CN106338314A - Control method for powdery solid material metering - Google Patents

Control method for powdery solid material metering Download PDF

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Publication number
CN106338314A
CN106338314A CN201610840464.2A CN201610840464A CN106338314A CN 106338314 A CN106338314 A CN 106338314A CN 201610840464 A CN201610840464 A CN 201610840464A CN 106338314 A CN106338314 A CN 106338314A
Authority
CN
China
Prior art keywords
valve
magnesium silicide
tank
metering
magnesium
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Pending
Application number
CN201610840464.2A
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Chinese (zh)
Inventor
李耀文
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
Beijing Sida Chemical Equipment Co Ltd
Original Assignee
Beijing Sida Chemical Equipment Co Ltd
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Beijing Sida Chemical Equipment Co Ltd filed Critical Beijing Sida Chemical Equipment Co Ltd
Priority to CN201610840464.2A priority Critical patent/CN106338314A/en
Publication of CN106338314A publication Critical patent/CN106338314A/en
Pending legal-status Critical Current

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Classifications

    • GPHYSICS
    • G01MEASURING; TESTING
    • G01FMEASURING VOLUME, VOLUME FLOW, MASS FLOW OR LIQUID LEVEL; METERING BY VOLUME
    • G01F11/00Apparatus requiring external operation adapted at each repeated and identical operation to measure and separate a predetermined volume of fluid or fluent solid material from a supply or container, without regard to weight, and to deliver it
    • G01F11/28Apparatus requiring external operation adapted at each repeated and identical operation to measure and separate a predetermined volume of fluid or fluent solid material from a supply or container, without regard to weight, and to deliver it with stationary measuring chambers having constant volume during measurement

Abstract

The invention relates to a control method for powdery solid material metering. The control method comprises the following steps of: 1) feeding magnesium silicide, namely opening a valve K3, then opening a valve K1, and regulating a valve F1 to a proper opening so as to ensure that a magnesium silicide solid can be fed into a magnesium silicide metering tank from a magnesium silicide storage tank; 2) metering magnesium silicide, namely giving out an alarm by a high-level sensor L1 of the magnesium silicide metering tank, closing the valve K1 at the moment, and closing the valve K3 and the valve F1 in delay time; and 3), discharging magnesium silicide, namely firstly opening a valve K4, then opening a valve K2 and a valve K5, discharging the magnesium silicide solid into a magnesium silicide buffer tank through the magnesium silicide metering tank, giving out an alarm by a low-level sensor L2 of the magnesium silicide metering tank, closing the valve K2 at the moment, and then closing the valve K4 and the valve K5 in delay time. The quantity of magnesium silicide is metered by virtue of the constant volume of the magnesium silicide metering tank, so that the problem of metering a powdery solid material is effectively solved, the equipment is durable, and abrasion to an air-locking control valve is reduced.

Description

A kind of control method of powdery solid material metering
[technical field]
The present invention relates to a kind of metering method, and in particular to a kind of control method of powdery solid material metering, belongs to silicon Alkane gas production technical field.
[background technology]
Silane gas can be used for producing polysilicon, monocrystal silicon, silicon nitride and other silicides.With magnesium silicide and ammonium chloride it is Raw material, liquefied ammonia be Media Production silane gas method because reaction yield height, process is simple, equipment investment lack the features such as enjoy pass Note.And the magnesium silicide as silicon source needs accurately to measure.
Magnesium silicide density 1.943g/cm3, is hard and crisp blue colored crystal, very strong not in contact with activity during air, in atmosphere Friction may occur from firing, and magnesium silicide has certain hardness, pipe fitting and valve can be caused to wear and tear during conveying.
The metering of general pressed powder uses weighs or volumetric method.Will be on measuring tank with regard to this technique magnesium silicide Weighing LOAD CELLS is installed, all pipelines being connected with tank body need to be installed and be flexible coupling.Purpose in order to reach accurate metering needs to select With the LOAD CELLS of high precision, increased equipment cost, and install and be also subject to certain restrictions.
Therefore, for solving above-mentioned technical problem, it is necessory to provide a kind of control of the powdery solid material metering of innovation Method, to overcome described defect of the prior art.
[content of the invention]
It is an object of the invention to provide a kind of control method of powdery solid material metering, it passes through using measuring tank pair The change of equipment working forms, reaches the abrasion reducing Solid-state valve, and can achieve simply accurately measuring of powdery solid.
For achieving the above object, the technical scheme that the present invention takes is: a kind of control method of powdery solid material metering, It adopts a kind of metering system, and this system includes magnesium silicide storage tank, magnesium silicide measuring tank and the magnesium silicide buffering being sequentially connected Tank;It is provided with valve k1 and valve k3 from top to bottom between described magnesium silicide storage tank and magnesium silicide measuring tank;Described magnesium silicide storage tank It is additionally provided with an offgas duct and magnesium silicide measuring tank between, offgas duct is provided with valve f1;The top of described magnesium silicide measuring tank sets There is high charge level sensor l1, bottom is provided with low level sensor l2;Between described magnesium silicide measuring tank and magnesium silicide surge tank certainly Upper and under be sequentially provided with valve k2 and valve k4;It is additionally provided with a valve between described magnesium silicide surge tank and magnesium silicide measuring tank k5;
It includes following rate-determining steps:
1), magnesium silicide charging, Open valve k3, are then then turned on valve k1, and control valve f1, to suitable aperture, make Magnesium silicide solid is by magnesium silicide storage tank blanking to magnesium silicide measuring tank;
2), magnesium silicide metering, magnesium silicide measuring tank high charge level sensor l1 reports to the police, and now closes valve k1, then time delay is closed Valve closing door k3 and valve f1.
3), magnesium silicide discharging, first turns on valve k4, is then turned on valve k2 and valve k5, magnesium silicide solid is by silication Magnesium measuring tank blanking is to magnesium silicide surge tank;Magnesium silicide measuring tank low level sensor l2 reports to the police, and now closes valve k2, then Valve closed with time delay k4 and valve k5.
The control method of the powdery solid material metering of the present invention is further: described high charge level sensor l1 connects and controls Make described valve k1;Described low level sensor l2 connects and controls described valve valve k2.
The control method of the powdery solid material metering of the present invention is also: described step 2) and 3) delay time be 5s.
Compared with prior art, the invention has the following beneficial effects: the control of the powdery solid material metering of the present invention Method measures the amount of magnesium silicide by the constant volume of magnesium silicide measuring tank, and the metering efficiently solving powdery solid material is asked Topic, this equipment durable, decrease the abrasion to lock gas control valve door, extend the normal time producing.
[brief description]
Fig. 1 is the structural representation of the powdery solid material measuring system of the present invention.
[specific embodiment]
Refer to shown in Figure of description 1, the present invention is a kind of control method of powdery solid material metering, using one kind Metering system, this system includes magnesium silicide storage tank 1, magnesium silicide measuring tank 2 and the magnesium silicide surge tank 3 being sequentially connected.
It is provided with valve k1 and valve k3 from top to bottom, valve k1 uses between described magnesium silicide storage tank 1 and magnesium silicide measuring tank 2 To close solid material, valve k3 is used for locking gas, sends start stop signal by control system.Described magnesium silicide storage tank 1 and magnesium silicide It is additionally provided with an offgas duct 4, offgas duct 4 is provided with valve f1, valve f1 controls aperture by control system between measuring tank 2, thus Control capacity
It is sequentially provided with valve k2 and valve k4, valve from top to bottom between described magnesium silicide measuring tank 2 and magnesium silicide surge tank 3 Door k2 is used for closing solid material, and valve k4 is used for locking gas, sends start stop signal by control system.Described magnesium silicide surge tank 3 It is additionally provided with a valve k5 and magnesium silicide measuring tank 2 between, valve k5 is used for two pressure inside the tanks when balancing magnesium silicide discharging, by controlling System sends start stop signal.
The top of described magnesium silicide measuring tank 2 is provided with high charge level sensor l1, and bottom is provided with low level sensor l2, high material Level sensor l1 and low level sensor l2 is contacting and separating triggering by material, and signal is fed back to control system.Described height Level sensor l1 connects and controls described valve k1;Described low level sensor l2 connects and controls described valve valve k2.
The control method of the powdery solid material metering of the present invention comprises the steps:
1), magnesium silicide charging, Open valve k3, are then then turned on valve k1, and control valve f1, to suitable aperture, make Magnesium silicide solid is by magnesium silicide storage tank 1 blanking to magnesium silicide measuring tank 2;
2), magnesium silicide metering, magnesium silicide measuring tank 2 high charge level sensor l1 reports to the police, and now closes valve k1, then time delay is closed Valve closing door k3 and valve f1.
3), magnesium silicide discharging, first turns on valve k4, is then turned on valve k2 and valve k5, magnesium silicide solid is by silication Magnesium measuring tank 2 blanking is to magnesium silicide surge tank 3;The low level sensor l2 of magnesium silicide measuring tank 2 reports to the police, and now closes valve K2, then valve closed with time delay k4 and valve k5
Due to will first pass through valve k1 and valve k3 when magnesium silicide feeds, in the case of having material, opening/shutting valve can be to close Front cover causes to damage.First Open valve k3 is then turned on valve k1, prevents from damaging the valve k3 as lock gas effect.And regulating valve The suitable aperture of door f1, prevents a large amount of dust from discharging.
Magnesium silicide metering when, high charge level sensor l1 report to the police after valve closed with time delay k1 it is ensured that in measuring tank 2 material fill Accurate measurement, system is thrown and automatically controlled rear delay time is 10s.Valve k1 valve closed with time delay is more first closed when closing valve K3, delay time is 5s.
During magnesium silicide discharging, Open valve k5 balances the pressure in magnesium silicide measuring tank 2 and surge tank 3, makes blanking smooth. Low level sensor l2 report to the police after valve closed with time delay k2 it is ensured that material emptying in tank, system is thrown and is automatically controlled rear delay time For 10s.It is ensured that pipeline material emptying, delay time is 5s to valve closed with time delay k4 again.
Above specific embodiment is only the preferred embodiment of this creation, not in order to limit this creation, all in this wound Any modification, equivalent substitution and improvement of being done etc. within the spirit made and principle, should be included in this creation protection domain it Interior.

Claims (3)

1. a kind of control method of powdery solid material metering it is characterised in that: it adopts a kind of metering system, and this system includes Magnesium silicide storage tank, magnesium silicide measuring tank and the magnesium silicide surge tank being sequentially connected;Described magnesium silicide storage tank and magnesium silicide metering It is provided with valve k1 and valve k3 from top to bottom between tank;It is additionally provided with a tail gas between described magnesium silicide storage tank and magnesium silicide measuring tank Pipe, offgas duct is provided with valve f1;The top of described magnesium silicide measuring tank is provided with high charge level sensor l1, and bottom is provided with low material position Sensor l2;It is sequentially provided with valve k2 and valve k4 from top to bottom between described magnesium silicide measuring tank and magnesium silicide surge tank;Institute State and between magnesium silicide surge tank and magnesium silicide measuring tank, be additionally provided with a valve k5;
It includes following rate-determining steps:
1), magnesium silicide charging, Open valve k3, are then then turned on valve k1, and control valve f1, to suitable aperture, make silication Magnesium solid is by magnesium silicide storage tank blanking to magnesium silicide measuring tank;
2), magnesium silicide metering, magnesium silicide measuring tank high charge level sensor l1 reports to the police, and now closes valve k1, then time-delay shutting valve Door k3 and valve f1;
3), magnesium silicide discharging, first turns on valve k4, is then turned on valve k2 and valve k5, magnesium silicide solid is by magnesium silicide meter Measuring tank blanking is to magnesium silicide surge tank;Magnesium silicide measuring tank low level sensor l2 reports to the police, and now closes valve k2, then time delay Close valve k4 and valve k5.
2. powdery solid material metering as claimed in claim 1 control method it is characterised in that: described high charge level sensor L1 connects and controls described valve k1;Described low level sensor l2 connects and controls described valve valve k2.
3. powdery solid material metering as claimed in claim 1 control method it is characterised in that: described step 2) and 3) Delay time is 5s.
CN201610840464.2A 2016-09-21 2016-09-21 Control method for powdery solid material metering Pending CN106338314A (en)

Priority Applications (1)

Application Number Priority Date Filing Date Title
CN201610840464.2A CN106338314A (en) 2016-09-21 2016-09-21 Control method for powdery solid material metering

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
CN201610840464.2A CN106338314A (en) 2016-09-21 2016-09-21 Control method for powdery solid material metering

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CN106338314A true CN106338314A (en) 2017-01-18

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Cited By (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN107883189A (en) * 2017-11-17 2018-04-06 金川集团股份有限公司 A kind of metering method of metering device and carbonyl liquid in carbonylation metallurgical production

Citations (6)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
JP2000065621A (en) * 1998-08-20 2000-03-03 Nippon Steel Corp Powder dispensing device
CN202562541U (en) * 2012-04-17 2012-11-28 浙江万盛新型材料有限公司 Intelligent display device for material in storage bin
CN102815708A (en) * 2012-08-10 2012-12-12 中国恩菲工程技术有限公司 Silicon tetrachloride hydrogenation reaction device and solid raw material continuous feeding device thereof
CN203065406U (en) * 2013-01-12 2013-07-17 山东寿光鲁清石化有限公司 Catalyst metering adding device
CN204338122U (en) * 2014-11-12 2015-05-20 茂名西南石化机械设备有限公司 A kind of catalyst automatic feeding apparatus
CN104650677A (en) * 2013-11-22 2015-05-27 广东美涂士建材股份有限公司 Distributive green environmentally-friendly paint manufacturing system

Patent Citations (6)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
JP2000065621A (en) * 1998-08-20 2000-03-03 Nippon Steel Corp Powder dispensing device
CN202562541U (en) * 2012-04-17 2012-11-28 浙江万盛新型材料有限公司 Intelligent display device for material in storage bin
CN102815708A (en) * 2012-08-10 2012-12-12 中国恩菲工程技术有限公司 Silicon tetrachloride hydrogenation reaction device and solid raw material continuous feeding device thereof
CN203065406U (en) * 2013-01-12 2013-07-17 山东寿光鲁清石化有限公司 Catalyst metering adding device
CN104650677A (en) * 2013-11-22 2015-05-27 广东美涂士建材股份有限公司 Distributive green environmentally-friendly paint manufacturing system
CN204338122U (en) * 2014-11-12 2015-05-20 茂名西南石化机械设备有限公司 A kind of catalyst automatic feeding apparatus

Cited By (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN107883189A (en) * 2017-11-17 2018-04-06 金川集团股份有限公司 A kind of metering method of metering device and carbonyl liquid in carbonylation metallurgical production

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