CN106393341A - Elm softening processing method - Google Patents
Elm softening processing method Download PDFInfo
- Publication number
- CN106393341A CN106393341A CN201610846201.2A CN201610846201A CN106393341A CN 106393341 A CN106393341 A CN 106393341A CN 201610846201 A CN201610846201 A CN 201610846201A CN 106393341 A CN106393341 A CN 106393341A
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- Prior art keywords
- elm
- temperature
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- processing
- treatment method
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Classifications
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- B—PERFORMING OPERATIONS; TRANSPORTING
- B27—WORKING OR PRESERVING WOOD OR SIMILAR MATERIAL; NAILING OR STAPLING MACHINES IN GENERAL
- B27K—PROCESSES, APPARATUS OR SELECTION OF SUBSTANCES FOR IMPREGNATING, STAINING, DYEING, BLEACHING OF WOOD OR SIMILAR MATERIALS, OR TREATING OF WOOD OR SIMILAR MATERIALS WITH PERMEANT LIQUIDS, NOT OTHERWISE PROVIDED FOR; CHEMICAL OR PHYSICAL TREATMENT OF CORK, CANE, REED, STRAW OR SIMILAR MATERIALS
- B27K3/00—Impregnating wood, e.g. impregnation pretreatment, for example puncturing; Wood impregnation aids not directly involved in the impregnation process
- B27K3/02—Processes; Apparatus
- B27K3/0207—Pretreatment of wood before impregnation
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B27—WORKING OR PRESERVING WOOD OR SIMILAR MATERIAL; NAILING OR STAPLING MACHINES IN GENERAL
- B27K—PROCESSES, APPARATUS OR SELECTION OF SUBSTANCES FOR IMPREGNATING, STAINING, DYEING, BLEACHING OF WOOD OR SIMILAR MATERIALS, OR TREATING OF WOOD OR SIMILAR MATERIALS WITH PERMEANT LIQUIDS, NOT OTHERWISE PROVIDED FOR; CHEMICAL OR PHYSICAL TREATMENT OF CORK, CANE, REED, STRAW OR SIMILAR MATERIALS
- B27K3/00—Impregnating wood, e.g. impregnation pretreatment, for example puncturing; Wood impregnation aids not directly involved in the impregnation process
- B27K3/16—Inorganic impregnating agents
- B27K3/163—Compounds of boron
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B27—WORKING OR PRESERVING WOOD OR SIMILAR MATERIAL; NAILING OR STAPLING MACHINES IN GENERAL
- B27K—PROCESSES, APPARATUS OR SELECTION OF SUBSTANCES FOR IMPREGNATING, STAINING, DYEING, BLEACHING OF WOOD OR SIMILAR MATERIALS, OR TREATING OF WOOD OR SIMILAR MATERIALS WITH PERMEANT LIQUIDS, NOT OTHERWISE PROVIDED FOR; CHEMICAL OR PHYSICAL TREATMENT OF CORK, CANE, REED, STRAW OR SIMILAR MATERIALS
- B27K3/00—Impregnating wood, e.g. impregnation pretreatment, for example puncturing; Wood impregnation aids not directly involved in the impregnation process
- B27K3/16—Inorganic impregnating agents
- B27K3/20—Compounds of alkali metals or ammonium
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B27—WORKING OR PRESERVING WOOD OR SIMILAR MATERIAL; NAILING OR STAPLING MACHINES IN GENERAL
- B27K—PROCESSES, APPARATUS OR SELECTION OF SUBSTANCES FOR IMPREGNATING, STAINING, DYEING, BLEACHING OF WOOD OR SIMILAR MATERIALS, OR TREATING OF WOOD OR SIMILAR MATERIALS WITH PERMEANT LIQUIDS, NOT OTHERWISE PROVIDED FOR; CHEMICAL OR PHYSICAL TREATMENT OF CORK, CANE, REED, STRAW OR SIMILAR MATERIALS
- B27K3/00—Impregnating wood, e.g. impregnation pretreatment, for example puncturing; Wood impregnation aids not directly involved in the impregnation process
- B27K3/34—Organic impregnating agents
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B27—WORKING OR PRESERVING WOOD OR SIMILAR MATERIAL; NAILING OR STAPLING MACHINES IN GENERAL
- B27K—PROCESSES, APPARATUS OR SELECTION OF SUBSTANCES FOR IMPREGNATING, STAINING, DYEING, BLEACHING OF WOOD OR SIMILAR MATERIALS, OR TREATING OF WOOD OR SIMILAR MATERIALS WITH PERMEANT LIQUIDS, NOT OTHERWISE PROVIDED FOR; CHEMICAL OR PHYSICAL TREATMENT OF CORK, CANE, REED, STRAW OR SIMILAR MATERIALS
- B27K5/00—Treating of wood not provided for in groups B27K1/00, B27K3/00
- B27K5/003—Treating of wood not provided for in groups B27K1/00, B27K3/00 by using electromagnetic radiation or mechanical waves
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- Life Sciences & Earth Sciences (AREA)
- Engineering & Computer Science (AREA)
- Wood Science & Technology (AREA)
- Forests & Forestry (AREA)
- Chemical & Material Sciences (AREA)
- Inorganic Chemistry (AREA)
- Physics & Mathematics (AREA)
- Electromagnetism (AREA)
- Mechanical Engineering (AREA)
- Paper (AREA)
Abstract
The invention discloses an elm softening processing method, comprising the following steps: salty water soaking processing, balancing in an environment with an air relative humidity being 80% and a temperature being 40 DEG C, soaking in absolute ethyl alcohol, fumigating by adopting a boric acid solution, fumigating by adopting a saturated ammonium hydroxide solution, and processing under conditions of 55 DEG C and a relative humidity being 40%. According to the softening processing method, elm can obtain a better softening effect, processing time is less, safety is high, the softened elm has prominent plasticity and processing stability, use performance of the elm is effectively ensured, a strength of a molded elm workpiece is improved by more than 56% on average, the elm softened by the method can obtain a smaller bending radius of curvature, after processing by the method of the invention, hydrophobicity, anti-corrosive property and size stability of the elm can be improved greatly, and the method can be used for improving the humidity resistance and reducing their moisture absorption deformation rate.
Description
Technical field
The present invention relates to treating of wood field, more particularly to a kind of elm sofening treatment method.
Background technology
Elm is a kind of important furniture and handicraft raw material, and elm is a kind of material lacking plasticity, and elm is in processing
Generally require during for product first to carry out a series of sofening treatment, improve its plasticity, so that the machine-shaping with the later stage.Generally adopt
With sofening treatment method be that water boils, sprays the physical methods such as steaming or carry out sofening treatment with chemical liquids such as liquefied ammonia, liquid caustic soda, tradition
The problem of elm fiber generally existing intensity decreases crossed of disposal methods, and the time that softens is long, and resource loss is many.
Content of the invention
Above-mentioned in order to overcome the shortcomings of, the invention provides a kind of elm sofening treatment method.
The present invention is achieved through the following technical solutions:
A kind of elm sofening treatment method, comprises the following steps:
(1), that elm surface clean is clean, be then placed on relative air humidity to be 75%, temperature be reach in 38 DEG C of environment flat
After weighing apparatus, take out;Can the distance between adding molecular chain, be that subsequent processing steps are layed foundation such that it is able to lift elm further
The effect that wood softens;
(2), the elm that step (1) is processed is carried out surface uniform irradiation 15min using the ultraviolet that intensity is 4000 μ W/cm;
(3), after, the elm processing step (2) is put into and soaked 5 minutes in glycerine, take out immediately;
(4) mass concentration, adding container volume 1/3rd in closed container is 63% BAS, then by step
(3) elm handled well is placed on above boric acid, and BAS is heated, and heating-up temperature is less than 92 DEG C, after 15 minutes, stops
Only heat, after 3-3.5 hour, closed container is lowered the temperature, cooling minimum temperature is not less than 12 DEG C, takes out elm;By this
Process, a part of hemicellulose easily decomposes and is dissolved into liquid, the free hydroxyl group adsorption moisture on cellulose unformed area strand,
Moisture film in cellulose gap is thickened, intermolecular distance increases, attraction reduces, be easy to produce under external force relatively sliding
Move such that it is able to improve elm bating effect;
(5) in closed container, add the saturation ammoniacal liquor of container volume 1/3rd, the elm then step (4) handled well
It is placed on saturated ammonia side waterborne, saturation ammoniacal liquor is heated, heating-up temperature is less than 96 DEG C, after 25 minutes, stop heating, 4-6
After hour, closed container is lowered the temperature, cooling minimum temperature is not less than 16 DEG C, takes out elm;
(6), the elm that step (5) is handled well is processed 2 hours under the conditions of 50 DEG C, relative air humidity 45%, air-dry to containing
The water yield is 48-50%, by this step process, it is possible to increase elm soften stability, and can make shape after
Elm intensity is improved.
Further, the sodium chloride solution that in described step (1), salt solution is 0.18% for mass concentration.
Further, in described step (4), elm and BAS distance are not less than 18 centimetres.
Further, in described step (5), elm and saturation ammonia spirit distance are not less than 14 centimetres.
The invention has the beneficial effects as follows:Sofening treatment method of the present invention, can make elm obtain preferable bating effect, place
The reason time is few, and safe, and the elm plasticity after sofening treatment and processing stability project, and effectively ensure that elm
Serviceability, the elm workpiece strength after sizing averagely improves 56%, and structure is compacted, and solves common wood softening method band
The intensity decreases problem come and soak only with ammoniacal liquor and soften the time longer problem spending so that through present invention softening side
Elm after method process, the intensity after dryness finalization is high, good toughness, and structure is compacted, and is conducive to the Quality advance of bool, bending
When percent defective reduce 80% compared to common softening method, the elm after sofening treatment of the present invention can obtain less
Bending curvature radius, after the inventive method is processed, can be greatly enhanced hydrophobicity, anti-corrosive properties and the dimensionally stable of elm
Property, it is simultaneously available for strengthening humidity resistance, reduce their moisture absorption and deformation rate.
Specific embodiment
A kind of elm sofening treatment method, comprises the following steps:
(1), that elm surface clean is clean, be then placed on relative air humidity to be 75%, temperature be reach in 38 DEG C of environment flat
After weighing apparatus, take out;
(2), the elm that step (1) is processed is carried out surface uniform irradiation 15min using the ultraviolet that intensity is 4000 μ W/cm;
(3), after, the elm processing step (2) is put into and soaked 5 minutes in glycerine, take out immediately;
(4) mass concentration, adding container volume 1/3rd in closed container is 63% BAS, then by step
(3) elm handled well is placed on above boric acid, and BAS is heated, and heating-up temperature is less than 92 DEG C, after 15 minutes, stops
Only heat, after 3-3.5 hour, closed container is lowered the temperature, cooling minimum temperature is not less than 12 DEG C, takes out elm;
(5) in closed container, add the saturation ammoniacal liquor of container volume 1/3rd, the elm then step (4) handled well
It is placed on saturated ammonia side waterborne, saturation ammoniacal liquor is heated, heating-up temperature is less than 96 DEG C, after 25 minutes, stop heating, 4-6
After hour, closed container is lowered the temperature, cooling minimum temperature is not less than 16 DEG C, takes out elm;
(6), the elm that step (5) is handled well is processed 2 hours under the conditions of 50 DEG C, relative air humidity 45%, air-dry to containing
The water yield is 48-50%.
The sodium chloride solution that in step (1), salt solution is 0.18% for mass concentration.
In step (4), elm and BAS distance are not less than 18 centimetres.
In step (5), elm and saturation ammonia spirit distance are not less than 14 centimetres.
Elm workpiece using 1mm thickness carries out performance test(With the contrast of untreated elm workpiece):
Intensity improves % | Density improves % | 24h water absorption rate reduces % | Shrinkage factor % | Minimum profile curvature radius | |
The present invention | 56 | 14.2 | 46.3 | 1.4 | 4.05 |
Comparative example 1 | 51 | 13.3 | 42.6 | 1.8 | 4.09 |
Comparative example 2 | 41 | 8.6 | 22.6 | 4.7 | 4.17 |
Comparative example 3 | 43 | 10.3 | 36.3 | 2.1 | 4.19 |
Table 1
Wherein, comparative example 1 is:Omit step in the present invention(1)Process, other process steps are constant;
Comparative example 2 is:Omit step in the present invention(4)Process, other process steps are constant;
Comparative example 3 is:Omit step in the present invention(5)Process, other process steps are constant;
As can be seen from Table 1, the elm workpiece superior performance after present invention process, bating effect is good, the workpiece after softening
Good stability of the dimension;Omit step of the present invention(4)Afterwards, the elm workpiece performance after softening substantially reduces, and bating effect is also obvious
Reduce, omit step of the present invention(1)Afterwards, the elm workpiece after softening, various aspects of performance has and to a certain degree reduces, and omits this
Bright step(5)Afterwards, the elm strength enhancing effect of process and water-fast have to a certain degree decline, bating effect bating effect is obvious
Decline.
Claims (4)
1. a kind of elm sofening treatment method is it is characterised in that comprise the following steps:
(1), that elm surface clean is clean, be then placed on relative air humidity to be 75%, temperature be reach in 38 DEG C of environment flat
After weighing apparatus, take out;
(2), the elm that step (1) is processed is carried out surface uniform irradiation 15min using the ultraviolet that intensity is 4000 μ W/cm;
(3), after, the elm processing step (2) is put into and soaked 5 minutes in glycerine, take out immediately;
(4) mass concentration, adding container volume 1/3rd in closed container is 63% BAS, then by step
(3) elm handled well is placed on above boric acid, and BAS is heated, and heating-up temperature is less than 92 DEG C, after 15 minutes, stops
Only heat, after 3-3.5 hour, closed container is lowered the temperature, cooling minimum temperature is not less than 12 DEG C, takes out elm;
(5) in closed container, add the saturation ammoniacal liquor of container volume 1/3rd, the elm then step (4) handled well
It is placed on saturated ammonia side waterborne, saturation ammoniacal liquor is heated, heating-up temperature is less than 96 DEG C, after 25 minutes, stop heating, 4-6
After hour, closed container is lowered the temperature, cooling minimum temperature is not less than 16 DEG C, takes out elm;
(6), the elm that step (5) is handled well is processed 2 hours under the conditions of 50 DEG C, relative air humidity 45%, air-dry to containing
The water yield is 48-50%.
2. a kind of elm sofening treatment method according to claim 1 it is characterised in that in described step (1) salt solution be
Mass concentration is 0.18% sodium chloride solution.
3. a kind of elm sofening treatment method according to claim 1 it is characterised in that in described step (4) elm with
BAS distance is not less than 18 centimetres.
4. a kind of elm sofening treatment method according to claim 1 it is characterised in that in described step (5) elm with
Saturation ammonia spirit distance is not less than 14 centimetres.
Priority Applications (1)
Application Number | Priority Date | Filing Date | Title |
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CN201610846201.2A CN106393341A (en) | 2016-09-23 | 2016-09-23 | Elm softening processing method |
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CN201610846201.2A CN106393341A (en) | 2016-09-23 | 2016-09-23 | Elm softening processing method |
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CN106393341A true CN106393341A (en) | 2017-02-15 |
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CN201610846201.2A Pending CN106393341A (en) | 2016-09-23 | 2016-09-23 | Elm softening processing method |
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Cited By (2)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN107443517A (en) * | 2017-07-28 | 2017-12-08 | 阜南县金威工艺品有限公司 | A kind of drying means for preventing elm from ftractureing |
CN109551593A (en) * | 2018-11-15 | 2019-04-02 | 江苏大学 | A kind of preparation method of application type wood skin bating liquor |
Citations (6)
Publication number | Priority date | Publication date | Assignee | Title |
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CN102303332A (en) * | 2011-09-14 | 2012-01-04 | 山东省纤维检验局 | Wood softener, and preparation method and application thereof |
CN104397071A (en) * | 2014-11-07 | 2015-03-11 | 安徽洪福工艺品有限公司 | Sterilizing processing liquid for processing rattans |
CN104441157A (en) * | 2014-11-07 | 2015-03-25 | 安徽洪福工艺品有限公司 | Softening steam for treating wicker |
CN104942944A (en) * | 2015-06-09 | 2015-09-30 | 安徽省阜南志峰工艺品有限公司 | Toon tree wood antiquing treatment agent |
CN105382895A (en) * | 2015-10-21 | 2016-03-09 | 苏州东邦家具有限公司 | Preparing method of modified composite wood for furniture manufacturing |
CN105599082A (en) * | 2015-12-24 | 2016-05-25 | 安吉汉洲生物科技有限公司 | Multifunctional preservative |
-
2016
- 2016-09-23 CN CN201610846201.2A patent/CN106393341A/en active Pending
Patent Citations (6)
Publication number | Priority date | Publication date | Assignee | Title |
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CN102303332A (en) * | 2011-09-14 | 2012-01-04 | 山东省纤维检验局 | Wood softener, and preparation method and application thereof |
CN104397071A (en) * | 2014-11-07 | 2015-03-11 | 安徽洪福工艺品有限公司 | Sterilizing processing liquid for processing rattans |
CN104441157A (en) * | 2014-11-07 | 2015-03-25 | 安徽洪福工艺品有限公司 | Softening steam for treating wicker |
CN104942944A (en) * | 2015-06-09 | 2015-09-30 | 安徽省阜南志峰工艺品有限公司 | Toon tree wood antiquing treatment agent |
CN105382895A (en) * | 2015-10-21 | 2016-03-09 | 苏州东邦家具有限公司 | Preparing method of modified composite wood for furniture manufacturing |
CN105599082A (en) * | 2015-12-24 | 2016-05-25 | 安吉汉洲生物科技有限公司 | Multifunctional preservative |
Cited By (3)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN107443517A (en) * | 2017-07-28 | 2017-12-08 | 阜南县金威工艺品有限公司 | A kind of drying means for preventing elm from ftractureing |
CN109551593A (en) * | 2018-11-15 | 2019-04-02 | 江苏大学 | A kind of preparation method of application type wood skin bating liquor |
CN109551593B (en) * | 2018-11-15 | 2020-06-26 | 江苏大学 | Preparation method of coating type veneer softening liquid |
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Application publication date: 20170215 |