CN106380928A - Printing ink with negative ion generation actions and manufacturing technique thereof - Google Patents
Printing ink with negative ion generation actions and manufacturing technique thereof Download PDFInfo
- Publication number
- CN106380928A CN106380928A CN201610860840.4A CN201610860840A CN106380928A CN 106380928 A CN106380928 A CN 106380928A CN 201610860840 A CN201610860840 A CN 201610860840A CN 106380928 A CN106380928 A CN 106380928A
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- parts
- ink
- printing
- silicate mineral
- anion
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Classifications
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- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09D—COATING COMPOSITIONS, e.g. PAINTS, VARNISHES OR LACQUERS; FILLING PASTES; CHEMICAL PAINT OR INK REMOVERS; INKS; CORRECTING FLUIDS; WOODSTAINS; PASTES OR SOLIDS FOR COLOURING OR PRINTING; USE OF MATERIALS THEREFOR
- C09D11/00—Inks
- C09D11/02—Printing inks
- C09D11/03—Printing inks characterised by features other than the chemical nature of the binder
-
- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09D—COATING COMPOSITIONS, e.g. PAINTS, VARNISHES OR LACQUERS; FILLING PASTES; CHEMICAL PAINT OR INK REMOVERS; INKS; CORRECTING FLUIDS; WOODSTAINS; PASTES OR SOLIDS FOR COLOURING OR PRINTING; USE OF MATERIALS THEREFOR
- C09D11/00—Inks
- C09D11/02—Printing inks
- C09D11/10—Printing inks based on artificial resins
- C09D11/102—Printing inks based on artificial resins containing macromolecular compounds obtained by reactions other than those only involving unsaturated carbon-to-carbon bonds
- C09D11/103—Printing inks based on artificial resins containing macromolecular compounds obtained by reactions other than those only involving unsaturated carbon-to-carbon bonds of aldehydes, e.g. phenol-formaldehyde resins
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- Chemical & Material Sciences (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Life Sciences & Earth Sciences (AREA)
- Engineering & Computer Science (AREA)
- Materials Engineering (AREA)
- Wood Science & Technology (AREA)
- Organic Chemistry (AREA)
- General Chemical & Material Sciences (AREA)
- Inks, Pencil-Leads, Or Crayons (AREA)
Abstract
The invention provides a printing ink with negative ion generation actions and a manufacturing technique thereof. The printing ink comprises the following components in parts by mass: 50-60 parts of pigment, 20-30 parts of branched alkane (C9H20-C30H62), 10-20 parts of fatty acid triglyceride (C18H37NO3), 10-20 parts of phenol/aldehyde-polycondensed copolymer, 10-20 parts of modified ultramicro boron cyclosilicate mineral, 1-2 parts of excitant and 1-2 parts of stabilizer. By optimizing the composition, proportioning and technique of the modified ink, the technique solves the technical problem in giving consideration to negative ion release concentration of the ink, printing quality of the ink and control on the printing cost.
Description
Technical field
The present invention relates to print field is and in particular to a kind of have printing-ink and its manufacture work that anion is had an effect
Skill.
Background technology
Anion is a kind of negatively charged gas ion of in the air, and it can facilitate human body synthesis and vitamin storage, by force
Change the physiological activity with human activin.The thirties in 20th century, German Dissuader started air positive and negative ion (negative oxygen from
Son) biological research.A large amount of papers, research and laboratory report are it was demonstrated that anion (negative oxygen ion) has to human body and significantly has
Benefit effect：In medical circle, it is to have the effective means killing pathogenic bacteria and purify air that anion is identified；In the air is electronegative
Microgranule makes oxygen content in blood increase, and is conducive to blood oxygen conveying, absorbs and utilize, can promote human metabolism, improves human body and exempt from
Epidemic disease ability, strengthens human body flesh energy, adjusts body function balance.
According to the existing cognition of scientific circles, a kind of ring silicate mineral based on boracic【Chemical formula is：Na(Mg,
Fe,Mn,Li,Al)3Al6<Si6O18><BO3>3<OH,F>4】, possess and be automatically releasable anion and emitting far-infrared work(
Can, this kind of material is commonly referred to as tourmaline.Tourmaline is natural mineral, is the inclusion aluminum of feature based on boracic, sodium, ferrum, lithium
Deng circulus silicate material.Pyroelectricity and piezoelectricity that tourmaline has because of itself are so as to polar ion is flat
The vibration of weighing apparatus position causes dipole moment change to produce the electromagnetic radiation of far infrared band, defines stronger radiation broadband.20 generation
Record the eighties, Japanese scholars T.Kubo has made intensive studies to the electric polarity of tourmaline, propose tourmaline first and exist certainly
There is electrostatic field phenomenon in generating pole, tourmaline particle, and expand a series of applied researcies to the field effect of tourmaline micropowder.
Hereafter, the state scholar such as Japanese, American-European starts the action oriented research to this one side one after another, has applied for many patents successively.But
China but starts late to the research of tourmaline, lags behind the countries such as Japan, America and Europe.
Meanwhile, the mankind propagate history and show, the leaflet future such as newspaper, periodical, teaching material, demonstration, product description
Will life-time service.Therefore, researched and developed by new material and new technique, can give paper printing industry new function.Tourmaline is
Be currently known in nature uniquely can voluntarily anion releasing natural minerals, it is combined with ink, by typography
Give common printed product effect controlled negative ion releasing function, can avoid exciting anion band using high pressure or strong ray merely
The potential risk such as the energy consumption come and safety.After leaflet has negative ion releasing function, can not only transmission information, also can adjust or
Improve region air quality, have using value and environmental benefit concurrently.The self poling of such material is weaker at present, release bear from
Son amount less stable, and there is no ripe application in print field.
First, the composition of modified ink, proportioning, technique are one of current problem demanding prompt solutions.Although in prior art
The existing scheme adding the compositions such as tourmaline in ink, but its constituent, proportioning and manufacturing process are all not up to preferable effect
So that the abundant anion releasing of modified printing-ink, negative ion concentration reaches most preferably fruit, well adapts to ink simultaneously again
The quality requirement of printing.
Meanwhile, the manufacture of the ultra-fine tourmaline anion powder that Ultra-fine and particle diameter select be problem demanding prompt solution it
Two.Tourmaline anion powder is through going after the removal of impurity tourmaline raw ore, the powder body obtaining through mechanical activation comminution.Because through adding
The tourmaline powder of work purification has higher anion yield, also known as tourmaline anion powder.According to test, anion powder
It is more than 90% to far emissivity.The negative oxygen ion producing in tourmaline anion powder has higher activity, has very
Strong redox, can destroy the cell membrane of antibacterial or the activity of cellular plasm organized enzyme, have excellent antibiotic and sterilizing
Function.Known technology only shows, after tourmaline powder, its specific surface area improves, and the particle diameter of powder is less, and it is born
Plasma diffusing W,Mo ability is stronger.Therefore, the tourmaline powder obtaining ultra-fine grain diameter is one of technological difficulties of this area.
Additionally, the control of ink processing cost is the three of problem demanding prompt solution.It is known that with tourmaline powder particle diameter
Reduction, powder processing cost then significantly rises.However, by our research it has furthermore been found that subtracting with tourmaline particle diameter
Little to a certain scope, the amplitude that its anion releasability improves substantially slows down.Therefore, select tourmaline powder in production and processing
The zone of reasonableness of ultra-fine grain diameter, is to ensure that ink printing quality it is ensured that the reasonable concentration of anion release, controls ink to add simultaneously
Work and the key of printing cost.
Content of the invention
Present invention offer is a kind of to have printing-ink and its manufacturing process that anion is had an effect, and main purpose has two
Individual：One is the element by rationally adding other compositions in cyclic silicate salt mineral, excites the intensity strengthening its self poling,
And so that the negative ion amount of release is tended towards stability；Two is to prepare the ink with negative ion-releasing function on this basis, by it
The change of formula, realizes the application in print field.
On the one hand, the invention provides a kind of composition with the printing-ink that anion is had an effect, including component：
Colorant, branched paraffin, fatty acid triglyceride, the copolymer that phenol is become with al combinate form, modified ultra micro boron class ring silicate mineral,
Exciting agent, stabilizer.
Preferably, the component that this ink includes according to mass ratio is：50 60 parts of colorant, branched paraffin (C9H20—
C30H62) 20 30 parts, fatty acid triglyceride (C18H37NO3) 10 20 parts, 0 20 parts of the copolymer 1 that phenol is become with al combinate form,
10 20 parts of modified ultra micro boron class ring silicate mineral, exciting agent 1-2 part, stabilizer 1-2 part.
Preferably, described exciting agent is one or more of rare earth element, magnetic powder or jade powder.
Preferably, the particle diameter d of the powder of described modification ultra micro boron class ring silicate mineral50For 0.3 μm～1.0 μm.
Preferably, the particle diameter d of the powder of described modification ultra micro boron class ring silicate mineral50It is about 0.3 μm.
On the other hand, the invention provides a kind of manufacturing process with the printing-ink that anion is had an effect, specifically
Comprise the steps：
Step 1：Boron class ring silicate mineral is pulverized with pulverizer, forms tourmaline boron class ring silicate mineral broken
Material；
Step 2：Boron class ring silicate mineral is carried out one-level ball milling with ball mill, form boron class ring silicate mineral
Powder；
Step 3：Take described step 2) in obtain boron class ring silicate mineral powder, using fluid bed high velocity air grind into
Row superfine grinding, obtains modified ultra micro boron class ring silicate mineral powder；
Step 4：By weight, 50 60 parts of colorant, branched paraffin (C are taken9H20—C30H62) 20 30 parts, fatty acid three
Sweet ester (C18H37NO3) 10 20 parts, 0 20 parts of the copolymer 1 that phenol is become with al combinate form, the modified ultra micro that described step 3 obtains
10 20 parts of boron class ring silicate mineral, 12 parts of exciting agent, 12 parts of stabilizer, in stirrer for mixing uniformly, in ball
Carry out two grades of ball millings in grinding machine, obtain semi-finished product；
Step 5：The semi-finished product of step 4 are inserted stirring, vibration at high speed, vacuum mistake in the constant temperature a mixing bowl of 85-90 degree
Filter, obtains ink finished product.
Preferably, in described step 3, boron class ring silicate mineral powder is pulverized, obtain modified ultra micro boron class ring
The particle diameter d of shape silicate mineral powder50It is about 0.3 μm.
Preferably, described exciting agent is one or more of rare earth element, magnetic powder or jade powder.
Another aspect, the invention provides a kind of have the printing-ink that anion is had an effect, it adopts as above-mentioned print
The manufacturing process of brush ink is fabricated by.
Based on such scheme, in modified ink manufacture processing, excellent by the constituent of modified ink, proportioning, technique
Change, solve the technical problem how taking into account anion release concentration and ink printing quality further；
Based on such scheme, by the optimization of manufacturing process, obtain the tourmaline powder of ultra-fine grain diameter so that anion
Fully discharge, solve the problems, such as the Comminution Technology for Ultrafine Powders of tourmaline anion powder further；
Based on such scheme, by reasonable selection tourmaline anion powder particle size range, tourmaline powder particle diameter is selected
For 0.3 μm about, solve further to take into account the technical problem that anion release concentration and ink processing and printing cost control.
Brief description
Fig. 1 is the printing-ink manufacturing process of the present invention.
Specific embodiment
Below in conjunction with the accompanying drawings, the present invention is described in further detail.
The printing-ink preparation technology of the present invention as shown in Figure 1, specifically includes following steps：
Step 1)：Boron class ring silicate mineral is pulverized with pulverizer, forms boron class ring silicate mineral particle；
Step 2)：Boron class ring silicate mineral is carried out one-level ball milling with ball mill, form boron class cyclic silicate salt mine
Thing powder；
Step 3)：Take above-mentioned steps 2) middle acquisition boron class ring silicate mineral powder, using fluid bed high velocity air mill
Carry out superfine grinding, obtain modified ultra micro boron class ring silicate mineral powder, by powder diameter d50It is machined to 0.3 μm about
(d50There is clear and definite definition in this area)；
Step 4)：By weight, 50 60 parts of colorant, branched paraffin (C are taken9H20—C30H62) 20 30 parts, fatty acid three
Sweet ester (C18H37NO3) 10 20 parts, 0 20 parts of the copolymer 1 that phenol is become with al combinate form, step 3) the modified ultra micro boron class that obtains
10 20 parts of ring silicate mineral, 12 parts of exciting agent, 12 parts of stabilizer, in stirrer for mixing uniformly, in ball mill
In carry out two grades of ball millings, obtain semi-finished product；
Step 5)：By step 4) semi-finished product insert in the constant temperature a mixing bowl of 85-90 degree and stir, vibration at high speed, vacuum mistake
Filter, obtains ink finished product.
First, in above-mentioned technique, tested by continuous, adjustment, the best composition proportioning of modified ink is finally set out, makes
Obtain the modified abundant anion releasing of printing-ink, well adapt to the quality requirement to ink for the typography simultaneously again.Warp
Cross the modified ink of above-mentioned technique preparation, modified every square metre of full coat cloth anion releasing total amount about 300ions of ink～
1600ions, modified every square metre of netted coating anion releasing total amount about 200ions～1200ions of ink；Meanwhile, lead to
Cross to the performance synthesis evaluation such as ink fineness, viscosity, adhesive force, drying property, form and aspect, the ink of said components proportioning processing and manufacturing
Printing performance is substantially better than Experimental Comparison example (referring to table 1).The ink of comparative example, fineness, viscosity, adhesive force, drying property, form and aspect
Poor etc. performance indications.
Secondly, in order that ultra-fine tourmaline anion powder reaches ultra micro granularity requirements, employ in the present invention mechanical activation comminution/
One-level ball milling/high velocity air grinds the processing step of/bis- grades of ball millings, effectively prevent ultra-fine grain diameter material in process of lapping again
Assembly effect so that tourmaline mineral powder can reach Ultra-fine requirement, distribution that simultaneously can be highly uniform.By ball milling
With the control of the airflow milling course of processing, tourmaline powder particle diameter d50It is smaller than 1.0 μm.
Additionally, test finds, with tourmaline powder particle diameter d50It is decreased to 0.3 μm about, its anion burst size improves
Amplitude substantially slow down.In above-mentioned technique, select the zone of reasonableness of tourmaline powder ultra-fine grain diameter it is ensured that d in production and processing50Plus
Work, to 0.3 μm about, had both guaranteed the reasonable concentration of anion release, controlled the cost of ink processing and printing simultaneously again.
Through above-mentioned technique, provide has the printing-ink that anion is had an effect to the present invention, including component according to
Mass ratio is：50 60 parts of colorant, branched paraffin (C9H20—C30H62) 20 30 parts, fatty acid triglyceride (C18H37NO3)10—
20 parts, 0 20 parts of the copolymer 1 that phenol is become with al combinate form, 10 20 parts of modified ultra micro boron class ring silicate mineral, exciting agent
1-2 part, stabilizer 1-2 part.
Preferably, the particle diameter d of modified ultra micro boron class ring silicate mineral powder50For 0.3 μm about.
Preferably, described exciting agent is rare earth element, magnetic powder, jade powder etc.；
The component proportion of the printing-ink of the present invention and technique effect enter with reference to specific embodiment 1-12 as shown in table 1
Row explanation.Embodiment in table is only to be illustrated, and does not represent the total Test data of this programme.
Table 1 (component unit：Part；Tourmaline powder particle diameter d50It is about 0.3 μm)
In upper table, embodiment 13-20 can be considered the comparative example of the present invention.
Those skilled in the art, under conditions of the spirit and scope of the present invention determining without departing from claims, goes back
Various modifications can be carried out to above content.Therefore the scope of the present invention is not limited in above explanation, but by
The scope of claims is determining.
Claims (10)
1. a kind of have the printing-ink that anion has an effect it is characterised in that the group including is divided into：Colorant, branched paraffin,
Fatty acid triglyceride, the copolymer that phenol is become with al combinate form, modified ultra micro boron class ring silicate mineral, exciting agent, stabilizer.
2. there is printing-ink that anion is had an effect as claimed in claim 1, the component that it includes according to mass ratio is：
50 60 parts of colorant, branched paraffin (C9H20—C30H62) 20 30 parts, fatty acid triglyceride (C18H37NO3) 10 20 parts, phenol with
0 20 parts of the copolymer 1 that al combinate form becomes, 10 20 parts of modified ultra micro boron class ring silicate mineral, exciting agent 1-2 part, surely
Determine agent 1-2 part.
3. there is printing-ink that anion is had an effect as claimed in claim 2, including component according to mass ratio be：Color
55 parts of material, branched paraffin (C9H20—C30H62) 28 30 parts, fatty acid triglyceride (C18H37NO3) 10 20 parts, phenol is gathered with al
0 20 parts of the copolymer 1 being formed, 12 20 parts of modified ultra micro boron class ring silicate mineral, exciting agent 1-2 part, stabilizer
1-2 part.
4. as any one of claim 2-3, there is the printing-ink that anion is had an effect, described exciting agent is dilute
One or more of earth elements, magnetic powder or jade powder.
5. as any one of claim 2-3 there is the printing-ink that anion is had an effect, described modification ultra micro boron
The particle diameter d of the powder of class ring silicate mineral50For 0.3 μm～1.0 μm.
6. as any one of claim 2-3 there is the printing-ink that anion is had an effect, described modification ultra micro boron
The particle diameter d of the powder of class ring silicate mineral50It is about 0.3 μm.
7. a kind of manufacturing process with the printing-ink that anion is had an effect is it is characterised in that specifically include following steps：
Step 1：Boron class ring silicate mineral is pulverized with pulverizer, forms boron class ring silicate mineral particle；
Step 2：Boron class ring silicate mineral is carried out one-level ball milling with ball mill, form boron class ring silicate mineral powder
End；
Step 3：Take described step 2) middle acquisition boron class ring silicate mineral powder, surpassed using fluid bed high velocity air mill
Finely divided, obtain modified ultra micro boron class ring silicate mineral powder；
Step 4：By weight, 50 60 parts are taken, branched paraffin (C9H20—C30H62) 20 30 parts, fatty acid triglyceride
(C18H37NO3) 10 20 parts, 0 20 parts of the copolymer 1 that phenol is become with al combinate form, the modified ultra micro boron class that described step 3 obtains
10 20 parts of ring silicate mineral, 12 parts of exciting agent, 12 parts of stabilizer, in stirrer for mixing uniformly, in ball mill
In carry out two grades of ball millings, obtain semi-finished product；
Step 5：The semi-finished product of step 4 are inserted stirring, vibration at high speed, vacuum filter in the constant temperature a mixing bowl of 85-90 degree, obtain
To ink finished product.
8. there is the manufacturing process of the printing-ink that anion is had an effect as described in claim 7, in described step 3
Boron class ring silicate mineral powder is pulverized, obtains the particle diameter d of modified ultra micro boron class ring silicate mineral powder50It is about
0.3μm.
9. there is the manufacturing process of the printing-ink that anion is had an effect as claimed in claim 7, described exciting agent is dilute
One or more of earth elements, magnetic powder or jade powder.
10. a kind of have the printing-ink that anion is had an effect, and it adopts the printing as described in any one of claim 7-9
The manufacturing process of ink is fabricated by.
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| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201610860840.4A CN106380928B (en) | 2016-09-28 | 2016-09-28 | A kind of printing-ink being had an effect with anion and its manufacturing process |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201610860840.4A CN106380928B (en) | 2016-09-28 | 2016-09-28 | A kind of printing-ink being had an effect with anion and its manufacturing process |
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| CN106380928A true CN106380928A (en) | 2017-02-08 |
| CN106380928B CN106380928B (en) | 2017-06-16 |
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Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN112662227A (en) * | 2020-12-11 | 2021-04-16 | 上海美美良虹印刷有限公司 | Carbon-free environment-friendly offset printing black ink and preparation method thereof |
Citations (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| JP2004155899A (en) * | 2002-11-06 | 2004-06-03 | Hidekazu Itaka | Structured ink |
| CN104693894A (en) * | 2015-03-26 | 2015-06-10 | 广东三水大鸿制釉有限公司 | Anion ink for ink jet printing and preparation method and coating method thereof |
| CN104845440A (en) * | 2015-03-12 | 2015-08-19 | 杭州海维特化工科技有限公司 | Water-based ink for negative ion decorative paper and preparation method therefor |
-
2016
- 2016-09-28 CN CN201610860840.4A patent/CN106380928B/en active Active
Patent Citations (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| JP2004155899A (en) * | 2002-11-06 | 2004-06-03 | Hidekazu Itaka | Structured ink |
| CN104845440A (en) * | 2015-03-12 | 2015-08-19 | 杭州海维特化工科技有限公司 | Water-based ink for negative ion decorative paper and preparation method therefor |
| CN104693894A (en) * | 2015-03-26 | 2015-06-10 | 广东三水大鸿制釉有限公司 | Anion ink for ink jet printing and preparation method and coating method thereof |
Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN112662227A (en) * | 2020-12-11 | 2021-04-16 | 上海美美良虹印刷有限公司 | Carbon-free environment-friendly offset printing black ink and preparation method thereof |
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| Publication number | Publication date |
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| CN106380928B (en) | 2017-06-16 |
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