CN106400512B - A kind of soft finish method of silk hemp fabric - Google Patents

A kind of soft finish method of silk hemp fabric Download PDF

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Publication number
CN106400512B
CN106400512B CN201610814835.XA CN201610814835A CN106400512B CN 106400512 B CN106400512 B CN 106400512B CN 201610814835 A CN201610814835 A CN 201610814835A CN 106400512 B CN106400512 B CN 106400512B
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silk
hemp fabric
silk hemp
fabric
soft
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CN106400512A (en
Inventor
吴改红
刘淑强
张晓芳
师洁
许安
郭红霞
邵芬娟
卢建军
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Taiyuan University of Technology
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Taiyuan University of Technology
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    • DTEXTILES; PAPER
    • D06TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
    • D06MTREATMENT, NOT PROVIDED FOR ELSEWHERE IN CLASS D06, OF FIBRES, THREADS, YARNS, FABRICS, FEATHERS OR FIBROUS GOODS MADE FROM SUCH MATERIALS
    • D06M16/00Biochemical treatment of fibres, threads, yarns, fabrics, or fibrous goods made from such materials, e.g. enzymatic
    • D06M16/003Biochemical treatment of fibres, threads, yarns, fabrics, or fibrous goods made from such materials, e.g. enzymatic with enzymes or microorganisms
    • DTEXTILES; PAPER
    • D06TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
    • D06MTREATMENT, NOT PROVIDED FOR ELSEWHERE IN CLASS D06, OF FIBRES, THREADS, YARNS, FABRICS, FEATHERS OR FIBROUS GOODS MADE FROM SUCH MATERIALS
    • D06M10/00Physical treatment of fibres, threads, yarns, fabrics, or fibrous goods made from such materials, e.g. ultrasonic, corona discharge, irradiation, electric currents, or magnetic fields; Physical treatment combined with treatment with chemical compounds or elements
    • D06M10/001Treatment with visible light, infrared or ultraviolet, X-rays
    • DTEXTILES; PAPER
    • D06TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
    • D06MTREATMENT, NOT PROVIDED FOR ELSEWHERE IN CLASS D06, OF FIBRES, THREADS, YARNS, FABRICS, FEATHERS OR FIBROUS GOODS MADE FROM SUCH MATERIALS
    • D06M15/00Treating fibres, threads, yarns, fabrics, or fibrous goods made from such materials, with macromolecular compounds; Such treatment combined with mechanical treatment
    • D06M15/19Treating fibres, threads, yarns, fabrics, or fibrous goods made from such materials, with macromolecular compounds; Such treatment combined with mechanical treatment with synthetic macromolecular compounds
    • D06M15/37Macromolecular compounds obtained otherwise than by reactions only involving carbon-to-carbon unsaturated bonds
    • D06M15/53Polyethers
    • DTEXTILES; PAPER
    • D06TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
    • D06MTREATMENT, NOT PROVIDED FOR ELSEWHERE IN CLASS D06, OF FIBRES, THREADS, YARNS, FABRICS, FEATHERS OR FIBROUS GOODS MADE FROM SUCH MATERIALS
    • D06M2101/00Chemical constitution of the fibres, threads, yarns, fabrics or fibrous goods made from such materials, to be treated
    • D06M2101/02Natural fibres, other than mineral fibres
    • D06M2101/04Vegetal fibres
    • D06M2101/06Vegetal fibres cellulosic
    • DTEXTILES; PAPER
    • D06TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
    • D06MTREATMENT, NOT PROVIDED FOR ELSEWHERE IN CLASS D06, OF FIBRES, THREADS, YARNS, FABRICS, FEATHERS OR FIBROUS GOODS MADE FROM SUCH MATERIALS
    • D06M2101/00Chemical constitution of the fibres, threads, yarns, fabrics or fibrous goods made from such materials, to be treated
    • D06M2101/02Natural fibres, other than mineral fibres
    • D06M2101/10Animal fibres
    • D06M2101/12Keratin fibres or silk
    • DTEXTILES; PAPER
    • D06TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
    • D06MTREATMENT, NOT PROVIDED FOR ELSEWHERE IN CLASS D06, OF FIBRES, THREADS, YARNS, FABRICS, FEATHERS OR FIBROUS GOODS MADE FROM SUCH MATERIALS
    • D06M2200/00Functionality of the treatment composition and/or properties imparted to the textile material
    • D06M2200/50Modified hand or grip properties; Softening compositions

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  • Engineering & Computer Science (AREA)
  • Textile Engineering (AREA)
  • Chemical & Material Sciences (AREA)
  • Life Sciences & Earth Sciences (AREA)
  • Biochemistry (AREA)
  • Microbiology (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • General Chemical & Material Sciences (AREA)
  • Chemical Or Physical Treatment Of Fibers (AREA)
  • Treatments For Attaching Organic Compounds To Fibrous Goods (AREA)
  • Treatment Of Fiber Materials (AREA)

Abstract

The present invention relates to a kind of mellowing methods of silk hemp fabric, after selection concentration pre-processes silk hemp fabric for the cellulase of 1.5%(o.w.f), second dipping and rolling soft treatment is carried out to silk hemp fabric using the softening agent being formulated by natural softening agent ester based quaternary ammonium salt and SF low-foaming penetrating agent and OP-10 emulsifier, the flexibility of silk hemp fabric is effectively increased with the method, prodding and itching feeling is eliminated, while ensure that the physical mechanical property of silk hemp fabric is not affected by big influence.

Description

A kind of soft finish method of silk hemp fabric
Technical field
The invention belongs to the post-processing technology fields of fabric, and in particular to a kind of soft finish side of silk hemp fabric Method.
Background technique
Silk is a kind of natural protein fibre, acidproof not alkaline-resisting, light and elongated, and fabric sheen is good, comfortable and easy to wear, hand Feel smooth plentiful, moisture absorption is ventilative, and for weaving various silks and satins and knitwear, silk just has the beauty of " fiber queen " since ancient times Reputation.
There are china-hemp fibers other fibers such as high temperature resistant, rub resistance, moisture absorption rapid heat dissipation, antiallergy, anti-electrostatic antibiotic to be difficult to The advantage of analogy is natural harmless, renewable and cheap green fiber.But contain more hemicellulose in flaxen fiber Element, lignin and pectin, in addition higher crystallinity and the degree of orientation, so that fiber rigidity is big, brittleness is high, wiriness, with skin Skin contact has prodding and itching feeling.
The well-pressed nice and cool style of the existing linen of silk Chinese fiber crops intertexture, and have the gloss as silk, and have than silk broadcloth Body bone is perspired not personal, is high-grade summer clothes fabric.But because flaxen fiber there are the shortcomings that, make silk Chinese fiber crops intertexture Rigid degree of holding out through, feel is coarse, and has prodding and itching feeling, influences appearance of fabrics and comfort.For this purpose, silk Chinese fiber crops intertexture is in final finishing In to carry out soft finish, to assign the smooth feel of soft fabric and higher resilience.Conventional soft method for sorting cost Height, seriously polluted, process provides a kind of environmental soft method for sorting for silk hemp fabric.
Summary of the invention
The technical problems to be solved by the present invention are: how to improve the feel of silk hemp fabric, prodding and itching feeling is eliminated, is improved The flexibility of fabric.
The technical scheme adopted by the invention is that a kind of soft finish method of silk hemp fabric, according to following step It is rapid to carry out:
Step 1: cellulase pre-processes: selections concentration is 1.5%-3%(o.w.f) cellulase to silk Chinese hemp Object is pre-processed, bath raio 1:20, is adjusted pH value to 4-5 with the hydrochloric acid solution of 0.1mol/L, is handled under the conditions of 40 DEG C -60 DEG C 30min-60min;
Step 2: soft finish: soft using being formulated by ester based quaternary ammonium salt, SF low-foaming penetrating agent, OP-10 emulsifier Soft dose carries out dipping soft treatment, second dipping and rolling, pick-up 80%-90%, bath raio 1:20, every time 50 to silk hemp fabric 20min-30min is impregnated under the conditions of DEG C -60 DEG C, wherein in softening agent ester based quaternary ammonium salt concentration is 1g/L-3g/L, the low bubble infiltration of SF The concentration of saturating agent is 0.5g/L-1.5g/L, and OP-10 emulsifier concentration is 0.3g/L-1.2g/L.
Step 3: the processed silk hemp fabric of step 2 is dried under the irradiation of ultraviolet lamp, ultraviolet lamp is irradiated Keep silk hemp fabric temperature at 100 DEG C -120 DEG C in journey.Silk hemp fabric is set to become fluffy soft using action of ultraviolet light It is soft.
The silk hemp fabric raw material used is the Chinese dimity point that specification is 2.616tex silk and specification is 25.196tex It Wei not the plain weave intertexture that is made into of warp thread and weft yarn.
The beneficial effects of the present invention are: the ester based quaternary ammonium salt that the present invention uses is a kind of decomposable, easily biological-degradable and right Biological non-toxicity, environment amenable functional surfactant, have excellent flexibility, and fabric adsorbs this surface-active After agent, surface tension reduces, and interfibrous coefficient of friction reduces, and stretches fiber more easily in the fabric, to make fabric Become fluffy, plentiful, generate soft feel, is reducing production cost, effectively eliminating the silk Chinese while reducing environmental pollution The prodding and itching feeling of linen improves the flexibility of fabric, it is ensured that the physical mechanical property of fabric is substantially injury-free.
Specific embodiment
The present invention is further illustrated below by embodiment, but is not limited to following embodiment.
Step 1: tieing up plain enzyme pretreatment: selections concentration for 1.5%-3%(o.w.f) cellulase to silk hemp fabric (the silk hemp fabric used be the Chinese dimity that specification is 2.616tex silk and specification is 25.196tex be respectively warp thread and The plain weave intertexture that weft yarn is made into) it is pre-processed, bath raio 1:20, it is adjusted with the hydrochloric acid solution of the homemade 0.1mol/L in laboratory PH value handles 60min under the conditions of 40 DEG C to 4;
Step 2: soft finish: soft using being formulated by ester based quaternary ammonium salt, SF low-foaming penetrating agent, OP-10 emulsifier Soft dose carries out dipping soft treatment, second dipping and rolling, pick-up 90%, bath raio 1:20, every time in 60 DEG C of items to silk hemp fabric 20min is impregnated under part.Wherein ester based quaternary ammonium salt concentration is 1g/L, and the concentration of SF low-foaming penetrating agent is 0.5g/L, OP-10 emulsifier Concentration is 0.6g/L;
Step 3: the processed silk hemp fabric of step 2 is dried under the irradiation of ultraviolet lamp, ultraviolet lamp is irradiated Keep silk hemp fabric temperature at 100 DEG C -120 DEG C in journey.Silk hemp fabric is set to become fluffy soft using action of ultraviolet light It is soft.For a more fluffy softness, softness is sprayed after through the irradiation of ultraviolet lamp drying, then on silk hemp fabric surface Then agent is dried under the irradiation of ultraviolet lamp again, dry under the irradiation of ultraviolet lamp after repeating sprinkling softening agent 3 times, not only Silk hemp fabric can be made to become more fluffy softness, and the softening agent not in two is added and is easy by silk hemp fabric It absorbs, improves the physical mechanical property of fabric, the quality for spraying softening agent every time is the 0.8- of silk hemp fabric quality 1.1%。

Claims (3)

1. a kind of soft finish method of silk hemp fabric, it is characterised in that carried out according to following step:
Step 1: cellulase pre-processes: the cellulase that concentration is 1.5%-3% o.w.f being selected to carry out silk hemp fabric Pretreatment, bath raio 1:20 adjust pH value to 4-5 with the hydrochloric acid solution of 0.1mol/L, handle 30min- under the conditions of 40 DEG C -60 DEG C 60min;
Step 2: soft finish: using the softening agent being formulated by ester based quaternary ammonium salt, SF low-foaming penetrating agent, OP-10 emulsifier Dipping soft treatment carried out to silk hemp fabric, second dipping and rolling, pick-up 80%-90%, bath raio 1:20, every time 50 DEG C- 20min-30min is impregnated under the conditions of 60 DEG C;
Step 3: the processed silk hemp fabric of step 2 is dried under the irradiation of ultraviolet lamp, in ultraviolet lamp irradiation process Keep silk hemp fabric temperature at 100 DEG C -120 DEG C.
2. a kind of soft finish method of silk hemp fabric according to claim 1, it is characterised in that: institute in step 1 The fabric used is silk hemp fabric, and the Chinese dimity that specification is 2.616tex silk and specification is 25.196tex is respectively The plain weave intertexture that warp thread and weft yarn are made into.
3. a kind of soft finish method of silk hemp fabric according to claim 1, it is characterised in that: in step 2, Ester based quaternary ammonium salt concentration is 1g/L-3g/L in softening agent, and the concentration of SF low-foaming penetrating agent is 0.5g/L-1.5g/L, OP-10 emulsification Agent concentration is 0.3g/L-1.2g/L.
CN201610814835.XA 2016-09-12 2016-09-12 A kind of soft finish method of silk hemp fabric Active CN106400512B (en)

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Families Citing this family (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN110438613A (en) * 2019-07-10 2019-11-12 杭州丝绸之路文化艺术有限公司 A kind of production method of silk composite material
CN113089309A (en) * 2021-03-27 2021-07-09 安徽省伊贝雅纺织有限公司 Towel treatment process
CN115161843B (en) * 2022-06-13 2024-04-26 雅戈尔服装制造有限公司 Processing method of natural antibacterial super-soft China hemp silk high-count high-density fine fabric

Citations (8)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
EP2526224A1 (en) * 2010-01-21 2012-11-28 Advantage Nature (A Unit Of Advantage Television Pvt. Ltd.) A novel process of dyeing and processing a natural textile product using natural dyes alongside neem and tulsi
CN104420214A (en) * 2013-09-06 2015-03-18 青岛三秀新科技复合面料有限公司 Softening finishing method for fabric
CN104695240A (en) * 2015-04-07 2015-06-10 太仓天龙化纤有限公司 Chemical fiber dyeing technology with ultraviolet protection function
CN104988768A (en) * 2015-07-28 2015-10-21 太仓市宝明化纤有限公司 Flax fabric dyeing and finishing process
CN105064074A (en) * 2015-07-28 2015-11-18 太仓市宝明化纤有限公司 Dyeing and finishing process for mulberry silk fabric
CN105220447A (en) * 2015-10-21 2016-01-06 际华三五零九纺织有限公司 A kind of soft finish technique of hemp fabric
CN105463841A (en) * 2015-12-18 2016-04-06 张莘蔓 Silk softener and preparation method thereof
CN105696177A (en) * 2014-11-25 2016-06-22 江阴市长泾花园毛纺织有限公司 Technology for producing han-hemp knitted home fabric

Patent Citations (8)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
EP2526224A1 (en) * 2010-01-21 2012-11-28 Advantage Nature (A Unit Of Advantage Television Pvt. Ltd.) A novel process of dyeing and processing a natural textile product using natural dyes alongside neem and tulsi
CN104420214A (en) * 2013-09-06 2015-03-18 青岛三秀新科技复合面料有限公司 Softening finishing method for fabric
CN105696177A (en) * 2014-11-25 2016-06-22 江阴市长泾花园毛纺织有限公司 Technology for producing han-hemp knitted home fabric
CN104695240A (en) * 2015-04-07 2015-06-10 太仓天龙化纤有限公司 Chemical fiber dyeing technology with ultraviolet protection function
CN104988768A (en) * 2015-07-28 2015-10-21 太仓市宝明化纤有限公司 Flax fabric dyeing and finishing process
CN105064074A (en) * 2015-07-28 2015-11-18 太仓市宝明化纤有限公司 Dyeing and finishing process for mulberry silk fabric
CN105220447A (en) * 2015-10-21 2016-01-06 际华三五零九纺织有限公司 A kind of soft finish technique of hemp fabric
CN105463841A (en) * 2015-12-18 2016-04-06 张莘蔓 Silk softener and preparation method thereof

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