CN106344433A - Cleansing water capable of being non-irritating to eyes and preparation method thereof - Google Patents
Cleansing water capable of being non-irritating to eyes and preparation method thereof Download PDFInfo
- Publication number
- CN106344433A CN106344433A CN201610875150.6A CN201610875150A CN106344433A CN 106344433 A CN106344433 A CN 106344433A CN 201610875150 A CN201610875150 A CN 201610875150A CN 106344433 A CN106344433 A CN 106344433A
- Authority
- CN
- China
- Prior art keywords
- eye
- pleasing
- makeup
- inirritative
- makeup remover
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
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Classifications
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/72—Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds
- A61K8/84—Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds obtained by reactions otherwise than those involving only carbon-carbon unsaturated bonds
- A61K8/86—Polyethers
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/33—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing oxygen
- A61K8/34—Alcohols
- A61K8/345—Alcohols containing more than one hydroxy group
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q1/00—Make-up preparations; Body powders; Preparations for removing make-up
- A61Q1/14—Preparations for removing make-up
Abstract
The invention relates to makeup remover which is not irritating to eyes and a preparation method thereof. The makeup removing component of the makeup removing water which is not irritating to eyes comprises polyglycerol-10 laurate, di (PPG-2 myristyl polyether-10) adipate and 1, 3-propylene glycol. The preparation method comprises the following steps: s1, adding the auxiliary ingredient raw materials into a stirring pot, heating to 80-85 ℃, stirring to dissolve uniformly, then preserving heat for 30 minutes, and cooling to 40-45 ℃; s2, adding the makeup removing component raw materials into a stirring pot, and uniformly stirring and dissolving; s3, adding the preservative component raw materials into a stirring pot, and stirring and dissolving uniformly. The combination of the polyglycerol-10 laurate, the di (PPG-2 myristyl alcohol polyether-10) adipate and the 1, 3-propylene glycol can achieve the effect of efficiently removing makeup and can not excessively degrease the skin. The polyglycerol-10 laurate can fully exert the makeup removing capability under the proportion of the invention and has synergistic effect with the 1, 3-propylene glycol.
Description
Technical field
The present invention relates to household chemicals field, more particularly, to a kind of pleasing to the eye inirritative makeup remover and preparation method thereof.
Background technology
It is the nature of the mankind to beautiful pursuit, with growth in the living standard, the women of cosmetics is more and more daily, in
It is to have removed ornaments and formal dress into the critically important part of people's daily life.Makeup removing ability and mildness are evaluate makeup removal products quality two
Very important index.On the one hand it is because that the residual component of color make-up may block pore, affects skin if removing ornaments and formal dress not thorough
Skin homergy, even results in accelerated skin ageing.Another aspect makeup removal products will use around eyes, needs to eyes no
Stimulate.
Makeup remover on the market, is much to be removed ornaments and formal dress with traditional surfactant, there are many with base containing peg at present
Removing ornaments and formal dress, the makeup removing ability of both schemes is strong for the water-soluble grease (conventional is peg-6 caprylic/capric glyceride type) of group,
But not gentle, there is stimulation to eyes, and group containing peg has dioxanes residual, there is security risk.Additionally, also having
Portioned product makes makeup removing agent of poloxamer 184, and product is gentle, but makeup removing effect bad.
Content of the invention
In view of this it is necessary to for above-mentioned problem, provide a kind of pleasing to the eye inirritative makeup remover and preparation method thereof.
In order to achieve the above object, the present invention adopts below scheme:
A kind of pleasing to the eye inirritative makeup remover, makeup removing component comprises Natrulon H-10 laurate, two (ppg-2 Semen Myristicae oils
Alcohol polyethers -10) adipate ester and 1,3- propylene glycol.
Preferably, in described makeup removing component, weight percentage in pleasing to the eye inirritative makeup remover for each raw material is as follows:
Natrulon H-10 laurate 7.5～15.0%,
Two (ppg-2 Semen Myristicae oleth -10) adipate ester 0.5～5.0%,
1,3- propylene glycol 2.0～10.0%.
Preferably, described makeup removing weight percentage in pleasing to the eye inirritative makeup remover for the component is 10～30%.
Preferably, described pleasing to the eye inirritative makeup remover also comprises auxiliary agent, and each raw material of described auxiliary agent is pleasing to the eye inirritative
Weight percentage in makeup remover is as follows:
Preferably, described pleasing to the eye inirritative makeup remover also comprises preservative, and described preservative inirritative unloads pleasing to the eye
Weight percentage in adornment water is 0.1～0.3%.
It is highly preferred that the weight percentage of each component is as follows in described pleasing to the eye inirritative makeup remover:
A, makeup removing component
Natrulon H-10 laurate 10.0～15.0%,
Two (ppg-2 Semen Myristicae oleth -10) adipate ester 1.5～5%,
1,3- propylene glycol 5.0～10.0%；
B, adjuvant component
C, preservative 0.2～0.3%.
Preferably, described preservative is polyaminopropyl biguanide.Polyaminopropyl biguanide is a kind of new disinfectant sterilization and prevents
Rotten agent, can be used for skin degerming and washing contact glasses, as mild as a dove, pleasing to the eye non-stimulated.
The preparation method of above-mentioned pleasing to the eye inirritative makeup remover, comprises the steps:
S1, by adjuvant component raw material add agitated kettle in, be heated to 80-85 DEG C of stirring and dissolving uniformly afterwards be incubated 30 minutes
Afterwards, cooling down is to 40-45 DEG C；
S2, component raw material of removing ornaments and formal dress add in agitated kettle, and stirring and dissolving is uniform；
S3, by preservative component raw material add agitated kettle in, stirring and dissolving is uniformly.
The present invention compared with prior art, has the advantage that
The pleasing to the eye inirritative makeup remover of present invention ability of not only removing ornaments and formal dress is strong, also as mild as a dove, pleasing to the eye does not stimulate.In the present invention
The oils and fatss that the Natrulon H-10 laurate of use is common to color make-up have good solvability, as mild as a dove.Use in the present invention
Two (ppg-2 Semen Myristicae oleth -10) adipate ester be a kind of esters as mild as a dove, can be with Glycerin, can be notable
Reduce the zest to skin for the surfactant.Used in the present invention, 1,3- propylene glycol has good moisture, oil and carbon
Hydrogen compound altogether molten ability and also abnormal smells from the patient slight, to skin irritation very little, have certain moistening effect.
Natrulon H-10 laurate, two (ppg-2 Semen Myristicae oleth -10) adipate esters and 1,3- third in the present invention
The combination of glycol can play the effect of efficient makeup removing, again will not the excessive defat to skin.Under the ratio of the present invention polyglycereol-
10 laurates can give full play to its makeup removing ability, with 1,3-PD, synergism occurs.
Specific embodiment
In order to better illustrate the present invention, it is described further with reference to specific embodiment.Agents useful for same in the present invention
Or instrument all can be buied by market, detection method of use etc. is all known in the art.
Used in the present invention, Natrulon H-10 laurate trade name pglla 110wkc, is charkit
The product of chemical corp., is a kind of polyglycereol esters surface active agent, has hydrophilic and oleophilic double grading concurrently, has good
Emulsion dispersion property, be the surfactant as mild as a dove of natural botanical source, all can use in foods and cosmetics.
Described two (ppg-2 Semen Myristicae oleth -10) adipate ester trade name cromollienttmSce, is the product of croda company
Product, are a kind of esters as mild as a dove, can significantly reduce the zest to skin for the surfactant with Glycerin.Described
1,3- propylene glycol trade namePropanediol, is the product of dupont tate＆lyle bioproducts, is
Natural, the highly purified no tryptophol being obtained by the fermentation technology of sustainable and reproducible glucose, is good moisturizing
Agent, has certain makeup removing ability.Raw material used in adjuvant component of the present invention is the common raw material of household chemicals field, no longer describes in detail
Trade name and the place of production.
Embodiment 1
A kind of pleasing to the eye inirritative makeup remover, the weight percentage of its each component is as follows:
A, makeup removing component
Natrulon H-10 laurate 7.5%,
Two (ppg-2 Semen Myristicae oleth -10) adipate ester 0.5%,
1,3- propylene glycol 2%；
B, adjuvant component
C, preservative
Polyaminopropyl biguanide 0.2%.
The preparation method of above-mentioned pleasing to the eye inirritative makeup remover, comprises the steps:
S1, by b adjuvant component raw material add agitated kettle in, be heated to 80-85 DEG C of stirring and dissolving uniformly afterwards be incubated 30 minutes
Afterwards, cooling down is to 40-45 DEG C；
S2, component raw material that a removes ornaments and formal dress add in agitated kettle, and stirring and dissolving is uniform；
S3, by c preservative component raw material add agitated kettle in, stirring and dissolving is uniformly.
Embodiment 2
A kind of pleasing to the eye inirritative makeup remover, the weight percentage of its each component is as follows:
A, makeup removing component
Natrulon H-10 laurate 10%,
Two (ppg-2 Semen Myristicae oleth -10) adipate ester 2.5%,
1,3- propylene glycol 7%；
B, adjuvant component
C, preservative
Polyaminopropyl biguanide 0.2%.
In the present embodiment, the preparation method of pleasing to the eye inirritative makeup remover is same as Example 1.
Embodiment 3
A kind of pleasing to the eye inirritative makeup remover, the weight percentage of its each component is as follows:
A, makeup removing component
Natrulon H-10 laurate 15%,
Two (ppg-2 Semen Myristicae oleth -10) adipate ester 5%,
1,3- propylene glycol 10%；
B, adjuvant component
C, preservative
Polyaminopropyl biguanide 0.2%.
In the present embodiment, the preparation method of pleasing to the eye inirritative makeup remover is same as Example 1.
Comparative example 1
A kind of makeup remover, the weight percentage of its each component is as follows:
A, makeup removing component
Natrulon H-10 laurate 15%,
Two (ppg-2 Semen Myristicae oleth -10) adipate ester 5%,
B, adjuvant component
C, preservative
Polyaminopropyl biguanide 0.2%.
In this comparative example, the preparation method of makeup remover is same as Example 1.
Comparative example 2
A kind of makeup remover, the weight percentage of its each component is as follows:
A, makeup removing component
Two (ppg-2 Semen Myristicae oleth -10) adipate ester 5%,
1,3- propylene glycol 10%；
B, adjuvant component
C, preservative
Polyaminopropyl biguanide 0.2%.
In this comparative example, the preparation method of makeup remover is same as Example 1.
Comparative example 3
A kind of makeup remover, the weight percentage of its each component is as follows:
A, makeup removing component
Natrulon H-10 laurate 15%,
1,3- propylene glycol 10%；
B, adjuvant component
C, preservative
Polyaminopropyl biguanide 0.2%.
In this comparative example, the preparation method of makeup remover is same as Example 1.
For the ease of comparing, will be as follows for the composition list 1 of each embodiment and comparative example.
The formula of makeup remover in table 1, each embodiment and comparative example
Effect example 1, physical and chemical testing
Physical and chemical testing is done to the makeup remover of each embodiment, the method for testing of each physical and chemical index is that those skilled in the art institute is ripe
Know, will not be described here.Test result is as follows:
Outward appearance: transparency liquid；Ph value: 5.5-7.5；Heat-resistant stability investigates (48 DEG C × 24h): qualified；Cold-resistant stability
Investigate (- 15 DEG C × 24h): qualified.
Makeup remover of the present invention items physical and chemical index is qualified from the above results, heat-resisting, cold-resistant has good stability.
Effect example 2, security test
Choose 10 voluntary testers, to do comparison test inside left and right arm, apply the present invention inside left hand every time and produce
Product 0.5g, applies deionized water 0.5g inside the right hand, twice daily, and records the dermoreaction phenomenon after 24h, 72h.
After applying product 24h, 72h of the present invention, have no skin rubefaction or the allergic phenomenas such as erythema occur, illustrate that the present invention is pleasing to the eye
Inirritative makeup remover is safe, does not have any bad phenomenon.
Effect example 3, the stimulation test of human eye
Makeup remover in the various embodiments described above and comparative example is diluted to respectively 10% solution, and is maintained at
37-38℃.This test material Deca 2 is dripped in the left eye of tester, then the deionized water sterilized Deca 2 is dripped to survey
In the right eye of examination person.Complete the Deca of eyes in 20 seconds, get rid of the experimenter of sensory stimuli after Deca deionization, record test
The feedback of person, 10 testers of each sample test.The stimulation test test result of human eye is shown in Table 2.
Table 2, the stimulation test test result of human eye
As shown in Table 2,70% tester is non-stimulated to the pleasing to the eye inirritative makeup remover in embodiment 1,20% survey
Examination person feels very slight stimulation to the pleasing to the eye inirritative makeup remover in embodiment 1, and 10% tester is in embodiment 1
Pleasing to the eye inirritative makeup remover feel medium stimulation.90% tester is to the pleasing to the eye inirritative makeup remover in embodiment 2
Non-stimulated, 10% tester feels very slight stimulation to the pleasing to the eye inirritative makeup remover in embodiment 1.100%
Tester is non-stimulated to the pleasing to the eye inirritative makeup remover in embodiment 3.Do not have tester that the pleasing to the eye of embodiment 1-3 is not stimulated
Makeup remover feel seriously to stimulate.
100% tester is non-stimulated to the makeup remover in comparative example 1 and comparative example 2.50% tester is to comparative example 3
In makeup remover non-stimulated, 30% tester feels very slight stimulation, 20% test to the makeup remover in comparative example 3
Person feels medium stimulation to the makeup remover in comparative example 3.Do not have tester that the makeup remover of comparative example 1-3 is felt seriously to stimulate.
Effect example 4, makeup removing effect test:
Makeup remover in the various embodiments described above and comparative example is used for the removal of facial color make-up, records the feedback of tester,
10 testers of each sample test.The test result of makeup removing effect is shown in Table 3.
Table 3, the test result of makeup removing effect
| Numbering | Makeup removing effect is good | Makeup removing effect is general | Makeup removing effect is not good |
| Embodiment 1 | 8 people (80%) | 2 people (20%) | 0 people |
| Embodiment 2 | 9 people (90%) | 1 people (10%) | 0 people |
| Embodiment 3 | 10 people (100%) | 0 people | 0 people |
| Comparative example 1 | 7 people (70%) | 2 people (20%) | 1 people (10%) |
| Comparative example 2 | 0 people | 7 people (70%) | 3 people (30%) |
| Comparative example 3 | 10 people (100%) | 0 people | 0 people |
As shown in table 3,80% tester thinks that the makeup removing effect of pleasing to the eye inirritative makeup remover in embodiment 1 is good,
20% tester thinks that the makeup removing effect of pleasing to the eye inirritative makeup remover in embodiment 1 is general.90% tester thinks real
The makeup removing effect applying pleasing to the eye inirritative makeup remover in example 2 is good, and 10% tester thinks pleasing to the eye in embodiment 2 and inirritative unloads
The makeup removing effect of adornment water is general.100% tester thinks that the makeup removing effect of pleasing to the eye inirritative makeup remover in embodiment 3 is good.
No tester thinks that the makeup removing effect of pleasing to the eye inirritative makeup remover in embodiment 1-3 is not good.
70% tester thinks that the makeup removing effect of makeup remover in comparative example 1 is good, and 20% tester thinks in comparative example 1
The makeup removing effect of makeup remover is general, and 10% tester thinks that the makeup removing effect of makeup remover in comparative example 1 is not good.No tester recognizes
Good for the makeup removing effect of makeup remover in comparative example 2,70% tester thinks that the makeup removing effect of makeup remover in comparative example 2 is general,
30% tester thinks that the makeup removing effect of makeup remover in comparative example 2 is not good.100% tester thinks makeup removing in embodiment 3
The makeup removing effect of water is good.
As shown in table 2 and table 3, comparative example 3 mildness is not good enough, and comparative example 1 and comparative example 2 makeup removing ability be not good enough, and uses
It is good that the tester of the pleasing to the eye inirritative makeup remover of embodiment feeds back the gentle makeup removing effect of product, and two (ppg-2 Semen Myristicae oils are described
Alcohol polyethers -10) adipate ester can substantially reduce the zest of product, and Natrulon H-10 laurate and 1,3-PD compound
The makeup removing effect using is better than and is used alone.
Embodiment described above only have expressed the several embodiments of the present invention, and its description is more concrete and detailed, but simultaneously
Therefore the restriction to the scope of the claims of the present invention can not be interpreted as.It should be pointed out that for those of ordinary skill in the art
For, without departing from the inventive concept of the premise, some deformation can also be made and improve, these broadly fall into the guarantor of the present invention
Shield scope.Therefore, the protection domain of patent of the present invention should be defined by claims.
Claims (8)
1. a kind of pleasing to the eye inirritative makeup remover is it is characterised in that makeup removing component comprises Natrulon H-10 laurate, two (ppg-
2 Semen Myristicae oleth -10) adipate ester and 1,3- propylene glycol.
2. pleasing to the eye inirritative makeup remover according to claim 1 is not it is characterised in that described makeup removing component is pierced pleasing to the eye
Weight percentage in sharp makeup remover is 10～30%.
3. pleasing to the eye inirritative makeup remover according to claim 2 it is characterised in that in described makeup removing component each raw material exist
Weight percentage in pleasing to the eye inirritative makeup remover is as follows:
Natrulon H-10 laurate 7.5～15.0%,
Two (ppg-2 Semen Myristicae oleth -10) adipate ester 0.5～5.0%,
1,3- propylene glycol 2.0～10.0%.
4., it is characterised in that also comprising auxiliary agent, described auxiliary agent is each for pleasing to the eye inirritative makeup remover according to claim 1
Weight percentage in pleasing to the eye inirritative makeup remover for the raw material is as follows:
5. pleasing to the eye inirritative makeup remover according to claim 4 is it is characterised in that also comprising preservative, described anti-corrosion
Weight percentage in pleasing to the eye inirritative makeup remover for the agent is 0.1～0.3%.
6. pleasing to the eye inirritative makeup remover according to claim 5 is it is characterised in that described pleasing to the eye inirritative makeup remover
In each component weight percentage as follows:
A, makeup removing component
Natrulon H-10 laurate 10.0～15.0%,
Two (ppg-2 Semen Myristicae oleth -10) adipate ester 1.5～5%,
1,3- propylene glycol 5.0～10.0%；
B, adjuvant component
C, preservative 0.2～0.3%.
7. pleasing to the eye inirritative makeup remover according to claim 1 is it is characterised in that described preservative is poly- aminopropyl pair
Guanidine.
8. the preparation method of pleasing to the eye inirritative makeup remover described in any one of claim 1-7, comprises the steps:
S1, by adjuvant component raw material add agitated kettle in, be heated to 80-85 DEG C of stirring and dissolving uniformly afterwards insulation 30 minutes after, fall
Temperature is cooled to 40-45 DEG C；
S2, component raw material of removing ornaments and formal dress add in agitated kettle, and stirring and dissolving is uniform；
S3, by preservative component raw material add agitated kettle in, stirring and dissolving is uniformly.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201610875150.6A CN106344433A (en) | 2016-09-30 | 2016-09-30 | Cleansing water capable of being non-irritating to eyes and preparation method thereof |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201610875150.6A CN106344433A (en) | 2016-09-30 | 2016-09-30 | Cleansing water capable of being non-irritating to eyes and preparation method thereof |
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| Publication Number | Publication Date |
|---|---|
| CN106344433A true CN106344433A (en) | 2017-01-25 |
Family
ID=57866152
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN201610875150.6A Pending CN106344433A (en) | 2016-09-30 | 2016-09-30 | Cleansing water capable of being non-irritating to eyes and preparation method thereof |
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Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN110151606A (en) * | 2019-06-19 | 2019-08-23 | 上海美浮特生物科技有限公司 | A kind of pure natural cleansing composition and preparation method thereof |
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Application publication date: 20170125 |