CN106395827B - A kind of silicon carbide micro-powder purifying and classifying production technology and its production equipment - Google Patents

A kind of silicon carbide micro-powder purifying and classifying production technology and its production equipment Download PDF

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Publication number
CN106395827B
CN106395827B CN201610768221.2A CN201610768221A CN106395827B CN 106395827 B CN106395827 B CN 106395827B CN 201610768221 A CN201610768221 A CN 201610768221A CN 106395827 B CN106395827 B CN 106395827B
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silicon carbide
powder
pond
micro
carbide micro
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CN106395827A (en
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游振华
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Jianou City Fujian Province Rich Crystal Bao Particles Co Ltd
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Jianou City Fujian Province Rich Crystal Bao Particles Co Ltd
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    • CCHEMISTRY; METALLURGY
    • C01INORGANIC CHEMISTRY
    • C01PINDEXING SCHEME RELATING TO STRUCTURAL AND PHYSICAL ASPECTS OF SOLID INORGANIC COMPOUNDS
    • C01P2006/00Physical properties of inorganic compounds
    • C01P2006/80Compositional purity

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Abstract

The present invention relates to a kind of silicon carbide micro-powder purifying and classifying production technology and its production equipments.The technique includes that raw material adds water that silicon carbide micro-powder suspension, filtering and impurity removing, first pickling alkali cleaning again, classification of sedimentation, drying drying, fine screen packaging and other steps are made.The technique can simply, fast and efficiently remove the impurity of silicon carbide micro-powder, to improve the fineness and purity of silicon carbide micro-powder.The production equipment includes that production equipment is packed in automatic washing stirring pool, removal filtration sieve, the clear matter pond of pickling, the clear matter pond of alkali cleaning, classification of sedimentation processing pond, drying unit, feed system and micro mist fine screen.The production equipment high degree of automation, needs manpower few, and high production efficiency, energy consumption is small, energy conservation and environmental protection.

Description

A kind of silicon carbide micro-powder purifying and classifying production technology and its production equipment
Technical field
The present invention relates to the purifications of micro mist and classification technique field, and in particular to a kind of silicon carbide micro-powder purifying and classifying production Technique and its production equipment.
Background technique
Silicon carbide micro-powder is production solar silicon wafers, semi-conductor silicon chip, engineering ceramics, heating element, high grade refractory The important materials of equal products, it is higher and higher to the quality requirement of silicon carbide micro-powder with greatly developing for new material science.And show Equipment used by some clear matter of silicon carbide micro-powder cleans falls behind, and complex process, clear matter dust removal rate is low, and energy consumption is high, is not suitable for The further development of industry.
Summary of the invention
Based on above-mentioned the deficiencies in the prior art, the purpose of the present invention is to provide a kind of productions of silicon carbide micro-powder purifying and classifying Technique and its production equipment.
Technical program of the present invention lies in: a kind of silicon carbide micro-powder purifying and classifying production technology sequentially includes the following steps:
Step 1: silicon carbide micro-powder raw material being added to automatic washing stirring pool, is put into suitable water, and stir evenly, shape At silicon carbide micro-powder suspension.
Step 2: silicon carbide micro-powder suspension being pumped in removal filtration sieve and carries out primary filtration, forms filtrate and filter Slag.
Step 3: filtrate being pumped in the clear matter pond of pickling, the concentrated sulfuric acid and suspended oil is added, the dosage of the concentrated sulfuric acid is carbonization The 1 ~ 4% of silicon powder raw material weight is stood, after impurity is reacted completely and floated up, by liquid level surface layer after mixing evenly Impurity is pulled out or overflow goes out.After impurity discharge, constantly plus water is washed and dilution, and silicon carbide micro-powder suspension is made to become neutral molten Liquid.
Step 4: the silicon carbide micro-powder suspension after pickling is pumped in the clear matter pond of alkali cleaning, piece alkali and suspended oil is added, The dosage of piece alkali is the 0.1 ~ 1.5% of silicon carbide micro-powder raw material weight, after mixing evenly, stands, reacts and float completely to impurity After coming up, the impurity on liquid level surface layer is pulled out or overflow goes out.
Step 5: the silicon carbide micro-powder suspension in the clear matter pond of alkali cleaning being pumped into classification of sedimentation processing pond, is added suitable Dispersing agent carries out classification of sedimentation;
Step 6: after the difference silicon carbide micro-powder suspension after classification is sieved again, being sent into centrigugal swing dryer and dry;
Step 7: the wet silicon carbide micro-powder after drying being fitted into be put into drying unit after drying tray and is dried, is formed dry Silicon carbide micro-powder;
Step 8: dry silicon carbide micro-powder is weighed through feed system transport micro mist fine screen packaging production equipment, is packed.
The automatic washing stirring pool includes pond body in step 1, and the two sides pool wall upper end of the pond body is provided with track, The vehicle frame that can be moved back and forth along track is installed on the track, it is vertically-mounted on the vehicle frame to have an agitating shaft, it is described to stir It mixes axis to be driven by stirring motor, stroke motor is also equipped on the vehicle frame, to drive the idler wheel of vehicle frame bottom along rail Road movement;Block is respectively set in the both ends of the track, and the lower part both ends of the vehicle frame are correspondingly arranged on travel switch, described Travel switch is linked into the control circuit in electric cabinet through connecting line, and the control circuit is connected through connecting line with stroke motor It connects, is automatically moved back and forth to control vehicle frame along track.
The removal filtration sieve includes feed well, filtering table, receiver and support body in step 2, and the feed well is set It sets in the upper end of filtering table, the upper cover of the feed well, which may be reversed, opens, and is provided with charging pipe fitting, institute in the middle part of the upper cover The inner cavity for stating feed well is provided with initial filter sieve, and the lower part of the feed well is provided with discharging long slot hole;It the filtering table and connects Charging tray is inclined on support body, and filtering table is located at the top of receiver, and the bottom plate of the filtering table is smart filter screen, institute The circumference for stating filtering table is provided with splashproof shading cloth, and the lower end of the splashproof shading cloth extends on the inside of the peripheral wall of receiver;Institute It states and is respectively arranged with discharging pipe fitting on the lower one end of filtering table and receiver.
The clear matter pond of the pickling includes rectangle pond body in step 3, and the two sidewalls upper end of the rectangle pond body is respectively set There is track, being equipped on the track vertically-mounted on the vehicle frame of track reciprocating motion, the vehicle frame can have agitating shaft, The lower end of the agitating shaft extends on the upside of the bottom of pond of rectangle pond body, to stir the intracorporal micro mist suspension of rectangle form pool;It is described One end of rectangle pond body is water inlet end, and the Sidewall Height of water inlet end is higher;In the case where the rectangle pool bottom of water inlet end is provided with into The mouth of a river is equipped with upper water inlet, the other end of the upper water inlet towards rectangle pond body in the middle part of the rectangle pond body of water inlet end;It is described The other end of rectangle pond body is effluent head, and the Sidewall Height of effluent head is shorter, when water level goes up, swims in the impurity on the water surface It is flowed out from effluent head;The different drainage hole of several absolute altitudes is set on the rectangle form pool body sidewall of effluent head, on the drainage hole Closure has stopple, and the stopple is removable.
The clear matter pond of the alkali cleaning includes pond body and the bracket that is erected above pond body in step 4, the periphery of the pond body Heat-conducting oil pipes and insulating layer are surrounded with, the pond body intracavity bottom is additionally provided with aeration tube, to suspend to the intracorporal micro mist in pond Liquid carries out bubbling -cleaning;Vertically-mounted on the bracket to have agitating shaft, the lower end of the agitating shaft extends on the bottom of pond body Side, so as to the intracorporal micro mist suspension of stirring pool;The bottom of the pond body is provided with discharge valve and feeder pipe.
The classification of sedimentation processing pond includes settling tank and grading pool in steps of 5, and the grading pool is arranged in settling tank Side, the settling tank is higher than grading pool, and is provided with several points on the side wall that settling tank is higher by grading pool upper surface Grade drainage hole, closure has stopple on the classification drainage hole, and the stopple is removable;The outer side wall of several classification drainage holes Equipped with collecting tank, the bottom of the collecting tank is circumscribed with movable isocon, and the activity isocon leads to grading pool;The sedimentation Be provided with multiple detection mouths on the pond body side wall in pond from top to bottom, the detection mouth is the outlet pipe with shut-off valve, so as to It is detected before classification drain.
The drying unit includes drying cabinet in step 7, before drying box is arranged in the chamber door of the drying cabinet Side, the chamber door are detachable;The drying cabinets cavity is provided with drying layer frame, the drying layer frame be by several side by side Petroleum pipeline from bottom to top S type layer around and formed, be placed with drying tray in the drying layer frame;Several oil transportations side by side Pipe oil inlet end is commonly connected to oil inlet tap, and the oil inlet tap connects fuel feeding general pipeline, and is arranged on fuel feeding general pipeline There is oil inlet control valve;The end of several petroleum pipelines side by side is commonly connected to confluence connector, the confluence connector connection Return header.
The feed system includes dry micro mist bunker workshop, bucket type transfer car(buggy) and suspension gear to be packaged, institute in step 8 Stating dry micro mist bunker workshop to be packaged includes workshop ontology and melt pit, and a side-lower of workshop ontology is arranged in the melt pit, i.e., Workshop ontology side is hung on above melt pit.And the side of the workshop ontology is internally provided with aggregate bin, the aggregate bin Configured with bracket.The lower end material blanking tube of the aggregate bin passes through the floor of workshop ontology, and extends one section to melt pit, forms blanking Pipe extension;It is provided with dust hood above the aggregate bin, dust suction connecting leg, the dust suction are provided at the top of the dust hood Connecting leg is linked into dust suction general pipeline, and the upper end of the dust suction general pipeline is provided with the first control valve, the lower end of the dust suction general pipeline to Under extend to the discharge port side of material blanking tube lower end, be provided with the second control valve on the lower end discharge port of the dust suction general pipeline;Institute It states and is placed with bucket type transfer car(buggy) in melt pit.The suspension gear is arranged in the top of melt pit, and the suspension gear is most uphang Hang the height that height is higher by least one bucket type transfer car(buggy) of frame body.
Micro mist fine screen packaging production equipment includes workshop ontology, ultrasonic wave fine screen device and micro- in step 8 Powder sack-filling device, the workshop ontology include fine screen workshop and packing shop, and the ultrasonic wave fine screen device is mounted on essence It sieves in workshop, the ultrasonic wave fine screen device is two-stage ultrasonic wave fine screen device;The micro mist sack-filling device includes first, second With third micro mist sack-filling device;The two-stage ultrasonic wave fine screen in fine screen workshop is arranged in the first, second micro mist sack-filling device Below device discharge port, the terminal discharge mouth of the two-stage ultrasonic wave fine screen device is extend into packing shop, and the third is micro- Powder sack-filling device is arranged in packing shop;And the third micro mist sack-filling device is located at the end of two-stage ultrasonic wave fine screen device The lower section of discharge port.
Another technical solution of the invention is: the production equipment includes automatic washing stirring pool, removal filtration sieve, pickling Production equipment is packed in clear matter pond, the clear matter pond of alkali cleaning, classification of sedimentation processing pond, drying unit, feed system and micro mist fine screen.It is each It elaborated above the detail of equipment, just repeated no more here.
The beneficial effects of the present invention are: the technique can quickly, efficiently remove the impurity of silicon carbide micro-powder, thus Improve the precision of silicon carbide micro-powder.And equipment employed in the technique also respectively has specific superiority and first carries out, specifically It is as follows:
Automatic washing stirring pool comes vehicle frame physical efficiency automatically along track automatically due to being additionally arranged travel switch and control circuit It returns and moves back and forth, high degree of automation, save trouble and labor, and washing and mixing effect are good, controllability is strong.In addition, water inlet pipe is set It counts on the side wall close to pool bottom, is conducive to disturb the micro mist material of pool bottom, raising is stirred efficiency. When pond body is cleaned and cleaned, the design of the water inlet also helps the flushing to pond body bottom surface, improves cleaning efficiency.
The filter screen of primary filtration is arranged in removal filtration sieve in feed well, can preliminarily will be larger in micro mist suspension Particulate matter filter out, after filtering, these biggish particulate matters can be taken out by opening upper cover.Therefore, the removal of impurities Screen can not only carry out primary filtration and more fine secondary filter to the micro mist suspension after washing, and due to filtering The circumference of disk, which increases, is provided with splashproof shading cloth, can be effectively prevented the micro mist suspension in filtering and splash out, reduce loss of material. Make removal filtration sieve be able to achieve mobile use in addition, castor and positioning support structure is arranged in the bottom of support body, so as to One micro mist suspension removal filtration sieve can wash stirring pool at times for multiple micro mists automatically and provide filtering and impurity removing service, mention Its high use value.
The clear matter pond of pickling mainly utilize the silicon carbide micro-powder in suspension be easy deposit buildup characteristic and pickling after it is miscellaneous Matter can swim in the characteristic on liquid level, in conjunction with dexterously designing the drain different with overflow port and multiple absolute altitudes of upper and lower water inlet Hole, when the close full pond of material, it can push liquid level water layer to flow to overflow port, and will not be to the particulate deposits of clear matter bottom of pond portion Layer generates excessive disturbance.Under the premise of avoiding particulate deposits logistics from losing, the overflows such as liquid level bubble and impurity are removed.Work as object Material is when keeping off full pond, according to actual liquid level height be it is desirable, open the stopple on the drainage hole of corresponding height, then allow again Upper water inlet is passed through clear water, allows impurity according to the practical overflow operation for perhaps needing to carry out impurity.
The clear matter pond of alkali cleaning is able to achieve alkalinity washing and the processing of clear matter to micro mist (silicon carbide), and clear matter is high-efficient.First lead to Crossing stirring power is sufficiently mixed micro mist suspension with alkalinity removal of impurities liquid, then improves reaction temperature by heat-conducting oil pipes, adds Fast micro mist suspension is reacted with alkalinity removal of impurities liquid, and finally by the mode of bubbling -cleaning, rapidly impurity suspends from micro mist It separates, and is swum on liquid level in liquid.
Classification of sedimentation processing pond is different using the time that micro powder granule staticly settles in micro mist suspension, by corresponding Sedimentation time will be layered respectively containing the micro mist sedimentation liquid of different micro powder granule sizes be discharged from top to bottom, to realize that micro mist is outstanding The classification of sedimentation of supernatant liquid is processed, in case procedure processing uses.
Drying unit is mainly used for the wet micro mist after drying drying, and drying efficiency is high, high-quality, and micro mist is avoided to fly upward damage It loses, energy conservation and environmental protection.
Rationally, structure is simple, is mainly used for focusing on the micro mist in drying tray into bucket type transfer car(buggy) for feed system design On hopper in, so that micro mist is transferred to fine screen and packing shop.Bucket type transfer car(buggy) is mainly used in the charging of micro mist fine screening machine Transhipment between system and fine screen and packing shop, cooperation suspension gear use, by the bunker lift on bucket type transfer car(buggy) to essence The feed inlet of sieve apparatus.
Micro mist fine screen packaging production equipment is mainly used for the final step of micro mist purification and classification processing, is conducive to further Improve effectiveness of classification and pack efficiency.Meanwhile setting up fine screen and packaging in different workshops separately, be conducive to the ring for improving workshop Border health.Loading platform or so can be made to be switched fast by track and castor, reduce and avoid micro mist be scattered ground the case where, because This, micro mist fine screen packaging production equipment adapts to continuously continual packed.Meanwhile the micro mist fine screen packaging production is set Standby side is additionally provided with weigher.The circumference of the weigher is provided with the bracket of semi-surrounding, and bag is sent out when preventing from weighing Life is toppled over.
Detailed description of the invention
Fig. 1 is the simple process figure of silicon carbide micro-powder purifying and classifying production technology of the invention.
Fig. 2 is the schematic view of the front view for washing stirring pool in embodiment automatically.
Fig. 3 is the vehicle frame and associated components structure enlargement diagram thereon for washing stirring pool in embodiment automatically.
Fig. 4 is the schematic view of the front view of removal filtration sieve in embodiment.
Fig. 5 is the schematic cross-sectional view of the feed well of removal filtration sieve in embodiment.
Fig. 6 is the filtering table and receiver cross-section diagram of removal filtration sieve in embodiment.
Fig. 7 is the structural schematic diagram of the positioning support structure of removal filtration sieve in embodiment.
Fig. 8 is the structural schematic diagram in the clear matter pond of pickling in embodiment.
Fig. 9 is the vehicle frame and the mounting structure schematic diagram of associated components thereon in the clear matter pond of pickling in embodiment.
Figure 10 is the schematic view of the front view of the effluent head side plate in the clear matter pond of pickling in embodiment.
Figure 11 is the partial enlargement structural representation in Figure 10 at I.
Figure 12 is by the structural schematic diagram after bolt hinged in Figure 11 to the left side to overturn.
Figure 13 is the structural schematic diagram in the clear matter pond of alkali cleaning in embodiment.
Figure 14 is the overlooking structure diagram of classification of sedimentation processing pond in embodiment.
Figure 15 is the schematic view of the front view of classification of sedimentation processing pond in embodiment.
Figure 16 is the schematic cross-sectional view of sedimentation basin in embodiment.
Figure 17 is the vehicle frame and associated components structure enlargement diagram thereon of classification of sedimentation processing pond in embodiment.
Figure 18 is the schematic view of the front view of collecting tank internal classification drainage hole and stopple.
Figure 19 is structural schematic diagram at A in Figure 18.
Figure 20 is Figure 19 by the structural schematic diagram after hinged bolt to the left side to overturn.
The structural schematic diagram of drying unit in Figure 21 embodiment.
The structural schematic diagram of oil inlet tap in Figure 22 embodiment.
The structural schematic diagram of feed system in Figure 23 embodiment.
The structural schematic diagram in dry micro mist bunker workshop to be packaged in Figure 24 embodiment.
Figure 25 is the structural schematic diagram of charging hopper in embodiment.
Figure 26 is the structural schematic diagram of trolley in embodiment.
Figure 27 is the structural schematic diagram of bucket type transfer car(buggy) in embodiment.
Figure 28 is the structural schematic diagram that production equipment is packed in micro mist fine screen in embodiment.
Figure 29 is the schematic view of the front view of third micro mist sack-filling device in embodiment.
Figure 30 is the overlooking structure diagram of third micro mist sack-filling device in embodiment.
Figure 31 is the right side structural representation of third micro mist sack-filling device in embodiment.
Label declaration:
First part: 1- pond body 2- track 3- lip block 4- vehicle frame 5- agitating shaft 6- stirring motor 7- stirring rod 8- third belt gear 9- stroke motor 10- idler wheel 11- block 12- travel switch 13- Electric cabinet 14- water inlet pipe 15- the first belt gear 16- retarder the second belt transmission agency of 17-.
Second part: 20- feed well 21- filtering table 22- receiver 23- upper cover 24- feeds pipe fitting 25- initial filter sieve 26- discharging long slot hole 27- essence filter screen 28- splashproof shading cloth 29- discharging pipe fitting 30- foot Take turns support chip 34- upper cover under 31- handwheel 32- screw rod 33-.
Part III: 1- pond body 2- track 3- lip block 4- vehicle frame 5- agitating shaft 6- stirring motor 7- stirring rod 8- third belt gear 9- stroke motor 10- idler wheel 11- block 12- travel switch 13- The first belt gear of water inlet 15- 16- retarder the second belt transmission agency of 17- 18- on electric cabinet 14- Water inlet 20- effluent head 21- stopple 22- pressing plate 23-U type groove 24- screw rod 25- butterfly under water inlet end 19- Nut.
Part IV: 1- pond body 2- bracket 3- heat-conducting oil pipes 4- insulating layer 5- aeration tube 6- agitating shaft 7- discharge valve 8- feeder pipe 9- oil feed line 10- return line 11- protective net 12- air inlet pipeline 13- motor 14- belt.
Part V: 1- settling tank 2- track 3- lip block 4- vehicle frame 5- agitating shaft 6- stirring electricity Machine 7- stirring rod 8- third belt gear 9- stroke motor 10- idler wheel 11- block 12- travel switch 13- electric cabinet 14- detection mouth 15- the first belt gear 16- retarder the second belt transmission agency of 17-; 20- grading pool 21- stopple 22- collecting tank 23- activity isocon 24- platform board 25- stair 26- water inlet pipe 27- control valve 28- branched pipe 29- water inlet manifold 30- pressing plate 31-U type groove 32- screw rod 33- wing nut.
Part VI: 1- dries cabinet 2- chamber door 3- and dries layer frame 4- drying tray 5- oil inlet tap 6- fuel feeding general pipeline 7- oil inlet control valve 8- confluence connector 9- return header 10- recycle control valve 11- card slot 12- shunts general pipeline 13- shunt pipe 14- pull ring 15- thermometer.
Part VII: 30- bucket type transfer car(buggy) 31- suspension gear 32- guardrail 33- stair 34- remote controler; The workshop 20- ontology 21- melt pit 22- aggregate bin 23- bracket 24- material blanking tube 25- dust hood 26- dust suction connecting leg 27- dust suction general pipeline 28- the first control valve 29- the second control valve 1- trolley 2- charging hopper 3- cylindrical portions 4- cone bucket part 5- feed opening 6- upper sealing plate 7- feed opening 8- suspension hook or lifting lug 9- baiting valve 10- support frame 11- support ring 12- universal caster wheel 13- upright bar.
Part VIII: 20- workshop ontology 21- ultrasonic wave fine screen device 22- fine screen workshop 23- packs vehicle Between the workshop 24- dust suction air hose 25- door 26- interlayer 27- platform 28- stair;10- feed bin 11- baiting valve 12- feeding passage 13- level-one ultrasonic activation sieves 14- second level ultrasonic activation and sieves the first micro mist of 15- sack-filling device 16- the second micro mist sack-filling device 17- third micro mist sack-filling device 18- vibrating motor 19- dustcloth;1- track 2- U-shaped frame 7- support rod 8- weigher 9- among U-shaped frame 6- on castor 3- loading platform 4- bag bracket 5- The bracket of semi-surrounding.
Specific embodiment
In order to describe the technical content, the structural feature, the achieved object and the effect of this invention in detail, below in conjunction with embodiment And attached drawing is cooperated to be explained in detail.
As shown in Figure 1, silicon carbide micro-powder purifying and classifying production technology of the invention, sequentially includes the following steps:
Step 1: silicon carbide micro-powder raw material being added to automatic washing stirring pool, is put into suitable water, and stir evenly, shape At silicon carbide micro-powder suspension.
Step 2: silicon carbide micro-powder suspension being pumped in removal filtration sieve and carries out primary filtration, forms filtrate and filter Slag.
Step 3: filtrate being pumped in the clear matter pond of pickling, the concentrated sulfuric acid and suspended oil is added, the dosage of the concentrated sulfuric acid is carbonization The 1 ~ 4% of silicon powder raw material weight is stood, after impurity is reacted completely and floated up, by liquid level surface layer after mixing evenly Impurity is pulled out or overflow goes out.After impurity discharge, constantly plus water is washed and dilution, and silicon carbide micro-powder suspension is made to become neutral molten Liquid.Specifically plus water water-washing process are as follows: the impurity on liquid level surface layer is pulled out or overflow go out after, first supernatant liquor is discharged again, Clear water, stirring washing and dilution are added into pond, then staticly settles, is then exhausted from supernatant liquor;So repeat, until carbonization Silicon powder suspension or precipitated liquid become neutral.
Step 4: the silicon carbide micro-powder suspension after pickling is pumped in the clear matter pond of alkali cleaning, piece alkali and suspended oil is added, The dosage of piece alkali is the 0.1 ~ 1.5% of silicon carbide micro-powder raw material weight, after mixing evenly, stands, reacts and float completely to impurity After coming up, the impurity on liquid level surface layer is pulled out or overflow goes out.
Step 5: the silicon carbide micro-powder suspension in the clear matter pond of alkali cleaning being pumped into classification of sedimentation processing pond, is added suitable Dispersing agent carries out classification of sedimentation;
Step 6: after the difference silicon carbide micro-powder suspension after classification is sieved again, being sent into centrigugal swing dryer and dry;
Step 7: the wet silicon carbide micro-powder after drying being fitted into be put into drying unit after drying tray and is dried, is formed dry Silicon carbide micro-powder;
Step 8: dry silicon carbide micro-powder is weighed through feed system transport micro mist fine screen packaging production equipment, is packed.
It is clear to the automatic washing stirring pool, removal filtration sieve, pickling that arrive used in above-mentioned technique to be divided into four parts below Production equipment this eight is packed in matter pond, the clear matter pond of alkali cleaning, classification of sedimentation processing pond, drying unit, feed system and micro mist fine screen Equipment does specific illustration and description.
First part: stirring pool is washed automatically
As shown in Figures 2 and 3, the automatic washing stirring pool includes pond body 1, and the pond body 1 is the pond body of rectangle, long It spends longer.The two sides pool wall upper end of the pond body 1 is provided with track 2, the two sides pool wall upper end of the track 2 and pond body 1 it Between be additionally provided with lip block 3.On the one hand the design of the lip block 3 plays the role of support, on the other hand play buffer vehicle Vibration when frame body moves in orbit.
As shown in Fig. 2, being equipped with the vehicle frame 4 that can be moved back and forth along track on the track 2, the vehicle frame 4 is to adopt The rectangle frame frame body being welded with fashioned iron or angle steel.
As shown in Figures 2 and 3, vertically-mounted on the vehicle frame 4 to have agitating shaft 5, the agitating shaft 5 has two, two Agitating shaft 5 is disposed side by side on vehicle frame 4 in parallel along pond body width direction, and the agitating shaft 5 is driven by stirring motor 6, described The lower end of agitating shaft is provided with stirring rod 7.The stirring motor 6 drives two agitating shafts simultaneously through third belt gear 8 Operating.
As shown in Figures 2 and 3, it is also equipped with stroke motor 9 on the vehicle frame 4, to drive the rolling of 4 bottom of vehicle frame Wheel 10 is moved along track 2.Block 11 is respectively set in the both ends of the track 2, and the lower part both ends of the vehicle frame 4 are correspondingly arranged on Travel switch 12, the travel switch 12 are linked into the control circuit in electric cabinet 13 through connecting line, and the control circuit is Control relay circuit, single chip machine controlling circuit or PLC control circuit.The control circuit is through connecting line and stroke motor 9 It is connected, is automatically moved back and forth to control vehicle frame 4 along track.
As shown in Figures 2 and 3, the stroke motor 9 is sequentially connected through the first belt gear 15 with retarder 16, institute It states retarder 16 and is connect through the second belt transmission agency 17 with the rotating shaft transmission of the idler wheel 10 of 4 bottom of vehicle frame, the stroke electricity Machine 9 and retarder 16 are installed on vehicle frame.
It is assumed that the travel switch 12 of 4 lower part of vehicle frame is by block 11 when vehicle frame 4 is moved to the left part of track 2 Extruding, so that travel switch 12 is triggered, generate trigger signal, which passes to the control in electric cabinet 13 through connecting line Circuit processed, control circuit carry out commutation power supply to stroke motor 9, rotate backward stroke motor 9, to drive 4 edge of vehicle frame Track 2 is moved towards other direction, and so on, it is manually controlled until shutting down or being switched to.
As shown in Fig. 2, washing stirring pool further includes water inlet pipe 14 automatically, the water inlet pipe 14 is positioned close to 1 bottom of pond body On the left side wall (side wall in width direction) in portion.By the design of intake of water inlet pipe 14 on the side wall close to pool bottom, Be conducive to disturb the micro mist material of pool bottom, raising is stirred efficiency.In addition, when pond body cleaning is cleaned It waits, the design of the water inlet also helps the flushing to pond body bottom surface, improves cleaning efficiency.
Second part: removal filtration sieve
As shown in Figure 4, Figure 5, Figure 6 and Figure 7, removal filtration sieve includes feed well 20, filtering table 21, receiver 22 With support body 23.The upper end (higher end) of inclined filtering table 21 is arranged in the feed well 20, the feed well 20 Upper cover 34, which may be reversed, opens, and charging pipe fitting 24 is provided in the middle part of the upper cover, the inner cavity of the feed well 20 is provided with initial filter Sieve 25, the lower part of the feed well 20 are provided with discharging long slot hole 26;The filtering table 21 and receiver 22 are inclined at On support body 23, and filtering table 21 is located at the top of receiver 22, and the bottom plate of the filtering table 21 is smart filter screen 27, the mistake The circumference of filter disc 21 is provided with splashproof shading cloth 28, and the lower end of the splashproof shading cloth 28 extends in the peripheral wall of receiver 22 Side;Discharging pipe fitting 29 is respectively arranged on the lower one end of the filtering table 21 and receiver 22.
In order to further more comprehensively improve the ability that anti-material splashes out, the discharging long slot hole side of the feed well 20 is also set It is equipped with splashproof shading cloth.
It, can at times to be sieved in a micro mist suspension removal filtration in order to facilitate the mobile use of removal filtration sieve Stirring pool being washed automatically for multiple micro mists, filtering and impurity removing service being provided, the bottom of the support body is provided with castor 30.
For the ease of realizing the movement and positioning of removal filtration sieve, positioning branch is provided on the bottom bar of the support body Support structure.More specifically, the positioning support structure includes that handwheel 31, screw rod 32 and lower support chip 33, the screw rod are worn On the bottom bar of support body, the handwheel is mounted on the upper end of screw rod, and the lower support chip is mounted on the lower end of screw rod.
Part III: the clear matter pond of pickling
If Fig. 8 is extremely and shown in Figure 12, the clear matter pond of the pickling includes rectangle pond body 1, and the rectangle pond body is by two What long side wall and two broad side walls surrounded.The two sidewalls upper end of the rectangle pond body 1 is respectively arranged with track 2, the track 2 with Lip block 3 is additionally provided between the two sidewalls upper end of pond body.On the one hand the design of the lip block 3 plays the work of support With on the other hand playing vibration of buffering vehicle frame when moving in orbit.
If Fig. 8 is extremely and shown in Figure 12, the vehicle frame 4 that can be moved back and forth along track, the vehicle frame are installed on the track 2 Body 4 is the rectangle frame frame body being welded using fashioned iron or angle steel.
If Fig. 8 is extremely and shown in Figure 12, vertically-mounted on the vehicle frame 4 to have agitating shaft 5, the lower end of the agitating shaft 5 is prolonged On the upside of the bottom of pond for extending to rectangle pond body 1, to stir the suspension in rectangle pond body 1.
If Fig. 8 to and Figure 12 shown in, vertically-mounted on the vehicle frame 4 to have an agitating shaft 5, the agitating shaft 5 has two, two Root agitating shaft 5 is disposed side by side on vehicle frame 4 in parallel along pond body width direction, and the agitating shaft 5 is driven by stirring motor 6, institute The lower end for stating agitating shaft is provided with stirring rod 7.The stirring motor 6 drives two agitating shafts same through third belt gear 8 Shi Yunzhuan.
If Fig. 8 is extremely and shown in Figure 12, it is also equipped with stroke motor 9 on the vehicle frame 4, to drive 4 bottom of vehicle frame Idler wheel 10 moved along track 2.Block 11 is respectively set in the both ends of the track 2, and the lower part both ends correspondence of the vehicle frame 4 is set It is equipped with travel switch 12, the travel switch 12 is linked into the control circuit in electric cabinet 13 through connecting line, the control electricity Road is control relay circuit, single chip machine controlling circuit or PLC control circuit.The control circuit is through connecting line and stroke electricity Machine 9 is connected, and automatically moves back and forth to control vehicle frame 4 along track.
If Fig. 8 is extremely and shown in Figure 12, the stroke motor 9 connects through the first belt gear 15 and the transmission of retarder 16 It connects, the retarder 16 is connect through the second belt transmission agency 17 with the rotating shaft transmission of the idler wheel 10 of 4 bottom of vehicle frame, the row Journey motor 9 and retarder 16 are installed on vehicle frame.
It is assumed that the travel switch 12 of 4 lower part of vehicle frame is by block 11 when vehicle frame 4 is moved to the left part of track 2 Extruding, so that travel switch 12 is triggered, generate trigger signal, which passes to the control in electric cabinet 13 through connecting line Circuit processed, control circuit carry out commutation power supply to stroke motor 9, rotate backward stroke motor 9, to drive 4 edge of vehicle frame Track 2 is moved towards other direction, and so on, it is manually controlled until shutting down or being switched to.
If Fig. 8 to and Figure 12 shown in, one end of the rectangle pond body 1 is water inlet end 18, the Sidewall Height of water inlet end 18 compared with It is high;Rectangle pool bottom close to water inlet end 18 is provided with lower water inlet 19, is equipped with close to the rectangle pond body top of water inlet end upper Water inlet 14 is opened on the upper water inlet 14 and is evenly equipped with apopore, the other end of the apopore towards rectangle pond body;The square The other end of shape pond body is effluent head 20, and the Sidewall Height of effluent head is shorter, when water level goes up, swims in the impurity on the water surface It is flowed out from effluent head.
One end of the rectangle pond body is water inlet end 18, and the Sidewall Height of water inlet end 18 is higher;In the rectangle form pool of water inlet end Body bottom is provided with lower water inlet 19, and upper water inlet 14, upper 14 court of water inlet are equipped in the middle part of the rectangle pond body of water inlet end To the other end of rectangle pond body.
The other end of the rectangle pond body is effluent head 20, and the Sidewall Height of effluent head is shorter, when water level goes up, floating Impurity on the water surface is flowed out from effluent head.
If Fig. 8 is extremely and shown in Figure 12, the different drain of several absolute altitudes is set on the rectangle form pool body sidewall of effluent head 20 Hole, blocking on the drainage hole has stopple, and the stopple 21 is removable.
The back of the stopple 21 is connected with pressing plate 22, and one end of the pressing plate 22 is hinged on outside the effluent head of rectangle pond body On wall, the other end of the pressing plate 22 is movable end, and the movable end is equipped with U-type groove 23, rectangle form pool corresponding with movable end Screw rod 24 is hinged on external side wall, the screw rod 24 may be reversed and be caught in U-type groove 23, be additionally provided with use on the screw rod 24 In the wing nut 25 being pressed on movable end on screw rod.
In use, first pumping to micro mist suspension in the clear matter pond of pickling, it is passed through by water inlet under rectangle pool bottom Clear water after reaching liquid level actually required, stops being passed through for clear water;Suitable acid solution is added in clear matter pond, and passes through Agitating shaft is stirred the suspension in clear matter pond, is uniformly mixed it with acid solution, allows the impurity of acid solution and micro mist suspension Sufficiently reaction;Stand, after micro mist suspension sedimentation, according to actual liquid level height be it is desirable, open the drain of corresponding height Stopple on hole, then allows water inlet to be passed through clear water again, allows impurity according to the practical overflow for perhaps needing to carry out impurity Operation, while excessive disturbance will not be generated to settled micro mist again.
Part IV: the clear matter pond of alkali cleaning
As shown in figure 13, the clear matter pond of the alkali cleaning includes pond body 1 and the bracket 2 that is erected above pond body, the pond body 1 Periphery coiling have heat-conducting oil pipes 3 and insulating layer 4,1 intracavity bottom of pond body is additionally provided with aeration tube 5, so as to in pond body 1 Micro mist suspension carry out bubbling -cleaning;Vertically-mounted on the bracket 2 to have agitating shaft 6, the lower end of the agitating shaft 6 extends to On the upside of the bottom of pond body 1, so as to the intracorporal micro mist suspension of stirring pool;The bottom of the pond body is provided with discharge valve 7 and blanking Pipe 8.
In the present embodiment, the lower end oil inlet of the heat-conducting oil pipes 3 is connected with oil feed line 9, the heat-conducting oil pipes 3 Upper end oil outlet be connected with return line 10.
Protective net 11 is surrounded by the outside of the aeration tube 5, to prevent the gas blocked on aeration tube in micro mist suspension Hole.
The clear matter pond of alkali cleaning further includes air inlet pipeline 12, and the air inlet pipeline 12 extends downwardly into pond body from the upper opening of pond body Chamber, and be connected with the air inlet of aerating pipelines 5.
The pond body is stainless steel pond body, and on the one hand the relatively good heat transfer by heat-conducting oil pipes of energy is intracorporal to pond Micro mist suspension;On the other hand, stainless steel pond body also has stronger corrosion resistance, avoids rotten by alkalinity removal of impurities liquid Erosion.
In use, first pump to the micro mist suspension for needing alkali cleaning in pond body 1, after suitable alkalinity removal of impurities liquid is added, First passing through stirring power is sufficiently mixed micro mist suspension with alkalinity removal of impurities liquid, then reaction temperature is improved by heat-conducting oil pipes Degree is accelerated micro mist suspension and the alkalinity liquid that cleans and is reacted, finally by the mode of bubbling -cleaning, rapidly by impurity from micro mist It separates, and is swum on liquid level in suspension, to pull out.
Part V: classification of sedimentation processing pond
As shown in Figure 14 and Figure 15, the classification of sedimentation processing pond includes settling tank 1 and grading pool 20, the settling tank 1 For the concrete pond of rectangle, length is longer.The grading pool 20 is plastics pond body, and plastics pond body periphery is provided with reinforcement Muscle.Three grading pools 20 are disposed side by side on a side of settling tank 1, and the settling tank 1 is higher than grading pool 20, and in settling tank 1 It is higher by the side wall of 20 upper surface of grading pool and is provided with several classification drainage holes, the classification drainage hole is arranged two neighboring The intersection of grading pool 20, blocking on the classification drainage hole has stopple 21, and the stopple 21 is removable;Several classifications row The outer side wall of fluid apertures is equipped with collecting tank 22, and the bottom of the collecting tank is circumscribed with movable isocon 23, and the activity isocon can Rotation;The activity isocon leads to grading pool 20.On the side of settling tank 1, also it has been horizontally set on three grading pools 20 flat Platen 24, the both ends of the platform board are provided with stair 25.One end of the settling tank 1 is additionally provided with several water inlet pipes 26, institute It states 26 outer end of water inlet pipe and is provided with control valve 27, the water inlet pipe 26 is connected through branched pipe 28 with water inlet manifold 29.It is described heavy It dropping and is provided with multiple detection mouths 14 on the pond body side wall in pond 1 from top to bottom, the detection mouth 14 is the outlet pipe with shut-off valve, To be detected before being classified drain, effectiveness of classification is improved.
As shown in figure 16, the two sides pool wall upper end of the settling tank 1 is provided with track 2, the track 2 and settling tank 1 Two sides are additionally provided with lip block 3 between pool wall upper end.On the one hand the design of the lip block 3 plays the role of support, separately On the one hand vibration when buffering vehicle frame moves in orbit is played.
As shown in figure 16, the vehicle frame 4 that can be moved back and forth along track is installed, the vehicle frame 4 is to adopt on the track 2 The rectangle frame frame body being welded with fashioned iron or angle steel.
As shown in Figure 16 and Figure 17, vertically-mounted on the vehicle frame 4 to have an agitating shaft 5, the agitating shaft 5 has two, and two Root agitating shaft 5 is disposed side by side on vehicle frame 4 in parallel along settling tank width direction, and the agitating shaft 5 is driven by stirring motor 6, The lower end of the agitating shaft is provided with stirring rod 7.The stirring motor 6 drives two agitating shafts through third belt gear 8 It operates simultaneously.
As shown in Figure 16 and Figure 17, it is also equipped with stroke motor 9 on the vehicle frame 4, to drive 4 bottom of vehicle frame Idler wheel 10 is moved along track 2.Block 11 is respectively set in the both ends of the track 2, and the lower part both ends of the vehicle frame 4 are correspondingly arranged There is travel switch 12, the travel switch 12 is linked into the control circuit in electric cabinet 13 through connecting line, the control circuit For control relay circuit, single chip machine controlling circuit or PLC control circuit.The control circuit is through connecting line and stroke motor 9 are connected, and automatically move back and forth to control vehicle frame 4 along track.
As shown in Figure 16 and Figure 17, the stroke motor 9 is sequentially connected through the first belt gear 15 with retarder 16, The retarder 16 is connect through the second belt transmission agency 17 with the rotating shaft transmission of the idler wheel 10 of 4 bottom of vehicle frame, the stroke Motor 9 and retarder 16 are installed on vehicle frame.
It is assumed that the travel switch 12 of 4 lower part of vehicle frame is by block 11 when vehicle frame 4 is moved to the left part of track 2 Extruding, so that travel switch 12 is triggered, generate trigger signal, which passes to the control in electric cabinet 13 through connecting line Circuit processed, control circuit carry out commutation power supply to stroke motor 9, rotate backward stroke motor 9, to drive 4 edge of vehicle frame Track 2 is moved towards other direction, and so on, it is manually controlled until shutting down or being switched to.
As shown in Figure 18, Figure 19 and Figure 20, the back of the stopple 21 is connected with pressing plate 30, one end hinge of the pressing plate 30 It connects on the outer wall of sedimentation basin, the other end of the pressing plate 30 is movable end, and the movable end is equipped with U-type groove 31, with activity It holds and is hinged with screw rod 32 on the outer wall of corresponding sedimentation basin, the screw rod 32 may be reversed and be caught in U-type groove 31, the screw rod 32 On be additionally provided with wing nut 33 for being pressed on movable end on screw rod.
Part VI: drying unit
As shown in figure 21, the drying unit of the wet micro mist mainly includes drying cabinet 1, the chamber door 2 of the drying cabinet 1 The front side of drying box 1 is set, and the chamber door 2 is detachable;1 inner cavity of drying cabinet is provided with drying layer frame 3, the drying Layer frame 3 be by several petroleum pipelines side by side from bottom to top S type layer around and formed, be placed with drying in the drying layer frame 3 Disk 4;Described several petroleum pipeline oil inlet ends side by side are commonly connected to oil inlet tap 5, and the oil inlet tap 5 connects Fuel feeding general pipeline 6, and oil inlet control valve 7 is provided on fuel feeding general pipeline 6;The end of several petroleum pipelines side by side connects jointly To confluence connector 8, the confluence connector 8 connects return header 9, is provided with recycle control valve 10 on the return header 9.
As shown in figure 21, it is provided with card slot 11 on the drying cabinet front side door frame, the chamber door 2 is plugged on card slot 11 It is interior.The drying cabinet includes angle frame frame body and galvanized iron sheet, and the galvanized iron sheet is coated on angle frame frame body.The drying box Body includes internal layer, outer layer and intermediate guarantor's confluence connector temperature layer.
As shown in figure 22, the oil inlet tap includes shunting general pipeline 12 and several shunt pipes 13, and described several points Stream branch tube side-by-side, which is connected to, to be shunted on general pipeline.Similarly, the confluence connector includes confluence general pipeline and several confluence branch pipes, if described Dry confluence branch tube side-by-side is connected on confluence connector.
In the present embodiment, the drying tray 4 is using discoid body made of galvanized iron sheet, the two sides setting of the discoid body There is pull ring 14.
In the present embodiment, it is provided with thermometer 15 on the drying cabinet, is convenient for the intracorporal baking of real-time monitoring drying box Dry temperature.
Part VII: feed system
As shown in figure 23, the feed system mainly includes dry micro mist bunker workshop (20,21) to be packaged, bucket type transhipment 30 With suspension gear 31.The suspension gear is electric block.Stair 33, the workshop are provided on the side wall of the melt pit 21 The upside of ontology 20 is provided with guardrail 32.
As shown in figure 23 and figure 24, the micro mist fine screening machine feed system includes workshop ontology 20 and melt pit 21, describedly A side-lower of workshop ontology 20 is arranged in hole 21, i.e. 20 side of workshop ontology is hung on above melt pit.And the workshop ontology 20 side is internally provided with aggregate bin 22, and the aggregate bin is configured with bracket 23.The lower end material blanking tube of the aggregate bin 22 24 pass through the floor of workshop ontology 20, and extend one section to melt pit 21, form 24 extension of material blanking tube;The aggregate bin 22 it is upper Side is provided with dust hood 25, and the top of the dust hood 25 is provided with dust suction connecting leg 26, and the dust suction connecting leg 26 is linked into dust suction In general pipeline 27, the upper end of the dust suction general pipeline 27 is provided with the first control valve 28, and the lower end of the dust suction general pipeline 27 extends downwardly To the discharge port side of 24 lower end of material blanking tube, the second control valve 29 is provided on the lower end discharge port of the dust suction general pipeline 27;Institute It states and is placed with bucket type transfer car(buggy) 30 in melt pit.
As shown in Figure 25, Figure 26 and Figure 27, the bucket type transfer car(buggy) 30 includes trolley 1 and charging hopper 2, the charging hopper 2 include cylindrical portions 3, cone bucket part 4 and feed opening 5;The upper end of the cylindrical portions 3 is provided with upper sealing plate 6, the upper sealing plate Feed opening 7 is offered on 6, suspension hook or lifting lug 8 is provided on the outer wall of the cylindrical portions 3, and the cylindrical portions 3 are connected to The upper end of cone bucket part 4;The lower end of the cone bucket part 4 opens up feed opening 5, installs baiting valve 9 on the feed opening 5;It is described Support frame 10 is provided on trolley 1;The charging hopper 2 is erected on support frame 10, the upper support ring of support frame as described above 10 11 is inconsistent with 4 outer wall of cone bucket part of charging hopper 2.
In the present embodiment, the front side portion of the trolley is provided with handspike 1.The front side wheel of the trolley is ten thousand To castor 12.Support frame as described above 10 includes support ring 11 and several upright bars 13, the loading plane of the support ring 11 and trolley 1 In parallel, the support ring 11 is fixed in the loading plane of trolley 1 through several upright bars 13.The baiting valve 9 is to manually control Valve.
Part VIII: production equipment is packed in micro mist fine screen
As shown in figure 28, the micro mist fine screen packaging production equipment mainly includes workshop ontology 20, ultrasonic wave fine screen Device 21 and micro mist sack-filling device (15,16,17).The workshop ontology includes fine screen workshop 22 and packing shop 23, institute It states ultrasonic wave fine screen device 21 to be mounted in fine screen workshop 22, the ultrasonic wave fine screen device 21 is two-stage ultrasonic wave fine screen dress It sets;The micro mist sack-filling device (15,16,17) includes the first, second, and third micro mist sack-filling device;Described first, second is micro- Powder sack-filling device (15,16) is arranged in below the two-stage ultrasonic wave fine screen device discharge port in fine screen workshop, the two-stage ultrasound The terminal discharge mouth of wave fine screen device is extend into packing shop 23, and the third micro mist sack-filling device 17 is arranged in packing shop In 23;And the third micro mist sack-filling device 17 is located at the lower section of the terminal discharge mouth of two-stage ultrasonic wave fine screen device.Described The top of three micro mist sack-filling devices 17 is provided with dust suction air hose 24.
As shown in figure 28, the ultrasonic wave fine screen device 21 is super including feed bin 10, baiting valve 11, feeding passage 12, level-one Acoustic vibration sieve 13 and second level ultrasonic activation sieve 14;The lower end discharge port of the feed bin 10 is equipped with baiting valve 11, under described Expect that the discharge port of valve 11 is connected to the upper end feed inlet of level-one ultrasonic activation sieve 13 through feeding passage 12;The level-one ultrasonic wave Vibrating screen 13 has the outlet of level-one coarse fodder and the outlet of level-one fine fodder, and the lower section of the level-one coarse fodder outlet is provided with the first micro mist dress Packed to set 15, the level-one fine fodder outlet extends to the feed inlet of second level ultrasonic activation sieve 14;The second level ultrasonic activation Sieve 14 has the outlet of second level coarse fodder and the outlet of second level fine fodder, and the lower section of the second level coarse fodder outlet is provided with the second micro mist pack dress 16 are set, second level fine fodder outlet lower section is provided with third micro mist sack-filling device 17.
As shown in figure 28, in the present embodiment, the feed bin is taper feed bin, and the lower part of the taper feed bin is that taper is received Mouthful, vibrating motor 18 is installed on the lateral wall that the taper closes up.
As shown in figure 28, in the present embodiment, dustcloth 19, the dustcloth are installed on the discharge port of the baiting valve Tubular is surrounded, and the lower end of the dustcloth is extend into the upper end feed inlet of level-one ultrasonic activation sieve.The level-one coarse fodder Dustcloth 19 is installed, the dustcloth surrounds tubular, and the lower end of the dustcloth extend into the pack of the first micro mist in outlet In packing bag mouth on device.Dustcloth 19 is installed in the second level coarse fodder outlet, the dustcloth surrounds tubular, and institute The lower end for stating dustcloth is extend into the packing bag mouth on the second micro mist sack-filling device.It is equipped in the second level fine fodder outlet Dustcloth 19, the dustcloth surrounds tubular, and the lower end of the dustcloth extend into the packaging on third micro mist sack-filling device In bag sack.
As shown in Figure 29, Figure 30 and Figure 31, the third micro mist sack-filling device includes two tracks being parallel to each other 1, feet Wheel 2, loading platform 3 and bag bracket 4.Described two tracks 1 being parallel to each other are horizontally installed on the ground below micro mist discharge port On face, the loading platform 3 be mounted on its downside castor 2 carry on track 1, the loading platform 3 it is upper side by side It is provided at least two bag bracket 4.In the present embodiment, there are three bag brackets 4 on loading platform 3.
In the present embodiment, the bag bracket 4 includes upper U-shaped frame 5, intermediate U-shaped frame 6 and several support rods 7, it is described on U-shaped frame 5 and intermediate U-shaped frame 6 are horizontally disposed, and the central axis of upper U-shaped frame 5 and intermediate U-shaped frame 6 is located on same vertical line, Several support rods 7 are uniformly arranged along the circumference of upper U-shaped frame 5, and are successively connected respectively with upper U-shaped frame 5 and intermediate U-shaped frame 6.
In the present embodiment, the track 1 is angle steel track, and the castor 2 is angle guide wheel.The micro mist fine screen packet The side of dress production equipment is additionally provided with weigher 8.The circumference of the weigher 8 is provided with the bracket 9 of semi-surrounding, to prevent from claiming Bag is toppled over when amount.
The above description is only an embodiment of the present invention, is not intended to limit the scope of the invention, all to utilize this hair Equivalent structure or equivalent flow shift made by bright specification and accompanying drawing content is applied directly or indirectly in other relevant skills Art field is included in scope of patent protection of the invention.

Claims (10)

1. a kind of silicon carbide micro-powder purifying and classifying production technology, which is characterized in that sequentially include the following steps:
Step 1: silicon carbide micro-powder raw material being added to automatic washing stirring pool, suitable water is put into, and stir evenly, forms carbon SiClx micro mist suspension;
Step 2: silicon carbide micro-powder suspension being pumped in removal filtration sieve and carries out primary filtration, forms filtrate and filter residue;
Step 3: filtrate being pumped in the clear matter pond of pickling, the concentrated sulfuric acid and suspended oil is added, the dosage of the concentrated sulfuric acid is that silicon carbide is micro- The 1 ~ 4% of powder raw material weight is stood, after impurity is reacted completely and floated up, by the impurity on liquid level surface layer after mixing evenly It pulls out or overflow goes out;After impurity discharge, constantly plus water is washed and dilution, and silicon carbide micro-powder suspension is made to become neutral solution;
Step 4: the silicon carbide micro-powder suspension after pickling being pumped in the clear matter pond of alkali cleaning, piece alkali and suspended oil, piece alkali is added Dosage be silicon carbide micro-powder raw material weight 0.1 ~ 1.5%, after mixing evenly, stand, react and float up completely to impurity Afterwards, the impurity on liquid level surface layer is pulled out or overflow goes out;
Step 5: the silicon carbide micro-powder suspension in the clear matter pond of alkali cleaning being pumped into classification of sedimentation processing pond, suitable dispersion is added Agent carries out classification of sedimentation;
Step 6: after the difference silicon carbide micro-powder suspension after classification is sieved again, being sent into centrigugal swing dryer and dry;
Step 7: the wet silicon carbide micro-powder after drying being fitted into be put into drying unit after drying tray and is dried, dry carbonization is formed Silicon powder;
Step 8: dry silicon carbide micro-powder is weighed through feed system transport micro mist fine screen packaging production equipment, is packed.
2. silicon carbide micro-powder purifying and classifying production technology according to claim 1, it is characterised in that: described in step 1 Automatic washing stirring pool includes pond body, and the two sides pool wall upper end of the pond body is provided with track, and being equipped on the track can edge The vehicle frame that track moves back and forth, vertically-mounted on the vehicle frame to have agitating shaft, the agitating shaft is driven by stirring motor, institute It states and is also equipped with stroke motor on vehicle frame, to drive the idler wheel orbital motion of vehicle frame bottom;The both ends of the track Block is respectively set, the lower part both ends of the vehicle frame are correspondingly arranged on travel switch, and the travel switch is accessed through connecting line In control circuit in electric cabinet, the control circuit is connected through connecting line with stroke motor, to control vehicle frame edge Track automatically moves back and forth.
3. silicon carbide micro-powder purifying and classifying production technology according to claim 1, it is characterised in that: clean in step 2 Filter screen includes feed well, filtering table, receiver and support body, and the feed well is arranged in the upper end of filtering table, it is described into The upper cover of hopper, which may be reversed, opens, and is provided with charging pipe fitting in the middle part of the upper cover, the inner cavity of the feed well is provided with initial filter Sieve, the lower part of the feed well are provided with discharging long slot hole;The filtering table and receiver are inclined on support body, and Filtering table is located at the top of receiver, and the bottom plate of the filtering table is smart filter screen, and the circumference of the filtering table is provided with splashproof Shading cloth, the lower end of the splashproof shading cloth extend on the inside of the peripheral wall of receiver;Lower the one of the filtering table and receiver Discharging pipe fitting is respectively arranged on end.
4. silicon carbide micro-powder purifying and classifying production technology according to claim 1, it is characterised in that: described in step 3 The clear matter pond of pickling includes rectangle pond body, and the two sidewalls upper end of the rectangle pond body is respectively arranged with track, is installed on the track Having vertically-mounted on the vehicle frame of track reciprocating motion, the vehicle frame can have agitating shaft, and the lower end of the agitating shaft extends To on the upside of the bottom of pond of rectangle pond body, to stir the intracorporal micro mist suspension of rectangle form pool;One end of the rectangle pond body is water inlet End, the Sidewall Height of water inlet end are higher;The rectangle pool bottom of water inlet end is provided with lower water inlet, in the rectangle form pool of water inlet end Upper water inlet, the other end of the upper water inlet towards rectangle pond body are equipped in the middle part of body;The other end of the rectangle pond body is excessive End is flowed, the Sidewall Height of effluent head is shorter, and when water level goes up, the impurity swum on the water surface is flowed out from effluent head;In overflow Several absolute altitudes different drainage hole is set on the rectangle form pool body sidewall at end, and blocking on the drainage hole has stopple, the stopple It is removable.
5. silicon carbide micro-powder purifying and classifying production technology according to claim 1, it is characterised in that: described in step 4 The clear matter pond of alkali cleaning includes pond body and the bracket that is erected above pond body, and the periphery of the pond body is surrounded with heat-conducting oil pipes and heat preservation Layer, the pond body intracavity bottom are additionally provided with aeration tube, to carry out bubbling -cleaning to the intracorporal micro mist suspension in pond;The branch Vertically-mounted on frame to have agitating shaft, the lower end of the agitating shaft extends on the upside of the bottom of pond body, so that stirring pool is intracorporal micro- Powder suspension;The bottom of the pond body is provided with discharge valve and feeder pipe.
6. silicon carbide micro-powder purifying and classifying production technology according to claim 1, it is characterised in that: described in steps of 5 Classification of sedimentation processing pond includes settling tank and grading pool, and the side of settling tank is arranged in the grading pool, and the settling tank is higher than Grading pool, and several classification drainage holes, the classification drain are provided on the side wall that settling tank is higher by grading pool upper surface Blocking on hole has stopple, and the stopple is removable;The outer side wall of several classification drainage holes is equipped with collecting tank, the collecting tank Bottom be circumscribed with movable isocon, the activity isocon leads to grading pool;On the pond body side wall of the settling tank from upper and Multiple detection mouths are arranged with, the detection mouth is the outlet pipe with shut-off valve, to be detected before being classified drain.
7. silicon carbide micro-powder purifying and classifying production technology according to claim 1, it is characterised in that: described in step 7 Drying unit includes drying cabinet, and the front side of drying box is arranged in the chamber door of the drying cabinet, and the chamber door is detachable;It is described Drying cabinets cavity is provided with drying layer frame, the drying layer frame be by several petroleum pipelines side by side from bottom to top S type layer around And formed, drying tray is placed in the drying layer frame;Described several petroleum pipeline oil inlet ends side by side be commonly connected into Oily tap, the oil inlet tap connects fuel feeding general pipeline, and oil inlet control valve is provided on fuel feeding general pipeline;It is described several The end of the petroleum pipeline of item side by side is commonly connected to confluence connector, and the confluence connector connects return header.
8. silicon carbide micro-powder purifying and classifying production technology according to claim 1, it is characterised in that: described in step 8 Feed system includes dry micro mist bunker workshop, bucket type transfer car(buggy) and suspension gear to be packaged, the dry micro mist bunker vehicle to be packaged Between include workshop ontology and melt pit, workshop ontology side is hung on above melt pit, and inside the side of the workshop ontology It is provided with aggregate bin, the lower end material blanking tube of the aggregate bin passes through the floor of workshop ontology, and extends one section to melt pit, and formation is fallen Expects pipe extension;It is provided with dust hood above the aggregate bin, dust suction connecting leg, the suction are provided at the top of the dust hood Dirt connecting leg is linked into dust suction general pipeline, and the upper end of the dust suction general pipeline is provided with the first control valve, the lower end of the dust suction general pipeline The discharge port side of material blanking tube lower end is extended downwardly into, is provided with the second control valve on the lower end discharge port of the dust suction general pipeline; Bucket type transfer car(buggy) is placed in the melt pit;The top of melt pit, and the highest of the suspension gear is arranged in the suspension gear Suspention height is higher by the height of at least one bucket type transfer car(buggy) of frame body.
9. silicon carbide micro-powder purifying and classifying production technology according to claim 1, it is characterised in that: micro mist in step 8 It includes workshop ontology, ultrasonic wave fine screen device and micro mist sack-filling device, the workshop sheet that production equipment is packed in fine screen Body includes fine screen workshop and packing shop, and the ultrasonic wave fine screen device is mounted in fine screen workshop, the ultrasonic wave fine screen dress It is set to two-stage ultrasonic wave fine screen device;The micro mist sack-filling device includes the first, second, and third micro mist sack-filling device;Described One, the second micro mist sack-filling device is arranged in below the two-stage ultrasonic wave fine screen device discharge port in fine screen workshop, and the two-stage is super The terminal discharge mouth of sound wave fine screen device is extend into packing shop, and the third micro mist sack-filling device is arranged in packing shop In;And the third micro mist sack-filling device is located at the lower section of the terminal discharge mouth of two-stage ultrasonic wave fine screen device.
10. a kind of silicon carbide micro-powder such as the described in any item silicon carbide micro-powder purifying and classifying production technologies of claim 2-9 mentions The production equipment of pure classification, it is characterised in that: the production equipment includes the automatic washing stirring pool set gradually, removal filtration Sieve, the clear matter pond of pickling, the clear matter pond of alkali cleaning, classification of sedimentation processing pond, drying unit, feed system and micro mist fine screen packaging production are set It is standby.
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