CN106190581A - A kind of extraction process for orange blossom quintessence oil - Google Patents
A kind of extraction process for orange blossom quintessence oil Download PDFInfo
- Publication number
- CN106190581A CN106190581A CN201610731690.7A CN201610731690A CN106190581A CN 106190581 A CN106190581 A CN 106190581A CN 201610731690 A CN201610731690 A CN 201610731690A CN 106190581 A CN106190581 A CN 106190581A
- Authority
- CN
- China
- Prior art keywords
- orange blossom
- illumination
- extraction
- quintessence oil
- mixed solution
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Pending
Links
- 238000000605 extraction Methods 0.000 title claims abstract description 17
- 238000005286 illumination Methods 0.000 claims abstract description 15
- 239000011259 mixed solution Substances 0.000 claims abstract description 8
- LFQSCWFLJHTTHZ-UHFFFAOYSA-N Ethanol Chemical compound CCO LFQSCWFLJHTTHZ-UHFFFAOYSA-N 0.000 claims abstract description 4
- 229960000935 dehydrated alcohol Drugs 0.000 claims abstract description 4
- 238000001035 drying Methods 0.000 claims abstract description 4
- 239000012535 impurity Substances 0.000 claims abstract description 4
- 238000000874 microwave-assisted extraction Methods 0.000 claims abstract description 4
- 238000004321 preservation Methods 0.000 claims abstract description 4
- 238000000926 separation method Methods 0.000 claims abstract description 4
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims abstract description 4
- 239000003921 oil Substances 0.000 description 20
- 238000007796 conventional method Methods 0.000 description 2
- 230000006866 deterioration Effects 0.000 description 2
- 238000005516 engineering process Methods 0.000 description 2
- 238000000034 method Methods 0.000 description 2
- 230000003647 oxidation Effects 0.000 description 2
- 238000007254 oxidation reaction Methods 0.000 description 2
- 239000000341 volatile oil Substances 0.000 description 2
- 206010011224 Cough Diseases 0.000 description 1
- 206010062717 Increased upper airway secretion Diseases 0.000 description 1
- 206010044565 Tremor Diseases 0.000 description 1
- 230000002159 abnormal effect Effects 0.000 description 1
- 230000000507 anthelmentic effect Effects 0.000 description 1
- 230000009286 beneficial effect Effects 0.000 description 1
- 238000011161 development Methods 0.000 description 1
- 238000004821 distillation Methods 0.000 description 1
- 239000000796 flavoring agent Substances 0.000 description 1
- 235000019634 flavors Nutrition 0.000 description 1
- 238000002169 hydrotherapy Methods 0.000 description 1
- 239000007788 liquid Substances 0.000 description 1
- 238000012423 maintenance Methods 0.000 description 1
- 239000000203 mixture Substances 0.000 description 1
- 238000012986 modification Methods 0.000 description 1
- 230000004048 modification Effects 0.000 description 1
- 208000026435 phlegm Diseases 0.000 description 1
- 230000035943 smell Effects 0.000 description 1
- 239000000243 solution Substances 0.000 description 1
- 239000002904 solvent Substances 0.000 description 1
- 210000002784 stomach Anatomy 0.000 description 1
- 238000006467 substitution reaction Methods 0.000 description 1
- 231100000331 toxic Toxicity 0.000 description 1
- 230000002588 toxic effect Effects 0.000 description 1
- 230000037303 wrinkles Effects 0.000 description 1
Classifications
-
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11B—PRODUCING, e.g. BY PRESSING RAW MATERIALS OR BY EXTRACTION FROM WASTE MATERIALS, REFINING OR PRESERVING FATS, FATTY SUBSTANCES, e.g. LANOLIN, FATTY OILS OR WAXES; ESSENTIAL OILS; PERFUMES
- C11B9/00—Essential oils; Perfumes
- C11B9/02—Recovery or refining of essential oils from raw materials
- C11B9/025—Recovery by solvent extraction
-
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11B—PRODUCING, e.g. BY PRESSING RAW MATERIALS OR BY EXTRACTION FROM WASTE MATERIALS, REFINING OR PRESERVING FATS, FATTY SUBSTANCES, e.g. LANOLIN, FATTY OILS OR WAXES; ESSENTIAL OILS; PERFUMES
- C11B9/00—Essential oils; Perfumes
- C11B9/02—Recovery or refining of essential oils from raw materials
- C11B9/022—Refining
Landscapes
- Chemical & Material Sciences (AREA)
- Life Sciences & Earth Sciences (AREA)
- Engineering & Computer Science (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Oil, Petroleum & Natural Gas (AREA)
- Wood Science & Technology (AREA)
- Organic Chemistry (AREA)
- Cosmetics (AREA)
Abstract
The present invention discloses a kind of extraction process for orange blossom quintessence oil, comprises the steps: that orange blossom remove impurity post-drying to moisture is less than the orange blossom sheet of 10% by (1), is crushed to 40 mesh standby；(2) LED light is used to irradiate orange blossom grain: the concrete light application time using 15 25min, intensity of illumination is 15 20lx, and the colour temperature of illumination is 5500 6000K；(3) adding weight is its dehydrated alcohol of 3 times, stands 1h at 20 degrees celsius, obtains mixed solution；(4) mixed solution after step (3) being processed is inserted in Microwave Extraction Apparatus, under the conditions of the microwave power of 400w, carries out microwave treatment 10min；(5) vapor extraction is then carried out, and thick product cold preservation 2 h in the refrigerator of 5 degrees Celsius that will collect, it is centrifuged operation, oil-water separation the most again.
Description
Technical field
The present invention relates to extract the technical field of quintessence oil from plant, particularly relate to a kind of extraction work for orange blossom quintessence oil
Skill.
Background technology
Along with the development of economic society, improving constantly of people's living standard, to the demand of plants essential oil increasingly
Greatly, quintessence oil be that a class is volatile, there is intense flavors and abnormal smells from the patient, can be with the general name of vapor distillation oily liquids out.Essence
The active composition of oil, is of wide application, such as expelling phlegm for arresting cough, stomach invigorating of dispeling the wind, anthelmintic, wrinkle resistant maintenance etc., the most popular
Hydrotherapy (SPA), its marrow is exactly natural plant essence oil.For extraction of essential oil, the most conventional method is that steam steams
Evaporate and extraction, but have that yield is low, purity is low and the shortcoming such as toxic solvent residual, it is difficult to meet current quintessence oil industry right
The requirement of high-quality quintessence oil, therefore seeks new substitute technology imperative.
Summary of the invention
For solving the problems referred to above present in prior art and practical situation, the invention provides a kind of for orange blossom quintessence oil
Extraction process, it is characterised in that comprise the steps:
(1) orange blossom remove impurity post-drying to moisture is less than the orange blossom sheet of 10%, is crushed to 40 mesh standby；
(2) LED light is used to irradiate orange blossom grain: the concrete light application time using 15-25min, intensity of illumination is 15-20lx, illumination
Colour temperature be 5500-6000K；
(3) adding weight is its dehydrated alcohol of 3 times, stands 1h at 20 degrees celsius, obtains mixed solution；
(4) mixed solution after step (3) being processed is inserted in Microwave Extraction Apparatus, under the conditions of the microwave power of 400w, enters
Row microwave treatment 10min；
(5) vapor extraction is then carried out, and thick product cold preservation 2 h in the refrigerator of 5 degrees Celsius that will collect, enter the most again
Row centrifugally operated, oil-water separation.
Beneficial effect:
A kind of extraction process for orange blossom quintessence oil disclosed by the invention so that the rate that raises of orange blossom quintessence oil has than conventional method
Significantly improve, and extraction time is short, and the orange blossom quintessence oil stability produced is preferable, and (quintessence oil has volatility and shakiness because of it
Qualitative, it is easy to oxidation deterioration).
Detailed description of the invention
Technical solution of the present invention is described in detail below.
A kind of extraction process for orange blossom quintessence oil, comprises the steps:
(1) orange blossom remove impurity post-drying to moisture is less than the orange blossom sheet of 10%, is crushed to 40 mesh standby.
(2) LED light is used to irradiate orange blossom grain: specifically using the light application time of 15-25min, intensity of illumination is 15-20lx,
The colour temperature of illumination is 5500-6000K；As one embodiment of the present invention, LED light irradiation time is 20min, and illumination is strong
Degree is 20lx, and the colour temperature of illumination is 5500K.Certainly, as another embodiment of the invention, LED light irradiation time is
25min, intensity of illumination is 15lx, and the colour temperature of illumination is 6000K；Or, LED light irradiation time is 15min, and intensity of illumination is
20lx, the colour temperature of illumination is 5800K；Employing LED illumination orange blossom grain under above-described embodiment so that its later stage produces orange blossom essence
The stability of oil is preferable.
(3) adding weight is its dehydrated alcohol of 3 times, stands 1h at 20 degrees celsius, obtains mixed solution.
(4) mixed solution after step (3) being processed is inserted in Microwave Extraction Apparatus, in the microwave power condition of 400w
Under, carry out microwave treatment 10min；
(5) vapor extraction is then carried out, and thick product cold preservation 2 h in the refrigerator of 5 degrees Celsius that will collect, enter the most again
Row centrifugally operated, oil-water separation, obtain orange blossom quintessence oil.
A kind of extraction process for orange blossom quintessence oil disclosed by the invention so that the rate that raises of orange blossom quintessence oil is than routine side
Method is significantly improved, and extraction time is short, and the orange blossom quintessence oil stability produced preferably (quintessence oil because of its have volatility and
Unstability, it is easy to oxidation deterioration).
Finally it is noted that the foregoing is only the preferred embodiments of the present invention, it is not limited to the present invention,
Although being described in detail the present invention with reference to previous embodiment, for a person skilled in the art, it still may be used
So that the technical scheme described in foregoing embodiments to be modified, or wherein portion of techniques feature is carried out equivalent.
All within the spirit and principles in the present invention, any modification, equivalent substitution and improvement etc. made, should be included in the present invention's
Within protection domain.
Claims (1)
1. the extraction process for orange blossom quintessence oil, it is characterised in that comprise the steps:
(1) orange blossom remove impurity post-drying to moisture is less than the orange blossom sheet of 10%, is crushed to 40 mesh standby；
(2) LED light is used to irradiate orange blossom grain: the concrete light application time using 15-25min, intensity of illumination is 15-20lx, illumination
Colour temperature be 5500-6000K；
(3) adding weight is its dehydrated alcohol of 3 times, stands 1h at 20 degrees celsius, obtains mixed solution；
(4) mixed solution after step (3) being processed is inserted in Microwave Extraction Apparatus, under the conditions of the microwave power of 400w, enters
Row microwave treatment 10min；
(5) vapor extraction is then carried out, and thick product cold preservation 2 h in the refrigerator of 5 degrees Celsius that will collect, enter the most again
Row centrifugally operated, oil-water separation.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201610731690.7A CN106190581A (en) | 2016-08-26 | 2016-08-26 | A kind of extraction process for orange blossom quintessence oil |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201610731690.7A CN106190581A (en) | 2016-08-26 | 2016-08-26 | A kind of extraction process for orange blossom quintessence oil |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| CN106190581A true CN106190581A (en) | 2016-12-07 |
Family
ID=57525720
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN201610731690.7A Pending CN106190581A (en) | 2016-08-26 | 2016-08-26 | A kind of extraction process for orange blossom quintessence oil |
Country Status (1)
| Country | Link |
|---|---|
| CN (1) | CN106190581A (en) |
Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN119040072A (en) * | 2024-09-13 | 2024-11-29 | 威尔芬(北京)科技发展有限公司 | Preparation process and device of sweet orange flower essential oil |
Citations (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN102911791A (en) * | 2012-09-25 | 2013-02-06 | 常州亚环环保科技有限公司 | Method for extracting gardenia essential oil |
-
2016
- 2016-08-26 CN CN201610731690.7A patent/CN106190581A/en active Pending
Patent Citations (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN102911791A (en) * | 2012-09-25 | 2013-02-06 | 常州亚环环保科技有限公司 | Method for extracting gardenia essential oil |
Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN119040072A (en) * | 2024-09-13 | 2024-11-29 | 威尔芬(北京)科技发展有限公司 | Preparation process and device of sweet orange flower essential oil |
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Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| C06 | Publication | ||
| PB01 | Publication | ||
| C10 | Entry into substantive examination | ||
| SE01 | Entry into force of request for substantive examination | ||
| RJ01 | Rejection of invention patent application after publication | ||
| RJ01 | Rejection of invention patent application after publication |
Application publication date: 20161207 |