CN106281677A - A kind of safety and effectivity natural lavender solid quintessence oil and preparation method thereof - Google Patents
A kind of safety and effectivity natural lavender solid quintessence oil and preparation method thereof Download PDFInfo
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- CN106281677A CN106281677A CN201610085429.4A CN201610085429A CN106281677A CN 106281677 A CN106281677 A CN 106281677A CN 201610085429 A CN201610085429 A CN 201610085429A CN 106281677 A CN106281677 A CN 106281677A
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- quintessence oil
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- sodium alginate
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- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11B—PRODUCING, e.g. BY PRESSING RAW MATERIALS OR BY EXTRACTION FROM WASTE MATERIALS, REFINING OR PRESERVING FATS, FATTY SUBSTANCES, e.g. LANOLIN, FATTY OILS OR WAXES; ESSENTIAL OILS; PERFUMES
- C11B9/00—Essential oils; Perfumes
- C11B9/0003—Compounds of unspecified constitution defined by the chemical reaction for their preparation
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Abstract
The invention discloses a kind of safety and effectivity natural lavender solid quintessence oil and preparation method thereof.Solid quintessence oil is made up of natural lavender quintessence oil, beta cyclodextrin and calcium alginate.Preparation method step: (1) prepares sodium alginate aqueous solution；(2) calcium chloride solution is prepared；(3) natural lavender quintessence oil, emulsifying agent and deionized water are carried out emulsifying, obtain emulsifying liquid, pouring in sodium alginate aqueous solution by emulsifying liquid, stir to obtain uniform mixed liquor, (4) add beta cyclodextrin in the mixed liquor of step (3) gained；(5) (4) gained mixed liquor is dropped in (2), solidify 2h, obtain solid quintessence oil suspension；(6) by the solid quintessence oil suspension of step (5) gained through decompression sucking filtration, wash, be dried, obtain solid quintessence oil.The present invention fundamentally solves the drawback of liquid essential oil, and fragrance remaining time is long, non-leakage and contamination, easy to use, and preparation method science is easily implemented.
Description
Technical field
The present invention relates to a kind of lavandula angustifolia solid quintessence oil and preparation method thereof, particularly to a kind of safety and effectivity sky
So lavandula angustifolia solid quintessence oil and preparation method thereof
Background technology
It is known that fragrance is the sensory response of people's olfactory sensation, fragrance can affect the emotion of people even to people
Produce the impact in terms of physiology.Fragrance not only has makes that people is pleasing, ease off the pressure, allaying tiredness, excellent
Change environment, prominent image, set off the function such as atmosphere, raising efficiency by contrast, and also appetite strengthening, sterilization is gone out
Bacterium, the multiple medical care effect such as anti-inflammatory analgesic.Research shows: the fragrance of lavandula angustifolia can make people produce one
The most quietly mood, its quintessence oil hasPain relieving, anti-tic, anti-depression, antibacterial, anti-Spasm, anti-Virus、
The effect of sterilization.Can decongest with swelling, deodorization, removing toxic substances, diuresis, stimulate the menstrual flow, antifungal, reduction blood
Press, get well, calm.Scientist finds by testing the brain wave of part experimenter: lavandula angustifolia essence
Oil can produce quiet type brain wave, and it can stabilize emotion, so there is the effect in front to not normal mental status.
Can purify, pacify soul, alleviate angry and beaten sensation, make people can even-tempered and good-humouredly in the face of give birth to
Live.Because its energy centre of equilibrium is neural, so helpful to alarmed and dejected state.Also have significantly
Calmness and function of releiving, have goodish to insomniacShu FangConsole with spirit.Spy based on Herba Lysimachiae foenum-graeci quintessence oil
Distinguished service is imitated, and the exploitation of lavandula angustifolia aroma type product is constantly subjected to the extensive concern of people.But, the most existing
Herba Lysimachiae foenum-graeci quintessence oil is all liquid essential oil, does not has a solid quintessence oil, and lavandula angustifolia liquid essential oil not only fragrance remaining time is short,
Seepage, contamination easily occurring, and carries inconvenience, aircraft is just forbidden carrying with liquid essential oil, causes day
Often use very inconvenient.
Summary of the invention
It is an object of the invention to provide a kind of fragrance remaining time length, easy to use, the safety of preparation method science
Long-acting natural lavender solid quintessence oil and preparation method thereof
The technical solution used in the present invention is, this safety and effectivity natural lavender solid quintessence oil is smoked by natural
Clothing grass quintessence oil, beta-schardinger dextrin-and calcium alginate composition, wherein, calcium alginate is by sodium alginate and calcium chloride
Reaction gained, reaction mass ratio is sodium alginate: calcium chloride is 1: 1-3.
The preparation method of above-mentioned safety and effectivity natural lavender solid quintessence oil, comprises the following steps: (1) is by sea
Sodium alginate is dissolved in deionized water, is stirred and heated to 40-50 DEG C, obtains mass percent concentration and is
0.8-1.5% sodium alginate aqueous solution, and it is cooled to room temperature；(2) calcium chloride is dissolved in deionized water, stir
Mixing dissolving, obtaining mass percent concentration is 1.0-3.0% calcium chloride solution；(3) by natural lavender quintessence oil,
Emulsifying agent and deionized water carry out emulsifying 3-5min at rotating speed 10000-13000r/min, obtain emulsifying
Liquid, above-mentioned natural lavender quintessence oil and emulsifying agent and the consumption of deionized water, in mass ratio natural lavender essence
Oil: emulsifying agent: deionized water is the ratio calculating of 1.0: 0.05: 5-10, pours the emulsifying liquid of gained into step
Suddenly, in the sodium alginate aqueous solution of (1), stir 30-40min, obtain uniform mixed liquor, emulsifying liquid and step
Suddenly the amount of the sodium alginate of (1), calculates according to mass ratio, i.e. natural smokes clothing used by the preparation of emulsifying liquid
Grass quintessence oil: the sodium alginate in the sodium alginate aqueous solution of step (1) is 2-4: 1；(4) mixing speed is controlled
500-2000r/min, is slowly added to beta-schardinger dextrin-7-20g in the mixed liquor of step (3) gained, stirring
30-40min；(5) control drop rate 5-20ml/min, (4) gained mixed liquor is dropped in (2), control
Mixing speed 500-2000r/min processed, waits to drip complete, solidifies 2h, obtains solid quintessence oil suspension, step (4)
In the consumption of uniform mixed liquor, according to sodium alginate in the uniform mixed liquor in (4): mass percent is dense
Degree is 1: 1-3 for the anhydrous calcium chloride in 1.0-3.0% calcium chloride solution；(6) by the solid of step (5) gained
Quintessence oil suspension is through decompression sucking filtration, and the solid of gained washs with the ethanol solution of 20%, then controls temperature
Degree is 50 DEG C and is dried, and obtains safety and effectivity natural lavender solid quintessence oil.
Owing to taking technique scheme, therefore the present invention fundamentally solves the drawback of liquid essential oil, stays
Fragrant time lengthening, to more than one month, will not occur seepage and stain phenomenon, can arbitrarily be placed on the ground of needs
Side, it is the most convenient to use.Solid material degradable, to environment without any murder by poisoning.It addition, preparation method section
Learn rationally, easily implement.
Detailed description of the invention
Below in conjunction with specific embodiment, the present invention is described in further detail.
Embodiment 1, the preparation of large capsule type natural lavender solid quintessence oil, with natural lavender quintessence oil as core,
With natural polymer sodium alginate for wall material, big with modified starch beta-schardinger dextrin-for the preparation of curable type skeleton
Capsule solid quintessence oil, calculates, i.e. sodium alginate in mass ratio: natural lavender quintessence oil is 1: 4, prepares mesospore
Material and the amount of curable type skeleton, ratio calculates in mass ratio, sodium alginate: beta-schardinger dextrin-is 1: 10-15.
The preparation method of above-mentioned large capsule type natural lavender solid quintessence oil, specifically includes following steps: (1)
Being joined in deionized water by sodium alginate, and be heated to 40 DEG C of stirrings, obtaining mass percent concentration is 0.8%
Sodium alginate aqueous solution, and it is cooled to room temperature；(2) calcium chloride is dissolved in deionized water, stirring and dissolving,
Obtaining mass percent concentration is 1.0-3.0% calcium chloride solution；(3) by natural lavender quintessence oil, emulsifying agent and
It is that 10000r/min carries out emulsifying 3min that deionized water controls rotating speed in high-speed emulsifying machine, obtains homogenizing
Emulsion；Above-mentioned natural lavender quintessence oil: emulsifying agent and the consumption of deionized water, by natural Herba Lysimachiae foenum-graeci quintessence oil:
Emulsifying agent: deionized water is the ratio calculating of 1.0: 0.05: 5；Described emulsifying agent is multiple by tween 80 and Arlacel-80
Joining and form, ratio is 3: 7；The emulsifying liquid of gained is poured in the sodium alginate aqueous solution of step (1),
Stirring 30min, obtains uniform mixed liquor；The amount of the sodium alginate of emulsifying liquid and step (1), according to matter
Amount ratio calculates, i.e. Herba Lysimachiae foenum-graeci quintessence oil used by the preparation of emulsifying liquid: the sodium alginate aqueous solution of step (1)
In sodium alginate be 2: 1；(4) mixing speed 500r/min is controlled, in the mixed liquor of step (3) gained
It is slowly added to beta-schardinger dextrin-15g, stirs 30min；(5) drop rate 15ml/min is controlled, by (4) gained
Mixed liquor drops in (2), controls mixing speed 500r/min, waits to drip complete, solidifies 2h, obtains big glue
Capsule solution；The consumption of the uniform mixed liquor in step (4), according to Sargassum in the uniform mixed liquor in (4)
Acid sodium: mass percent concentration be the anhydrous calcium chloride in 1.0% calcium chloride solution be 1: 1；(6) by step (5)
The solution of gained is through decompression sucking filtration, and the solid content of gained washs with the ethanol solution of 20%, then controls
Temperature is 50 DEG C and is dried, and obtaining large capsule solid quintessence oil, product cut size scope is between 3-5mm.
Embodiment 2, the preparation of Caplet natural lavender solid quintessence oil, with natural lavender quintessence oil as core,
With natural polymer sodium alginate for wall material, prepare little with modified starch beta-schardinger dextrin-for curable type skeleton
The solid quintessence oil of capsule form, calculates in mass ratio, the core wall i.e. sodium alginate of ratio: essence is 1: 4, in preparation
Wall material and the amount of curable type skeleton, ratio calculates in mass ratio, sodium alginate: beta-schardinger dextrin-is 1: 10.
The preparation method of above-mentioned Caplet pattern solid quintessence oil, specifically includes following steps: (1) is by alginic acid
Sodium joins in deionized water, and is heated to 40 DEG C of stirrings, and obtaining mass percent concentration is 0.8% alginic acid
Sodium water solution, and it is cooled to room temperature；(2) calcium chloride is dissolved in deionized water, stirring and dissolving, obtain
Mass percent concentration is 1.0-3.0% calcium chloride solution；(3) by natural lavender quintessence oil, emulsifying agent and go from
It is that 10000r/min carries out emulsifying 3min that sub-water controls rotating speed in high-speed emulsifying machine, obtains emulsifying
Liquid；Above-mentioned Herba Lysimachiae foenum-graeci quintessence oil: emulsifying agent and the consumption of deionized water, by Herba Lysimachiae foenum-graeci quintessence oil: emulsifying agent: go
Ionized water is the ratio calculating of 1.0: 0.05: 5；Described emulsifying agent is formed by tween 80 and Arlacel-80 are compounding, than
Example is 3: 7.The emulsifying liquid of gained is poured in the sodium alginate aqueous solution of step (1), stirs 30min,
Obtain uniform mixed liquor；The amount of the sodium alginate of emulsifying liquid and step (1), calculates according to mass ratio, i.e.
Natural lavender quintessence oil used by the preparation of emulsifying liquid: the Sargassum in the sodium alginate aqueous solution of step (1)
Acid sodium is 2: 1；(4) control mixing speed 1000r/min, slowly add in the mixed liquor of step (3) gained
Enter beta-schardinger dextrin-10g, stir 30min；(5) drop rate 10ml/min is controlled, by (4) gained mixed liquor
Drop in (2), control mixing speed 1000r/min, wait to drip complete, solidify 2h, obtain microcapsule molten
Liquid；The consumption of the uniform mixed liquor in step (4), according to sodium alginate in the uniform mixed liquor in (4):
Mass percent concentration be the anhydrous calcium chloride in 1.0% calcium chloride solution be 1: 1；(6) by step (5) institute
The solution obtained is through decompression sucking filtration, and the solid content of gained washs with the ethanol solution of 20%, then controls temperature
Degree is 50 DEG C and is dried, and obtains Caplet solid essential oil product particle size range between 1-2mm.
Embodiment 3, the preparation of powder-type natural lavender solid quintessence oil, with natural lavender quintessence oil as core,
With natural polymer sodium alginate for wall material, big with modified starch beta-schardinger dextrin-for the preparation of curable type skeleton
Capsule, calculates in mass ratio, the core wall i.e. sodium alginate of ratio: natural lavender quintessence oil is 1: 4, prepares mesospore material
With the amount of curable type skeleton, ratio calculates in mass ratio, sodium alginate: beta-schardinger dextrin-is 1: 8.
The preparation method of above-mentioned powder-type natural lavender solid quintessence oil, specifically includes following steps: (1) will
Sodium alginate deionized water dissolving, and heat 45 DEG C of stirrings, obtaining mass percent concentration is 1% alginic acid
Sodium water solution, and it is cooled to room temperature；(2) calcium chloride is dissolved in deionized water, stirring and dissolving, obtain
Mass percent concentration is 2% calcium chloride solution；(3) by natural lavender quintessence oil, emulsifying agent and deionized water
Telling emulsifying centralized Control rotating speed to be, 13000r/min carries out emulsifying 5min, emulsifying liquid；On
State natural lavender quintessence oil: emulsifying agent and the consumption of deionized water, by natural Herba Lysimachiae foenum-graeci quintessence oil: emulsifying agent:
Deionized water is the ratio calculating of 1.0g: 0.05: 8ml；Described emulsifying agent is formed by tween 80 and Arlacel-80 are compounding,
Ratio is 3: 7.The emulsifying liquid of gained is poured in the sodium alginate aqueous solution of step (1), stirs 35min,
Obtain uniform mixed liquor；The amount of the sodium alginate of emulsifying liquid and step (1), calculates according to mass ratio, i.e.
Natural lavender quintessence oil used by the preparation of emulsifying liquid: the Sargassum in the sodium alginate aqueous solution of step (1)
Acid sodium is 3: 1；(4) control mixing speed 2000r/min, slowly add in the mixed liquor of step (3) gained
Enter beta-schardinger dextrin-8g, stir 35min；(5) drop rate 6ml/min is controlled, by (4) gained mixing drop
Add in (2), control mixing speed 2000r/min, wait to drip complete, solidify 2h, obtain powder suspension；
The consumption of the uniform mixed liquor in step (4), according to sodium alginate in the uniform mixed liquor in (4): matter
Amount percent concentration be the anhydrous calcium chloride in 1.0-3.0% calcium chloride solution be 1: 2；(6) by step (5) institute
The powder suspension obtained, through decompression sucking filtration, washs with the ethanol solution of 20%, and then controlling temperature is 50 DEG C
Being dried, obtain powder-type solid quintessence oil, product cut size scope is between 80-120 μm.
Claims (2)
1. a safety and effectivity natural lavender solid quintessence oil, it is characterised in that lavandula angustifolia solid quintessence oil is by sky
So Herba Lysimachiae foenum-graeci quintessence oil, beta-schardinger dextrin-and calcium alginate composition, wherein, calcium alginate is by sodium alginate and chlorine
Changing calcium reaction gained, reaction mass ratio is sodium alginate: calcium chloride is 1: 1-3.
2. a preparation method for safety and effectivity natural lavender solid quintessence oil, its feature described in claim 1
It is to comprise the following steps: sodium alginate is dissolved in deionized water by (1), is stirred and heated to 40-50 DEG C,
Obtaining mass percent concentration is 0.8-1.5% sodium alginate aqueous solution, and is cooled to room temperature；(2) by calcium chloride
Dissolving in deionized water, stirring and dissolving, obtaining mass percent concentration is 1.0-3.0% calcium chloride solution；(3)
Natural lavender quintessence oil, emulsifying agent and deionized water are carried out emulsifying at rotating speed 10000-13000r/min
3-5min, obtains emulsifying liquid, above-mentioned natural lavender quintessence oil and emulsifying agent and the consumption of deionized water, presses
Quality ratio natural lavender quintessence oil: emulsifying agent: deionized water is the ratio calculating of 1.0: 0.05: 5-10, by gained
Emulsifying liquid pour in the sodium alginate aqueous solution of step (1), stir 30-40min, obtain and uniformly mix
Liquid, the amount of the sodium alginate of emulsifying liquid and step (1), calculate according to mass ratio, i.e. emulsifying liquid
Natural lavender quintessence oil used by preparation: the sodium alginate in the sodium alginate aqueous solution of step (1) is 2-4: 1；
(4) control mixing speed 500-2000r/min, in the mixed liquor of step (3) gained, be slowly added to β-ring
Dextrin 7-20g, stirs 30-40min；(5) drop rate 5-20ml/min is controlled, by (4) gained mixed liquor
Drop in (2), control mixing speed 500-2000r/min, wait to drip complete, solidify 2h, obtain solid essence
Oil suspension, the consumption of the uniform mixed liquor in step (4), according to sea in the uniform mixed liquor in (4)
Sodium alginate: mass percent concentration be the anhydrous calcium chloride in 1.0-3.0% calcium chloride solution be 1: 1-3；(6) will
The solid quintessence oil suspension of step (5) gained is through decompression sucking filtration, and the solid of gained enters with the ethanol solution of 20%
Row washing, then controls temperature and is 50 DEG C and is dried, obtain safety and effectivity natural lavender solid quintessence oil.
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Cited By (4)
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| CN107550764A (en) * | 2017-10-20 | 2018-01-09 | 上海应用技术大学 | A kind of preparation method of the oil and fat of sacha inchi water profit Q hoodles of high stability |
| CN113845977A (en) * | 2021-10-13 | 2021-12-28 | 上海应用技术大学 | Lavender essential oil microcapsule and preparation method thereof |
| CN114208858A (en) * | 2021-12-24 | 2022-03-22 | 中国农业科学院都市农业研究所 | Plant extract mosquito-proof slow-release material and preparation method thereof |
| CN115006443A (en) * | 2022-07-19 | 2022-09-06 | 山东福瑞达生物股份有限公司 | Lavender oil nanoemulsion and preparation method thereof |
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| CN107550764A (en) * | 2017-10-20 | 2018-01-09 | 上海应用技术大学 | A kind of preparation method of the oil and fat of sacha inchi water profit Q hoodles of high stability |
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Application publication date: 20170104 |