CN106281699A - The extraction of a kind of Flos Tagetis Erectae quintessence oil and processing method - Google Patents
The extraction of a kind of Flos Tagetis Erectae quintessence oil and processing method Download PDFInfo
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- CN106281699A CN106281699A CN201610673567.4A CN201610673567A CN106281699A CN 106281699 A CN106281699 A CN 106281699A CN 201610673567 A CN201610673567 A CN 201610673567A CN 106281699 A CN106281699 A CN 106281699A
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- flos tagetis
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- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11B—PRODUCING, e.g. BY PRESSING RAW MATERIALS OR BY EXTRACTION FROM WASTE MATERIALS, REFINING OR PRESERVING FATS, FATTY SUBSTANCES, e.g. LANOLIN, FATTY OILS OR WAXES; ESSENTIAL OILS; PERFUMES
- C11B9/00—Essential oils; Perfumes
- C11B9/02—Recovery or refining of essential oils from raw materials
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- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11B—PRODUCING, e.g. BY PRESSING RAW MATERIALS OR BY EXTRACTION FROM WASTE MATERIALS, REFINING OR PRESERVING FATS, FATTY SUBSTANCES, e.g. LANOLIN, FATTY OILS OR WAXES; ESSENTIAL OILS; PERFUMES
- C11B9/00—Essential oils; Perfumes
- C11B9/0003—Compounds of unspecified constitution defined by the chemical reaction for their preparation
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- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11B—PRODUCING, e.g. BY PRESSING RAW MATERIALS OR BY EXTRACTION FROM WASTE MATERIALS, REFINING OR PRESERVING FATS, FATTY SUBSTANCES, e.g. LANOLIN, FATTY OILS OR WAXES; ESSENTIAL OILS; PERFUMES
- C11B9/00—Essential oils; Perfumes
- C11B9/02—Recovery or refining of essential oils from raw materials
- C11B9/022—Refining
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- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11B—PRODUCING, e.g. BY PRESSING RAW MATERIALS OR BY EXTRACTION FROM WASTE MATERIALS, REFINING OR PRESERVING FATS, FATTY SUBSTANCES, e.g. LANOLIN, FATTY OILS OR WAXES; ESSENTIAL OILS; PERFUMES
- C11B9/00—Essential oils; Perfumes
- C11B9/02—Recovery or refining of essential oils from raw materials
- C11B9/027—Recovery of volatiles by distillation or stripping
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- Oil, Petroleum & Natural Gas (AREA)
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- General Chemical & Material Sciences (AREA)
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- Fats And Perfumes (AREA)
Abstract
The invention discloses extraction and the processing method of a kind of Flos Tagetis Erectae quintessence oil, comprise the following steps: the aerial parts then cutting of Tagetes erecta of gathering in fine day, spread 36 hours on ground；Putting into after adding deionized water in boiler, with direct steam heating to 80 DEG C, then use indirect steam heating extremely micro-boiling instead, condensed fluid carries out oil-water separation and obtains a Flos Tagetis Erectae quintessence oil；Distillate after single flash separation Flos Tagetis Erectae quintessence oil is rejoined in boiler, carries out heating with indirect steam and obtain secondary Flos Tagetis Erectae quintessence oil；By Flos Tagetis Erectae quintessence oil with secondary Flos Tagetis Erectae quintessence oil ratio for 1.5:1 in mass ratio mix homogeneously and obtain standard Flos Tagetis Erectae quintessence oil, it is sequentially added into anhydrous sodium sulfate, activated carbon, and stir 48 hours at normal temperatures, it is filtrated to get the standard Flos Tagetis Erectae quintessence oil of dehydration and decolorization；Through dehydration and decolorization standard Flos Tagetis Erectae quintessence oil bottle, seal be placed under the sun irradiation 7 days.The quality better of the Flos Tagetis Erectae quintessence oil that the method for the invention obtains.
Description
Technical field
The present invention relates to chemical field, be specifically related to extraction and the processing method of a kind of Flos Tagetis Erectae quintessence oil.
Background technology
Flos Tagetis Erectae quintessence oil is the volatile oil extracted from the flower or branch and leaf of Compositae Tagetes annual herb plant.Wan Shou
Containing 30 Multiple components in chrysanthemum quintessence oil, be mainly composed of dihydrotagetone, trauls-ss-Ocimene, trans-tagetone,
Alkene etc..Flos Tagetis Erectae quintessence oil can be used for modulation and intends the graceful perfume of odor type, floral water and fragrance medical-type cosmetics, it may also be used for join
Edible essence processed, flavouring essence for tobacco and health beverage.The poor quality of the Flos Tagetis Erectae quintessence oil that prior art is extracted, trauls-ss-Ocimene,
The content of trans-tagetone, alkene etc. is relatively low.
Summary of the invention
In view of this, it is an object of the invention to provide extraction and the processing method of a kind of Flos Tagetis Erectae quintessence oil.
For achieving the above object, the technical solution used in the present invention is as follows:
A, the aerial parts of Flos Tagetis Erectae of gathering in fine day, then cutting, spread 3-6 hour on ground；
B, add in the Flos Tagetis Erectae through spreading and put in boiler, with direct steam heating to 80 after deionized water
DEG C, then use indirect steam heating extremely boiling instead, condensed fluid enters oil water separator and carries out oil-water separation, collects in oil water separator
Flos Tagetis Erectae quintessence oil, obtain a Flos Tagetis Erectae quintessence oil；
C, the distillate after single flash separation Flos Tagetis Erectae quintessence oil is rejoined in boiler, add with indirect steam
Heat, collects the Flos Tagetis Erectae quintessence oil in oil water separator, obtains secondary Flos Tagetis Erectae quintessence oil；
D, Flos Tagetis Erectae oil is mixed homogeneously by weight the ratio of 1.5:1 with secondary Flos Tagetis Erectae oil, marked
Quasi-Flos Tagetis Erectae quintessence oil, adds anhydrous sodium sulfate dry filter and makees processed；
E, in the standard Flos Tagetis Erectae quintessence oil of processed add activated carbon, and at normal temperatures stirring 48 hours, mistake
Filter obtains the standard Flos Tagetis Erectae quintessence oil of dehydration and decolorization；
F, through dehydration and decolorization standard Flos Tagetis Erectae quintessence oil bottle, seal be placed under the sun irradiation 7 days.
Special, boiling described in step B refers to micro-boiling, has the most just started to generate blister.
Further, in step A, gather Flos Tagetis Erectae aerial parts in fine day, be then cut into the section of a length of 9.5-10.5cm.
Further, during spreading described in step A, the thickness of flower layer is less than 20cm.
Further, the amount of the deionized water added described in step B is the 3 of the quality of the Flos Tagetis Erectae branch section through spreading
Times.
Further, in step B, with concretely comprising the following steps of indirect steam distillation: first condensate temperature be 30-35 DEG C,
Connecing quantity of steam is to carry out under the conditions of 200L/ hour 1 hour；Then condensate temperature be 35-40 DEG C, indirect steam amount be
Carry out under the conditions of 300L/ hour 1 hour.
Further, in step C, the design parameter of distillation is set to: indirect steam amount is 300L/ hour, and distillate exports
Temperature is 35-40 DEG C, and distillation time is 2-3 hour.
Further, in step D, the amount of the anhydrous sodium sulfate of addition is the 5% of standard Flos Tagetis Erectae quintessence oil quality.
Further, in step E, add amount is standard Flos Tagetis Erectae quintessence oil quality the 5% of activated carbon.
Further, further comprising the steps of, the activated carbon having adsorbed Flos Tagetis Erectae quintessence oil after filtering heavily is steamed
To reclaim Flos Tagetis Erectae quintessence oil.
The invention has the beneficial effects as follows:
The quality better of the Flos Tagetis Erectae quintessence oil that the method for the invention obtains.Compared with prior art, the method for the invention
The content of the trauls-ss-Ocimene in the Flos Tagetis Erectae quintessence oil obtained improves 28.70%；The content of trans-tagetone improves
34.64%；The content of alkene improves 26.13%；The content of cis-tagetone improves 30.86%；Trans-Herba Ocimi (Herba Ocimi Pilosi)
The content of ketenes improves 27.71%；The content of cis-Ocimene ketone improves 25.80%.
Detailed description of the invention
Embodiment 1
The extraction of a kind of Flos Tagetis Erectae quintessence oil and processing method, comprise the following steps:
A, the aerial parts of Flos Tagetis Erectae of gathering in fine day, be then cut into the section of a length of 10.5cm and be placed in ground and spread 6
Hour, during spreading, the thickness of flower layer is less than 20cm；
B, add in the Flos Tagetis Erectae branch section through spreading and put in boiler after deionized water, the deionized water of addition
3 times of the quality that amount is Flos Tagetis Erectae branch section through spreading, with direct steam heating to 80 DEG C, then use indirect steam instead and add
Heat is to micro-boiling, and condensed fluid enters oil water separator and carries out oil-water separation, first condensate temperature be 35 DEG C, indirect steam amount be
Carry out under the conditions of 200L/ hour 1 hour；Then condensate temperature be 35 DEG C, indirect steam amount be to enter under the conditions of 300L/ hour
Row 1 hour, collects the Flos Tagetis Erectae quintessence oil in oil water separator, obtains a Flos Tagetis Erectae quintessence oil, and Flos Tagetis Erectae extraction of essential oil rate is
0.019%；
C, the distillate after single flash separation Flos Tagetis Erectae quintessence oil is rejoined in boiler, add with indirect steam
Heat, indirect steam amount is 300L/ hour, and distillate outlet temperature is 40 DEG C, and distillation time is 2 hours, collects oil water separator
In Flos Tagetis Erectae quintessence oil, obtain secondary Flos Tagetis Erectae quintessence oil, Flos Tagetis Erectae extraction of essential oil rate is single flash liquid 0.014%；
D, by Flos Tagetis Erectae quintessence oil with secondary Flos Tagetis Erectae quintessence oil ratio for 1.5:1 in mass ratio mix homogeneously and marked
Quasi-Flos Tagetis Erectae quintessence oil, is subsequently adding anhydrous sodium sulfate dry filter and carries out processed, and the amount of the anhydrous sodium sulfate of addition is mark
The 5% of quasi-Flos Tagetis Erectae quintessence oil quality；
E, in the standard Flos Tagetis Erectae quintessence oil of processed add activated carbon, add activated carbon amount be standard ten thousand longevity
The 5% of chrysanthemum quintessence oil quality, and stirring 48 hours at normal temperatures, be filtrated to get the standard Flos Tagetis Erectae quintessence oil of dehydration and decolorization；To process
The activated carbon having adsorbed Flos Tagetis Erectae quintessence oil after filtration heavily steams to reclaim Flos Tagetis Erectae quintessence oil；
F, through dehydration and decolorization standard Flos Tagetis Erectae quintessence oil bottle, seal be placed under the sun irradiation 7 days.
Embodiment 2
The extraction of a kind of Flos Tagetis Erectae quintessence oil and processing method, comprise the following steps:
A, become the section of a length of 9.5cm to be placed in ground to spread 3 hours, spread in fine day Flos Tagetis Erectae branch rear cutout of gathering
In journey, the thickness of flower layer is less than 20cm；
B, add in the Flos Tagetis Erectae branch section through spreading and put in boiler after deionized water, the deionized water of addition
3 times of the quality that amount is Flos Tagetis Erectae branch section through spreading, with direct steam heating to 80 DEG C, then use indirect steam instead and add
Heat is to micro-boiling, and condensed fluid enters oil water separator and carries out oil-water separation, and first is that 30 DEG C of indirect steam amounts are at condensate temperature
Carry out under the conditions of 200L/ hour 1 hour；Then condensate temperature be 40 DEG C, indirect steam amount be to enter under the conditions of 300L/ hour
Row 1 hour, collects the Flos Tagetis Erectae quintessence oil in oil water separator, obtains a Flos Tagetis Erectae quintessence oil, and Flos Tagetis Erectae extraction of essential oil rate is
0.18%；
C, the distillate after single flash separation Flos Tagetis Erectae quintessence oil is rejoined in boiler, add with indirect steam
Heat, indirect steam amount is 300L/ hour, and distillate outlet temperature is 35 DEG C, and distillation time is 3 hours, collects oil water separator
In Flos Tagetis Erectae quintessence oil, obtain secondary Flos Tagetis Erectae quintessence oil, Flos Tagetis Erectae extraction of essential oil rate is the 0.010% of single flash liquid；
D, by Flos Tagetis Erectae quintessence oil with secondary Flos Tagetis Erectae quintessence oil ratio for 1.5:1 in mass ratio mix homogeneously and marked
Quasi-Flos Tagetis Erectae quintessence oil, is subsequently adding anhydrous sodium sulfate dry filter and carries out processed, and the amount of the anhydrous sodium sulfate of addition is mark
The 5% of quasi-Flos Tagetis Erectae quintessence oil quality；
E, in the standard Flos Tagetis Erectae quintessence oil of processed add activated carbon, add activated carbon amount be standard ten thousand longevity
The 5% of chrysanthemum quintessence oil quality, and stirring 48 hours at normal temperatures, be filtrated to get the standard Flos Tagetis Erectae quintessence oil of dehydration and decolorization；To process
The activated carbon having adsorbed Flos Tagetis Erectae quintessence oil after filtration heavily steams to reclaim Flos Tagetis Erectae quintessence oil；
F, through dehydration and decolorization standard Flos Tagetis Erectae quintessence oil bottle, seal be placed under the sun irradiation 7 days.
Embodiment 3
The extraction of a kind of Flos Tagetis Erectae quintessence oil and processing method, comprise the following steps:
A, become the section of a length of 10cm to be placed in ground to spread 4.5 hours, spread in fine day Flos Tagetis Erectae branch rear cutout of gathering
During the thickness of flower layer less than 20cm；
B, add in the Flos Tagetis Erectae branch section through spreading and put in boiler after deionized water, the deionized water of addition
3 times of the quality that amount is Flos Tagetis Erectae branch section through spreading, with direct steam heating to 80 DEG C, then use indirect steam instead and add
Heat is to micro-boiling, and condensed fluid enters oil water separator and carries out oil-water separation, first condensate temperature be 32 DEG C, indirect steam amount be
Carry out under the conditions of 200L/ hour 1 hour；Then condensate temperature be 37 DEG C, indirect steam amount be to enter under the conditions of 300L/ hour
Row 1 hour, collects the Flos Tagetis Erectae quintessence oil in oil water separator, obtains a Flos Tagetis Erectae quintessence oil, and Flos Tagetis Erectae extraction of essential oil rate is
0.021%；
C, the distillate after single flash separation Flos Tagetis Erectae quintessence oil is rejoined in boiler, add with indirect steam
Heat, indirect steam amount is 300L/ hour, and distillate outlet temperature is 38 DEG C, and distillation time is 2.5 hours, collects oil-water separation
Flos Tagetis Erectae quintessence oil in device, obtains secondary Flos Tagetis Erectae quintessence oil, and Flos Tagetis Erectae extraction of essential oil rate is the 0.015% of single flash liquid；
D, by Flos Tagetis Erectae quintessence oil with secondary Flos Tagetis Erectae quintessence oil ratio for 1.5:1 in mass ratio mix homogeneously and marked
Quasi-Flos Tagetis Erectae quintessence oil, is subsequently adding anhydrous sodium sulfate dry filter and carries out processed, and the amount of the anhydrous sodium sulfate of addition is mark
The 5% of quasi-Flos Tagetis Erectae quintessence oil quality；
E, in the standard Flos Tagetis Erectae quintessence oil of processed add activated carbon, add activated carbon amount be standard ten thousand longevity
The 5% of chrysanthemum quintessence oil quality, and stirring 48 hours at normal temperatures, be filtrated to get the standard Flos Tagetis Erectae quintessence oil of dehydration and decolorization；To process
The activated carbon having adsorbed Flos Tagetis Erectae quintessence oil after filtration heavily steams to reclaim Flos Tagetis Erectae quintessence oil；
F, through dehydration and decolorization standard Flos Tagetis Erectae quintessence oil bottle, seal be placed under the sun irradiation 7 days.
Comparative example 1
The extraction of a kind of Flos Tagetis Erectae quintessence oil and processing method, comprise the following steps:
A, become the section of a length of 9.8cm to be placed in ground to spread 5 hours, spread in fine day Flos Tagetis Erectae branch rear cutout of gathering
In journey, the thickness of flower layer is less than 20cm；
B, add in the Flos Tagetis Erectae branch section through spreading and put in boiler after deionized water, the deionized water of addition
3 times of the quality that amount is Flos Tagetis Erectae branch section through spreading, with direct steam heating to 60 DEG C, then use indirect steam instead and add
Heat is to micro-boiling, and condensed fluid enters oil water separator and carries out oil-water separation, first condensate temperature be 34 DEG C, indirect steam amount be
Carry out under the conditions of 200L/ hour 1 hour；Then condensate temperature be 38 DEG C, indirect steam amount be to enter under the conditions of 300L/ hour
Row 1 hour, collects the Flos Tagetis Erectae quintessence oil in oil water separator, obtains a Flos Tagetis Erectae quintessence oil, and Flos Tagetis Erectae extraction of essential oil rate is
0.012%；
C, the distillate after single flash separation Flos Tagetis Erectae quintessence oil is rejoined in boiler, add with indirect steam
Heat, indirect steam amount is 300L/ hour, and distillate outlet temperature is 38 DEG C, and distillation time is 2.5 hours, collects oil-water separation
Flos Tagetis Erectae quintessence oil in device, obtains secondary Flos Tagetis Erectae quintessence oil, and Flos Tagetis Erectae extraction of essential oil rate is the 0.08% of single flash liquid；
D, by Flos Tagetis Erectae quintessence oil with secondary Flos Tagetis Erectae quintessence oil ratio for 1.5:1 in mass ratio mix homogeneously and marked
Quasi-Flos Tagetis Erectae quintessence oil, is subsequently adding anhydrous sodium sulfate dry filter and carries out processed, and the amount of the anhydrous sodium sulfate of addition is mark
The 5% of quasi-Flos Tagetis Erectae quintessence oil quality；
E, in the standard Flos Tagetis Erectae quintessence oil of processed add activated carbon, add activated carbon amount be standard ten thousand longevity
The 5% of chrysanthemum quintessence oil quality, and stirring 48 hours at normal temperatures, be filtrated to get the standard Flos Tagetis Erectae quintessence oil of dehydration and decolorization；To process
The activated carbon having adsorbed Flos Tagetis Erectae quintessence oil after filtration heavily steams to reclaim Flos Tagetis Erectae quintessence oil；
F, through dehydration and decolorization standard Flos Tagetis Erectae quintessence oil bottle, seal be placed under the sun irradiation 7 days.
Comparative example 2
The extraction of a kind of Flos Tagetis Erectae quintessence oil and processing method, comprise the following steps:
A, become the section of a length of 10.2cm to be placed in ground to spread 5 hours, spread in fine day Flos Tagetis Erectae branch rear cutout of gathering
During the thickness of flower layer less than 20cm；
B, add in the Flos Tagetis Erectae branch section through spreading and put in boiler after deionized water, the deionized water of addition
3 times of the quality that amount is Flos Tagetis Erectae branch section through spreading, with direct steam heating to 80 DEG C, then use indirect steam instead and add
Heat is to micro-boiling, and condensed fluid enters oil water separator and carries out oil-water separation, condensate temperature be 35 DEG C, indirect steam amount be
Carry out under the conditions of 200L/ hour 2 hours, collect the Flos Tagetis Erectae quintessence oil in oil water separator, obtain a Flos Tagetis Erectae quintessence oil, Wan Shou
Chrysanthemum extraction of essential oil rate is 0.015%；
C, the distillate after single flash separation Flos Tagetis Erectae quintessence oil is rejoined in boiler, add with indirect steam
Heat, indirect steam amount is 300L/ hour, and distillate outlet temperature is 39 DEG C, and distillation time is 3 hours, collects oil water separator
In Flos Tagetis Erectae quintessence oil, obtain secondary Flos Tagetis Erectae quintessence oil, Flos Tagetis Erectae extraction of essential oil rate is the 0.09% of single flash liquid；
D, by Flos Tagetis Erectae quintessence oil with secondary Flos Tagetis Erectae quintessence oil ratio for 1.5:1 in mass ratio mix homogeneously and marked
Quasi-Flos Tagetis Erectae quintessence oil, is subsequently adding anhydrous sodium sulfate dry filter and carries out processed, and the amount of the anhydrous sodium sulfate of addition is mark
The 5% of quasi-Flos Tagetis Erectae quintessence oil quality；
E, in the standard Flos Tagetis Erectae quintessence oil of processed add activated carbon, add activated carbon amount be standard ten thousand longevity
The 5% of chrysanthemum quintessence oil quality, and stirring 48 hours at normal temperatures, be filtrated to get the standard Flos Tagetis Erectae quintessence oil of dehydration and decolorization；To process
The activated carbon having adsorbed Flos Tagetis Erectae quintessence oil after filtration heavily steams to reclaim Flos Tagetis Erectae quintessence oil；
F, through dehydration and decolorization standard Flos Tagetis Erectae quintessence oil bottle, seal be placed under the sun irradiation 7 days.
Flos Tagetis Erectae quintessence oil physical and chemical index measures
To in embodiment 1-3 (respectively experimental group 1-3) and comparative example 1-2 (respectively matched group 1-2) without anhydrous sulfur
The standard Flos Tagetis Erectae quintessence oil that acid sodium processes carries out trauls-ss-Ocimene, trans-tagetone, alkene, cis-tagetone, anti-
Formula-ocimenone and the assay of cis-Ocimene ketone, result is as shown in the table:
From the above results, compared with common Flos Tagetis Erectae quintessence oil, in the Flos Tagetis Erectae quintessence oil that the method for the invention obtains
The content of trauls-ss-Ocimene improve 28.70%；The content of trans-tagetone improves 34.64%；Containing of alkene
Amount improves 26.13%；The content of cis-tagetone improves 30.86%；The content of trans-ocimenone improves
27.71%；The content of cis-Ocimene ketone improves 25.80%.Thus prove, the Flos Tagetis Erectae that the method for the invention obtains
The quality better of quintessence oil.
Finally illustrating, above example is only in order to illustrate technical scheme and unrestricted, although with reference to relatively
The present invention has been described in detail by good embodiment, it will be understood by those within the art that, can be to the skill of the present invention
Art scheme is modified or equivalent, and without deviating from objective and the scope of technical solution of the present invention, it all should be contained at this
In the middle of the right of invention.
Claims (9)
1. the extraction of a Flos Tagetis Erectae quintessence oil and processing method, it is characterised in that comprise the following steps:
A, gather Flos Tagetis Erectae aerial parts, then cutting in fine day, spread 3-6 hour on ground；
B, add in the Flos Tagetis Erectae through spreading and put in boiler after deionized water, with direct steam heating to 80 DEG C, then
Use indirect steam heating instead to carry out oil-water separation to boiling, condensed fluid entrance oil water separator, collect ten thousand in oil water separator
Longevity chrysanthemum quintessence oil, obtains a Flos Tagetis Erectae quintessence oil；
C, the distillate after single flash separation Flos Tagetis Erectae quintessence oil is rejoined in boiler, heats with indirect steam,
Collect the Flos Tagetis Erectae quintessence oil in oil water separator, obtain secondary Flos Tagetis Erectae quintessence oil；
D, Flos Tagetis Erectae oil is mixed homogeneously by weight the ratio of 1.5:1 with secondary Flos Tagetis Erectae oil, obtain standard ten thousand
Longevity chrysanthemum quintessence oil, adds anhydrous sodium sulfate dry filter and makees processed；
E, in the standard Flos Tagetis Erectae quintessence oil of processed add activated carbon, and at normal temperatures stirring 48 hours, filter
Standard Flos Tagetis Erectae quintessence oil to dehydration and decolorization；
F, through dehydration and decolorization standard Flos Tagetis Erectae quintessence oil bottle, seal be placed under the sun irradiation 7 days.
The extraction of Flos Tagetis Erectae quintessence oil the most according to claim 1 and processing method, it is characterised in that in step A, in fine day
Gather Flos Tagetis Erectae aerial parts, be then cut into the section of a length of 9.5-10.5cm.
The extraction of Flos Tagetis Erectae quintessence oil the most according to claim 1 and processing method, it is characterised in that spread described in step A
During the thickness of flower layer less than 20cm.
The extraction of Flos Tagetis Erectae quintessence oil the most according to claim 1 and processing method, it is characterised in that add described in step B
3 times that amount is the quality through the Flos Tagetis Erectae spread of deionized water.
The extraction of Flos Tagetis Erectae quintessence oil the most according to claim 1 and processing method, it is characterised in that in step B, with indirectly
Steam distilled concretely comprise the following steps: first condensate temperature be 30-35 DEG C, indirect steam amount be to carry out 1 under the conditions of 200L/ hour
Hour；Then condensate temperature be 35-40 DEG C, indirect steam amount be to carry out 1 hour under the conditions of 300L/ hour.
The extraction of Flos Tagetis Erectae quintessence oil the most according to claim 1 and processing method, it is characterised in that in step C, distillation
Design parameter is set to: indirect steam amount is 300L/ hour, and distillate outlet temperature is 35-40 DEG C, and distillation time is that 2-3 is little
Time.
The extraction of Flos Tagetis Erectae quintessence oil the most according to claim 1 and processing method, it is characterised in that in step D, addition
The amount of anhydrous sodium sulfate is the 5% of standard Flos Tagetis Erectae quintessence oil quality.
The extraction of Flos Tagetis Erectae quintessence oil the most according to claim 1 and processing method, it is characterised in that in step E, add and live
Amount is standard Flos Tagetis Erectae quintessence oil quality the 5% of property charcoal.
The extraction of Flos Tagetis Erectae quintessence oil the most according to claim 1 and processing method, it is characterised in that also include following step
Suddenly, heavily steam to reclaim Flos Tagetis Erectae quintessence oil to the activated carbon having adsorbed Flos Tagetis Erectae quintessence oil after filtering.
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