CN106281784A - A kind of preparation method of efficient detergent for toilet - Google Patents
A kind of preparation method of efficient detergent for toilet Download PDFInfo
- Publication number
- CN106281784A CN106281784A CN201610721559.2A CN201610721559A CN106281784A CN 106281784 A CN106281784 A CN 106281784A CN 201610721559 A CN201610721559 A CN 201610721559A CN 106281784 A CN106281784 A CN 106281784A
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- China
- Prior art keywords
- toilet
- filtrate
- detergent
- subsequently
- efficient detergent
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Classifications
-
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
- C11D7/00—Compositions of detergents based essentially on non-surface-active compounds
- C11D7/22—Organic compounds
- C11D7/40—Products in which the composition is not well defined
- C11D7/44—Vegetable products
-
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
- C11D7/00—Compositions of detergents based essentially on non-surface-active compounds
- C11D7/02—Inorganic compounds
- C11D7/04—Water-soluble compounds
Abstract
The invention discloses the preparation method of a kind of efficient detergent for toilet, belong to detergent for toilet preparing technical field.After the present invention takes rice and distilled water steaming and decocting, filter to get filtrate and filtering residue, filtering residue mixing with Fructus Citri Limoniae making beating, sealed insulation, vibrates, centrifugal to obtain supernatant, to be mixed to prepare efficient detergent for toilet base fluid standby with filtrate, take the combination drying such as Herba Plantaginis, Calyx Hibisci Sabdariffae again, size-reduced, sieve after, mix insulation with water, then after pressurize, normal pressure stand, obtain filtrate through filtration under diminished pressure, mix homogeneously with standby efficient detergent for toilet base fluid and prepare efficient detergent for toilet.The invention has the beneficial effects as follows: preparation process of the present invention is simple, production process good dispersion, low cost;Products obtained therefrom adhesiving effect is good, and efficiency time is long, and dirt-removing power is strong.
Description
Technical field
The present invention relates to the preparation method of a kind of efficient detergent for toilet, belong to detergent for toilet preparing technical field.
Background technology
Detergent for toilet makes again cleaning toilet precious, toilet cleaner, toilet cleaner is a kind of cleaning, sterilize, WC pans of sterilizing Clean-
Product.Detergent for toilet is broadly divided into three major types by its formula composition difference: acidic products;Neutral products;Basic products.On market with
Acidic products is main, and cleaning performance is optimal.The feature of detergent for toilet is specifically designed exclusively for the stain in water closet pan;Can be rapidly
Effectively decompose the tough stains in water closet pan, need not arduously clean;More having biocidal efficacies, cleaning is hidden in can also killing basin simultaneously
Antibacterial;Light and do not damage water closet pan surface.
Along with raising and the improvement of living conditions of people's living standard, detergent for toilet has become as familiar daily
Product.Except for the cleaning of glaze porcelain sanitary equipment and taste removal, removing outside the Organic substance of body discharges, it is possible to remove the ferrum of tap water
Rust, incrustation scale etc..Detergent for toilet product is divided by form can be divided into liquid and the big class of solid (powdery that can let go) two.Acidic Liquid
Body cleaning agent is modal detergent for toilet.The surface of water closet pan is porcelain surface, and its bind dirt is generally incrustation scale, soap slag, ferrum
Rust and urine alkali etc., the most easily need to remove in acid medium.But currently used detergent for toilet adhesiving effect is poor, and efficiency time is short, goes
Dirty ability is weak.
Summary of the invention
The technical problem to be solved: poor for currently used detergent for toilet adhesiving effect, efficiency time is short, goes
The drawback that dirty ability is weak, it is provided that after one takes rice and distilled water steaming and decocting, filter to get filtrate and filtering residue, filtering residue is mixed with Fructus Citri Limoniae
Closing making beating, sealed insulation, vibrate, centrifugal to obtain supernatant, to be mixed to prepare efficient detergent for toilet base fluid standby with filtrate, then before picking up the car
The combination dryings such as grass, Calyx Hibisci Sabdariffae, size-reduced, sieve after, mix insulation with water, then after pressurize, normal pressure stand, obtain through filtration under diminished pressure
Filtrate, mixs homogeneously the method preparing efficient detergent for toilet with standby efficient detergent for toilet base fluid.Preparation process of the present invention is simple, gained
Product adhesion is effective, and efficiency time is long, and dirt-removing power is strong, is worthy to be popularized and uses.
For solving above-mentioned technical problem, the present invention uses the technical scheme as described below to be:
(1) 1:3 in mass ratio, takes rice and distilled water is put in steamer, and design temperature is 45~50 DEG C, is incubated 30~40min,
Filter subsequently, collect filtrate and filtering residue, the Fructus Citri Limoniae of filtering residue and its quality 20~25% is put in beater, beats with 500r/min
Slurry 10~15min, obtains slurry, puts in container by slurry subsequently, seals container, and in holding container, temperature is 35~40 DEG C, protects
Temperature 2~4h;
(2) after above-mentioned insulation terminates, being placed in ultrasonator by container, setpoint frequency is 45~55kHz, vibration 20~
25min, then stand 5~10min, it is subsequently placed in centrifuge, is centrifuged 10~15min with 2000r/min, collect supernatant, and
Mixing homogeneously with the filtrate of above-mentioned collection, obtain mixed liquor, using mass fraction is 10% ammonia regulation pH to 5.5~6.0, obtains high
Effect detergent for toilet base fluid, standby;
(3) count by weight, take 30~40 portions of Herba Plantaginiss, 20~25 parts of Calyx Hibisci Sabdariffaes, 10~15 parts of Fructus Gleditsia skins, 8~10 parts of Chinese mugworts
Grass and 5~7 parts of lavandula angustifoliaes, put in drying baker, and design temperature is 45 DEG C, is dried 3~5h, subsequently drying composite is put into powder
Pulverizing in broken machine, cross 100 mesh sieves, collect the granule that sieves, by solid-liquid mass ratio 1:3, the granule that will sieve is put in ceramic pot with water,
Ceramic pot is heated to 60~70 DEG C, is incubated 6~7h;
(4) after above-mentioned insulation terminates, the mixture in ceramic pot is put in autoclave, use nitrogen protect and boost
To 6~8MPa, keep pressure 16~18min, in 1~2min, be depressurized to normal atmosphere subsequently, stand 30~50min and go out
Material, carries out filtration under diminished pressure to discharging thing, collects filtrate, is mixed homogeneously by the active hargil of filtrate and its quality 2.2~2.6%,
Filter after decolouring 10~15min, collect filtrate, obtain clear liquid, by volume 3:2, by efficient detergent for toilet base fluid standby for step (2)
Mix homogeneously with clear liquid, efficient detergent for toilet.
The application process of the present invention: the efficient detergent for toilet present invention prepared is poured in water closet pan in an orbiting manner, covers
Toilet lid soaks 6~8min, opens toilet lid, scrubs toilet inwall and outlet by closet bowl brush, after scrubbing, presses water outlet
Button, rinses 2~3 times with clear water.This detergent for toilet can effectively remove the dirts such as the urine alkali in toilet, incrustation scale, dirt-removing power
By force, speed fast, efficiency time is long.
The present invention is compared with additive method, and Advantageous Effects is:
(1) preparation process of the present invention is simple, production process good dispersion, low cost;
(2) products obtained therefrom adhesiving effect is good, and efficiency time is long, and dirt-removing power is strong.
Detailed description of the invention
1:3 the most in mass ratio, takes rice and distilled water is put in steamer, and design temperature is 45~50 DEG C, insulation 30~
40min, filters subsequently, collects filtrate and filtering residue, puts in beater by the Fructus Citri Limoniae of filtering residue and its quality 20~25%, with
500r/min making beating 10~15min, obtains slurry, puts in container by slurry subsequently, seals container, and in holding container, temperature is 35
~40 DEG C, it is incubated 2~4h;Then, after above-mentioned insulation terminates, container is placed in ultrasonator, setpoint frequency be 45~
55kHz, vibration 20~25min, then stand 5~10min, it is subsequently placed in centrifuge, is centrifuged 10~15min with 2000r/min,
Collecting supernatant, and mix homogeneously with the filtrate of above-mentioned collection, obtain mixed liquor, using mass fraction is that 10% ammonia regulates pH extremely
5.5~6.0, obtain efficient detergent for toilet base fluid, standby;Count by weight, take 30~40 portions of Herba Plantaginiss, 20~25 portions of Calyx Hibisci Sabdariffaes,
10~15 parts of Fructus Gleditsia skins, 8~10 parts of Folium Artemisiae Argyis and 5~7 parts of lavandula angustifoliaes, put in drying baker, and design temperature is 45 DEG C, be dried 3~
5h, puts into drying composite subsequently in pulverizer and pulverizes, and crosses 100 mesh sieves, collects the granule that sieves, by solid-liquid mass ratio 1:3, and will
The granule that sieves is put in ceramic pot with water, and ceramic pot is heated to 60~70 DEG C, is incubated 6~7h;Finally terminate in above-mentioned insulation
After, the mixture in ceramic pot is put in autoclave, uses nitrogen to protect and boost to 6~8MPa, keeping pressure 16
~18min, in 1~2min, it is depressurized to normal atmosphere subsequently, stands 30~50min dischargings, discharging thing was reduced pressure
Filter, collects filtrate, is mixed homogeneously by the active hargil of filtrate and its quality 2.2~2.6%, filters, receipts after decolouring 10~15min
Collection filtrate, obtains clear liquid, by volume 3:2, is mixed homogeneously with clear liquid by standby efficient detergent for toilet base fluid, efficient cleaning toilet
Agent.
Example 1
1:3 the most in mass ratio, takes rice and distilled water is put in steamer, and design temperature is 45 DEG C, is incubated 30min, subsequently mistake
Filter, collects filtrate and filtering residue, puts in beater by the Fructus Citri Limoniae of filtering residue Yu its quality 20%, with 500r/min making beating 10min,
Slurry, puts in container by slurry subsequently, seals container, and in holding container, temperature is 35 DEG C, is incubated 2h;Then in above-mentioned insulation
After end, being placed in ultrasonator by container, setpoint frequency is 45kHz, and vibrate 20min, then stands 5min, be subsequently placed into from
In scheming, it is centrifuged 10min with 2000r/min, collects supernatant, and mix homogeneously with the filtrate of above-mentioned collection, obtain mixed liquor, make
It is 10% ammonia regulation pH to 5.5 with mass fraction, obtains efficient detergent for toilet base fluid, standby;Count by weight, take 30 parts of Herba Plantaginis
Grass, 20 portions of Calyx Hibisci Sabdariffaes, 10 parts of Fructus Gleditsia skins, 8 parts of Folium Artemisiae Argyis and 5 parts of lavandula angustifoliaes, put in drying baker, and design temperature is 45 DEG C, is dried
3h, puts into drying composite subsequently in pulverizer and pulverizes, and crosses 100 mesh sieves, collects the granule that sieves, by solid-liquid mass ratio 1:3, and will
The granule that sieves is put in ceramic pot with water, and ceramic pot is heated to 60 DEG C, is incubated 6h;Last after above-mentioned insulation terminates, will pottery
Mixture in porcelain jar is put in autoclave, uses nitrogen to protect and boost to 6MPa, keeps pressure 16min, exist subsequently
Be depressurized to normal atmosphere in 1min, stand 30min discharging, discharging thing is carried out filtration under diminished pressure, collect filtrate, by filtrate and its
The active hargil mix homogeneously of quality 2.2%, filters after decolouring 10min, collects filtrate, obtain clear liquid, by volume 3:2, by standby
Efficient detergent for toilet base fluid mix homogeneously with clear liquid, efficient detergent for toilet.
The efficient detergent for toilet present invention prepared is poured in water closet pan in an orbiting manner, covers toilet lid and soaks 6min, beats
Open toilet lid, scrub toilet inwall and outlet by closet bowl brush, after scrubbing, press water outlet button, rinse 2 times i.e. with clear water
Can.This detergent for toilet can effectively remove the dirts such as the urine alkali in toilet, incrustation scale, and dirt-removing power is strong, speed is fast, and efficiency time is long.
Example 2
1:3 the most in mass ratio, takes rice and distilled water is put in steamer, and design temperature is 48 DEG C, is incubated 35min, subsequently mistake
Filter, collects filtrate and filtering residue, puts in beater by the Fructus Citri Limoniae of filtering residue Yu its quality 23%, with 500r/min making beating 13min,
Slurry, puts in container by slurry subsequently, seals container, and in holding container, temperature is 38 DEG C, is incubated 3h;Then in above-mentioned insulation
After end, being placed in ultrasonator by container, setpoint frequency is 50kHz, and vibrate 23min, then stands 8min, be subsequently placed into from
In scheming, it is centrifuged 13min with 2000r/min, collects supernatant, and mix homogeneously with the filtrate of above-mentioned collection, obtain mixed liquor, make
It is 10% ammonia regulation pH to 5.8 with mass fraction, obtains efficient detergent for toilet base fluid, standby;Count by weight, take 35 parts of Herba Plantaginis
Grass, 23 portions of Calyx Hibisci Sabdariffaes, 13 parts of Fructus Gleditsia skins, 9 parts of Folium Artemisiae Argyis and 6 parts of lavandula angustifoliaes, put in drying baker, and design temperature is 45 DEG C, is dried
4h, puts into drying composite subsequently in pulverizer and pulverizes, and crosses 100 mesh sieves, collects the granule that sieves, by solid-liquid mass ratio 1:3, and will
The granule that sieves is put in ceramic pot with water, and ceramic pot is heated to 65 DEG C, is incubated 7h;Last after above-mentioned insulation terminates, will pottery
Mixture in porcelain jar is put in autoclave, uses nitrogen to protect and boost to 7MPa, keeps pressure 17min, exist subsequently
Be depressurized to normal atmosphere in 2min, stand 40min discharging, discharging thing is carried out filtration under diminished pressure, collect filtrate, by filtrate and its
The active hargil mix homogeneously of quality 2.4%, filters after decolouring 13min, collects filtrate, obtain clear liquid, by volume 3:2, by standby
Efficient detergent for toilet base fluid mix homogeneously with clear liquid, efficient detergent for toilet.
The efficient detergent for toilet present invention prepared is poured in water closet pan in an orbiting manner, covers toilet lid and soaks 7min, beats
Open toilet lid, scrub toilet inwall and outlet by closet bowl brush, after scrubbing, press water outlet button, rinse 3 times i.e. with clear water
Can.This detergent for toilet can effectively remove the dirts such as the urine alkali in toilet, incrustation scale, and dirt-removing power is strong, speed is fast, and efficiency time is long.
Example 3
1:3 the most in mass ratio, takes rice and distilled water is put in steamer, and design temperature is 50 DEG C, is incubated 40min, subsequently mistake
Filter, collects filtrate and filtering residue, puts in beater by the Fructus Citri Limoniae of filtering residue Yu its quality 25%, with 500r/min making beating 15min,
Slurry, puts in container by slurry subsequently, seals container, and in holding container, temperature is 40 DEG C, is incubated 4h;Then in above-mentioned insulation
After end, being placed in ultrasonator by container, setpoint frequency is 55kHz, and vibrate 25min, then stands 10min, is subsequently placed into
In centrifuge, it is centrifuged 15min with 2000r/min, collects supernatant, and mix homogeneously with the filtrate of above-mentioned collection, obtain mixed liquor,
Using mass fraction is 10% ammonia regulation pH to 6.0, obtains efficient detergent for toilet base fluid, standby;Count by weight, take 40 parts of cars
Front grass, 25 portions of Calyx Hibisci Sabdariffaes, 15 parts of Fructus Gleditsia skins, 10 parts of Folium Artemisiae Argyis and 7 parts of lavandula angustifoliaes, put in drying baker, and design temperature is 45 DEG C, dry
Dry 5h, puts into drying composite subsequently in pulverizer and pulverizes, and crosses 100 mesh sieves, collects the granule that sieves, by solid-liquid mass ratio 1:3,
The granule that will sieve is put in ceramic pot with water, and ceramic pot is heated to 70 DEG C, is incubated 7h;Last after above-mentioned insulation terminates, will
Mixture in ceramic pot is put in autoclave, uses nitrogen to protect and boost to 8MPa, keeps pressure 18min, subsequently
In 2min, be depressurized to normal atmosphere, stand 50min discharging, discharging thing is carried out filtration under diminished pressure, collect filtrate, by filtrate with
The active hargil mix homogeneously of its quality 2.6%, filters after decolouring 15min, collects filtrate, obtain clear liquid, by volume 3:2, will
Standby efficient detergent for toilet base fluid is mixed homogeneously with clear liquid, efficient detergent for toilet.
The efficient detergent for toilet present invention prepared is poured in water closet pan in an orbiting manner, covers toilet lid and soaks 8min, beats
Open toilet lid, scrub toilet inwall and outlet by closet bowl brush, after scrubbing, press water outlet button, rinse 3 times i.e. with clear water
Can.This detergent for toilet can effectively remove the dirts such as the urine alkali in toilet, incrustation scale, and dirt-removing power is strong, speed is fast, and efficiency time is long.
Claims (1)
1. the preparation method of an efficient detergent for toilet, it is characterised in that concrete preparation process is:
(1) 1:3 in mass ratio, takes rice and distilled water is put in steamer, and design temperature is 45~50 DEG C, is incubated 30~40min,
Filter subsequently, collect filtrate and filtering residue, the Fructus Citri Limoniae of filtering residue and its quality 20~25% is put in beater, beats with 500r/min
Slurry 10~15min, obtains slurry, puts in container by slurry subsequently, seals container, and in holding container, temperature is 35~40 DEG C, protects
Temperature 2~4h;
(2) after above-mentioned insulation terminates, being placed in ultrasonator by container, setpoint frequency is 45~55kHz, vibration 20~
25min, then stand 5~10min, it is subsequently placed in centrifuge, is centrifuged 10~15min with 2000r/min, collect supernatant, and
Mixing homogeneously with the filtrate of above-mentioned collection, obtain mixed liquor, using mass fraction is 10% ammonia regulation pH to 5.5~6.0, obtains high
Effect detergent for toilet base fluid, standby;
(3) count by weight, take 30~40 portions of Herba Plantaginiss, 20~25 parts of Calyx Hibisci Sabdariffaes, 10~15 parts of Fructus Gleditsia skins, 8~10 parts of Chinese mugworts
Grass and 5~7 parts of lavandula angustifoliaes, put in drying baker, and design temperature is 45 DEG C, is dried 3~5h, subsequently drying composite is put into powder
Pulverizing in broken machine, cross 100 mesh sieves, collect the granule that sieves, by solid-liquid mass ratio 1:3, the granule that will sieve is put in ceramic pot with water,
Ceramic pot is heated to 60~70 DEG C, is incubated 6~7h;
(4) after above-mentioned insulation terminates, the mixture in ceramic pot is put in autoclave, use nitrogen protect and boost
To 6~8MPa, keep pressure 16~18min, in 1~2min, be depressurized to normal atmosphere subsequently, stand 30~50min and go out
Material, carries out filtration under diminished pressure to discharging thing, collects filtrate, is mixed homogeneously by the active hargil of filtrate and its quality 2.2~2.6%,
Filter after decolouring 10~15min, collect filtrate, obtain clear liquid, by volume 3:2, by efficient detergent for toilet base fluid standby for step (2)
Mix homogeneously with clear liquid, efficient detergent for toilet.
Priority Applications (1)
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CN201610721559.2A CN106281784A (en) | 2016-08-25 | 2016-08-25 | A kind of preparation method of efficient detergent for toilet |
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CN201610721559.2A CN106281784A (en) | 2016-08-25 | 2016-08-25 | A kind of preparation method of efficient detergent for toilet |
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Cited By (2)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN110437940A (en) * | 2019-09-07 | 2019-11-12 | 阜阳洁平日化有限公司 | A kind of high-efficiency environment friendly deodorization agent for toilet and preparation method thereof |
CN111329009A (en) * | 2020-04-16 | 2020-06-26 | 江西师范大学 | Method for making nutritional and convenient fish head vermicelli pot |
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US20150164087A1 (en) * | 2008-06-23 | 2015-06-18 | Novozymes A/S | Bacillus Subtilis Strain |
CN104830578A (en) * | 2015-04-30 | 2015-08-12 | 威莱(广州)日用品有限公司 | High-efficiency toilet cleaning agent and preparation method thereof |
CN105524739A (en) * | 2016-02-03 | 2016-04-27 | 常州市好利莱光电科技有限公司 | Preparation method of natural detergent powder |
CN105733850A (en) * | 2016-03-21 | 2016-07-06 | 陈国丰 | Multifunctional cleaning liquid and preparation method thereof |
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2016
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Patent Citations (6)
Publication number | Priority date | Publication date | Assignee | Title |
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CN1570057A (en) * | 2003-07-21 | 2005-01-26 | 梁浩东 | Natural highly effective environmental protection type cleaning agent and its making method |
EP1916295A2 (en) * | 2006-10-25 | 2008-04-30 | Miura Co., Ltd. | Cleaning Agent |
US20150164087A1 (en) * | 2008-06-23 | 2015-06-18 | Novozymes A/S | Bacillus Subtilis Strain |
CN104830578A (en) * | 2015-04-30 | 2015-08-12 | 威莱(广州)日用品有限公司 | High-efficiency toilet cleaning agent and preparation method thereof |
CN105524739A (en) * | 2016-02-03 | 2016-04-27 | 常州市好利莱光电科技有限公司 | Preparation method of natural detergent powder |
CN105733850A (en) * | 2016-03-21 | 2016-07-06 | 陈国丰 | Multifunctional cleaning liquid and preparation method thereof |
Cited By (2)
Publication number | Priority date | Publication date | Assignee | Title |
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CN110437940A (en) * | 2019-09-07 | 2019-11-12 | 阜阳洁平日化有限公司 | A kind of high-efficiency environment friendly deodorization agent for toilet and preparation method thereof |
CN111329009A (en) * | 2020-04-16 | 2020-06-26 | 江西师范大学 | Method for making nutritional and convenient fish head vermicelli pot |
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