CN106390499A - Distillation device uniformly receiving heat to prevent bumping - Google Patents
Distillation device uniformly receiving heat to prevent bumping Download PDFInfo
- Publication number
- CN106390499A CN106390499A CN201611038636.0A CN201611038636A CN106390499A CN 106390499 A CN106390499 A CN 106390499A CN 201611038636 A CN201611038636 A CN 201611038636A CN 106390499 A CN106390499 A CN 106390499A
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- CN
- China
- Prior art keywords
- zeolite
- condensing tube
- asbestos
- inner chamber
- distillation
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- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
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- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01D—SEPARATION
- B01D3/00—Distillation or related exchange processes in which liquids are contacted with gaseous media, e.g. stripping
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- Chemical & Material Sciences (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Vaporization, Distillation, Condensation, Sublimation, And Cold Traps (AREA)
Abstract
The invention discloses a distillation device uniformly receiving heat to prevent bumping. The distillation device comprises a bottle neck, a bottle body, a branched pipe passage, a first rubber plug, a thermometer, a first inner cavity, a second inner cavity, asbestos, zeolite, a condensing pipe, a second rubber plug, a third rubber plug, a water inlet, a water outlet, a tail connecting pipe, an air collection bottle and a screen net, the bottle body is divided into the first inner cavity and the outer cavity by the screen net, zeolite is placed in the second inner cavity, and asbestos is arranged on the outer side of the bottom of the bottle body. Water in zeolite when at high temperature is discharged; when being burnt by flame, most zeolite expands and foams like boiling; due to porous silicate property of zeolite, a certain amount of air is stored in small pores, and bumping is prevented; zeolite does not need to be added into a distillation flask in each experiment, so that damage to the distillation flask caused when zeolite is put into is reduced, and experiment safety is improved; asbestos is arranged on the outer side of the bottom of the bottle body, so that the distillation device is heated uniformly, and distillation effect of the distillation device is improved.
Description
Technical field
The present invention relates to a kind of distilling apparatus are and in particular to a kind of thermally equivalent is in case the distilling apparatus of bumping, belonging to
Learn technical field.
Background technology
Distillation is a kind of thermodynamic (al) separating technology, and it utilizes each component boiling point in mixing liquid or liquid-solid system different,
So that low boiling component is evaporated, then condense to separate the unit process of whole component, be evaporation and two kinds of unit operations of condensation
Joint.With other separation means, such as extraction, filtering for crystallizing etc. compare, its advantage be not require the use of system components with
Outer other solvents, thus ensure to introduce new impurity.But the distilling apparatus commonly used at present are uneven due to being heated, and lead
Cause distilling effect poor, put into zeolite simultaneously and easily injure distilling flask by a crashing object, the safety of experiment reduces.
Content of the invention
The technical problem to be solved in the present invention overcomes existing distilling apparatus bottom to be heated uneven and and be also easy to produce bumping
Defect, provides a kind of thermally equivalent in case the distilling apparatus of bumping.
In order to solve above-mentioned technical problem, the invention provides following technical scheme：
The invention provides a kind of thermally equivalent, in case the distilling apparatus of bumping, including bottleneck, body, is in charge of passage, the first rubber
Leather plug, thermometer, first inner chamber, second inner chamber, asbestos, zeolite, condensing tube, the second rubber closure, the 3rd rubber closure, water inlet,
Outlet, tail adapter, gas collecting bottle and screen cloth, the top open part of described bottleneck is provided with described first rubber closure, described first rubber
Described thermometer is inserted with leather plug, the side on described bottleneck top be provided with described in be in charge of passage, described one end being in charge of passage
It is provided with described condensing tube, the top of described condensing tube is provided with described outlet, and the bottom of described condensing tube is provided with described water inlet,
One end of described condensing tube is provided with described tail adapter, and one end of described tail adapter is placed in the inside of described gas collecting bottle, described bottleneck
Bottom is communicated with described body, and described body has described first inner chamber and a described second inner chamber by the segmentation of described screen cloth, and described the
In two, intracavity is placed with described zeolite, and the outside of described body bottom is provided with described asbestos.
As a preferred technical solution of the present invention, described passage of being in charge of passes through described second rubber with described condensing tube
Plug connects, and described condensing tube is connected by described 3rd rubber closure with the adapter of described tail.
The beneficial effect that the present invention is reached is：This device body has first inner chamber and second inner chamber by screen cloth segmentation, the
In two, intracavity is placed with zeolite, and zeolite moisture when running into high temperature can eject, and when such as going to burn with flame, most of zeolites will
Expanded foamed, seem that boiling is general, due to the porous silicate property of zeolite, have a certain amount of air in aperture, prevent
Bumping, it is not necessary to each experiment all needs to add zeolite toward in distilling flask, reduces the damage it being produced when putting into zeolite, with
When increased the safety of experiment, the outside of body bottom is provided with asbestos, can make its thermally equivalent, improves the effect of its distillation,
And structure is simply it is easy to use.
Brief description
Accompanying drawing is used for providing a further understanding of the present invention, and constitutes a part for description, the reality with the present invention
Apply example and be used for explaining the present invention together, be not construed as limiting the invention.In the accompanying drawings：
Fig. 1 is the structural representation of the present invention；
In figure:1st, bottleneck；2nd, body；3rd, it is in charge of passage；4th, the first rubber closure；5th, thermometer；6th, first inner chamber；7th, in second
Chamber；8th, asbestos；9th, zeolite；10th, condensing tube；11st, the second rubber closure；12nd, the 3rd rubber closure；13rd, water inlet；14th, outlet；
15th, tail adapter；16th, gas collecting bottle；17th, screen cloth.
Specific embodiment
Below in conjunction with accompanying drawing, the preferred embodiments of the present invention are illustrated it will be appreciated that preferred reality described herein
Apply example to be merely to illustrate and explain the present invention, be not intended to limit the present invention.
Embodiment 1
As shown in figure 1, the invention provides a kind of thermally equivalent, in case the distilling apparatus of bumping, including bottleneck 1, body 2, is in charge of
Passage 3, the first rubber closure 4, thermometer 5, first inner chamber 6, second inner chamber 7, asbestos 8, zeolite 9, condensing tube 10, the second rubber closure
11st, the 3rd rubber closure 12, water inlet 13, outlet 14, tail adapter 15, gas collecting bottle 16 and screen cloth 17, the top open part of bottleneck 1
It is provided with the first rubber closure 4, the first rubber closure 4 is inserted with thermometer 5, the side on bottleneck 1 top is provided with is in charge of passage 3, is in charge of
One end of passage 3 is provided with condensing tube 10, and the top of condensing tube 10 is provided with outlet 14, and the bottom of condensing tube 10 is provided with water inlet
13, one end of condensing tube 10 is provided with tail adapter 15, and one end of tail adapter 15 is placed in the inside of gas collecting bottle 16, and bottleneck 1 bottom connects
There is body 2, body 2 has first inner chamber 6 and second inner chamber 7 by screen cloth 17 segmentation, is placed with zeolite 9, body 2 bottom in second inner chamber 7
The outside in portion is provided with asbestos 8.
It is in charge of passage 3 to be connected by the second rubber closure 11 with condensing tube 10, condensing tube 10 passes through the 3rd rubber with tail adapter 15
Leather plug 12 connects.
Concrete principle：The mass transport process by Component seperation using the volatile difference of component each in liquid mixture.Will
The steam that liquid boiling produces imports condensing tube 10, is allowed to cool down a kind of evaporation, the process of condensation condensing into liquid.Body 2
First inner chamber 6 and second inner chamber 7 are had by screen cloth 17 segmentation, in second inner chamber 7, is placed with zeolite 9, zeolite 9 moisture when running into high temperature
Can eject, when such as going to burn with flame, most of zeolites will be expanded foamed, seem that boiling is general.Many due to zeolite 10
Permeability silicate property, has a certain amount of air in aperture, for anti-bumping.It is provided with stone in the outside of body 2 bottom simultaneously
Cotton 8, when being heated, enables to more uniform to the liquid heating in distilling flask and amount of liquid is less than the 2/ of volume
3, no less than the 1/3 of volume.
This device adds zeolite 9, prevents bumping it is not necessary to each experiment all needs to add zeolite 9 toward in distilling flask, reduces
Damage distilling flask being produced when putting into zeolite 9, increased the safety of experiment, the outside of body 2 bottom is provided with simultaneously
Asbestos 8, can make its thermally equivalent, improve the effect of its distillation, and structure is simply it is easy to use.
Finally it should be noted that：The foregoing is only the preferred embodiments of the present invention, be not limited to the present invention,
Although being described in detail to the present invention with reference to the foregoing embodiments, for a person skilled in the art, it still may be used
To modify to the technical scheme described in foregoing embodiments, or equivalent is carried out to wherein some technical characteristics.
All any modification, equivalent substitution and improvement within the spirit and principles in the present invention, made etc., should be included in the present invention's
Within protection domain.
Claims (2)
1. a kind of thermally equivalent is in case the distilling apparatus of bumping, including bottleneck（1）, body（2）, be in charge of passage（3）, the first rubber
Plug（4）, thermometer（5）, first inner chamber（6）, second inner chamber（7）, asbestos（8）, zeolite（9）, condensing tube（10）, the second rubber closure
（11）, the 3rd rubber closure（12）, water inlet（13）, outlet（14）, tail adapter（15）, gas collecting bottle（16）And screen cloth（17）, its
It is characterised by, described bottleneck（1）Top open part be provided with described first rubber closure（4）, described first rubber closure（4）Upper insertion
There is described thermometer（5）, described bottleneck（1）Passage is in charge of described in being provided with the side on top（3）, described it is in charge of passage（3）One
End is provided with described condensing tube（10）, described condensing tube（10）Top be provided with described outlet（14）, described condensing tube（10）'s
Bottom is provided with described water inlet（13）, described condensing tube（10）One end be provided with the adapter of described tail（15）, described tail adapter（15）
One end be placed in described gas collecting bottle（16）Inside, described bottleneck（1）Bottom is communicated with described body（2）, described body（2）By
Described screen cloth（17）Segmentation has described first inner chamber（6）With described second inner chamber（7）, described second inner chamber（7）Inside it is placed with described
Zeolite（9）, described body（2）The outside of bottom is provided with described asbestos（8）.
2. a kind of thermally equivalent according to claim 1 in case bumping distilling apparatus it is characterised in that described be in charge of logical
Road（3）With described condensing tube（10）By described second rubber closure（11）Connect, described condensing tube（10）With the adapter of described tail
（15）By described 3rd rubber closure（12）Connect.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201611038636.0A CN106390499A (en) | 2016-11-23 | 2016-11-23 | Distillation device uniformly receiving heat to prevent bumping |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201611038636.0A CN106390499A (en) | 2016-11-23 | 2016-11-23 | Distillation device uniformly receiving heat to prevent bumping |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| CN106390499A true CN106390499A (en) | 2017-02-15 |
Family
ID=58082292
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN201611038636.0A Pending CN106390499A (en) | 2016-11-23 | 2016-11-23 | Distillation device uniformly receiving heat to prevent bumping |
Country Status (1)
| Country | Link |
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| CN (1) | CN106390499A (en) |
Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN108014856A (en) * | 2017-12-20 | 2018-05-11 | 四会市华通金属筛网制品有限公司 | Asbestos gauge |
Citations (5)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| KR20100010279U (en) * | 2009-04-10 | 2010-10-20 | 주식회사 제이오텍 | Cover for flask |
| CN202700535U (en) * | 2012-07-16 | 2013-01-30 | 济南大学 | Simple distillation device |
| CN203724796U (en) * | 2014-03-11 | 2014-07-23 | 潍坊科技学院 | Novel reduced pressure distillation device |
| CN203916128U (en) * | 2014-06-25 | 2014-11-05 | 傅瑶婷 | A kind of steam distillation device |
| CN204275533U (en) * | 2014-12-09 | 2015-04-22 | 上海杏灵科技药业股份有限公司 | A kind of anti-evaporimeter that boils |
-
2016
- 2016-11-23 CN CN201611038636.0A patent/CN106390499A/en active Pending
Patent Citations (5)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| KR20100010279U (en) * | 2009-04-10 | 2010-10-20 | 주식회사 제이오텍 | Cover for flask |
| CN202700535U (en) * | 2012-07-16 | 2013-01-30 | 济南大学 | Simple distillation device |
| CN203724796U (en) * | 2014-03-11 | 2014-07-23 | 潍坊科技学院 | Novel reduced pressure distillation device |
| CN203916128U (en) * | 2014-06-25 | 2014-11-05 | 傅瑶婷 | A kind of steam distillation device |
| CN204275533U (en) * | 2014-12-09 | 2015-04-22 | 上海杏灵科技药业股份有限公司 | A kind of anti-evaporimeter that boils |
Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN108014856A (en) * | 2017-12-20 | 2018-05-11 | 四会市华通金属筛网制品有限公司 | Asbestos gauge |
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| C06 | Publication | ||
| PB01 | Publication | ||
| C10 | Entry into substantive examination | ||
| SE01 | Entry into force of request for substantive examination | ||
| TA01 | Transfer of patent application right | ||
| TA01 | Transfer of patent application right |
Effective date of registration: 20180830 Address after: 102600 3 floor, 2 building, No. 4 Daxing District Garden Road, Beijing, 1 unit 317 Applicant after: Beijing informed investment home intellectual property rights Operation Co., Ltd. Address before: 230000 Room 408, 40 Chuncheng Building, South Lake, East of Yandun Road and South of Xuanyuan Road, Hefei Economic and Technological Development Zone, Anhui Province Applicant before: Hefei he Education Technology Co., Ltd. |
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| RJ01 | Rejection of invention patent application after publication | ||
| RJ01 | Rejection of invention patent application after publication |
Application publication date: 20170215 |