CN106377917A - Novel rotary evaporator - Google Patents
Novel rotary evaporator Download PDFInfo
- Publication number
- CN106377917A CN106377917A CN201611027246.3A CN201611027246A CN106377917A CN 106377917 A CN106377917 A CN 106377917A CN 201611027246 A CN201611027246 A CN 201611027246A CN 106377917 A CN106377917 A CN 106377917A
- Authority
- CN
- China
- Prior art keywords
- motor
- cucurbit
- upside
- rotary evaporator
- distillation
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Granted
Links
- 238000003756 stirring Methods 0.000 claims abstract description 8
- 230000000903 blocking effect Effects 0.000 claims description 6
- 230000008878 coupling Effects 0.000 claims description 3
- 238000010168 coupling process Methods 0.000 claims description 3
- 238000005859 coupling reaction Methods 0.000 claims description 3
- 238000007789 sealing Methods 0.000 claims description 2
- 230000005611 electricity Effects 0.000 claims 1
- 238000004821 distillation Methods 0.000 abstract description 10
- 238000010521 absorption reaction Methods 0.000 abstract 4
- 238000005516 engineering process Methods 0.000 description 3
- 238000001704 evaporation Methods 0.000 description 3
- 230000000694 effects Effects 0.000 description 2
- 230000008020 evaporation Effects 0.000 description 2
- 238000000034 method Methods 0.000 description 2
- 239000006096 absorbing agent Substances 0.000 description 1
- 230000009286 beneficial effect Effects 0.000 description 1
- 229960000074 biopharmaceutical Drugs 0.000 description 1
- 238000002425 crystallisation Methods 0.000 description 1
- 230000008025 crystallization Effects 0.000 description 1
- 238000000354 decomposition reaction Methods 0.000 description 1
- 230000007850 degeneration Effects 0.000 description 1
- 239000003814 drug Substances 0.000 description 1
- 238000001035 drying Methods 0.000 description 1
- 239000000428 dust Substances 0.000 description 1
- 239000011521 glass Substances 0.000 description 1
- 238000010438 heat treatment Methods 0.000 description 1
- 239000000463 material Substances 0.000 description 1
- 238000002360 preparation method Methods 0.000 description 1
- 238000000746 purification Methods 0.000 description 1
- 238000005096 rolling process Methods 0.000 description 1
- 239000002904 solvent Substances 0.000 description 1
- 238000010025 steaming Methods 0.000 description 1
- 239000000126 substance Substances 0.000 description 1
Classifications
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01D—SEPARATION
- B01D3/00—Distillation or related exchange processes in which liquids are contacted with gaseous media, e.g. stripping
- B01D3/08—Distillation or related exchange processes in which liquids are contacted with gaseous media, e.g. stripping in rotating vessels; Atomisation on rotating discs
- B01D3/085—Distillation or related exchange processes in which liquids are contacted with gaseous media, e.g. stripping in rotating vessels; Atomisation on rotating discs using a rotary evaporator
Landscapes
- Chemical & Material Sciences (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Vaporization, Distillation, Condensation, Sublimation, And Cold Traps (AREA)
Abstract
The invention discloses a novel rotary evaporator. The novel rotary evaporator comprises a base, wherein the base is internally provided with a vibration absorption cushion; the vibration absorption cushion is internally provided with vibration absorption springs; a distillation chamber is arranged at the upper side of the base; a water-bath pot is arranged in the distillation chamber; heater is arranged at the bottom of the water-bath pot; a distillation flask is arranged at the upper end of the water-bath pot; hydraulic cylinders are arranged at left and right ends of the upper side of the distillation chamber; a motor chamber is arranged at the upper sides of the hydraulic cylinders; a fixed sleeve is arranged at a connecting part of the motor chamber and the distillation flask; a first motor is arranged at the right end in the motor chamber and a driving gear is arranged at the upper end of the first motor; a driven gear is arranged at the upper end of the distillation flask; a second motor is arranged at the upper side of the motor chamber; a stirring shaft is arranged at the lower side of the second motor; stirring blades are arranged at the lower end of the stirring shaft; an exhausting pipe is arranged at the lower side of the fixed sleeve; an air pump is arranged on the exhausting pipe. By arranging a hoisting device, a rotating device, a stirring device and a vibration absorption device, objects needing to be distilled can be effectively distilled, so that the distillation efficiency is improved and the surrounding environment is protected.
Description
Technical field
The present invention relates to a kind of distillation equipment, specifically a kind of Novel rotary evaporator.
Background technology
Rotary evaporator is mainly used in the concentration of the industries such as medicine, chemical industry and bio-pharmaceuticals, crystallization, drying, separates and molten
Matchmaker reclaims.Its principle is heated at constant temperature under vacuum, makes revolving bottle constant speed rotary, and it is thin that material forms large area in bottle wall
Film, high-efficiency evaporating.Solvent steam cools down through highly-efficient glass condenser, is recovered in receiving flask, greatly improves evaporation efficiency.Especially
It is suitable for the concentration purification of the biological products that high temperature is held with easy decomposition and degeneration.Existing rotary evaporator is due to can not control rotation well
Rolling bottle and the distance relation of water-bath, thus lead to evaporation efficiency low.Therefore, those skilled in the art provide a kind of novel rotary
Turn evaporimeter, to solve the problems, such as to propose in above-mentioned background technology.
Content of the invention
It is an object of the invention to provide a kind of Novel rotary evaporator, with asking of solving to propose in above-mentioned background technology
Topic.
For achieving the above object, the present invention provides following technical scheme：
A kind of Novel rotary evaporator, including base, described chassis interior is provided with cushion blocking, is provided with inside described cushion blocking
Shock-absorbing spring, is provided with distillery on the upside of described base, is provided with water-bath inside described distillery, and described water-bath pot bottom is provided with and adds
Hot device, described water-bath upper end is provided with cucurbit, and on the upside of described distillery, left and right two ends are provided with hydraulic cylinder, on the upside of described hydraulic cylinder
It is provided with motor room, described motor room and cucurbit junction are provided with fixed cover, the internal right-hand member in described motor room is provided with the first motor,
Described first motor upper end is provided with driving gear, and described cucurbit upper end is provided with driven gear, is provided with envelope on the upside of described cucurbit
Mouth plug, is provided with the second motor, is provided with shaft on the downside of described second motor, described shaft lower end is provided with the upside of described motor room
Stirring vane, is provided with blast pipe on the downside of described fixed cover, and described blast pipe is provided with aspiration pump.
As the further scheme of the present invention：Described distillery and cucurbit junction are provided with wearing layer.
As the further scheme of the present invention：Described second motor is connected with rotary shaft by shaft coupling.
As the further scheme of the present invention：It is provided with limit base on the downside of described rotary shaft.
As the present invention further scheme：It is provided with screen pack inside described blast pipe.
Compared with prior art, the invention has the beneficial effects as follows：The present invention passes through lowering or hoisting gear, whirligig and stirring dress
The article needing distillation can be distilled, can quickly finish still-process, and set by setting effectively effectively that put
Standby simple, easy and simple to handle, by vibration absorber, vibration, protection equipment can be efficiently reduced, decrease noise pollution.
Brief description
Fig. 1 is a kind of structural representation of Novel rotary evaporator.
Specific embodiment
Below in conjunction with the accompanying drawing in the embodiment of the present invention, the technical scheme in the embodiment of the present invention is carried out clear, complete
Site preparation description is it is clear that described embodiment is only a part of embodiment of the present invention, rather than whole embodiments.It is based on
Embodiment in the present invention, it is every other that those of ordinary skill in the art are obtained under the premise of not making creative work
Embodiment, broadly falls into the scope of protection of the invention.
Refer to Fig. 1, in the embodiment of the present invention, a kind of Novel rotary evaporator, including base 1, set inside described base 1
There is cushion blocking 2, be provided with shock-absorbing spring 3 inside described cushion blocking 2, vibration, protection equipment can be efficiently reduced, decrease noise
Pollution, is provided with distillery 4, is provided with water-bath 5 inside described distillery 4, described water-bath 5 bottom is provided with the upside of described base 1
Heater 6, can be used for the heating within water-bath 5, and described water-bath 5 upper end is provided with cucurbit 7, described distillery 4 and steaming
Evaporate bottle 7 junction and be provided with wearing layer, can effectively protect cucurbit 7, described distillery 4 upside left and right two ends are provided with hydraulic cylinder
8, moving up and down of cucurbit 7 can be efficiently controlled, such that it is able to efficiently control distilling effect, on the upside of described hydraulic cylinder 8
It is provided with motor room 9, described motor room 9 and cucurbit 7 junction are provided with fixed cover 10, the internal right-hand member in described motor room 9 is provided with the
One motor 11, described first motor 11 upper end is provided with driving gear 12, and described cucurbit 7 upper end is provided with driven gear 13, passes through
Gear engagement can drive the rotation of cucurbit 7 effectively, thus effectively improving distilling effect, sets on the upside of described cucurbit 7
There is sealing plug 14, the article within cucurbit 7 can be effectively prevented and pass through bottleneck airborne dust in the air, lead to the wave of resource
Take, destroy environment, be provided with the second motor 15 on the upside of described motor room 9, on the downside of described second motor 15, be provided with shaft 16, institute
State the second motor 15 to be connected with rotary shaft 16 by shaft coupling, described shaft 16 lower end is provided with stirring vane 17, can be effective
Ground is stirred to the article within cucurbit 7, so that article more fully contact hot-air, improves distillation efficiency,
It is provided with limit base on the downside of described rotary shaft 16, be provided with blast pipe 18 on the downside of described fixed cover 10, be provided with inside described blast pipe 18
Screen pack, described blast pipe 18 is provided with aspiration pump 19, because, in still-process, the air within cucurbit 7 expands with heat and contract with cold
Reason, the pressure in bottle increases, and by blast pipe, vapor can be taken the pressure it is also ensured that in bottle out of.
It is obvious to a person skilled in the art that the invention is not restricted to the details of above-mentioned one exemplary embodiment, Er Qie
In the case of the spirit or essential attributes of the present invention, the present invention can be realized in other specific forms.Therefore, no matter
From the point of view of which point, embodiment all should be regarded as exemplary, and be nonrestrictive, the scope of the present invention is by appended power
Profit requires rather than described above limits, it is intended that all in the implication and scope of the equivalency of claim by falling
Change is included in the present invention.Any reference in claim should not be considered as limiting involved claim.
Moreover, it will be appreciated that although this specification is been described by according to embodiment, not each embodiment only wraps
Containing an independent technical scheme, only for clarity, those skilled in the art should for this narrating mode of specification
Using specification as an entirety, the technical scheme in each embodiment can also form those skilled in the art through appropriately combined
Understandable other embodiment.
Claims (3)
1. a kind of Novel rotary evaporator, including base (1) it is characterised in that being provided with cushion blocking (2) inside described base (1),
It is provided with shock-absorbing spring (3) inside described cushion blocking (2), on the upside of described base (1), is provided with distillery (4), in described distillery (4)
Portion is provided with water-bath (5), and described water-bath (5) bottom is provided with heater (6), and described water-bath (5) upper end is provided with cucurbit
(7), on the upside of described distillery (4), left and right two ends are provided with hydraulic cylinder (8), are provided with motor room (9), institute on the upside of described hydraulic cylinder (8)
State motor room (9) and be provided with fixed cover (10) with cucurbit (7) junction, the internal right-hand member of described motor room (9) is provided with the first motor
(11), described first motor (11) upper end is provided with driving gear (12), and described cucurbit (7) upper end is provided with driven gear (13),
It is provided with sealing plug (14) on the upside of described cucurbit (7), on the upside of described motor room (9), be provided with the second motor (15), described second electricity
It is provided with shaft (16), described shaft (16) lower end is provided with stirring vane (17), under described fixed cover (10) on the downside of machine (15)
Side is provided with blast pipe (18), and described blast pipe (18) is provided with aspiration pump (19), and described distillery (4) is connected with cucurbit (7)
Place is provided with wearing layer, and described second motor (15) is connected with rotary shaft (16) by shaft coupling.
2. a kind of Novel rotary evaporator according to claim 1 is it is characterised in that be provided with the downside of described rotary shaft (16)
Limit base.
3. a kind of Novel rotary evaporator according to claim 1 is it is characterised in that be provided with inside described blast pipe (18)
Screen pack.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201611027246.3A CN106377917B (en) | 2016-11-22 | 2016-11-22 | A kind of Novel rotary evaporator |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201611027246.3A CN106377917B (en) | 2016-11-22 | 2016-11-22 | A kind of Novel rotary evaporator |
Publications (2)
| Publication Number | Publication Date |
|---|---|
| CN106377917A true CN106377917A (en) | 2017-02-08 |
| CN106377917B CN106377917B (en) | 2019-02-05 |
Family
ID=57957500
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN201611027246.3A Active CN106377917B (en) | 2016-11-22 | 2016-11-22 | A kind of Novel rotary evaporator |
Country Status (1)
| Country | Link |
|---|---|
| CN (1) | CN106377917B (en) |
Cited By (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN107504368A (en) * | 2017-09-14 | 2017-12-22 | 江苏航天惠利特环保科技有限公司 | A kind of energy-efficient bog retracting devices |
| CN110604939A (en) * | 2019-08-26 | 2019-12-24 | 南安市明誓汽配贸易有限公司 | Temperature control stirrer for concentrated and refined reamer of sanitary towel slurry |
| CN111318040A (en) * | 2020-04-02 | 2020-06-23 | 程俞小倩 | Rotary evaporation equipment for multi-liquid distillation work |
| CN111359245A (en) * | 2020-04-01 | 2020-07-03 | 广东两山科技有限公司 | Ionic liquid purification device and using method thereof |
Citations (5)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CH657715A5 (en) * | 1983-08-26 | 1986-09-15 | Yamato Scient Co Ltd | Rotary evaporator |
| CN203775838U (en) * | 2014-03-20 | 2014-08-20 | 北京鑫大禹华霖节水设备有限责任公司 | Novel garden irrigating machine |
| CN204159057U (en) * | 2014-09-01 | 2015-02-18 | 宿迁远扬生物科技有限公司 | Rotary evaporator |
| CN205269086U (en) * | 2016-01-06 | 2016-06-01 | 安徽瑞邦香料有限公司 | Special distillation reation kettle of ketone musk |
| CN205667724U (en) * | 2016-06-06 | 2016-11-02 | 滨州学院 | A kind of temperature control distilling apparatus |
-
2016
- 2016-11-22 CN CN201611027246.3A patent/CN106377917B/en active Active
Patent Citations (5)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CH657715A5 (en) * | 1983-08-26 | 1986-09-15 | Yamato Scient Co Ltd | Rotary evaporator |
| CN203775838U (en) * | 2014-03-20 | 2014-08-20 | 北京鑫大禹华霖节水设备有限责任公司 | Novel garden irrigating machine |
| CN204159057U (en) * | 2014-09-01 | 2015-02-18 | 宿迁远扬生物科技有限公司 | Rotary evaporator |
| CN205269086U (en) * | 2016-01-06 | 2016-06-01 | 安徽瑞邦香料有限公司 | Special distillation reation kettle of ketone musk |
| CN205667724U (en) * | 2016-06-06 | 2016-11-02 | 滨州学院 | A kind of temperature control distilling apparatus |
Cited By (5)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN107504368A (en) * | 2017-09-14 | 2017-12-22 | 江苏航天惠利特环保科技有限公司 | A kind of energy-efficient bog retracting devices |
| CN110604939A (en) * | 2019-08-26 | 2019-12-24 | 南安市明誓汽配贸易有限公司 | Temperature control stirrer for concentrated and refined reamer of sanitary towel slurry |
| CN111359245A (en) * | 2020-04-01 | 2020-07-03 | 广东两山科技有限公司 | Ionic liquid purification device and using method thereof |
| CN111359245B (en) * | 2020-04-01 | 2021-07-23 | 广东两山科技有限公司 | Ionic liquid purification device and using method thereof |
| CN111318040A (en) * | 2020-04-02 | 2020-06-23 | 程俞小倩 | Rotary evaporation equipment for multi-liquid distillation work |
Also Published As
| Publication number | Publication date |
|---|---|
| CN106377917B (en) | 2019-02-05 |
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Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| C06 | Publication | ||
| PB01 | Publication | ||
| C10 | Entry into substantive examination | ||
| SE01 | Entry into force of request for substantive examination | ||
| TA01 | Transfer of patent application right |
Effective date of registration: 20181219 Address after: 463700 Shizi Village, Guoji Town, Biyang County, Zhumadian City, Henan Province Applicant after: Henan Jianyuan Rosemary Products Co., Ltd. Address before: 450000 room C260, 1 tower, 96, Ruida Road, Zhengzhou high tech Industrial Development Zone, Henan Applicant before: Zhengzhou search information technology Co., Ltd. |
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| TA01 | Transfer of patent application right | ||
| GR01 | Patent grant | ||
| GR01 | Patent grant | ||
| PE01 | Entry into force of the registration of the contract for pledge of patent right |
Denomination of invention: A new type of rotary evaporator Effective date of registration: 20210609 Granted publication date: 20190205 Pledgee: Henan Biyang Rural Commercial Bank Co.,Ltd. Pledgor: Henan Jianyuan Rosemary Products Co.,Ltd. Registration number: Y2021980004619 |
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| PE01 | Entry into force of the registration of the contract for pledge of patent right | ||
| PC01 | Cancellation of the registration of the contract for pledge of patent right |
Date of cancellation: 20220602 Granted publication date: 20190205 Pledgee: Henan Biyang Rural Commercial Bank Co.,Ltd. Pledgor: Henan Jianyuan Rosemary Products Co.,Ltd. Registration number: Y2021980004619 |
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| PC01 | Cancellation of the registration of the contract for pledge of patent right | ||
| PE01 | Entry into force of the registration of the contract for pledge of patent right |
Denomination of invention: A new type of rotary evaporator Effective date of registration: 20220607 Granted publication date: 20190205 Pledgee: Henan Biyang Rural Commercial Bank Co.,Ltd. Pledgor: Henan Jianyuan Rosemary Products Co.,Ltd. Registration number: Y2022980007173 |
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| PE01 | Entry into force of the registration of the contract for pledge of patent right |