CN106333206A - Method for preparing momordica grosvenor juice with honey taste - Google Patents
Method for preparing momordica grosvenor juice with honey taste Download PDFInfo
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- CN106333206A CN106333206A CN201610737621.7A CN201610737621A CN106333206A CN 106333206 A CN106333206 A CN 106333206A CN 201610737621 A CN201610737621 A CN 201610737621A CN 106333206 A CN106333206 A CN 106333206A
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- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
- A23L—FOODS, FOODSTUFFS, OR NON-ALCOHOLIC BEVERAGES, NOT COVERED BY SUBCLASSES A21D OR A23B-A23J; THEIR PREPARATION OR TREATMENT, e.g. COOKING, MODIFICATION OF NUTRITIVE QUALITIES, PHYSICAL TREATMENT; PRESERVATION OF FOODS OR FOODSTUFFS, IN GENERAL
- A23L2/00—Non-alcoholic beverages; Dry compositions or concentrates therefor; Their preparation
- A23L2/385—Concentrates of non-alcoholic beverages
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- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
- A23L—FOODS, FOODSTUFFS, OR NON-ALCOHOLIC BEVERAGES, NOT COVERED BY SUBCLASSES A21D OR A23B-A23J; THEIR PREPARATION OR TREATMENT, e.g. COOKING, MODIFICATION OF NUTRITIVE QUALITIES, PHYSICAL TREATMENT; PRESERVATION OF FOODS OR FOODSTUFFS, IN GENERAL
- A23L2/00—Non-alcoholic beverages; Dry compositions or concentrates therefor; Their preparation
- A23L2/70—Clarifying or fining of non-alcoholic beverages; Removing unwanted matter
- A23L2/72—Clarifying or fining of non-alcoholic beverages; Removing unwanted matter by filtration
- A23L2/74—Clarifying or fining of non-alcoholic beverages; Removing unwanted matter by filtration using membranes, e.g. osmosis, ultrafiltration
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- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
- A23L—FOODS, FOODSTUFFS, OR NON-ALCOHOLIC BEVERAGES, NOT COVERED BY SUBCLASSES A21D OR A23B-A23J; THEIR PREPARATION OR TREATMENT, e.g. COOKING, MODIFICATION OF NUTRITIVE QUALITIES, PHYSICAL TREATMENT; PRESERVATION OF FOODS OR FOODSTUFFS, IN GENERAL
- A23L2/00—Non-alcoholic beverages; Dry compositions or concentrates therefor; Their preparation
- A23L2/70—Clarifying or fining of non-alcoholic beverages; Removing unwanted matter
- A23L2/80—Clarifying or fining of non-alcoholic beverages; Removing unwanted matter by adsorption
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Abstract
The invention discloses a method for preparing momordica grosvenor juice with honey taste and belongs to the technical field of natural product application. The method comprises the steps of (1) choosing raw material; (2) extracting; (3) passing adsorption resin column; (4) transmembrane; (5) concentration; (6) decoloration; (7) adjusting PH; (8) concentration. Through the steps of low temperature storage after-ripening of momordica grosvenor, low temperature extracting by adding pectinase, passing absorption resin column, membrane filtration, concentration, decoloration, adjusting PH and the like on the basis of not affecting production of mogroside V, momordica grosvenor juice with honey taste is prepared from waste liquor which pollutes environment if directly discharged, thus environmental pollution is reduced and applied range of momordica Grosvenor is widened.
Description
Technical field
The present invention relates to a kind of preparation method of honey taste arhat juice, belong to natural products applied technical field.
Background technology
Momordica grosvenori, is the ripening fruits of China's distinctive preciousness cucurbitaceous plant Momordica grosvenori, and autumn fruit is deepened by light green
Pluck when green.Momordica grosvenori have the title of the good fruit of good medicine, of many uses, and enjoy a good market both at home and abroad market, enjoys very high in the international market
Reputation.Mainly originate in the mountain area of lingui county,gui lin and Yongfu county, be the famous and precious local and special products in Guilin.
With the application of Modern New Technology, also people constantly further investigate, the base of the dry fruit applied always in ancient times
On plinth, develop Momordica-Glycosides v dry powder and grosvenor momordica fruit juice, expand the application of Momordica grosvenori.
Arhat juice is to be processed through the technique such as extracting, refining, concentrate with Momordica grosvenori, a kind of arhat produced
The thick fruit juice in fruity road, rich in compositions such as mogroside v, amino acid, vitamin, monose.
Chinese invention patent Authorization Notice No. is a kind of " method for preparing grosvenor momordica fruit juice " of cn1303914c, discloses one
Plant the preparation method of grosvenor momordica fruit juice, by three centrifugal filtration separation, ebuillition of heated, removing off-flavor precursors material, sheet frame pressure
The steps such as filter, addition preservative, micro-pore-film filtration, nanofiltration concentration, produce arhat juice.Its shortcoming is complex process, face
Color depth, the fruit juice sugariness produced are larger.
Existing arhat juice, mainly has fresh fruit fruit juice and dry fruit fruit juice.The sweet glucoside of fresh fruit fruit juice is higher, after being suitable for dilution
It is added in product.And dry fruit juice color is deep, the bitter smell of burning is heavier, is suitable for being applied in dark product.
Decolouring arhat juice is to extract concentration desolventing technology by fresh fruit to obtain, and sweet Momordica grosvenori salidroside content is than common fruit juice more
Height, directly edible sugariness is excessively sweet, is suitable for addition in light-colored product.
Existing Momordica grosvenori production technology, mainly point two classes, i.e. separately Momordica-Glycosides and produce full fruit juice, seldom there is synthesis
Using the research producing waste liquid, waste residue after Momordica-Glycosides.
In consideration of it, being necessary to develop a kind of preparation method of new grosvenor momordica fruit juice, to make up the deficiencies in the prior art.
Content of the invention
Present invention aim to address the deficiencies in the prior art, provide a kind of preparation method of honey taste arhat juice.
The present invention pass through Momordica grosvenori low tempertaure storage after-ripening, plus pectase low temperature extract, cross adsorption resin column, membrane filtration, concentration, decolouring,
The steps such as adjustment ph, the waste liquid of direct exhaust emission environment is produced a kind of arhat juice of honey taste, is decreased environment
Pollution, expands the range of application of arhat juice.
The technical scheme is that a kind of preparation method of honey taste arhat juice,
Comprise the steps:
(1) raw material selection: selected ripe, complete fresh fructus momordicae, place 60-120 days in 3-5 DEG C, obtain sieve of after-ripening
Chinese fruit；
(2) extract: the Momordica grosvenori of the after-ripening that step (1) is obtained, clean up, crush, plus the Momordica grosvenori of described after-ripening
The deionized water of 2-4 times of weight, the pectase of the Momordica grosvenori 0.1-0.3% weight of described after-ripening, extract 1- in 45-50 DEG C of stirring
2 hours, filter, obtain an extract and once extract slag；Again to the 2-4 times of weight of Momordica grosvenori once extracting slag and adding described after-ripening
Deionized water, in 45-50 DEG C stirring extract 1-2 hour, filter, obtain secondary raffinate, by an extract and second extraction
Liquid merges, and obtains Momordica grosvenori extract；
(3) cross adsorption resin column: the Momordica grosvenori extract that step (2) is obtained, cross adsorption resin column, by extract and suction
The weight of the polymeric adsorbent in attached resin column enters post than for 5-6:1, and flow velocity 1.5-2.0bv/h, with described Momordica grosvenori extract 6-8
The washing adsorption resin column of times weight, flow velocity 1.5-2.0bv/h, collects efflux and water lotion, merges into liquid one；Again with inhaling
The mass fraction of the 2.5 times of weight of polymeric adsorbent in attached resin column is 60% ethanol-eluting resin column, flow velocity 1.5-2.0bv/
H, collects eluent, concentrates, and is dried, obtains mogroside v dry powder；
(4) cross film: the liquid one that step (3) is obtained, cross ceramic membrane, then the washing pottery with one 0.5 times of weight of liquid
Film, collects and obtained film liquid；
(5) concentrate: the mistake film liquid that step (4) is obtained, cross reverse osmosis membrane, be concentrated into 4-6 Brix Scale, concentrated
Liquid；
(6) decolour: the concentrate that step (5) is obtained, cross decolorizing resin post, by the weight ratio of concentrate and decolorizing resin
2:1 enters post, flow velocity 0.5-1.5bv/h, then plus the water of 6 times of decolorizing resin weight washed, flow velocity 0.5-1.5bv/h, obtain
Destainer；
(7) adjust ph: take the destainer that 1/3 step (6) obtains to cross cationic resin column, by described after-ripening Momordica grosvenori and
The weight of the resin cation in cationic resin column enters post, flow velocity 5.0-6.0bv/h, then plus described cation tree than for 3:1
The water of 2-4 times of weight of fat is washed, and the destainer being obtained with 2/3 step (6) is merged, and adjusts ph5.0-5.5, obtains liquid
Two；
(8) concentrate: the liquid two that step (7) is obtained, first cross reverse osmosis membrane, be concentrated into 4-6 Brix Scale, then at≤70
DEG C it is concentrated in vacuo to 68-70 Brix Scale, that is, obtain described honey taste arhat juice.
Momordica grosvenori is first carried out low tempertaure storage after-ripening by the step (1) of the present invention, by fresh fructus momordicae in 3-5 DEG C, places 60-
120 days, fresh fructus momordicae after-ripening can be made, place storage for a long time through low temperature, and then produce honey taste.Step (3) will again
The efflux crossing polymeric adsorbent during producing mogroside v carries out reclaiming processing.Wherein, the mogroside v dry powder obtaining, be
It is worth highest part in Momordica grosvenori, is main sweet substance in Momordica grosvenori, be that Momordica grosvenori comprehensively produces the emphasis collected.
The present invention by the waste liquid of typically directly exhaust emission environment in prior art, through low tempertaure storage after-ripening, extraction, mistake
The production stages such as polymeric adsorbent, membrane filtration, concentration, decolouring, adjustment ph, produce and obtain a kind of arhat juice of honey taste.Step
Suddenly (7), main purpose is adjustment ph value, and destainer shows alkalescence, and after crossing cation, liquid shows acidity, and two parts can reach after merging
To the ph value (5.0-5.5) needing it is not necessary to adjust ph value with citric acid, keep the pure natural property of product.Step (8), because
Film thickening temperature is low, concentrates speed soon, keeps effect good product colour, local flavor, but concentration is not thick.And concentrated in vacuo,
Long-time concentration easily causes variable color, but can concentrate very thick.By counter-infiltration and both combinations concentrated in vacuo, product can be made
Product color, local flavor, concentration reach requirement.
The honey taste arhat juice of the present invention, taste is lighter than full arhat juice, in good taste, of light color, Momordica grosvenori taste
Light, directly can drink without dilution, expand the range of application of arhat juice, deepen the overall availability of Momordica grosvenori.
On the basis of technique scheme, the present invention can also do following improvement.
Further, the enzyme activity ＞ 40000u/g of the described pectase of step (2).
Using above-mentioned further beneficial effect it is: enzyme activity ＞ 40000u/g, Momordica grosvenori pectin can be made to digest, make fruit juice clear
Clearly.
Further, model d101 of the described adsorption resin column of step (3).
Using above-mentioned further beneficial effect it is: can separately obtain mogroside v and other nutritive effect materials, such as
Vitamin, monose, polysaccharide, polypeptide etc..
Further, the particle diameter of the described ceramic membrane of step (4) is 0.45 μm.
Further, model lx-700b of the described decolorizing resin post of step (6).
Further, the described resin cation of step (7) is highly acid.
Using above-mentioned further beneficial effect it is: for adjusting fruit juice ph value.
Further, the model 001 × 7 of described resin cation.
Further, state described in step (8) in honey taste arhat juice, the weight content of mogroside v is 0.05-
0.5%, ph4.5-6.0, light transmittance ＞ 95%.
Using above-mentioned further beneficial effect it is: low temperature concentrates it is ensured that juice color, mouthfeel, taste.
The invention has the beneficial effects as follows:
(1) Momordica grosvenori is first carried out low tempertaure storage after-ripening by the present invention, by fresh fructus momordicae in 3-5 DEG C, places 60-120 days, can
So that fresh fructus momordicae after-ripening, place storage for a long time through low temperature, and then produce honey taste.Mogroside v mistake will be produced again
The efflux crossing polymeric adsorbent in journey carries out reclaiming processing, by the waste liquid of typically directly exhaust emission environment in prior art, warp
Cross low tempertaure storage after-ripening, extraction, cross the production stages such as polymeric adsorbent, membrane filtration, concentration, decolouring, adjustment ph, produce a kind of honeybee
The arhat juice of sweet taste.
(2) the honey taste arhat juice of the present invention, taste is lighter than full arhat juice, in good taste, of light color, arhat fruity
Road is light, directly can drink without dilution, expand the range of application of arhat juice, deepen the comprehensive utilization of Momordica grosvenori
Degree.
(3) preparation method of the present invention is simple, wide market, suitable large-scale promotion application.
Specific embodiment
Below in conjunction with specific embodiment, the principle of the present invention and feature are described, example is served only for explaining this
Bright, it is not intended to limit the scope of the present invention.
Embodiment 1
The preparation method of the honey taste arhat juice of the present embodiment, comprises the steps:
(1) raw material selection: selected ripe, complete fresh fructus momordicae, place 120 days in 3 DEG C, obtain the Momordica grosvenori of after-ripening；
(2) extract: the Momordica grosvenori of the after-ripening that 1000g step (1) is obtained, clean up, crush, plus 2000ml deionization
Water, the pectase of 1g enzyme activity 41000u/g, extract 2 hours in 45 DEG C of stirrings, filter, and obtain an extract and once extract slag；
Add 2000ml deionized water to once extracting slag again, extract 2 hours in 45 DEG C of stirrings, filter, obtain secondary raffinate, will once carry
Take liquid and secondary raffinate to merge, obtain 6432g Momordica grosvenori extract；
(3) cross adsorption resin column: the extract that step (2) is obtained, cross d101 adsorption resin column, amount of resin 167g, stream
Fast 250ml/h, washes adsorption resin column, flow velocity 250ml/h with 1336ml, collects efflux and water lotion, merge into 7062g medicine
Liquid one；The ethanol elution adsorption resin column being 60% with 418ml mass fraction again, flow velocity 250ml/h, collect eluent, concentrate,
It is dried, obtain mogroside v dry powder；
(4) cross film: the 7062g liquid one that step (3) is obtained, cross 0.45 μm of ceramic membrane, then wash pottery with 4000ml
Film, collects and obtained film liquid；
(5) concentrate: the mistake film liquid that step (4) is obtained, cross reverse osmosis membrane, be concentrated into 4.8 Brix Scales, obtain 2492g
Concentrate；
(6) decolour: the 2492g concentrate that step (5) is obtained, cross lx-700b decolorizing resin post 1246g, flow velocity
623ml/h, then plus 3000ml water washed, flow velocity 623ml/h, obtain 5765g destainer；
(7) adjust ph: take the destainer that 1922g step (6) obtains to cross d101 × 7 cationic resin column, resin cation
Resin cation 112g in post, flow velocity 5.0bv/h, then plus 336ml water washed, the decolouring obtaining with 3773g step (6)
Liquid merges, and adjusts ph5.24, obtains 6216g liquid two；
(8) concentrate: the 6216g liquid two that step (7) is obtained, first cross reverse osmosis membrane, be concentrated into 5.2 Brix Scales, obtain
1698g, is concentrated in vacuo to 68.7 Brix Scales then at 68 DEG C, that is, obtain honey taste arhat juice described in 86.5g.
The honey taste arhat juice of the present embodiment, after testing, the weight content of mogroside v is 0.32%, ph5.1,
Light transmittance 95.7%.
Embodiment 2
The preparation method of the honey taste arhat juice of the present embodiment, comprises the steps:
(1) raw material selection: selected ripe, complete fresh fructus momordicae, place 90 days in 4 DEG C, obtain the Momordica grosvenori of after-ripening；
(2) extract: the Momordica grosvenori after the after-ripening that 3000g step (1) is obtained, clean up, crush, plus 9000ml go from
Sub- water, the pectase of 6g enzyme activity 43000u/g, extract 1.5 hours in 48 DEG C of stirrings, filter, obtain an extract and once extract
Slag；Add 9000ml deionized water to once extracting slag again, extract 1.5 hours in 48 DEG C of stirrings, filter, obtain secondary raffinate, will
Extract and secondary raffinate merge, and obtain 19302g Momordica grosvenori extract；
(3) cross adsorption resin column: the extract that step (2) is obtained, cross d101 adsorption resin column 500g, flow velocity 900ml/
H, washes adsorption resin column, flow velocity 900ml/h with 3500ml, collects efflux and water lotion, merge into 23412g liquid one；Again
The ethanol elution adsorption resin column being 60% with 1250ml mass fraction, flow velocity 900ml/h, collect eluent, concentrate, be dried,
Obtain mogroside v dry powder；
(4) cross film: the 23412g liquid one that step (3) is obtained, cross 0.45 μm of ceramic membrane, then wash pottery with 12000ml
Porcelain film, collects and obtained film liquid；
(5) concentrate: the mistake film liquid that step (4) is obtained, cross reverse osmosis membrane, be concentrated into 4.8 Brix Scales, obtain 7466g
Concentrate；
(6) decolour: the 7466g concentrate that step (5) is obtained, cross lx-700b decolorizing resin post 3733g, flow velocity
1866ml/h, then plus 9000ml water washed, flow velocity 1866ml/h, obtain 16542g destainer；
(7) adjust ph: take the destainer that 5514.2g step (6) obtains to cross d101 × 7 cationic resin column, cation tree
Resin cation 336g in fat post, flow velocity 6bv/h, then plus 336ml water washed, de- with what 11028g step (6) obtained
Color liquid merges, and adjusts ph5.3, obtains 17904g liquid two；
(8) concentrate: the 17904g liquid two that step (7) is obtained, first cross reverse osmosis membrane, be concentrated into 5.3 Brix Scales, obtain
5108g, is concentrated in vacuo to 68.5 Brix Scales then at 69 DEG C, that is, obtain honey taste arhat juice described in 261.6g.
The honey taste arhat juice of the present embodiment, after testing, the weight content of mogroside v is 0.23%, ph5.2,
Light transmittance 96.1%.
Embodiment 3
The preparation method of the honey taste arhat juice of the present embodiment, comprises the steps:
(1) raw material selection: selected ripe, complete fresh fructus momordicae, place 90 days in 4 DEG C, obtain the Momordica grosvenori of after-ripening；
(2) extract: the Momordica grosvenori after the after-ripening that 3000g step (1) is obtained, clean up, crush, plus 6000ml go from
Sub- water, the pectase of 6g enzyme activity 42000u/g, extract 2 hours in 50 DEG C of stirrings, filter, obtain an extract and once extract
Slag；Add 6000ml deionized water to once extracting slag again, extract 2 hours in 50 DEG C of stirrings, filter, obtain secondary raffinate, by one
Secondary extract and secondary raffinate merge, and obtain 12561g Momordica grosvenori extract；
(3) cross adsorption resin column: the extract that step (2) is obtained, cross d101 adsorption resin column 600g, flow velocity
1200ml/h, washes adsorption resin column, flow velocity 1200ml/h with 3600ml, collects efflux and water lotion, merge into 14116g
Liquid one；The ethanol elution adsorption resin column being 60% with 1500ml mass fraction again, flow velocity 1080/h, collect eluent, dense
Contracting, is dried, obtains mogroside v dry powder；
(4) cross film: the 14116g liquid one that step (3) is obtained, cross 0.45 μm of ceramic membrane, then wash pottery with 8000ml
Film, collects and obtained film liquid；
(5) concentrate: the mistake film liquid that step (4) is obtained, cross reverse osmosis membrane, be concentrated into 5.1 Brix Scales, obtain 4711g
Concentrate；
(6) decolour: the 4711g concentrate that step (5) is obtained, cross lx-700b decolorizing resin post 2355g, flow velocity
2355bv/h, then plus 6720ml water washed, flow velocity 2355ml/h, obtain 11853g destainer；
(7) adjust ph: take the destainer that 3951g step (6) obtains to cross d101 × 7 cationic resin column, resin cation
Resin cation 224g in post, flow velocity 1344ml/h, then plus 672ml water washed, de- with what 7902g step (6) obtained
Color liquid merges, and adjusts ph5.1, obtains 17904g liquid two；
(8) concentrate: the 17904g liquid two that step (7) is obtained, first cross reverse osmosis membrane, be concentrated into 5.7 Brix Scales, obtain
2981g, is concentrated in vacuo to 68.5 Brix Scales then at 69 DEG C, that is, obtain honey taste arhat juice described in 170.1g.
The honey taste arhat juice of the present embodiment, after testing, the weight content of mogroside v is 0.42%, ph5.4,
Light transmittance 96.2%.
Contrast test
A kind of " decolouring method for preparing grosvenor momordica fruit juice and by described of Chinese invention patent Publication No. cn101283831a
The fruit juice of method preparation ", disclose a kind of decolouring method for preparing grosvenor momordica fruit juice and the decolouring Momordica grosvenori prepared by methods described
Fruit juice, specifically Momordica grosvenori fresh fruit are through over cleaning, inactivation, broken, plus pectase extracts, microfiltration membranes crossed by extract, concentration, excessively positive
Ion exchange resin, decolouring, acidifying, concentration, it is acidified, obtain Brix Scale 10-60 fruit juice, mogroside ＞ 30% again.This technique is only
Fruit juice can be obtained, cannot mogroside v dry powder.
A kind of " extracting method of mogroside v " of Chinese invention patent Publication No. cn103923152a, discloses one
The extracting method of kind of mogroside v, specifically saccharification Momordica grosvenori fresh fruit through over cleaning, broken, water extracts, concentrate, centrifugation, macropore
Resin adsorption, separation, ion exchange resin refine, concentration and recovery ethanol, silica gel refine, concentrate and be spray-dried, obtain mogroside v and carry
Take thing.This technique can only obtain mogroside v dry powder, cannot get arhat juice.
The present invention pass through Momordica grosvenori low tempertaure storage after-ripening, plus pectase low temperature extract, cross adsorption resin column, membrane filtration, dense
The steps such as contracting, decolouring, adjustment ph, by the waste liquid of direct exhaust emission environment, on the basis of not affecting to produce mogroside v,
Produce a kind of arhat juice of honey taste, decrease environmental pollution, expand the range of application of arhat juice.The present invention can
To make full use of Momordica grosvenori resource, mogroside v dry powder and honey taste arhat juice can be produced simultaneously, decrease waste residue row
Put, and the honey taste arhat juice of the present invention, taste is lighter than full arhat juice, in good taste, of light color, Momordica grosvenori taste
Light, directly can drink without dilution, expand the range of application of arhat juice, widen the overall availability of Momordica grosvenori.
The foregoing is only presently preferred embodiments of the present invention, not in order to limit the present invention, all spirit in the present invention and
Within principle, any modification, equivalent substitution and improvement made etc., should be included within the scope of the present invention.
Claims (8)
1. a kind of preparation method of honey taste arhat juice is it is characterised in that comprise the steps:
(1) raw material selection: selected ripe, complete fresh fructus momordicae, place 60-120 days in 3-5 DEG C, obtain the Momordica grosvenori of after-ripening；
(2) extract: the Momordica grosvenori of the after-ripening that step (1) is obtained, clean up, crush, plus 2-4 times of the Momordica grosvenori of described after-ripening
The deionized water of weight, the pectase of the Momordica grosvenori 0.1-0.3% weight of described after-ripening, extract 1-2 in 45-50 DEG C of stirring little
When, filter, obtain an extract and once extract slag；Again to the Momordica grosvenori 2-4 times of weight once extracting slag and adding described after-ripening
Deionized water, extracts 1-2 hour in 45-50 DEG C of stirring, filters, obtain secondary raffinate, by an extract and secondary raffinate
Merge, obtain Momordica grosvenori extract；
(3) cross adsorption resin column: the Momordica grosvenori extract that step (2) is obtained, cross adsorption resin column, by extract and absorption tree
The weight of the polymeric adsorbent in fat post enters post than for 5-6:1, flow velocity 1.5-2.0bv/h, and with described Momordica grosvenori extract, 6-8 times weighs
The washing adsorption resin column of amount, flow velocity 1.5-2.0bv/h, collects efflux and water lotion, merges into liquid one；Again with absorption tree
The mass fraction of the 2.5 times of weight of polymeric adsorbent in fat post is 60% ethanol elution adsorption resin column, flow velocity 1.5-2bv/h,
Collect eluent, concentrate, be dried, obtain mogroside v dry powder；
(4) cross film: the liquid one that step (3) is obtained, cross ceramic membrane, then the washing ceramic membrane with one 0.5 times of weight of liquid, receive
Collection obtained film liquid；
(5) concentrate: the mistake film liquid that step (4) is obtained, cross reverse osmosis membrane, be concentrated into 4-6 Brix Scale, obtain concentrate；
(6) decolour: the concentrate that step (5) is obtained, cross decolorizing resin post, compare 2:1 by the weight of concentrate and decolorizing resin
Enter post, flow velocity 0.5-1.5bv/h, then plus the water of 6 times of decolorizing resin weight washed, flow velocity 0.5-1.5bv/h, decoloured
Liquid；
(7) adjust ph: take the destainer that 1/3 step (6) obtains to cross resin cation, by Momordica grosvenori and the cation of described after-ripening
The weight of the resin cation in resin column enters post, flow velocity 5.0-6.0bv/h, then plus 2-4 times of described resin cation than for 3:1
The water of weight is washed, and the destainer being obtained with 2/3 step (6) is merged, and adjusts ph5.0-5.5, obtains liquid two；
(8) concentrate: the liquid two that step (7) is obtained, first cross reverse osmosis membrane, be concentrated into 4-6 Brix Scale, true then at≤70 DEG C
Sky is concentrated into 68-70 Brix Scale, that is, obtain described honey taste arhat juice.
2. a kind of preparation method of honey taste arhat juice according to claim 1 is it is characterised in that step (2) institute
State the enzyme activity ＞ 40000u/g of pectase.
3. a kind of preparation method of honey taste arhat juice according to claim 1 is it is characterised in that step (3) institute
State model d101 of adsorption resin column.
4. a kind of preparation method of honey taste arhat juice according to claim 1 is it is characterised in that step (4) institute
The particle diameter stating ceramic membrane is 0.45 μm.
5. a kind of preparation method of honey taste arhat juice according to claim 1 is it is characterised in that step (6) institute
State model lx-700b of decolorizing resin post.
6. a kind of preparation method of honey taste arhat juice according to claim 1 is it is characterised in that step (7) institute
Stating resin cation is highly acid.
7. a kind of preparation method of honey taste arhat juice according to claim 5 is it is characterised in that described cation
The model 001 × 7 of resin.
8. a kind of preparation method of honey taste arhat juice according to claim 5 is it is characterised in that step (8) institute
State in honey taste arhat juice, the weight content of mogroside v is 0.05-0.5%, ph4.5-6.0, light transmittance ＞
95%.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201610737621.7A CN106333206B (en) | 2016-08-26 | 2016-08-26 | A kind of production method of honey taste arhat juice |
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| CN106923113A (en) * | 2017-03-10 | 2017-07-07 | 广西甙元植物制品有限公司 | The technique that mangosteen juice is produced from the waste liquid of Momordica-Glycosides adsorption resin column discharge |
| CN107232444A (en) * | 2017-06-20 | 2017-10-10 | 桂林莱茵生物科技股份有限公司 | A kind of preparation method of the Momordica grosvenori dry fruit fruit juice with burnt odor taste |
| CN107495363A (en) * | 2017-08-04 | 2017-12-22 | 浙江绍兴东灵保健食品有限公司 | A kind of Luo Han Guo Paste In Foods powder production technology |
| CN109247467A (en) * | 2018-08-23 | 2019-01-22 | 湖南华诚生物资源股份有限公司 | A kind of pure taste inspissated juice of no albumen Siraitia grosvenorii and its production method |
| WO2019109532A1 (en) * | 2017-12-08 | 2019-06-13 | 桂林莱茵生物科技股份有限公司 | Luo han guo juice and preparation method thereof |
| CN116098249A (en) * | 2021-11-10 | 2023-05-12 | 桂林莱茵生物科技股份有限公司 | Preparation method of multi-fold sweet momordica grosvenori pure juice with sugar replacing function |
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| CN106923113A (en) * | 2017-03-10 | 2017-07-07 | 广西甙元植物制品有限公司 | The technique that mangosteen juice is produced from the waste liquid of Momordica-Glycosides adsorption resin column discharge |
| CN106923113B (en) * | 2017-03-10 | 2021-03-16 | 湖南华诚生物资源股份有限公司 | Process for producing concentrated juice of Momordica grosvenori from waste liquid discharged from adsorption resin column of Momordica grosvenori glycoside |
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| CN107495363A (en) * | 2017-08-04 | 2017-12-22 | 浙江绍兴东灵保健食品有限公司 | A kind of Luo Han Guo Paste In Foods powder production technology |
| WO2019109532A1 (en) * | 2017-12-08 | 2019-06-13 | 桂林莱茵生物科技股份有限公司 | Luo han guo juice and preparation method thereof |
| CN109247467A (en) * | 2018-08-23 | 2019-01-22 | 湖南华诚生物资源股份有限公司 | A kind of pure taste inspissated juice of no albumen Siraitia grosvenorii and its production method |
| CN116098249A (en) * | 2021-11-10 | 2023-05-12 | 桂林莱茵生物科技股份有限公司 | Preparation method of multi-fold sweet momordica grosvenori pure juice with sugar replacing function |
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