 is combined with alignment pin 3.
In the middle of above-mentioned embodiment, described steam intubation 2 can adopt the flexible materials such as rubber.But work as steam intubation
2 when adopting flexible material, easily deforms because of deadweight.So preferably, steam intubation 2 adopts metal material
Make.
Claims (7)
1. a kind of cannula type titanium hydrolysis agitating device, including pot (1) and steam intubation (2) it is characterised in that：
Described steam intubation (2) is vertical and bottom that run through described pot (1), and the bottom of described steam intubation (2) and setting
Outfan in pot (1) vapour system outward is connected, and the top of described steam intubation (2) is disposed with from top to bottom determines
Position pin (3) and the first air port (4), described alignment pin (3) is coaxial with described steam intubation (2), described first air port (4) setting
On the side wall of described steam intubation (2) and so that the inner chamber of described steam intubation (2) is connected with the external world；
Also include the shaft (5) being driven by motor (14), described shaft (5) includes being arranged at described steam intubation (2) outward
The stirring pipe (6) enclosing and be coaxial therewith and be arranged at blade on described stirring pipe (6) lateral wall, in described stirring pipe (6)
It is provided with stirring tube cavity (8), the top of described stirring tube cavity (8) is provided with the positioning being adapted with described alignment pin (3)
Hole (9), the side wall of described stirring pipe (6) bottom is provided with the second air port making stirring tube cavity (8) be connected with the external world
(10), described stirring pipe (6) bottom offers the socket (11) that diameter is adapted, described steaming with described steam intubation (2) diameter
Vapour intubation (2) is passed through in described stirring tube cavity (8) of described socket (11) insertion, described alignment pin (3) and location hole (9) phase
Mutually combine to rotate and connect；It is provided with gap, institute between described steam intubation (2) lateral wall and described stirring tube cavity (8) side wall
State stirring pipe (6) to rotate centered on the axis of described steam intubation (2)；
Also include being arranged at the cantilever (12) above pot (1), described cantilever (12) is provided with decelerator (13) and motor
(14), the top of described shaft (5) is connected with the outfan of the decelerator (13) being arranged above pot (1), described subtracts
The input of fast device (13) is connected with motor (14).
2. according to the cannula type titanium hydrolysis agitating device described in claim 1 it is characterised in that：The bottom of described pot (1)
It is additionally provided with pulley (15).
3. according to the cannula type titanium hydrolysis agitating device described in claim 2 it is characterised in that：Also include lifting platform, institute
State lifting platform and include base (16), lifting plate (17) and lowering or hoisting gear (18), described lifting plate (17) is by being arranged at it
Track (19) on top surface and described pulley (15) are slidably connected, and described base (16) is arranged at the lower section of lifting plate (17), institute
State lifting plate (17) to move up and down by the lowering or hoisting gear (18) being arranged between described lifting plate (17) and described base (16)；
The distance that described lifting plate (17) can move up and down is more than hanging down of top to described pot (1) bottom of described alignment pin (3)
Directly apart from h.
4. cannula type titanium hydrolysis agitating device according to claim 3 it is characterised in that：Described first air port (4)
Position is higher than the rim of a cup position of described pot (1).
5. the cannula type titanium hydrolysis agitating device according to any one of claim 3 or 4 claim, its feature exists
In：Described lowering or hoisting gear (18) is hydraulic cylinder.
6. according to the cannula type titanium hydrolysis agitating device described in claim 5 it is characterised in that：Described track (19) is upper to be arranged
Limited location block (20), the position of described limited block (20) is fitted with the position phase of described location hole (9) and alignment pin (3) axis
Join.
7. the cannula type titanium hydrolysis agitating device according to any one of claim 1,2,3,4,6 claim, it is special
Levy and be：Described steam intubation (2) adopts metal material to make.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201611050893.6A CN106423019B (en) | 2016-11-25 | 2016-11-25 | Cannula type titanium hydrolysis agitating device |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201611050893.6A CN106423019B (en) | 2016-11-25 | 2016-11-25 | Cannula type titanium hydrolysis agitating device |
Publications (2)
| Publication Number | Publication Date |
|---|---|
| CN106423019A true CN106423019A (en) | 2017-02-22 |
| CN106423019B CN106423019B (en) | 2018-09-11 |
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| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN201611050893.6A Active CN106423019B (en) | 2016-11-25 | 2016-11-25 | Cannula type titanium hydrolysis agitating device |
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Citations (7)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| JPS596929A (en) * | 1982-07-02 | 1984-01-14 | Satake Eng Co Ltd | Rice mixing apparatus |
| JPS6257638A (en) * | 1985-09-04 | 1987-03-13 | Dai Ichi Kogyo Seiyaku Co Ltd | Stirrer |
| CN202427388U (en) * | 2011-12-15 | 2012-09-12 | 连云港通元机械有限公司 | Stirring kettle |
| CN202508888U (en) * | 2012-04-24 | 2012-10-31 | 河北麦森钛白粉有限公司 | Hydrolysis stirring device for producing titanium dioxide |
| CN203635204U (en) * | 2013-11-10 | 2014-06-11 | 刘芳圃 | Mechanical and pneumatic mixed stirring reaction kettle |
| CN204182326U (en) * | 2014-10-29 | 2015-03-04 | 重庆长风化学工业有限公司 | Hot blast stirring reaction device |
| CN206199279U (en) * | 2016-11-25 | 2017-05-31 | 攀枝花市钛都化工有限公司 | Cannula type titanium hydrolysis agitating device |
-
2016
- 2016-11-25 CN CN201611050893.6A patent/CN106423019B/en active Active
Patent Citations (7)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| JPS596929A (en) * | 1982-07-02 | 1984-01-14 | Satake Eng Co Ltd | Rice mixing apparatus |
| JPS6257638A (en) * | 1985-09-04 | 1987-03-13 | Dai Ichi Kogyo Seiyaku Co Ltd | Stirrer |
| CN202427388U (en) * | 2011-12-15 | 2012-09-12 | 连云港通元机械有限公司 | Stirring kettle |
| CN202508888U (en) * | 2012-04-24 | 2012-10-31 | 河北麦森钛白粉有限公司 | Hydrolysis stirring device for producing titanium dioxide |
| CN203635204U (en) * | 2013-11-10 | 2014-06-11 | 刘芳圃 | Mechanical and pneumatic mixed stirring reaction kettle |
| CN204182326U (en) * | 2014-10-29 | 2015-03-04 | 重庆长风化学工业有限公司 | Hot blast stirring reaction device |
| CN206199279U (en) * | 2016-11-25 | 2017-05-31 | 攀枝花市钛都化工有限公司 | Cannula type titanium hydrolysis agitating device |
Also Published As
| Publication number | Publication date |
|---|---|
| CN106423019B (en) | 2018-09-11 |
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