CN106362294A - Preparation method of graphene-based multifunctional physiotherapy magnet - Google Patents

Preparation method of graphene-based multifunctional physiotherapy magnet Download PDF

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Publication number
CN106362294A
CN106362294A CN201610822141.0A CN201610822141A CN106362294A CN 106362294 A CN106362294 A CN 106362294A CN 201610822141 A CN201610822141 A CN 201610822141A CN 106362294 A CN106362294 A CN 106362294A
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far
magnetitum
slurry
preparation
infrared
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CN106362294B (en
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曲丽君
田明伟
周珍卉
杜敏芝
于荣荣
赵壬海
赵洪涛
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Qingdao University
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    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61NELECTROTHERAPY; MAGNETOTHERAPY; RADIATION THERAPY; ULTRASOUND THERAPY
    • A61N2/00Magnetotherapy
    • A61N2/06Magnetotherapy using magnetic fields produced by permanent magnets
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61NELECTROTHERAPY; MAGNETOTHERAPY; RADIATION THERAPY; ULTRASOUND THERAPY
    • A61N5/00Radiation therapy
    • A61N5/06Radiation therapy using light
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61NELECTROTHERAPY; MAGNETOTHERAPY; RADIATION THERAPY; ULTRASOUND THERAPY
    • A61N5/00Radiation therapy
    • A61N5/06Radiation therapy using light
    • A61N2005/0658Radiation therapy using light characterised by the wavelength of light used
    • A61N2005/0659Radiation therapy using light characterised by the wavelength of light used infrared
    • A61N2005/066Radiation therapy using light characterised by the wavelength of light used infrared far infrared

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  • Health & Medical Sciences (AREA)
  • Engineering & Computer Science (AREA)
  • Biomedical Technology (AREA)
  • Public Health (AREA)
  • Nuclear Medicine, Radiotherapy & Molecular Imaging (AREA)
  • Radiology & Medical Imaging (AREA)
  • Life Sciences & Earth Sciences (AREA)
  • Animal Behavior & Ethology (AREA)
  • General Health & Medical Sciences (AREA)
  • Veterinary Medicine (AREA)
  • Pathology (AREA)
  • Magnetic Treatment Devices (AREA)
  • Medicinal Preparation (AREA)
  • Radiation-Therapy Devices (AREA)

Abstract

The invention discloses a preparation method of a graphene-based multifunctional physiotherapy magnet. The method comprises the following steps: 1, preparing crude ore slurry; 2, preparing spontaneous heating far-infrared function slurry; and 3, obtaining spontaneous heating far-infrared function powder after performing heating drying on the spontaneous heating far-infrared function slurry obtained in the second step, and then preparing the spontaneous heating far-infrared function powder into spontaneous heating far-infrared function circular slice, i.e., the physiotherapy magnet through pressing by a tablet press. According to the preparation method of the graphene-based multifunctional physiotherapy magnet, the physiotherapy magnet prepared by use of the preparation method has ideal spontaneous heating and far-infrared effects, can be cyclically used and is convenient to use.

Description

A kind of preparation method of the multifunctional physiotherapy Magnetitum based on Graphene
Technical field
The invention belongs to health care equipment technical field is and in particular to a kind of multifunctional physiotherapy Magnetitum based on Graphene Preparation method.
Background technology
Constantly accelerate with people's work, the change of life style and rhythm, the health to itself and household for the people Increasingly pay attention to, what doctor trained in Western medicine was controlled is disease, middle treatment is people, and the boundary that Traditional Chinese health is pursued is exactly to balance, treating cold syndrome with hot-nature drugs, heat Person trembles with fear it.So that neutralization.Cold will allow heat, heat will be trembled with fear, and knot will dissipate, ease will labor, labor will escape.It is just each got in the world Institute, all things on earth just growth promoter.It is exactly to cause to neutralize that Traditional Chinese health exactly reaches this perfect condition by various methods.The traditional Chinese medical science is for I Traditional quintessence of Chinese culture of state, it advocates that human body itself exists as an entirety, dirty " functional station " being respectively human body with body surface of internal organs, And meridians are then equivalent to " road ", it is responsible for transmission dirty the passed on information of each internal organs, there is holding partes corporis humani and coordinate and balance Effect, Chinese medicine is spread on epidermis, by heating, Chinese medicine volatilization is transmitted in meridians by pore again, and then acts on The vital organs of the human body, reach disease preventing and treating, take good care of the purpose of body, be the critical treatment method in China's folk medicine.
Chinese patent cn 101987053 b discloses a kind of natural mineral traditional Chinese medicinal hot bag, by plurality of Chinese and Ore one Rise and be coated in bag after soaking, spread at body foci after heating, this thermal pack is that Chinese medicine and Ore are mixed immersion of putting together, Clear up very inconvenient, the loose placement of middle medicine block itself and shared volume also make this thermal pack very not convenient when using, And now the adsorption effect of ore storage Chinese medicine and hot compression therapy effect also will not be fine.
Chinese patent cn 103767868 a discloses a kind of Chinese medicine and warms up patch and preparation method thereof, heat energy and Chinese medicine effective Branch is become to produce stimulation to human acupoints such as Yongquan acupoint, with health role while providing thermal effect, this warm patch Effective Component of Chinese Medicine is placed in the resin of high-hydroscopicity, and then acts on human body and produce curative effect, but only lean on heat energy, its drug effect is not Seem and can significantly efficiently be utilized very much, and not reproducible use.
Content of the invention
For defect present in prior art or deficiency, the present invention innovatively proposes a kind of many based on Graphene The preparation method of function physical therapy Magnetitum, the physical therapy Magnetitum obtained by this preparation method, there is preferable spontaneous heating and far infrared effect Really, can be recycled, easy to use.
The technical scheme is that and be achieved in that:
A kind of preparation method of the multifunctional physiotherapy Magnetitum based on Graphene, comprises the following steps:
(1) tcrude ore coarse fodder is gone the removal of impurity by supersound washing, then in turn through ball mill ball milling 1-5h, then through grinding Grinding machine grind 1-5h, after prepare tcrude ore slurry through levigator water mill 1-5h;
(2) put into, into high-speed shearing machine, the tcrude ore slurry that far-infrared functional auxiliary agent, dispersant and step (1) obtain, It is sufficiently mixed through high speed shear, obtain spontaneous heating far-infrared functional slurry;
(3) the spontaneous heating far-infrared functional slurry that step (2) obtains is carried out obtaining spontaneous heating far infrared after heating, drying Functional powders, then spontaneous heating far infrared functional powder is pressed into spontaneous heating far-infrared functional thin rounded flakes via tablet machine, that is, For physical therapy Magnetitum, and squeeze into buttonhole hole by the middle part of physical therapy Magnetitum;
Further, in step (1), the power of supersound washing is 30-120kw, and temperature is 10-30 DEG C, and the time is 10- 90min;In step (1), the tcrude ore coarse fodder after supersound washing is prepared into the granule of 1-3mm through ball mill ball milling, then warp Grinder grinds and is prepared into the granule of 0.1-1mm, after be prepared into 1-10 μm of tcrude ore slurry through levigator water mill.
Further, in step (1), described tcrude ore slurry is starched by the germanite of 50-70% tourmaline slurry, 10-20% The silica slurry of material, the stone needle slurry of 10-20% and 10% mixes.
Further, in step (2), the tcrude ore slurry containing 75-95% in described spontaneous heating far-infrared functional slurry, The far-infrared functional auxiliary agent of 1.5-20% and the dispersant of 3.5-5%.
Further, in step (2), described spontaneous heating far-infrared functional slurry contain 80% tcrude ore slurry, 15% Far-infrared functional auxiliary agent and 5% dispersant.
Further, in step (2), described far-infrared functional auxiliary agent is appointing in Graphene, CNT and fullerene Meaning is a kind of, or two or more is mixed with arbitrary proportion.
Further, in step (2), described dispersant is dodecylbenzene sodium sulfonate, Polyvinylpyrrolidone and carboxylic first Any one in base sodium cellulosate.
Further, the heating, drying mode in step (3) is dried for baking oven for heating, and the heating-up temperature of baking oven is 60-200 DEG C, heat time heating time is 10-90min.
Further, the heating, drying mode in step (3) is far-infrared lamp irradiation, the far infrared in far-infrared lamp irradiation The power of lamp is 100-600w, and heat time heating time is 5-60min.
Further, a diameter of 5-10mm of the physical therapy Magnetitum described in step (3), thickness is 2-4mm, described physical therapy magnetic The middle part of stone is at least provided with two buttonhole holes being used for the sewing of physical therapy Magnetitum on required object.
Compared with prior art, the beneficial effects of the present invention is:
The multifunctional physiotherapy Magnetitum based on Graphene of the present invention, that is, spontaneous heating far-infrared functional thin rounded flakes, are distributed The far infrared going out easily is rapidly absorbed by a human, horny layer softening layer, and far-infrared negative-ion penetrates to the skin depths, peroxynitrite decomposition lipid etc. Harmful substance simultaneously excludes external, expansion of blood vessels by sweat and urine, promotes blood circulation of human body, recovers the elasticity of blood vessel wall, Accelerate cell metabolism, adjust nerve.
Emphatically to multifunctional physiotherapy Magnetitum, that is, the material of spontaneous heating far-infrared functional thin rounded flakes and composition enter the present invention Go research, the nanometer carbon-based material such as Graphene, CNT and fullerene has been combined tourmaline, germanite, stone needle and titanium dioxide Silicon raw ore stone material, by Compound Machining, prepares and not only has spontaneous heating function but also have the spontaneous of far-infrared transmitting function Hot far-infrared functional thin rounded flakes;The middle part of physical therapy Magnetitum is used for sewing physical therapy Magnetitum in required object at least provided with two On buttonhole hole, the setting in buttonhole hole, arbitrarily flexibly can fix physical therapy Magnetitum, user can voluntarily be sewn into as needed On the corresponding object in required physical therapy position, such as clothes, neck protective pillow, Neck protection belt, knee cap, waist support etc..
The multifunctional physiotherapy Magnetitum based on Graphene of the present invention, far infrared transmissivity is 0.85-0.95, and temperature rise is up to 3- 6 DEG C, summary, the physical therapy Magnetitum of the present invention, there is more preferably spontaneous heating and far-infrared effect, can be widely applied to various In health-care physical therapy product.
Brief description
Fig. 1 is the structural representation of multifunctional physiotherapy Magnetitum of the present invention;
Reference: 1, multifunctional physiotherapy Magnetitum;2nd, buttonhole hole.
Specific embodiment
With reference to specific embodiment, the technical scheme in the embodiment of the present invention is clearly and completely described, shows So, described embodiment is only a part of embodiment of the present invention, rather than whole embodiments.Based on the reality in the present invention Apply example, the every other embodiment that those of ordinary skill in the art are obtained under the premise of not making creative work, all belong to In the scope of protection of the invention.
Embodiment 1:
The invention provides a kind of preparation method of the multifunctional physiotherapy Magnetitum based on Graphene, specifically include following step Rapid:
(1) the tcrude ore coarse fodder of tourmaline, germanite, stone needle and silicon dioxide is gone the removal of impurity by supersound washing, ultrasonic The power of washing is 30-120kw, and temperature is 10-30 DEG C, and the time is 10-90min;Then in turn through ball mill ball milling 1-5h, It is prepared into the granule of 1-3mm;Ground machine grinds 1-5h again, is prepared into the granule of 0.1-1mm;Through levigator water mill 1-5h after Prepare the slurry of 1-10 μm of tcrude ore, now, the germanite containing 70% tourmaline slurry, 10% in the middle of tcrude ore slurry The silica slurry of slurry, 10% stone needle slurry and 10%;
(2) put into, into high-speed shearing machine, the tcrude ore slurry that far-infrared functional auxiliary agent, dispersant and step (1) obtain, It is sufficiently mixed through high speed shear, obtain spontaneous heating far-infrared functional slurry.Far-infrared functional selection of auxiliary Graphene, dispersant selects With dodecylbenzene sodium sulfonate, now, in this spontaneous heating far-infrared functional slurry, the content of each component is respectively: Graphene accounts for 20%, dodecylbenzene sodium sulfonate accounts for 5%, and tcrude ore slurry accounts for 75%;
(3) the spontaneous heating far-infrared functional slurry that step (2) is obtained 60-200 DEG C of heating, drying 10- in baking oven 90min, to obtain spontaneous heating far infrared functional powder, then spontaneous heating far infrared functional powder is pressed into diameter via tablet machine It is the spontaneous heating far-infrared functional thin rounded flakes of 5-20mm for 2-10cm, thickness, as physical therapy Magnetitum 1, and by physical therapy Magnetitum Portion squeezes into buttonhole hole 2.
Embodiment 2:
As different from Example 1, in step (1), the germanium containing 60% tourmaline slurry, 15% in the middle of tcrude ore slurry The silica slurry of stone slurry, 15% stone needle slurry and 10%.In step (2), far-infrared functional selection of auxiliary Graphene, CNT and the mixture of fullerene, dispersant selects Polyvinylpyrrolidone, now, this spontaneous heating far-infrared functional slurry In the content of each component be respectively: Graphene accounts for 5%, and CNT accounts for 5%, and fullerene accounts for 5%, and Polyvinylpyrrolidone accounts for 5%, tcrude ore slurry accounts for 80%.
Embodiment 3:
As different from Example 1, in step (1), the germanium containing 50% tourmaline slurry, 20% in the middle of tcrude ore slurry The silica slurry of stone slurry, 20% stone needle slurry and 10%.In step (2), far-infrared functional selection of auxiliary Graphene, CNT and the mixture of fullerene, dispersant selects one of Polyvinylpyrrolidone or sodium carboxymethyl cellulose, this When, in this spontaneous heating far-infrared functional slurry, the content of each component is respectively: Graphene accounts for 0.5%, and CNT accounts for 0.5%, Fullerene accounts for 0.5%, and Polyvinylpyrrolidone or sodium carboxymethyl cellulose account for 3.5%, and tcrude ore slurry accounts for 95%.
Embodiment 4:
As different from Example 1, the heating, drying mode in step (3) selects far-infrared lamp irradiation, far-infrared lamp spoke According in far-infrared lamp power be 100-600w, heat time heating time be 5-60min.
After testing, the multifunctional physiotherapy Magnetitum based on Graphene being prepared by embodiment 1-4, its far infrared transmission Rate is 0.85-0.95, and temperature rise up to 3-6 DEG C, has more preferably spontaneous heating and far-infrared effect, can be widely applied to various guarantors In strong physical therapy product.
Above example is only in order to illustrating technical scheme, rather than is limited;Although with reference to aforementioned reality Apply example the present invention has been described in detail, for the person of ordinary skill of the art, still can be to aforementioned enforcement Technical scheme described in example is modified, or carries out equivalent to wherein some technical characteristics;And these are changed or replace Change, do not make the essence of appropriate technical solution depart from the spirit and scope of claimed technical solution of the invention.

Claims (10)

1. a kind of preparation method of the multifunctional physiotherapy Magnetitum based on Graphene it is characterised in that: comprise the following steps:
(1) tcrude ore coarse fodder is gone the removal of impurity by supersound washing, then in turn through ball mill ball milling 1-5h, more ground machine Grind 1-5h, after prepare tcrude ore slurry through levigator water mill 1-5h;
(2) put into, into high-speed shearing machine, the tcrude ore slurry that far-infrared functional auxiliary agent, dispersant and step (1) obtain, through height Speed shearing is sufficiently mixed, and obtains spontaneous heating far-infrared functional slurry;
(3) the spontaneous heating far-infrared functional slurry that step (2) obtains is carried out obtaining spontaneous heating far-infrared functional after heating, drying Powder, then spontaneous heating far infrared functional powder is pressed into spontaneous heating far-infrared functional thin rounded flakes via tablet machine, as manage Treat Magnetitum, and squeeze into buttonhole hole by the middle part of physical therapy Magnetitum.
2. the multifunctional physiotherapy Magnetitum based on Graphene according to claim 1 preparation method it is characterised in that: step (1), in, the power of supersound washing is 30-120kw, and temperature is 10-30 DEG C, and the time is 10-90min;Will be through ultrasonic in step (1) Tcrude ore coarse fodder after washing is prepared into the granule of 1-3mm through ball mill ball milling, more ground machine grinds and is prepared into 0.1-1mm Granule, after be prepared into 1-10 μm of tcrude ore slurry through levigator water mill.
3. the multifunctional physiotherapy Magnetitum based on Graphene according to claim 1 preparation method it is characterised in that: step (1) in, described tcrude ore slurry by 50-70% tourmaline slurry, the germanite slurry of 10-20%, the stone needle slurry of 10-20% and 10% silica slurry mixes;
4. the multifunctional physiotherapy Magnetitum based on Graphene according to claim 1 preparation method it is characterised in that: step (2) in, the tcrude ore slurry containing 75-95%, the far-infrared functional of 1.5-20% in described spontaneous heating far-infrared functional slurry Auxiliary agent and the dispersant of 3.5-5%.
5. the multifunctional physiotherapy Magnetitum based on Graphene according to claim 1 preparation method it is characterised in that: step (2), in, described spontaneous heating far-infrared functional slurry contains 80% tcrude ore slurry, 15% far-infrared functional auxiliary agent and 5% Dispersant.
6. the multifunctional physiotherapy Magnetitum based on Graphene according to claim 4 or 5 preparation method it is characterised in that: In step (2), described far-infrared functional auxiliary agent is any one in Graphene, CNT and fullerene, or two or more Mixed with arbitrary proportion.
7. the multifunctional physiotherapy Magnetitum based on Graphene according to claim 4 or 5 preparation method it is characterised in that: In step (2), described dispersant is any in dodecylbenzene sodium sulfonate, Polyvinylpyrrolidone and sodium carboxymethyl cellulose A kind of.
8. the multifunctional physiotherapy Magnetitum based on Graphene according to claim 1 preparation method it is characterised in that: step (3) the heating, drying mode in is dried for baking oven for heating, and the heating-up temperature of baking oven is 60-200 DEG C, and heat time heating time is 10- 90min.
9. the multifunctional physiotherapy Magnetitum based on Graphene according to claim 1 preparation method it is characterised in that: step (3) the heating, drying mode in is far-infrared lamp irradiation, and the power of the far-infrared lamp in far-infrared lamp irradiation is 100-600w, plus The hot time is 5-60min.
10. the multifunctional physiotherapy Magnetitum based on Graphene according to claim 1 preparation method it is characterised in that: step Suddenly a diameter of 5-10mm of the physical therapy Magnetitum described in (3), thickness is 2-4mm, the middle part of described physical therapy Magnetitum at least provided with Two buttonhole holes being used for the sewing of physical therapy Magnetitum on required object.
CN201610822141.0A 2016-08-31 2016-08-31 Preparation method of multifunctional physiotherapeutic magnet based on graphene Expired - Fee Related CN106362294B (en)

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Cited By (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN108892495A (en) * 2018-08-08 2018-11-27 陕西新容康医疗器械有限公司 A kind of clay granular materials and preparation method thereof that can generate far infrared
CN109164598A (en) * 2018-09-29 2019-01-08 深圳市视界之窗光学科技有限公司 A kind of stone needle glasses processing technology
CN113271693A (en) * 2020-12-23 2021-08-17 广州见正健康科技股份有限公司 Far infrared electrothermal film and its making process

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* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN103122491A (en) * 2013-02-04 2013-05-29 温州卓晟特鞋服有限公司 Process for manufacturing tourmaline fibers
CN105244117A (en) * 2015-09-29 2016-01-13 无锡同创石墨烯应用科技有限公司 Preparation method of graphene-modified reinforced far infrared conductive paste
CN105669158A (en) * 2016-01-23 2016-06-15 王秋芹 Graphene far-infrared heating coating and preparation method thereof
KR20160070621A (en) * 2014-12-10 2016-06-20 조현준 Heat belly band which combines far infrared ray emission and anti-microbial

Patent Citations (4)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN103122491A (en) * 2013-02-04 2013-05-29 温州卓晟特鞋服有限公司 Process for manufacturing tourmaline fibers
KR20160070621A (en) * 2014-12-10 2016-06-20 조현준 Heat belly band which combines far infrared ray emission and anti-microbial
CN105244117A (en) * 2015-09-29 2016-01-13 无锡同创石墨烯应用科技有限公司 Preparation method of graphene-modified reinforced far infrared conductive paste
CN105669158A (en) * 2016-01-23 2016-06-15 王秋芹 Graphene far-infrared heating coating and preparation method thereof

Cited By (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN108892495A (en) * 2018-08-08 2018-11-27 陕西新容康医疗器械有限公司 A kind of clay granular materials and preparation method thereof that can generate far infrared
CN109164598A (en) * 2018-09-29 2019-01-08 深圳市视界之窗光学科技有限公司 A kind of stone needle glasses processing technology
CN113271693A (en) * 2020-12-23 2021-08-17 广州见正健康科技股份有限公司 Far infrared electrothermal film and its making process

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