CN106318631A - Extracting and processing process of rose essential oil - Google Patents
Extracting and processing process of rose essential oil Download PDFInfo
- Publication number
- CN106318631A CN106318631A CN201610731712.XA CN201610731712A CN106318631A CN 106318631 A CN106318631 A CN 106318631A CN 201610731712 A CN201610731712 A CN 201610731712A CN 106318631 A CN106318631 A CN 106318631A
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- CN
- China
- Prior art keywords
- rose
- essential oil
- illumination
- carried out
- microwave
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
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Classifications
-
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11B—PRODUCING, e.g. BY PRESSING RAW MATERIALS OR BY EXTRACTION FROM WASTE MATERIALS, REFINING OR PRESERVING FATS, FATTY SUBSTANCES, e.g. LANOLIN, FATTY OILS OR WAXES; ESSENTIAL OILS; PERFUMES
- C11B9/00—Essential oils; Perfumes
- C11B9/02—Recovery or refining of essential oils from raw materials
-
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11B—PRODUCING, e.g. BY PRESSING RAW MATERIALS OR BY EXTRACTION FROM WASTE MATERIALS, REFINING OR PRESERVING FATS, FATTY SUBSTANCES, e.g. LANOLIN, FATTY OILS OR WAXES; ESSENTIAL OILS; PERFUMES
- C11B9/00—Essential oils; Perfumes
- C11B9/02—Recovery or refining of essential oils from raw materials
- C11B9/025—Recovery by solvent extraction
-
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11B—PRODUCING, e.g. BY PRESSING RAW MATERIALS OR BY EXTRACTION FROM WASTE MATERIALS, REFINING OR PRESERVING FATS, FATTY SUBSTANCES, e.g. LANOLIN, FATTY OILS OR WAXES; ESSENTIAL OILS; PERFUMES
- C11B9/00—Essential oils; Perfumes
- C11B9/02—Recovery or refining of essential oils from raw materials
- C11B9/027—Recovery of volatiles by distillation or stripping
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- Chemical & Material Sciences (AREA)
- Life Sciences & Earth Sciences (AREA)
- Engineering & Computer Science (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Oil, Petroleum & Natural Gas (AREA)
- Wood Science & Technology (AREA)
- Organic Chemistry (AREA)
- Fats And Perfumes (AREA)
Abstract
The invention discloses an extracting and processing process of rose essential oil. The process comprises the following steps that 1, after being subjected to impurity removal, roses are dried to obtain rose pieces with the water content not exceeding 10%, and the rose pieces are crushed to 40 mesh for use; 2, the rose particles are irradiated by LED light, wherein particularly the illumination time ranges from 15 min to 25 min, the illumination intensity ranges from 15 lx to 20 lx, and the color temperature of illumination ranges from 5,500 K to 6,000 K; 3, absolute ethyl alcohol with the weight three times that of the rose particles is added, still standing is carried out for 1 h at the temperature of 20 DEG C, and a mixed solution is obtained; 4, the mixed solution treated in the step 3 is placed in a microwave-assisted extraction instrument, and microwave treatment is carried out for 10 min at the microwave power of 400 w; 5, steam extraction is carried out, the collected crude product is refrigerated for 2 h in a refrigerator of the temperature of 5 DEG C, finally, centrifugal operation is carried out, and oil and water are separated. According to the extracting and processing process of the rose essential oil, the extraction rate of the rose essential oil is obviously increased compared with a conventional method, the extraction time is short, and the made rose essential oil is good in stability.
Description
Technical field
The present invention relates to extract the technical field of quintessence oil from plant, particularly relate to a kind of rose ethereal oil and extract processing work
Skill.
Background technology
Along with the development of economic society, improving constantly of people's living standard, to the demand of plants essential oil increasingly
Greatly, quintessence oil be that a class is volatile, there is intense flavors and abnormal smells from the patient, can be with the general name of vapor distillation oily liquids out.Essence
The active composition of oil, is of wide application, such as expelling phlegm for arresting cough, stomach invigorating of dispeling the wind, anthelmintic, wrinkle resistant maintenance etc., the most popular
Hydrotherapy (SPA), its marrow is exactly natural plant essence oil.For extraction of essential oil, the most conventional method is that steam steams
Evaporate and extraction, but have that yield is low, purity is low and the shortcoming such as toxic solvent residual, it is difficult to meet current quintessence oil industry right
The requirement of high-quality quintessence oil, therefore seeks new substitute technology imperative.
Summary of the invention
For solving the problems referred to above present in prior art and practical situation, the invention provides a kind of rose ethereal oil and carry
Take processing technique, it is characterised in that comprise the steps:
(1) Flos Rosae Rugosae remove impurity post-drying to moisture is less than the Flos Rosae Rugosae sheet of 10%, is crushed to 40 mesh standby；
(2) LED light is used to irradiate Flos Rosae Rugosae grain: the concrete light application time using 15-25min, intensity of illumination is 15-20lx, illumination
Colour temperature be 5500-6000K；
(3) adding weight is its dehydrated alcohol of 3 times, stands 1h at 20 degrees celsius, obtains mixed solution；
(4) mixed solution after step (3) being processed is inserted in Microwave Extraction Apparatus, under the conditions of the microwave power of 400w, enters
Row microwave treatment 10min；
(5) vapor extraction is then carried out, and thick product cold preservation 2 h in the refrigerator of 5 degrees Celsius that will collect, enter the most again
Row centrifugally operated, oil-water separation.
Beneficial effect:
A kind of rose ethereal oil disclosed by the invention extracts processing technique so that the rate that raises of Flos Rosae Rugosae quintessence oil has than conventional method
Significantly improve, and extraction time is short, and the Flos Rosae Rugosae quintessence oil stability produced is preferable, and (quintessence oil has volatility and shakiness because of it
Qualitative, it is easy to oxidation deterioration).
Detailed description of the invention
Technical solution of the present invention is described in detail below.
A kind of rose ethereal oil extracts processing technique, comprises the steps:
(1) Flos Rosae Rugosae remove impurity post-drying to moisture is less than the Flos Rosae Rugosae sheet of 10%, is crushed to 40 mesh standby.
(2) LED light is used to irradiate Flos Rosae Rugosae grain: specifically using the light application time of 15-25min, intensity of illumination is 15-20lx,
The colour temperature of illumination is 5500-6000K；As one embodiment of the present invention, LED light irradiation time is 20min, and illumination is strong
Degree is 20lx, and the colour temperature of illumination is 5500K.Certainly, as another embodiment of the invention, LED light irradiation time is
25min, intensity of illumination is 15lx, and the colour temperature of illumination is 6000K；Or, LED light irradiation time is 15min, and intensity of illumination is
20lx, the colour temperature of illumination is 5800K；Employing LED illumination Flos Rosae Rugosae grain under above-described embodiment so that its later stage produces rhodamine toner
The stability of oil is preferable.
(3) adding weight is its dehydrated alcohol of 3 times, stands 1h at 20 degrees celsius, obtains mixed solution.
(4) mixed solution after step (3) being processed is inserted in Microwave Extraction Apparatus, in the microwave power condition of 400w
Under, carry out microwave treatment 10min；
(5) vapor extraction is then carried out, and thick product cold preservation 2 h in the refrigerator of 5 degrees Celsius that will collect, enter the most again
Row centrifugally operated, oil-water separation.
A kind of rose ethereal oil disclosed by the invention extracts processing technique so that the rate that raises of Flos Rosae Rugosae quintessence oil is than routine side
Method is significantly improved, and extraction time is short, and the Flos Rosae Rugosae quintessence oil stability produced preferably (quintessence oil because of its have volatility and
Unstability, it is easy to oxidation deterioration).
Finally it is noted that the foregoing is only the preferred embodiments of the present invention, it is not limited to the present invention,
Although being described in detail the present invention with reference to previous embodiment, for a person skilled in the art, it still may be used
So that the technical scheme described in foregoing embodiments to be modified, or wherein portion of techniques feature is carried out equivalent.
All within the spirit and principles in the present invention, any modification, equivalent substitution and improvement etc. made, should be included in the present invention's
Within protection domain.
Claims (1)
1. a rose ethereal oil extracts processing technique, it is characterised in that comprise the steps:
(1) Flos Rosae Rugosae remove impurity post-drying to moisture is less than the Flos Rosae Rugosae sheet of 10%, is crushed to 40 mesh standby；
(2) LED light is used to irradiate Flos Rosae Rugosae grain: the concrete light application time using 15-25min, intensity of illumination is 15-20lx, illumination
Colour temperature be 5500-6000K；
(3) adding weight is its dehydrated alcohol of 3 times, stands 1h at 20 degrees celsius, obtains mixed solution；
(4) mixed solution after step (3) being processed is inserted in Microwave Extraction Apparatus, under the conditions of the microwave power of 400w, enters
Row microwave treatment 10min；
(5) vapor extraction is then carried out, and thick product cold preservation 2 h in the refrigerator of 5 degrees Celsius that will collect, enter the most again
Row centrifugally operated, oil-water separation.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201610731712.XA CN106318631A (en) | 2016-08-26 | 2016-08-26 | Extracting and processing process of rose essential oil |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201610731712.XA CN106318631A (en) | 2016-08-26 | 2016-08-26 | Extracting and processing process of rose essential oil |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| CN106318631A true CN106318631A (en) | 2017-01-11 |
Family
ID=57791779
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN201610731712.XA Pending CN106318631A (en) | 2016-08-26 | 2016-08-26 | Extracting and processing process of rose essential oil |
Country Status (1)
| Country | Link |
|---|---|
| CN (1) | CN106318631A (en) |
Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN109576054A (en) * | 2017-09-28 | 2019-04-05 | 王少平 | A kind of extracting method of Rosa Damascana |
Citations (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN101691522A (en) * | 2009-09-30 | 2010-04-07 | 云南省农业科学院药用植物研究所 | Method for extracting rose damascana and rose flower water from roses |
| CN105482897A (en) * | 2016-01-27 | 2016-04-13 | 江苏耐雀生物工程技术有限公司 | Microwave-assisted subcritical essential oil extracting method |
| CN105802735A (en) * | 2016-04-20 | 2016-07-27 | 李从喜 | Yunnan red rose essential oil extracting method |
| CN105802736A (en) * | 2016-05-28 | 2016-07-27 | 黄宇松 | Rose essential oil extraction method |
-
2016
- 2016-08-26 CN CN201610731712.XA patent/CN106318631A/en active Pending
Patent Citations (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN101691522A (en) * | 2009-09-30 | 2010-04-07 | 云南省农业科学院药用植物研究所 | Method for extracting rose damascana and rose flower water from roses |
| CN105482897A (en) * | 2016-01-27 | 2016-04-13 | 江苏耐雀生物工程技术有限公司 | Microwave-assisted subcritical essential oil extracting method |
| CN105802735A (en) * | 2016-04-20 | 2016-07-27 | 李从喜 | Yunnan red rose essential oil extracting method |
| CN105802736A (en) * | 2016-05-28 | 2016-07-27 | 黄宇松 | Rose essential oil extraction method |
Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN109576054A (en) * | 2017-09-28 | 2019-04-05 | 王少平 | A kind of extracting method of Rosa Damascana |
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| PB01 | Publication | ||
| PB01 | Publication | ||
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| SE01 | Entry into force of request for substantive examination | ||
| RJ01 | Rejection of invention patent application after publication | ||
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Application publication date: 20170111 |