CN106396304A - A harmlessness and reclamation treatment method for oil-containing sludge - Google Patents
A harmlessness and reclamation treatment method for oil-containing sludge Download PDFInfo
- Publication number
- CN106396304A CN106396304A CN201610622254.6A CN201610622254A CN106396304A CN 106396304 A CN106396304 A CN 106396304A CN 201610622254 A CN201610622254 A CN 201610622254A CN 106396304 A CN106396304 A CN 106396304A
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- China
- Prior art keywords
- sludge
- mud
- tank
- oily sludge
- oil
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- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
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Classifications
-
- C—CHEMISTRY; METALLURGY
- C02—TREATMENT OF WATER, WASTE WATER, SEWAGE, OR SLUDGE
- C02F—TREATMENT OF WATER, WASTE WATER, SEWAGE, OR SLUDGE
- C02F11/00—Treatment of sludge; Devices therefor
-
- C—CHEMISTRY; METALLURGY
- C02—TREATMENT OF WATER, WASTE WATER, SEWAGE, OR SLUDGE
- C02F—TREATMENT OF WATER, WASTE WATER, SEWAGE, OR SLUDGE
- C02F11/00—Treatment of sludge; Devices therefor
- C02F11/02—Biological treatment
-
- C—CHEMISTRY; METALLURGY
- C02—TREATMENT OF WATER, WASTE WATER, SEWAGE, OR SLUDGE
- C02F—TREATMENT OF WATER, WASTE WATER, SEWAGE, OR SLUDGE
- C02F11/00—Treatment of sludge; Devices therefor
- C02F11/12—Treatment of sludge; Devices therefor by de-watering, drying or thickening
-
- C—CHEMISTRY; METALLURGY
- C02—TREATMENT OF WATER, WASTE WATER, SEWAGE, OR SLUDGE
- C02F—TREATMENT OF WATER, WASTE WATER, SEWAGE, OR SLUDGE
- C02F11/00—Treatment of sludge; Devices therefor
- C02F11/12—Treatment of sludge; Devices therefor by de-watering, drying or thickening
- C02F11/121—Treatment of sludge; Devices therefor by de-watering, drying or thickening by mechanical de-watering
- C02F11/123—Treatment of sludge; Devices therefor by de-watering, drying or thickening by mechanical de-watering using belt or band filters
-
- C—CHEMISTRY; METALLURGY
- C02—TREATMENT OF WATER, WASTE WATER, SEWAGE, OR SLUDGE
- C02F—TREATMENT OF WATER, WASTE WATER, SEWAGE, OR SLUDGE
- C02F11/00—Treatment of sludge; Devices therefor
- C02F11/18—Treatment of sludge; Devices therefor by thermal conditioning
-
- C—CHEMISTRY; METALLURGY
- C02—TREATMENT OF WATER, WASTE WATER, SEWAGE, OR SLUDGE
- C02F—TREATMENT OF WATER, WASTE WATER, SEWAGE, OR SLUDGE
- C02F2101/00—Nature of the contaminant
- C02F2101/30—Organic compounds
- C02F2101/32—Hydrocarbons, e.g. oil
-
- C—CHEMISTRY; METALLURGY
- C02—TREATMENT OF WATER, WASTE WATER, SEWAGE, OR SLUDGE
- C02F—TREATMENT OF WATER, WASTE WATER, SEWAGE, OR SLUDGE
- C02F2103/00—Nature of the water, waste water, sewage or sludge to be treated
- C02F2103/10—Nature of the water, waste water, sewage or sludge to be treated from quarries or from mining activities
-
- C—CHEMISTRY; METALLURGY
- C02—TREATMENT OF WATER, WASTE WATER, SEWAGE, OR SLUDGE
- C02F—TREATMENT OF WATER, WASTE WATER, SEWAGE, OR SLUDGE
- C02F2103/00—Nature of the water, waste water, sewage or sludge to be treated
- C02F2103/34—Nature of the water, waste water, sewage or sludge to be treated from industrial activities not provided for in groups C02F2103/12 - C02F2103/32
- C02F2103/36—Nature of the water, waste water, sewage or sludge to be treated from industrial activities not provided for in groups C02F2103/12 - C02F2103/32 from the manufacture of organic compounds
- C02F2103/365—Nature of the water, waste water, sewage or sludge to be treated from industrial activities not provided for in groups C02F2103/12 - C02F2103/32 from the manufacture of organic compounds from petrochemical industry (e.g. refineries)
Abstract
A harmlessness and reclamation treatment method for oil-containing sludge is provided. The method includes steps of feeding the oil-containing sludge into a receiving tank, primarily fully mixing, feeding into a hot washing tank through a lifting pump, adding a biodegradable dispersing agent to separate crude oil from the sludge, feeding to a three-phase separator to separate oil, water and sludge, recovering top crude oil, feeding waste water and the sludge into a sludge washing tank, adding a biodegradable cleaning agent to further remove residual oil in the waste water and the sludge, feeding waste water of the sludge washing tank into a container air-floating device, recycling the waste water after the waste water is treated, feeding bottom sludge of the sludge washing tank and bottom sludge of the container air-floating device into a sludge centralizing tank, treating the sludge in the sludge centralizing tank by a double-belt filter press, adding a biological accelerant for treatment, and discharging when reaching standards through detection. The method is advantaged by meeting treatment requirements on sludge having different properties, achieving harmlessness, reclamation and reduction, and being free of no secondary pollution, low in energy consumption and low in running cost.
Description
Technical field
The present invention relates to resource and environment technical field, process with resource innoxious particularly to a kind of oily sludge
Method.
Background technology
Oily sludge is mainly derived from oil exploration, oil development, petroleum refining and crude storage and transportation
In, comprise the big tank of crude oil deposit bed mud, sewage disposal produce oily sludge and because sudden pollusion atmospheric event etc. is former
Land oily sludge etc. because cause.Newly produce oily sludge 4 × 10 through preliminary survey China every year6T about, oily sludge is
Clearly listed in as hazardous waste《National Hazard waste register》, according to《Administrative Regulations on Pollution Discharge Fee Levy》And " row
Dirty fee collecting standard management method ", does not meet the provisions of the relevant regulations issued by the State, hazardous waste collection of drainage dues mark to disposing hazardous waste
It is accurate that for 1000 yuan per ton every time, if processing, disposal is not up to standard, enterprise will pay heavy blowdown cost,《National clean manufacturing promotees
Enter method》With《Solid waste environmental pollution prevention and control method》Also require that and must carry out harmless treatment to oily sludge.
Oily sludge technical research personnel have carried out substantial amounts of research, mainly in terms of disposal of oily sludge both at home and abroad at present
Including：Quenched-mechanical centrifugal method, concentration method, burning method, thermal desorption method, solvent extraction, biological treatment etc., quenched-machinery
Centrifuging advantage is that technique is easily realized, and petroleum substance can reclaim, non-secondary pollution, but the selection of quenched medicament is difficult, builds
If addressing requires higher；Concentration method：Removable free water, to reduce pollution volume, but processes not thorough, there is secondary pollution hidden
Suffer from；Burning method can at utmost minimizing adaptable to raw material, but high energy consumption, equipment investment is big, and process specifications are high,
General heat utilization ratio is not high, it is understood that there may be dust, SO3Deng secondary pollution；The completely inorganization hydro carbons of thermal desorption method medium can return
Receive and utilize, but reaction condition requirement is higher, operation is more complicated；Solvent extraction efficiency high, processes thoroughly, most of petroleum-type
Material extracts and reclaims, but extractant is expensive, during to there is partial loss processing cost high；Biological treatment energy consumption is low,
Processing cost is low, but long processing period, to cycloalkane, aromatic hydrocarbons, heterocyclic treatment effect is poor, and high oil content pollution mud is difficult to be adapted to
Scale, resource cannot reuse；Above technology can carry out the disposal of oily sludge to a certain extent, but can not from innoxious,
Thoroughly oily sludge is solved the problems, such as in resource, minimizing.
Content of the invention
It is an object of the invention to provide a kind of innoxious processing method with resource of oily sludge, solve oil field and produced
The recycling treatment of oily sludge in journey, solves integrated treatment and the Utilizing question of oily sludge simultaneously.
To achieve these goals, present invention employs following technical scheme：Comprise the following steps：
A, oily sludge enter mix homogeneously after reception tank dilutes 2 times by recirculated water and enter through elevator pump to fluid state
Enter thermal washing tank, oily sludge is mixed with recirculated water, heating water, filter press filtrate in hot-water cylinder, and oily sludge is heated to 60-
80 DEG C, and it is diluted to 5 times of raw sewage further, so that crude oil is separated from mud by throwing in biodegradation dispersant, then
Enter three phase separator；
B, make oil, water, mud three phase separation and from oil drain out reclaim crude oil, sewage, mud enter mud purge tank；By throwing
Plus biodegradation abluent, remain oil content in further eccysis sewage, mud；
In c, mud purge tank, sewage enters container air-floating apparatus, and sewage recycles after treatment, mud purge tank bottom
Portion's mud and container air-floating apparatus base sludge enter mud centralized pool；
In d, mud centralized pool, mud is processed through biobelt pressure filter, processes and reaches afterwards after testing by adding Biostimulation agent
Mark discharge.
Wherein, the processing equipment described in step a-d includes：Reception tank, thermal washing tank, three phase separator, dissolved air flotation device,
Mud centralized pool, biobelt pressure filter, clean water tank, settling tank, elevator pump.
Wherein, the spoil disposal of the container air-floating apparatus described in step c-d squeezes into mud centralized pool by sludge pump, and then by biobelt
Pressure filter carries out sludge dewatering, dehydrated sludge, processes rear qualified discharge after testing by adding Biostimulation agent.
Wherein, the pressing filtering liquid producing in the dehydration described in step a-d, squeezes into reception tank, thermal washing tank by elevator pump.
The beneficial effects of the present invention is：After above-mentioned processing method, the Treatment of Sludge that can meet various trait requires
And treatment effect all can reach emission request；By comparing with existing method for sludge treatment, can reach innoxious, resource, subtract
Quantify, non-secondary pollution, energy consumption are low, operating cost is low；After process, oily sludge material oil content ＜ 0.3%, reaches innoxious
Require, can directly fill, meet environmental requirement.
Specific embodiment
A kind of innoxious processing method with resource of oily sludge, wherein processing equipment includes：Reception tank, thermal washing tank,
Three phase separator, dissolved air flotation device, mud centralized pool, biobelt pressure filter, clean water tank, settling tank and elevator pump.
Embodiment 1：Daqing oil field oil recovery factory scene sludge treatment pond oily sludge oil-containing 27.53wt%, aqueous
47.45wt%, contain miscellaneous 25.02, by oily sludge reception tank by recirculated water dilute 2 times, to fluid state enter heat
Cleaning of evaporator, oily sludge is diluted to 5 times of raw sewage further in thermal washing tank, oily sludge mixture is heated to 70 DEG C, passes through
Add biodegradable 0.5% dispersant, enter mud purge tank, then by adding biodegradable 0.5% abluent, make
Crude oil separates from mud；Mud, after mud centralized pool centralized collection, processes through pressure filter, adds 0.5% Biostimulation agent
Transport to outward airing field, after testing oily sludge oil-containing 0.28wt%, aqueous 39.45wt%, contain miscellaneous 60.27wt%, heavy metal from
Son reaches discharge standard, and sewage uses through air-flotation process Posterior circle.
Embodiment 2：Extend the oil field oil recovery factory scene untreated front mud oil-containing 21.99wt% in Treatment of Sludge station, aqueous
42.93wt%, contain miscellaneous 35.08, concrete processing method is identical with embodiment 1, transports to outward airing field, and oily sludge contains after treatment
Oily 0.30wt%, aqueous 37.87wt%, contain miscellaneous 61.83wt%, heavy metal ion reaches discharge standard, and sewage is through air-flotation process
Posterior circle uses.
Embodiment 3：Extend oil field oil recovery factory scene Treatment of Sludge station mud oil-containing after modifier treatment
25.18wt%, aqueous 32.27wt%, contain miscellaneous 42.55, concrete processing method is identical with embodiment 1, transports to outward airing field, through place
Oily sludge oil-containing 0.275wt% after reason, aqueous 38.89wt%, contain miscellaneous 60.835wt%, heavy metal ion reaches discharge mark
Standard, sewage uses through air-flotation process Posterior circle.
The foregoing is only presently preferred embodiments of the present invention, not in order to limit the present invention, all essences in the present invention
Within god and principle, any modification, equivalent substitution and improvement made etc., should be included within the scope of the present invention.
Claims (9)
1. a kind of oily sludge is innoxious and the processing method of resource it is characterised in that：Comprise the following steps：
A, oily sludge enter the preliminary mix homogeneously of reception tank, enter thermal washing tank through elevator pump, subsequently into three phase separator,
Make oil, water, mud three phase separation, top crude oil is recycled；
B, sewage, mud enter mud purge tank, add biodegradation abluent, oil residues in further eccysis sewage, mud
Part；
In c, mud purge tank, sewage enters container air-floating apparatus, and sewage recycles after treatment, and mud cleaning pot bottom is dirty
Mud and container air-floating apparatus base sludge enter mud centralized pool；
In d, mud centralized pool, mud is processed through biobelt pressure filter, by adding Biostimulation agent and processing and rear row up to standard after testing
Put.
2. a kind of oily sludge according to claim 1 is innoxious and the processing method of resource it is characterised in that：Process
Equipment includes：Reception tank, thermal washing tank, three phase separator, dissolved air flotation device, mud centralized pool, biobelt pressure filter, clean water tank,
Settling tank, elevator pump.
3. a kind of oily sludge according to claim 1 is innoxious and the processing method of resource it is characterised in that：Step
Oily sludge described in a dilutes 2 times in reception tank by recirculated water, enters thermal washing tank to fluid state.
4. a kind of oily sludge according to claim 1 is innoxious and the processing method of resource it is characterised in that：Step
Oily sludge described in a is mixed with recirculated water, heating water, filter press filtrate in thermal washing tank, and oily sludge is heated to 60-80
DEG C, and it is diluted to 5 times of raw sewage further, so that crude oil is separated from mud by adding biodegradation dispersant.
5. a kind of oily sludge according to claim 1 is innoxious and the processing method of resource it is characterised in that：Step
Three phase separator described in a will make crude oil and water and solids separation, and reclaims crude oil from oil drain out.
6. a kind of oily sludge according to claim 1 is innoxious and the processing method of resource it is characterised in that：Step
Mud purge tank described in b will be by adding biodegradation abluent, further eccysis sewage, remaining oil content in mud.
7. a kind of innoxious and resource of oily sludge according to claim 1 processing method it is characterised in that：Step
Rapid container air-floating apparatus described in c are quickly and efficiently removed oil and solid matter in mud purge tank water outlet, through container gas
After floating process, sewage will act as recirculated water, is back to reception tank, and service sink dilutes oily sludge, and partial containers flotation tank water outlet will
It is used for improving purge tank coolant-temperature gage after heating, reach thermal washing effect.
8. a kind of innoxious and resource of oily sludge according to claim 1 processing method it is characterised in that：Step
The spoil disposal of rapid device air-floating apparatus described in d squeezes into mud centralized pool by sludge pump, and then carries out sludge dewatering by biobelt pressure filter,
Dehydrated sludge rear qualified discharge after testing.
9. a kind of innoxious and resource of oily sludge according to claim 1 processing method it is characterised in that：Step
The pressing filtering liquid producing in rapid dehydration described in a-d, squeezes into reception tank, thermal washing tank by elevator pump.
Priority Applications (2)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201610622254.6A CN106396304A (en) | 2016-07-20 | 2016-07-20 | A harmlessness and reclamation treatment method for oil-containing sludge |
| CN201710110949.0A CN106904801A (en) | 2016-07-20 | 2017-02-28 | The processing method and technique of a kind of innoxious and resource of oily sludge |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201610622254.6A CN106396304A (en) | 2016-07-20 | 2016-07-20 | A harmlessness and reclamation treatment method for oil-containing sludge |
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| Publication Number | Publication Date |
|---|---|
| CN106396304A true CN106396304A (en) | 2017-02-15 |
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|---|---|---|---|
| CN201610622254.6A Pending CN106396304A (en) | 2016-07-20 | 2016-07-20 | A harmlessness and reclamation treatment method for oil-containing sludge |
| CN201710110949.0A Pending CN106904801A (en) | 2016-07-20 | 2017-02-28 | The processing method and technique of a kind of innoxious and resource of oily sludge |
Family Applications After (1)
| Application Number | Title | Priority Date | Filing Date |
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| CN201710110949.0A Pending CN106904801A (en) | 2016-07-20 | 2017-02-28 | The processing method and technique of a kind of innoxious and resource of oily sludge |
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Cited By (7)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN106904801A (en) * | 2016-07-20 | 2017-06-30 | 西安华诺环保股份有限公司 | The processing method and technique of a kind of innoxious and resource of oily sludge |
| CN107176775A (en) * | 2017-05-05 | 2017-09-19 | 郑旭东 | A kind of technological process for purifying oily sludge |
| CN108558155A (en) * | 2018-04-03 | 2018-09-21 | 任航 | A kind of processing method of oily sludge harmless resource |
| CN108706843A (en) * | 2018-05-25 | 2018-10-26 | 中科海创环境科技（大连）有限公司 | A kind of processing method of tank bottom oil sludge |
| CN110590087A (en) * | 2019-07-24 | 2019-12-20 | 中国石油大学(华东) | Treatment method of oily sludge |
| CN111790741A (en) * | 2020-06-09 | 2020-10-20 | 中国检验检疫科学研究院 | Method for intensively cleaning gas-liquid-solid multiphase flow field |
| CN115321769A (en) * | 2022-09-08 | 2022-11-11 | 河北皓清环保科技有限公司 | Oil sludge treatment device and process |
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| Publication number | Priority date | Publication date | Assignee | Title |
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| AT405299B (en) * | 1995-02-06 | 1999-06-25 | Koenig Wolfgang | DE-CONSERVATION SYSTEM FOR PERMANENT FULLY AUTOMATIC TREATMENT OF THE WASTEWATER WHEN REMOVING THE SURFACE PROTECTIVE LAYER OF FACTORY-NEW VEHICLES OR THE LIKE |
| CN102826728A (en) * | 2012-09-06 | 2012-12-19 | 中国石油天然气股份有限公司 | Cleaning agent for treating oily sludge by using hot washing method and preparation method of cleaning agent |
| CN203033864U (en) * | 2012-12-03 | 2013-07-03 | 孙树春 | Oily sludge treatment system |
| CN106396304A (en) * | 2016-07-20 | 2017-02-15 | 西安华诺环保股份有限公司 | A harmlessness and reclamation treatment method for oil-containing sludge |
-
2016
- 2016-07-20 CN CN201610622254.6A patent/CN106396304A/en active Pending
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2017
- 2017-02-28 CN CN201710110949.0A patent/CN106904801A/en active Pending
Cited By (8)
| Publication number | Priority date | Publication date | Assignee | Title |
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| CN106904801A (en) * | 2016-07-20 | 2017-06-30 | 西安华诺环保股份有限公司 | The processing method and technique of a kind of innoxious and resource of oily sludge |
| CN107176775A (en) * | 2017-05-05 | 2017-09-19 | 郑旭东 | A kind of technological process for purifying oily sludge |
| CN108558155A (en) * | 2018-04-03 | 2018-09-21 | 任航 | A kind of processing method of oily sludge harmless resource |
| CN108558155B (en) * | 2018-04-03 | 2020-09-25 | 任航 | Harmless recycling treatment method for oily sludge |
| CN108706843A (en) * | 2018-05-25 | 2018-10-26 | 中科海创环境科技（大连）有限公司 | A kind of processing method of tank bottom oil sludge |
| CN110590087A (en) * | 2019-07-24 | 2019-12-20 | 中国石油大学(华东) | Treatment method of oily sludge |
| CN111790741A (en) * | 2020-06-09 | 2020-10-20 | 中国检验检疫科学研究院 | Method for intensively cleaning gas-liquid-solid multiphase flow field |
| CN115321769A (en) * | 2022-09-08 | 2022-11-11 | 河北皓清环保科技有限公司 | Oil sludge treatment device and process |
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|---|---|
| CN106904801A (en) | 2017-06-30 |
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