CN106281777A - Cleanout fluid for fixed reference electrode - Google Patents
Cleanout fluid for fixed reference electrode Download PDFInfo
- Publication number
- CN106281777A CN106281777A CN201610571255.2A CN201610571255A CN106281777A CN 106281777 A CN106281777 A CN 106281777A CN 201610571255 A CN201610571255 A CN 201610571255A CN 106281777 A CN106281777 A CN 106281777A
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- CN
- China
- Prior art keywords
- cleanout fluid
- rhizoma curcumae
- curcumae longae
- reference electrode
- electrode
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
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Classifications
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- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
- C11D7/00—Compositions of detergents based essentially on non-surface-active compounds
- C11D7/02—Inorganic compounds
- C11D7/04—Water-soluble compounds
- C11D7/10—Salts
-
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
- C11D7/00—Compositions of detergents based essentially on non-surface-active compounds
- C11D7/22—Organic compounds
-
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
- C11D7/00—Compositions of detergents based essentially on non-surface-active compounds
- C11D7/22—Organic compounds
- C11D7/26—Organic compounds containing oxygen
- C11D7/261—Alcohols; Phenols
-
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
- C11D7/00—Compositions of detergents based essentially on non-surface-active compounds
- C11D7/22—Organic compounds
- C11D7/40—Products in which the composition is not well defined
- C11D7/44—Vegetable products
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- Chemical & Material Sciences (AREA)
- Life Sciences & Earth Sciences (AREA)
- Engineering & Computer Science (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Oil, Petroleum & Natural Gas (AREA)
- Wood Science & Technology (AREA)
- Organic Chemistry (AREA)
- Inorganic Chemistry (AREA)
- Health & Medical Sciences (AREA)
- Emergency Medicine (AREA)
- Cosmetics (AREA)
Abstract
The present invention provides a kind of cleanout fluid for fixed reference electrode, the raw material of following mass ratio to make: Rhizoma Curcumae Longae 1.3, load silver silicone oil 2.5, Sucus Luffae 7, boric acid 0.2, ethanol 3；Rhizoma Curcumae Longae selects fresh Rhizoma Curcumae Longae, grinds to form the granularity slurry less than 20～80 microns stand-by；The slurry that Rhizoma Curcumae Longae grinds to form uniformly and get final product with carrying silver silicone oil, Sucus Luffae, boric acid, ethanol mixture in proportion.The cleanout fluid of the present invention is possible not only to skin surface is played disinfective action, the oil film of skin surface can also be dissolved, the oil film of skin surface is dissolved in cleanout fluid, eliminate the impedance that oil film produces, cleanout fluid can be with electrode cream rapid fusion, and have cleanout fluid and electrode cream is respectively provided with good electric conductivity, after cleanout fluid and electrode cream rapid fusion, electrode cream sticks to skin surface, being fixed by reference electrode, and electrode cream is big with skin contact, conductive effect is good, stable, do not have detection data discontinuously or the situation of unusual fluctuations.
Description
Technical field
The present invention relates to digestive tract power detection apparatus field, particularly relate to a kind of cleaning for fixed reference electrode
Liquid.
Background technology
At present, the monitoring of gastroesophageal reflux would generally be applied pH value of upper digestive tract dynamic monitoring by Digestive System Department clinically
Instrument, is monitored the upper digestive tract acid-base value of patient.I.e. there is electricity by the Digestive system of pH electrode probe with different pH values
Chemical reaction produces corresponding voltage signal, reflects upper gastrointestinal acid-base value information by this voltage signal.Existing skill
In art, pH electrode probe accuracy of detection is low, makes the detected value misalignment of pH, it is impossible to reflect the truth of patient real-time and accurately.And
And existing pH value of upper digestive tract dynamic monitor, during use, reference electrode is fixed, need use adhesive tape or stretch tight
Band, just can be fixed in the skin surface of person under inspection shirtfront, fixation procedure and the reference that to take off process the most very inconvenient, fixing
Often there is conducting electricity the best situation in electrode, affects the monitoring accuracy of pH value of upper digestive tract dynamic monitor.
Summary of the invention
It is an object of the invention to provide a kind of cleanout fluid for fixed reference electrode, and the fixing side of reference electrode
Method, designs the fixed solution of a kind of reference electrode, to solve above-mentioned technical problem for pH value of upper digestive tract dynamic monitor.
The technical problem to be solved realizes by the following technical solutions:
A kind of cleanout fluid for fixed reference electrode, it is characterised in that the raw material of following mass ratio is made: Rhizoma Curcumae Longae 1.3,
Carry silver silicone oil 2.5, Sucus Luffae 7, boric acid 0.2, ethanol 3；
Rhizoma Curcumae Longae selects fresh Rhizoma Curcumae Longae, grinds to form the granularity slurry less than 20～80 microns stand-by；
The slurry that Rhizoma Curcumae Longae grinds to form uniformly and get final product with carrying silver silicone oil, Sucus Luffae, boric acid, ethanol mixture in proportion.
As preferably, the described silver ion content carrying silver silicone oil is 2.3%～2.5%.
The reference electrode fixing means of a kind of pH value of upper digestive tract dynamic monitor, it is characterised in that step is:
(1) reference electrode is immersed in buffer, soak 2 hours, take out, dry with filter paper；
(2) coating electrode cream on reference electrode surface, electrode cream is uniformly wrapped in the surface of reference electrode, and thickness is 2-
5mm；
(3) the skin surface cotton swab of person under inspection shirtfront dips in cleanout fluid wiped clean；
(4), before the cleanout fluid at skin surface is not completely dried, reference electrode is affixed on the skin surface of wiped clean,
Make that electrode cream is as much as possible sticks to skin surface, i.e. fixed reference electrode.
As preferably, described buffer is prepared from by following raw material: glycerol, ethanol, water, 5% D/W, lemon
Lemon acid,
Preparation method is as follows:
(1) prepare the raw material of following mass ratio: glycerol 1.5, ethanol 2, water 15, and glycerol, ethanol are mixed in proportion with water
Synthetic solvent A；
(2) prepare the raw material of following mass ratio: 5% D/W, citric acid, take 5% D/W and lemon
Lemon acid is 5:1 mixing and stirring in mass ratio, obtains solution B；
(3) taking solution B to be slowly added dropwise in solution A, the pH value to mixed solution is 3.07, obtains buffer.
As preferably, described glycerol with aerosil for support dispersion in buffer, glycerol and gas phase titanium dioxide
The mass ratio of silicon is 2.03:17.5, and glycerol is dissolved in the hot water of 3 times of quality, and hot water temperature is not less than 80 DEG C, then with gas phase
Silicon dioxide mixes, and more than continuous stirring 5min, is placed in cold preservation 10min at a temperature of-12 DEG C；It is warming up to-2 DEG C, insulation
30min；It is warming up to 8 DEG C again, is incubated 10min；It is warming up to 20 DEG C again, is incubated 10min, rise gentle insulating process for three times all in negative pressure
Carrying out under state, the pressure of negative pressure state is less than 55kPa.
As preferably, described electrode cream is made up of the raw material of following mass ratio:
Resin 3, dimethylbenzene 6, zinc oxide 0.6, Colophonium 1.2, silver chloride 0.4, silica gel 5, Fructus Hordei Germinatus powder 5.2, white carbon 3.5,
By resin, dimethylbenzene, Colophonium mixing, obtain material A；
Adding silver chloride and zinc oxide again in silica gel, stir to obtain material B；
Material A is mixed with material B, continuously stirred during, add white carbon, after white carbon is uniformly dispersed, be warming up to
53 DEG C, add maltol, continue to stir and get final product.
As preferably, the particle diameter of described white carbon is distributed in 30-80 micron.
The invention has the beneficial effects as follows:
Clinical diagnosis that pH value of upper digestive tract dynamic monitor is gastro oesophageal reflux disease (GORD) and pathology, study mechanism provide
A kind of medical science detection means.
Through activation processing in buffer before reference electrode use, electrode reaction is sensitive, and electrode surface is distributed trickle
Granule, makes electrode surface have more fine and smooth lubricity, can play a protective role person's windpipe, improves conduction sensitivity,
To improve monitoring accuracy；
Cleanout fluid is possible not only to skin surface is played disinfective action, it is also possible to dissolve the oil film of skin surface, by skin
The oil film on surface dissolves in cleanout fluid, eliminates the impedance that oil film produces, and cleanout fluid with electrode cream rapid fusion, and can have cleaning
After liquid and electrode cream are respectively provided with good electric conductivity, cleanout fluid and electrode cream rapid fusion, electrode cream sticks to skin surface, will
Reference electrode is fixed, and electrode cream is big with skin contact, and conductive effect is good, stable, does not haves detection data interrupted
Or the situation of unusual fluctuations.
Electrode cream has preferable anti-corrosive properties, not stimulates skin.
The present invention is the fixed solution that pH value of upper digestive tract dynamic monitor devises a kind of reference electrode, solves existing
The problem that fixed form operation is inconvenient, also overcomes insensitive, unstable the asking of reference electrode electric conductivity after fixing simultaneously
Topic, it is to avoid Monitoring Data fluctuation or inaccurate situation occurs in pH value of upper digestive tract dynamic monitor.
Detailed description of the invention
For the technological means making the present invention realize, creation characteristic, reach purpose and be easy to understand with effect, below knot
Close specific embodiment, the present invention is expanded on further, but following embodiment is only the preferred embodiments of the present invention, and not all.
Based on the embodiment in embodiment, it is real that those skilled in the art are obtained other on the premise of not making creative work
Execute example, broadly fall into protection scope of the present invention.
Electrode cream is made up of the raw material of following mass ratio:
Resin 3, dimethylbenzene 6, zinc oxide 0.6, Colophonium 1.2, silver chloride 0.4, silica gel 5, Fructus Hordei Germinatus powder 5.2, white carbon 3.5,
Preparation process is:
By resin, dimethylbenzene, Colophonium mixing, obtain material A；
Adding silver chloride and zinc oxide again in silica gel, stir to obtain material B；
Material A is mixed with material B, continuously stirred during, add white carbon, after white carbon is uniformly dispersed, be warming up to
53 DEG C, add maltol, continue to stir and get final product.
Cleanout fluid is made up of the raw material of following mass ratio:
Rhizoma Curcumae Longae 1.3, load silver silicone oil 2.5, Sucus Luffae 7, boric acid 0.2, ethanol 3；
Rhizoma Curcumae Longae selects fresh Rhizoma Curcumae Longae, grinds to form the granularity slurry less than 20～80 microns stand-by；
The silver ion content carrying silver silicone oil is 2.3%～2.5%；
The slurry that Rhizoma Curcumae Longae grinds to form uniformly and get final product with carrying silver silicone oil, Sucus Luffae, boric acid, ethanol mixture in proportion.
Buffer is prepared from by following raw material: glycerol, ethanol, water, 5% D/W, citric acid,
Preparation method is as follows:
(1) prepare the raw material of following mass ratio: glycerol 1.5, ethanol 2, water 15, and glycerol, ethanol are mixed in proportion with water
Synthetic solvent A；
(2) prepare the raw material of following mass ratio: 5% D/W, citric acid, take 5% D/W and lemon
Lemon acid is 5:1 mixing and stirring in mass ratio, obtains solution B；
(3) taking solution B to be slowly added dropwise in solution A, the pH value to mixed solution is 3.07, obtains buffer.
A kind of reference electrode fixing means of pH value of upper digestive tract dynamic monitor, step is:
(1) reference electrode is immersed in buffer, soak 2 hours, take out, dry with filter paper；
(2) coating electrode cream on reference electrode surface, electrode cream is uniformly wrapped in the surface of reference electrode, and thickness is 2-
5mm；
(3) the skin surface cotton swab of person under inspection shirtfront dips in cleanout fluid wiped clean；
(4), before the cleanout fluid at skin surface is not completely dried, reference electrode is affixed on the skin surface of wiped clean,
Make that electrode cream is as much as possible sticks to skin surface, i.e. fixed reference electrode.
The ultimate principle of the present invention, principal character and advantages of the present invention have more than been shown and described.The technology of the industry
The personnel only present invention it should be appreciated that the present invention is not restricted to the described embodiments, described in above-described embodiment and description
Preference, be not intended to limit the present invention, without departing from the spirit and scope of the present invention, the present invention also has various
Changes and improvements, these changes and improvements both fall within scope of the claimed invention.Claimed scope is by institute
Attached claims and equivalent thereof define.
Claims (2)
1. the cleanout fluid for fixed reference electrode, it is characterised in that the raw material of following mass ratio is made: Rhizoma Curcumae Longae 1.3, load
Silver silicone oil 2.5, Sucus Luffae 7, boric acid 0.2, ethanol 3；
Rhizoma Curcumae Longae selects fresh Rhizoma Curcumae Longae, grinds to form the granularity slurry less than 20～80 microns stand-by；
The slurry that Rhizoma Curcumae Longae grinds to form uniformly and get final product with carrying silver silicone oil, Sucus Luffae, boric acid, ethanol mixture in proportion.
Cleanout fluid for fixed reference electrode the most according to claim 1, it is characterised in that the silver of described load silver silicone oil
Ion concentration is 2.3%～2.5%.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201610571255.2A CN106281777A (en) | 2016-07-19 | 2016-07-19 | Cleanout fluid for fixed reference electrode |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201610571255.2A CN106281777A (en) | 2016-07-19 | 2016-07-19 | Cleanout fluid for fixed reference electrode |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| CN106281777A true CN106281777A (en) | 2017-01-04 |
Family
ID=57651713
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN201610571255.2A Pending CN106281777A (en) | 2016-07-19 | 2016-07-19 | Cleanout fluid for fixed reference electrode |
Country Status (1)
| Country | Link |
|---|---|
| CN (1) | CN106281777A (en) |
Citations (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN1977820A (en) * | 2005-12-05 | 2007-06-13 | 刘建平 | Vegetable sponge beauty product |
| CN104450297A (en) * | 2013-09-23 | 2015-03-25 | 盛小华 | Rhizome-curcumae-longae composition cleaning fluid |
| CN104611162A (en) * | 2015-03-07 | 2015-05-13 | 孙华平 | Environment-friendly cleaning agent for mechanical equipment |
| CN105709260A (en) * | 2016-04-19 | 2016-06-29 | 陈兆权 | Electrostatic spinning solution based on epidermal growth factor and preparation method thereof |
-
2016
- 2016-07-19 CN CN201610571255.2A patent/CN106281777A/en active Pending
Patent Citations (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN1977820A (en) * | 2005-12-05 | 2007-06-13 | 刘建平 | Vegetable sponge beauty product |
| CN104450297A (en) * | 2013-09-23 | 2015-03-25 | 盛小华 | Rhizome-curcumae-longae composition cleaning fluid |
| CN104611162A (en) * | 2015-03-07 | 2015-05-13 | 孙华平 | Environment-friendly cleaning agent for mechanical equipment |
| CN105709260A (en) * | 2016-04-19 | 2016-06-29 | 陈兆权 | Electrostatic spinning solution based on epidermal growth factor and preparation method thereof |
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| RJ01 | Rejection of invention patent application after publication |
Application publication date: 20170104 |
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| RJ01 | Rejection of invention patent application after publication |