CN106281744B - 一种婴幼儿衣物用浓缩洗涤剂及其制备方法 - Google Patents
一种婴幼儿衣物用浓缩洗涤剂及其制备方法 Download PDFInfo
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Abstract
本发明提供了一种婴幼儿衣物用浓缩洗涤剂及其制备方法,洗涤剂的原料包括:氢化椰子油脂肪酸、氢氧化钾、脂肪醇聚氧乙烯醚、二甲苯磺酸盐、柠檬酸钠、二甲基硅油、蚕丝蛋白、壳聚糖、醋酸溶液、羟丙甲基纤维素、柠檬酸三正丁酯、聚乙烯醇、戊二醛、二羟甲基丙酸、卵磷脂、硬脂酸、碳酸氢钠和水。其制备方法是先制备洗涤剂组分,再制备壳聚糖组分,最后将其混合,即得。本发明的婴幼儿衣物用浓缩洗涤剂,洗涤衣物柔软性好,对婴儿皮肤具有很好的亲和力,并能有效洗去婴幼儿衣物的顽固污渍,显著降低洗涤后的残留。
Description
技术领域
本发明属于日化用品技术领域,具体涉及一种婴幼儿衣物用浓缩洗涤剂及其制备方法。
背景技术
当代快速的工业化进程正在导致全球气候变化,从而使全球生态系统受到破坏,中国洗涤用品工业协会发布报告称,浓缩洗涤剂在生产运输和使用过程中,能显著节约能源资源、减少排放,已成为全球尤其是发达国家洗涤剂市场的主流。
目前浓缩型洗涤剂产品在中国并不多,尤其是低泡浓缩型的产品更是空白,而国外尤其是欧洲和日本此类产品日益增多并深受消费者欢迎。调查数据显示,目前我国浓缩洗涤剂使用比例仅占3%,美国是90%,日本几乎达到100%;浓缩洗涤剂在所有的环境影响方面都比普通洗涤剂优异,以消费者每次洗涤剂算,相比普通型产品而言,浓缩洗衣液可以减少31毫克二氧化碳当量排放,减少0.12毫克二氧化硫当量排放,减少550千焦能源消耗。另外,浓缩型产品中更多的有效化学成分可以降低单次洗涤所消耗的洗涤剂用量,也更适用于低温洗涤。同时,浓缩型产品还可以减少包装材料的消耗,节约运输的费用并节省储存的空间。
目前市场上绝大部分的婴幼儿洗衣液主要强调的都是洗衣液的去污功能而忽视了柔软性和无剌激性,浓缩型洗衣液单次用量少,不仅能减少对婴幼儿皮肤的刺激,而且能降低洗衣液成分的残留量。
发明内容
本发明的目的是克服现有技术的不足而提供一种婴幼儿衣物用浓缩洗涤剂及其制备方法,该洗涤剂,洗涤衣物柔软性好,对婴儿皮肤具有很好的亲和力,并能有效洗去婴幼儿衣物的顽固污渍,显著降低洗涤后的残留。
一种婴幼儿衣物用浓缩洗涤剂,原料以重量份计包括:氢化椰子油脂肪酸8-12份,氢氧化钾8-12份,脂肪醇聚氧乙烯醚1-4份,二甲苯磺酸盐0.5-1.2份,柠檬酸钠0.3-0.9份,二甲基硅油0.1-0.5份,蚕丝蛋白0.05-0.15份,壳聚糖10份,醋酸溶液10-20份,羟丙甲基纤维素0.4-1.5份,柠檬酸三正丁酯1.2-2份,聚乙烯醇0.6-0.9份,戊二醛0.3-0.9份,二羟甲基丙酸0.6-1.1份,卵磷脂0.3-0.5份,硬脂酸0.2-0.7份,碳酸氢钠2-6份,水10份。
进一步地,所述脂肪醇聚氧乙烯醚为AEO3或AEO7。
进一步地,所述醋酸溶液的浓度为1-4v/v%。
上述婴幼儿衣物用浓缩洗涤剂的制备方法,包括以下步骤:
步骤1,将氢化椰子油脂肪酸、氢氧化钾加至水中,升温至65-75℃搅拌保温40-70min,在搅拌条件下加入脂肪醇聚氧乙烯醚、二甲苯磺酸盐、柠檬酸钠、二甲基硅油、蚕丝蛋白,分散,调节pH至8-8.5,得到混合物A;
步骤2,将壳聚糖加至醋酸溶液中,再加入羟丙甲基纤维素、柠檬酸三正丁酯、聚乙烯醇、戊二醛、二羟甲基丙酸、卵磷脂、硬脂酸,超声,得到混合物B;
步骤3,将混合物A加至混合物B中,加入碳酸氢钠,搅拌,升温至45-55℃,保温2-4h,再降温至5-10℃,保温2-4h,即得。
进一步地,步骤1中搅拌速度为100-150rpm。
进一步地,步骤1中分散速度为800-1000rp、时间为10-15min。
进一步地,步骤2中超声条件为70-120w。
进一步地,步骤3中搅拌条件为200-300rpm、30-60min。
本发明的婴幼儿衣物用浓缩洗涤剂,洗涤衣物柔软性好,对婴儿皮肤具有很好的亲和力,并能有效洗去婴幼儿衣物的顽固污渍,显著降低洗涤后的残留。
具体实施方式
实施例1
一种婴幼儿衣物用浓缩洗涤剂,原料以重量份计包括:氢化椰子油脂肪酸8份,氢氧化钾8份,脂肪醇聚氧乙烯醚AEO3 1份,二甲苯磺酸盐0.5份,柠檬酸钠0.3份,二甲基硅油0.1份,蚕丝蛋白0.05份,壳聚糖10份,1v/v%醋酸溶液10份,羟丙甲基纤维素0.4份,柠檬酸三正丁酯1.2份,聚乙烯醇0.6份,戊二醛0.3份,二羟甲基丙酸0.6份,卵磷脂0.3份,硬脂酸0.2份,碳酸氢钠2份,水10份。
上述婴幼儿衣物用浓缩洗涤剂的制备方法,包括以下步骤:
步骤1,将氢化椰子油脂肪酸、氢氧化钾加至水中,升温至65℃搅拌保温70min,在搅拌条件下加入脂肪醇聚氧乙烯醚、二甲苯磺酸盐、柠檬酸钠、二甲基硅油、蚕丝蛋白,分散,调节pH至8-8.5,得到混合物A;
步骤2,将壳聚糖加至醋酸溶液中,再加入羟丙甲基纤维素、柠檬酸三正丁酯、聚乙烯醇、戊二醛、二羟甲基丙酸、卵磷脂、硬脂酸,超声,得到混合物B;
步骤3,将混合物A加至混合物B中,加入碳酸氢钠,搅拌,升温至45℃,保温4h,再降温至5℃,保温4h,即得。
其中,步骤1中搅拌速度为100-150rpm,分散速度为800rpm、时间为15min;步骤2中超声条件为70-120w;步骤3中搅拌条件为200rpm、60min。
实施例2
一种婴幼儿衣物用浓缩洗涤剂,原料以重量份计包括:氢化椰子油脂肪酸10份,氢氧化钾8份,脂肪醇聚氧乙烯醚AEO7 3份,二甲苯磺酸盐0.9份,柠檬酸钠0.7份,二甲基硅油0.3份,蚕丝蛋白0.08份,壳聚糖10份,2v/v%醋酸溶液13份,羟丙甲基纤维素0.8份,柠檬酸三正丁酯1.7份,聚乙烯醇0.7份,戊二醛0.5份,二羟甲基丙酸0.9份,卵磷脂0.4份,硬脂酸0.5份,碳酸氢钠5份,水10份。
上述婴幼儿衣物用浓缩洗涤剂的制备方法,包括以下步骤:
步骤1,将氢化椰子油脂肪酸、氢氧化钾加至水中,升温至70℃搅拌保温50min,在搅拌条件下加入脂肪醇聚氧乙烯醚、二甲苯磺酸盐、柠檬酸钠、二甲基硅油、蚕丝蛋白,分散,调节pH至8-8.5,得到混合物A;
步骤2,将壳聚糖加至醋酸溶液中,再加入羟丙甲基纤维素、柠檬酸三正丁酯、聚乙烯醇、戊二醛、二羟甲基丙酸、卵磷脂、硬脂酸,超声,得到混合物B;
步骤3,将混合物A加至混合物B中,加入碳酸氢钠,搅拌,升温至45℃,保温4h,再降温至5℃,保温4h,即得。
其中,步骤1中搅拌速度为100-150rpm,分散速度为800rpm、时间为15min;步骤2中超声条件为70-120w;步骤3中搅拌条件为200rpm、60min。
实施例3
一种婴幼儿衣物用浓缩洗涤剂,原料以重量份计包括:氢化椰子油脂肪酸11份,氢氧化钾9份,脂肪醇聚氧乙烯醚AEO3 3份,二甲苯磺酸盐0.9份,柠檬酸钠0.4份,二甲基硅油0.5份,蚕丝蛋白0.11份,壳聚糖10份,1v/v%醋酸溶液17份,羟丙甲基纤维素1.2份,柠檬酸三正丁酯1.7份,聚乙烯醇0.8份,戊二醛0.7份,二羟甲基丙酸0.9份,卵磷脂0.3份,硬脂酸0.5份,碳酸氢钠4份,水10份。
上述婴幼儿衣物用浓缩洗涤剂的制备方法,包括以下步骤:
步骤1,将氢化椰子油脂肪酸、氢氧化钾加至水中,升温至65℃搅拌保温70min,在搅拌条件下加入脂肪醇聚氧乙烯醚、二甲苯磺酸盐、柠檬酸钠、二甲基硅油、蚕丝蛋白,分散,调节pH至8-8.5,得到混合物A;
步骤2,将壳聚糖加至醋酸溶液中,再加入羟丙甲基纤维素、柠檬酸三正丁酯、聚乙烯醇、戊二醛、二羟甲基丙酸、卵磷脂、硬脂酸,超声,得到混合物B;
步骤3,将混合物A加至混合物B中,加入碳酸氢钠,搅拌,升温至50℃,保温3h,再降温至8℃,保温3h,即得。
其中,步骤1中搅拌速度为100-150rpm,分散速度为900rpm、时间为15min;步骤2中超声条件为70-120w;步骤3中搅拌条件为200rpm、40min。
实施例4
一种婴幼儿衣物用浓缩洗涤剂,原料以重量份计包括:氢化椰子油脂肪酸12份,氢氧化钾12份,脂肪醇聚氧乙烯醚AEO3 4份,二甲苯磺酸盐1.2份,柠檬酸钠0.9份,二甲基硅油0.5份,蚕丝蛋白0.15份,壳聚糖10份,4v/v%醋酸溶液20份,羟丙甲基纤维素1.5份,柠檬酸三正丁酯2份,聚乙烯醇0.9份,戊二醛0.9份,二羟甲基丙酸1.1份,卵磷脂0.5份,硬脂酸0.7份,碳酸氢钠6份,水10份。
上述婴幼儿衣物用浓缩洗涤剂的制备方法,包括以下步骤:
步骤1,将氢化椰子油脂肪酸、氢氧化钾加至水中,升温至75℃搅拌保温40min,在搅拌条件下加入脂肪醇聚氧乙烯醚、二甲苯磺酸盐、柠檬酸钠、二甲基硅油、蚕丝蛋白,分散,调节pH至8-8.5,得到混合物A;
步骤2,将壳聚糖加至醋酸溶液中,再加入羟丙甲基纤维素、柠檬酸三正丁酯、聚乙烯醇、戊二醛、二羟甲基丙酸、卵磷脂、硬脂酸,超声,得到混合物B;
步骤3,将混合物A加至混合物B中,加入碳酸氢钠,搅拌,升温至55℃,保温2h,再降温至10℃,保温2h,即得。
其中,步骤1中搅拌速度为100-150rpm,分散速度为1000rpm、时间为10min;步骤2中超声条件为70-120w;步骤3中搅拌条件为300rpm、30min。
实施例5
本实施例与实施例2的区别在于:未加入蚕丝蛋白。
实施例6
本实施例与实施例2的区别在于:未加入卵磷脂。
去污力评价
采用国标炭黑污布JB-01、国标蛋白污布JB-02、国标皮脂污布JB-03,测试洗衣液的洗涤浓度为0.04g/L,具体实验条件及方法参照QB1224-2012。结果如下:
由上表结果可知,本发明的洗涤剂具有很好的去污能力,对蛋白类污垢、皮脂类污垢具有良好的乳化能力,去污效果好,能有效去除婴儿衣物的便尿渍、口水渍、食物油污等。
泡沫及漂洗性能评价:
洗涤浓度为样品浓度1g/L,150ppm硬水,采用白色毛巾作为洗涤对象,以手洗的方式进行洗涤,搓洗30次后静置30s,用刻度尺测量洗衣盆中的泡沫高度,洗涤完成后把毛巾拧干(控制湿重是干重的3倍)再用硬水进行漂洗,通过观察漂洗水中的泡沫判断是否漂洗干净,记录漂洗次数。结果如下:
由上表可知,本发明的洗涤剂泡沫较低,仅需1~2次漂洗即可漂清。
柔软性能测试
测试方法:①循环洗涤:将测试毛巾(纯棉)放入滚筒式洗衣机中,加入实施例2的洗涤剂,开启洗衣机,在相同条件下(快洗30分钟)自动完成洗涤过程,连续进行20次,取出置于衣架上自然晾干,待测试使用。
②感官测试:将标准毛巾和测试毛巾平铺于测试者手心(共10人),用适当的力度在两边脸颊上摩擦或者用手同时感受其柔软性,对比标准毛巾,对其柔软性能进行评分(10最软,1最硬)。
结果显示,本发明的洗涤剂具有良好的柔顺效果。
本发明采用壳聚糖包覆,将洗涤成分制成缓释洗涤剂,不仅能有效提高洗涤成分的洗涤效果,还能减少洗涤成分的残留量。实施例5中,由于未加入蚕丝蛋白,使得洗涤剂去污力降低,可能是因为蚕丝蛋白能减少皂基的氧化酸败,大大提升了洗涤剂的去污效果;实施例6中,由于未加入卵磷脂,导致洗涤剂泡沫高、漂洗难,这可能是因为卵磷脂能增强改性壳聚糖结构的致密性,从而提高改性壳聚糖对洗涤成分的包覆性。
Claims (1)
1.一种婴幼儿衣物用浓缩洗涤剂,其特征在于:原料以重量份计包括:氢化椰子油脂肪酸10份,氢氧化钾8份,脂肪醇聚氧乙烯醚AEO7 3份,二甲苯磺酸盐0.9份,柠檬酸钠0.7份,二甲基硅油0.3份,蚕丝蛋白0.08份,壳聚糖10份,2v/v%醋酸溶液13份,羟丙甲基纤维素0.8份,柠檬酸三正丁酯1.7份,聚乙烯醇0.7份,戊二醛0.5份,二羟甲基丙酸0.9份,卵磷脂0.4份,硬脂酸0.5份,碳酸氢钠5份,水10份;所述的婴幼儿衣物用浓缩洗涤剂的制备方法,包括以下步骤:步骤1,将氢化椰子油脂肪酸、氢氧化钾加至水中,升温至70℃搅拌保温50min,在搅拌条件下加入脂肪醇聚氧乙烯醚、二甲苯磺酸盐、柠檬酸钠、二甲基硅油、蚕丝蛋白,分散,调节pH至8-8.5,得到混合物A;步骤2,将壳聚糖加至醋酸溶液中,再加入羟丙甲基纤维素、柠檬酸三正丁酯、聚乙烯醇、戊二醛、二羟甲基丙酸、卵磷脂、硬脂酸,超声,得到混合物B;步骤3,将混合物A加至混合物B中,加入碳酸氢钠,搅拌,升温至45℃,保温4h,再降温至5℃,保温4h,即得;其中,步骤1中搅拌速度为100-150rpm,分散速度为800rpm、时间为15min;步骤2中超声条件为70-120w;步骤3中搅拌条件为200rpm、60min。
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