CN1064065C - Multifunctional leather clothing oiling cream and its preparation - Google Patents
Multifunctional leather clothing oiling cream and its preparation Download PDFInfo
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- CN1064065C CN1064065C CN98101912A CN98101912A CN1064065C CN 1064065 C CN1064065 C CN 1064065C CN 98101912 A CN98101912 A CN 98101912A CN 98101912 A CN98101912 A CN 98101912A CN 1064065 C CN1064065 C CN 1064065C
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- oil
- ammonium chloride
- polyethenoxy
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- Treatments For Attaching Organic Compounds To Fibrous Goods (AREA)
Abstract
The present invention relates to multifunctional leather clothes oiling cream and a preparation method thereof. The present invention is characterized in that the oiling cream is white cream prepared from hexadecyl trimethyl ammonium chloride, dodecyl dimethyl benzyl ammonium chloride, dodecyl dimethyl ammonium oxide, alkylphenol polyoxyethylene (10) ether, fatty alcohol polyoxyethylene (10) ether, synthesized bubulum oil, white oil, vaseline, silicon oil, dicyclohexyl phthalate, dibutyl phthalate and a solvent. The oiling cream has multiple functions, such as softening, sterilization, dry-cleaning, decontamination and mildew resistance, is suitable for various leather clothes to use and is capable of extending service life and improving beautiful appearance.
Description
The present invention relates to a kind of multifunctional leather clothing oiling cream, belong to fine chemical product, the invention still further relates to the preparation method of this innings ointment.
Finished product leather top layer is a kind of resin protective layer; great majority are with nitrocellulose, acrylic resin, polyurethane resin, casein resin making coatings; grown when times of wearing such as leather such as fur clothing, suitcase, leather shoes; softening agent and the grease in the fur clothing in its coating will volatilize, move and cause leather to wear out to harden; surface peeling or fried slurry; even fracture; thereby reduced work-ing life; not attractive in appearance yet; existing leather care products can only stuffing, decontamination, softness, and can not be to top layer plasticising; not only bother when using simultaneously, spraying can cause environmental pollution again.
Purpose of the present invention is the shortcoming and deficiency in order to overcome above-mentioned prior art just, and a kind of have plasticising, dry-cleaning, decontamination, sterilization, the multiple function leather clothing oiling cream of mildew-resistant are provided, thereby can improve work-ing life, and the protection leather has increased attractive in appearance again.
The present invention is the preparation method of Gai treatment wax of Ti Gong also.
The objective of the invention is to realize by following technical proposal:
Multifunctional leather clothing oiling cream is characterized in that it is made by following weight proportioning raw material:
Palmityl trimethyl ammonium chloride 1-3 part
Dodecyl benzyl dimethyl ammonium chloride 1-3 part
Dimethyl dodecyl amine oxide 0.5-2 part
Alkylphenol-polyethenoxy (10) ether 0.5-2 part
Aliphatic alcohol polyethenoxy (10) ether 1-3 part
Synthetic neat's foot oil 4-8 part
No. 18 white oil 5-8 parts
Medical ventolin 3-5 part
Stearyl alcohol 3-5 part
Silicone oil 1-3 part
N-BUTYL ACETATE 2-5 part
Dicyclohexyl phthalate 1-2 part
Dibutyl phthalate 3-5 part
Ethanol 3-5 part
Acetone 3-5 part
Water 50-60 part
Raw material preferred weight proportioning is:
Palmityl trimethyl ammonium chloride 1.5-2.5 part
Dodecyl benzyl dimethyl ammonium chloride 1.5-2.5 part
Dimethyl dodecyl amine oxide 0.5-1.5 part
Alkylphenol-polyethenoxy (10) ether 0.5-1.5 part
Aliphatic alcohol polyethenoxy (10) ether 1.5-2.5 part
Synthetic neat's foot oil 5-7 part
No. 18 white oil 6-8 parts
Medical ventolin 3.5-4.5 part
Stearyl alcohol 3.5-4.5 part
Silicone oil 0.5-1.5 part
N-BUTYL ACETATE 2-4 part
Dicyclohexyl phthalate 1-1.5 part
Dibutyl phthalate 3-5 part
Ethanol 3-5 part
Acetone 3-5 part
Water 50-55 part
Raw material optimum weight proportioning is:
2 parts of palmityl trimethyl ammonium chlorides
2 parts of dodecyl benzyl dimethyl ammonium chlorides
1 part of dimethyl dodecyl amine oxide
1 part in alkylphenol-polyethenoxy (10) ether
2 parts in aliphatic alcohol polyethenoxy (10) ether
6 parts of synthetic neat's foot oils
7 parts of No. 18 white oils
3 parts of medical ventolins
4 parts of stearyl alcohol
1 part of silicone oil
3 parts of N-BUTYL ACETATEs
1.5 parts of dicyclohexyl phthalates
4 parts of dibutyl phthalates
4 parts of ethanol
4 parts in acetone
54.5 parts in water
The also available organo-siloxane of silicone oil, dimethyl silicone oil, 3,5-dimethylphenyl silicone oil, water-soluble silicon oil one or both arbitrary proportion mixtures wherein replace.
The preparation method of treatment wax, it is characterized in that it is undertaken by following step: a) with 1-3 part palmityl trimethyl ammonium chloride, 1-3 part dodecyl benzyl dimethyl ammonium chloride, 0.5-2.0 part dimethyl dodecyl amine oxide, 0.5-2 part alkylphenol-polyethenoxy (10) ether, 1-3 part aliphatic alcohol polyethenoxy (10) ether and 25-35 part water, add in the retort and heat 60-83 ℃, stirred 20-40 minute, add 4-8 part synthetic neat's foot oil more successively, No. 18 white oils of 5-8 part, 3-5 part medical ventolin, 3-5 part stearyl alcohol, 1-3 part silicone oil continue to stir 10-20 minute, add the stirring of water 25-30 part water again and be cooled to below 40 ℃, make it the homogenizing emulsifying reaction and finish stand-by;
B) again with 2-5 part N-BUTYL ACETATE, 3-5 part ethanol, 3-5 part acetone, 1-2 part dicyclohexyl phthalate stirred 10-20 minute in 3-5 part phthalic acid dibutyl ester adding steel basin, made it to dissolve fully, and is stand-by;
C) be white emulsifiable paste shape with stirring to be in (b) material adding (a) material at last, be product.
De treatment wax of the present invention is to have the cats product of soft fungus and mildew resistance soil-removing action; nonionogenic tenside with emulsification infiltration soil-removing action; to nitrocellulose; resin coating has the softening agent of plastification; grease; protective material; solvent is that raw material is formed; the oyster white paste of making through processing and preparing; wherein cats product is a palmityl trimethyl ammonium chloride; it has softness; sterilization; antistatic; emulsification; foaming effect; dodecyl benzyl dimethyl ammonium chloride; it has softness; sterilization; antistatic; emulsification; foaming effect; dimethyl dodecyl amine oxide; it has sterilization; washing; decontamination; opsonization; nonionogenic tenside is alkylphenol-polyethenoxy (a 10) ether; it has washing; emulsification; wetting; disperse; decontamination; anlistatig effect; aliphatic alcohol polyethenoxy (10) ether, it has wetting; emulsification; decontamination; the effect of degrease and anti-hard water.Softening agent has dicyclohexyl phthalate, dibutyl phthalate, they are the resin plasticizers with intensive solvent ability, grease is synthetic neat's foot oil, No. 18 white oils, the another name whiteruss, medical ventolin, stearyl alcohol, effect is leather greasing, softness, and silicone oil has the adjusting feel, has stuffing, waterproof, light effect simultaneously.
Solvent is N-BUTYL ACETATE, ethanol and acetone.
Owing to take technique scheme to make the technology of the present invention compared with the prior art have following advantage and effect:
A) solvent of the present invention and softening agent compatibility can not destroy existing coating again to aging coating solubilising, help softening agent and greasy rapid osmotic.
B) the present invention's treatment oil is in the stuffing decontamination, increase certain softening agent to resin coating again, made existing coating more soft, anti-aging, can stop leather coating effectively simultaneously, because of the aging of fur clothing, the problem of hardening of causing extracted in the volatilization of existing softening agent out;
C) product has stuffing, the rapid sterilization of decontamination, soft and bright, and mildew-resistant, the multiple function of plasticising can be widely used in all kinds of leatherware and use.
D) easy to use, free from environmental pollution, nontoxic.
E) this product both can be given skin clothing treatment oil again in order to the nursing of daily leatherware in 60 ℃ warm air, made the fur clothing that hardens long neglected and in disrepair ease back in 20 minutes, recovered leather elasticity.
Embodiment:
Raw material of the present invention removes dicyclohexyl phthalate by the import of U.S. FMC Corp..All the other are production domesticization chemical products.
Embodiment 1:
With the 2kg palmityl trimethyl ammonium chloride, the 2kg dodecyl benzyl dimethyl ammonium chloride, 1kg dimethyl dodecyl amine oxide, 1kg alkylphenol-polyethenoxy (10) ether, 2kg aliphatic alcohol polyethenoxy (10) ether, heating is 80-83 ℃ in the 30kg water adding retort, stirs 20 minutes, adds the 6kg synthetic neat's foot oil more successively, the 7kg18 white oil, the 3kg medical ventolin, 4kg stearyl alcohol, 1kg silicone oil, continue to stir 10 minutes, add surplus water 24.5kg again, stirring is cooled to below 40 ℃, makes it homogenizing emulsifying, reaction finishes, in another steel basin, add 3kg N-BUTYL ACETATE, 4kg ethanol, 4kg acetone again, 1.5kg dicyclohexyl phthalate, the 4kg dibutyl phthalate stirred 20 minutes, made it to dissolve fully, add in the material of above-mentioned retort and stirred 15 minutes, the emulsifiable paste shape that makes it to be white in color is product, through packaging final prod.
Embodiment 2:
With the 1kg palmityl trimethyl ammonium chloride, the 3kg dodecyl benzyl dimethyl ammonium chloride, 0.5kg dimethyl dodecyl amine oxide, 2kg alkylphenol-polyethenoxy (10) ether, 1kg aliphatic alcohol polyethenoxy (10) ether, heating is 70-75 ℃ in the 30kg water adding retort, stirs 30 minutes, adds the 8kg synthetic neat's foot oil more successively, the 5kg18 white oil, the 5kg medical ventolin, 3kg stearyl alcohol, 2kg water-soluble silicon oil, continue to stir 15 minutes, add surplus water 30kg again, stirring is cooled to below 40 ℃, makes it homogenizing emulsifying, reaction finishes, in another steel basin, add 5kg N-BUTYL ACETATE, 3kg ethanol, 5kg acetone again, the 2kg dicyclohexyl phthalate, the 3kg dibutyl phthalate stirred 15 minutes, made it to dissolve fully, add in the material of above-mentioned retort and stirred 10 minutes, the emulsifiable paste shape that makes it to be white in color is product, through packaging final prod.
Embodiment 3:
With the 3kg palmityl trimethyl ammonium chloride, the 1kg dodecyl benzyl dimethyl ammonium chloride, 2kg dimethyl dodecyl amine oxide, 0.5kg alkylphenol-polyethenoxy (10) ether, 3kg aliphatic alcohol polyethenoxy (10) ether, heating is 60-65 ℃ in the 35kg water adding retort, stirs 40 minutes, adds the 4kg synthetic neat's foot oil more successively, the 8kg18 white oil, the 4kg medical ventolin, the 5kg stearyl alcohol, the 3kg water-soluble silicon oil mixes the back with dimethyl silicone oil and adds at 1: 1, continue to stir 20 minutes, add surplus water 20kg again, stirring is cooled to below 40 ℃, makes it homogenizing emulsifying, reaction finishes, in another steel basin, add 2kg acetic acid ester again, 5kg ethanol, 3kg acetone, the 1kg dicyclohexyl phthalate, the 5kg dibutyl phthalate stirred 10 minutes, made it to dissolve fully, add in the material of above-mentioned retort and stirred 20 minutes, the emulsifiable paste shape that makes it to be white in color is product, through packaging final prod.
Claims (5)
1, multifunctional leather clothing oiling cream is characterized in that it is made by following weight proportioning raw material:
Palmityl trimethyl ammonium chloride 1-3 part
Dodecyl benzyl dimethyl ammonium chloride 1-3 part
Dimethyl dodecyl amine oxide 0.5-2 part
Alkylphenol-polyethenoxy (10) ether 0.5-2 part
Aliphatic alcohol polyethenoxy (10) ether 1-3 part
Synthetic neat's foot oil 4-8 part
No. 18 white oil 5-8 parts
Medical ventolin 3-5 part
Stearyl alcohol 3-5 part
Silicone oil 1-3 part
N-BUTYL ACETATE 2-5 part
Dicyclohexyl phthalate 1-2 part
Dibutyl phthalate 3-5 part
Ethanol 3-5 part
Acetone 3-5 part
Water 50-60 part
2,, it is characterized in that described raw material weight proportioning is according to claim 1 Suo Shu De treatment wax:
Palmityl trimethyl ammonium chloride 1.5-2.5 part
Dodecyl benzyl dimethyl ammonium chloride 1.5-2.5 part
Dimethyl dodecyl amine oxide 0.5-1.5 part
Alkylphenol-polyethenoxy (10) ether 0.5-1.5 part
Aliphatic alcohol polyethenoxy (10) ether 1.5-2.5 part
Synthetic neat's foot oil 5-7 part
No. 18 white oil 6-8 parts
Medical ventolin 3.5-4.5 part
Stearyl alcohol 3.5-4.5 part
Silicone oil 0.5-1.5 part
N-BUTYL ACETATE 2-4 part
Dicyclohexyl phthalate 1-1.5 part
Dibutyl phthalate 3-5 part
Ethanol 3-5 part
Acetone 3-5 part
Water 50-55 part
3,, it is characterized in that described raw material weight proportioning is according to claim 1 Suo Shu De treatment wax:
2 parts of palmityl trimethyl ammonium chlorides
2 parts of dodecyl benzyl dimethyl ammonium chlorides
1 part of dimethyl dodecyl amine oxide
1 part in alkylphenol-polyethenoxy (10) ether
2 parts in aliphatic alcohol polyethenoxy (10) ether
6 parts of synthetic neat's foot oils
7 parts of No. 18 white oils
3 parts of medical ventolins
4 parts of stearyl alcohol
1 part of silicone oil
3 parts of N-BUTYL ACETATEs
1.5 parts of dicyclohexyl phthalates
4 parts of dibutyl phthalates
4 parts of ethanol
4 parts in acetone
54.5 parts in water
4,, it is characterized in that the also available organo-siloxane of silicone oil, dimethyl silicone oil, 3,5-dimethylphenyl silicone oil, water-soluble silicon oil one or both arbitrary proportion mixtures wherein replace according to claim 1,2 or 3 Shu De treatment waxes.
5, the preparation method of the treatment wax of stating according to claim 1 is characterized in that it is undertaken by following step:
A) with 1-3 part palmityl trimethyl ammonium chloride, 1-3 part dodecyl benzyl dimethyl ammonium chloride, 0.5-2.0 part dimethyl dodecyl amine oxide, 0.5-2 part alkylphenol-polyethenoxy (10) ether, 1-3 part aliphatic alcohol polyethenoxy (10) ether and 25-35 part water, add in the retort and heat 60-83 ℃, stirred 20-40 minute, add 4-8 part synthetic neat's foot oil more successively, No. 18 white oils of 5-8 part, 3-5 part medical ventolin, 3-5 part stearyl alcohol, 1-3 part silicone oil continues to stir 10-20 minute, adds the stirring of water 25-30 part water again and is cooled to below 40 ℃, makes it the homogenizing emulsifying reaction and finishes stand-by;
B) again with 2-5 part N-BUTYL ACETATE, 3-5 part ethanol, 3-5 part acetone, 1-2 part dicyclohexyl phthalate stirred 10-20 minute in 3-5 part phthalic acid dibutyl ester adding steel basin, made it to dissolve fully, and is stand-by;
C) be white emulsifiable paste shape with stirring to be in (b) material adding (a) material at last, be product.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN98101912A CN1064065C (en) | 1998-05-14 | 1998-05-14 | Multifunctional leather clothing oiling cream and its preparation |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN98101912A CN1064065C (en) | 1998-05-14 | 1998-05-14 | Multifunctional leather clothing oiling cream and its preparation |
Publications (2)
| Publication Number | Publication Date |
|---|---|
| CN1199762A CN1199762A (en) | 1998-11-25 |
| CN1064065C true CN1064065C (en) | 2001-04-04 |
Family
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Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN98101912A Expired - Fee Related CN1064065C (en) | 1998-05-14 | 1998-05-14 | Multifunctional leather clothing oiling cream and its preparation |
Country Status (1)
| Country | Link |
|---|---|
| CN (1) | CN1064065C (en) |
Families Citing this family (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN102516883B (en) * | 2011-11-22 | 2014-04-09 | 广州市美可生物科技有限公司 | Leather cleaning, nourishing and care cream and production method thereof |
| CN102978047A (en) * | 2012-12-12 | 2013-03-20 | 上海皇宇科技发展有限公司 | Multifunctional leather cleaner and preparation method thereof |
| CN107556924B (en) * | 2017-08-11 | 2020-07-17 | 广州市拓新化工科技有限公司 | Leather coating glazing agent and preparation method thereof |
Citations (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN1095085A (en) * | 1993-04-24 | 1994-11-16 | 龚有琳 | Ice-soluble paraffin wax brightening agent |
-
1998
- 1998-05-14 CN CN98101912A patent/CN1064065C/en not_active Expired - Fee Related
Patent Citations (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN1095085A (en) * | 1993-04-24 | 1994-11-16 | 龚有琳 | Ice-soluble paraffin wax brightening agent |
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| Publication number | Publication date |
|---|---|
| CN1199762A (en) | 1998-11-25 |
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| C10 | Entry into substantive examination | ||
| SE01 | Entry into force of request for substantive examination | ||
| C06 | Publication | ||
| PB01 | Publication | ||
| C14 | Grant of patent or utility model | ||
| GR01 | Patent grant | ||
| C17 | Cessation of patent right | ||
| CF01 | Termination of patent right due to non-payment of annual fee |
Granted publication date: 20010404 Termination date: 20100514 |