CN106276743A - A kind of method unsealing objects outside Earth sample sealing packaging containers - Google Patents
A kind of method unsealing objects outside Earth sample sealing packaging containers Download PDFInfo
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- CN106276743A CN106276743A CN201610796926.5A CN201610796926A CN106276743A CN 106276743 A CN106276743 A CN 106276743A CN 201610796926 A CN201610796926 A CN 201610796926A CN 106276743 A CN106276743 A CN 106276743A
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- Prior art keywords
- objects outside
- operational window
- packaging containers
- outside earth
- earth sample
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Classifications
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- B—PERFORMING OPERATIONS; TRANSPORTING
- B67—OPENING, CLOSING OR CLEANING BOTTLES, JARS OR SIMILAR CONTAINERS; LIQUID HANDLING
- B67B—APPLYING CLOSURE MEMBERS TO BOTTLES JARS, OR SIMILAR CONTAINERS; OPENING CLOSED CONTAINERS
- B67B7/00—Hand- or power-operated devices for opening closed containers
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B67—OPENING, CLOSING OR CLEANING BOTTLES, JARS OR SIMILAR CONTAINERS; LIQUID HANDLING
- B67B—APPLYING CLOSURE MEMBERS TO BOTTLES JARS, OR SIMILAR CONTAINERS; OPENING CLOSED CONTAINERS
- B67B7/00—Hand- or power-operated devices for opening closed containers
- B67B7/14—Hand- or power-operated devices for opening closed containers for removing tightly-fitting lids or covers, e.g. of shoe-polish tins, by gripping and rotating
-
- G—PHYSICS
- G01—MEASURING; TESTING
- G01N—INVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES
- G01N1/00—Sampling; Preparing specimens for investigation
- G01N1/28—Preparing specimens for investigation including physical details of (bio-)chemical methods covered elsewhere, e.g. G01N33/50, C12Q
-
- G—PHYSICS
- G01—MEASURING; TESTING
- G01N—INVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES
- G01N1/00—Sampling; Preparing specimens for investigation
- G01N1/28—Preparing specimens for investigation including physical details of (bio-)chemical methods covered elsewhere, e.g. G01N33/50, C12Q
- G01N1/36—Embedding or analogous mounting of samples
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- Engineering & Computer Science (AREA)
- Mechanical Engineering (AREA)
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- Health & Medical Sciences (AREA)
- Life Sciences & Earth Sciences (AREA)
- Chemical & Material Sciences (AREA)
- Analytical Chemistry (AREA)
- Biochemistry (AREA)
- General Health & Medical Sciences (AREA)
- General Physics & Mathematics (AREA)
- Immunology (AREA)
- Pathology (AREA)
- Vacuum Packaging (AREA)
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Abstract
The invention discloses a kind of method unsealing objects outside Earth sample sealing packaging containers, belong to technical field of vacuum.This device includes transfer chamber, operational window, solution batten down, gas circulating purifying device, gas cylinder and vacuum pump；Solution batten down divides and is made up of upper end rigid section and middle flexible section and lower end rigid section；Compliant section removably connects with lower end rigid section, when compliant section is connected with lower end rigid section, solves batten down and forms confined space；Transfer chamber is connected with operational window by push-pull valve, and passes through pipeline communication between transfer chamber and operational window；Transfer chamber is connected with vacuum pump by pipeline；Gas-recycling plant is connected with operational window and gas cylinder by pipeline respectively；The upper end rigid section and the lower end rigid section that solve batten down are affixed with operational window by the through hole on the upper and lower surface of operational window respectively, and lower rigid section is connected with vacuum pump by pipeline；Solve batten down to be connected with operational window by pipeline.
Description
Technical field
The present invention relates to a kind of method unsealing objects outside Earth sample sealing packaging containers, belong to technical field of vacuum.
Background technology
According to China's survey of deep space development plan, China samples realizing the unmanned of moon sample before 2017 and returns
Return.Planning according to follow-up developments, China is also visited carrying out a series of deep spaces such as the detection of Mars, Mars sample and return
Survey engineering.In survey of deep space, after gathering the sealing packaging containers return ground of objects outside Earth sample, according to objects outside Earth sample
Handling process, also needs to carry out the deblocking of objects outside Earth sample sealing packaging containers, objects outside Earth sample treatment and preservation etc. a series of
Process.American apollo planning studies shows, objects outside Earth sample is especially sensitive to the water in earth atmospheric environment and oxygen, one
Denier is exposed to earth atmosphere, will occur therewith physically or chemically to react, and make sample lose original characteristic.Therefore, objects outside Earth
Sample gathering, return to ground, unseal, process and during storage etc., how to avoid objects outside Earth sample few by ground as far as possible
On ball, the impact of the factor such as vital movement, water, oxidation, keeps the initial condition of sample as far as possible, is deep space exploration program emphasis
One of problem paid close attention to, is also engineering problem the most urgently to be resolved hurrily.Therefore, objects outside Earth sample sealing packaging containers need to be carried out
Deblocking, objects outside Earth sample treatment and the technique study of preservation and device development, to meet the demand of deep space exploration program.
The research of objects outside Earth sample treatment and preservation is shown by american apollo plan and moon sample museum, extraterrestrial
Process and the preservation of celestial body need to be carried out under high pure nitrogen gaseous environment, it is desirable to every 1,000,000 molecular in high pure nitrogen gas
In, hydrone is less than 50 moles, and less than 20 moles, (i.e. in high pure nitrogen environment, water content is less than 30ppm, oxygen content to oxygen molecule
Less than 20ppm).So can make objects outside Earth sample few as far as possible shadow by earth atmosphere environment during processing and preserving
Ring, it is to avoid sample contamination, and the result impact analysed sample scientifically and study is less.Application No.
The patent application of CN201310693058.4 proposes a kind of sample and seals the device and method of container, and this device can be close to sample
Envelope container unseals, and shortcoming is water and oxygen in high pure nitrogen environment to be circulated purification, it is impossible to maintain high pure nitrogen
, there is the risk of contaminated samples in environment.The patent application of Application No. CN201610086872.3 proposes a kind of objects outside Earth
Sample collecting seal container method, use the method device can realize objects outside Earth sample collecting seal container deblocking and
Maintain high pure nitrogen environment, shortcoming be device be three cabin structures, vacuum movement mechanism is many, and motion runs in vacuum environment
Time there is the risk of bite, device reliability is relatively low, and deblocking flow process is complicated, and the operating time is long, improves objects outside Earth sample
The risk that product pollute in deblocking, process and storing process.
Summary of the invention
In view of this, it is an object of the invention to provide a kind of method unsealing objects outside Earth sample sealing packaging containers,
Objects outside Earth sample is processed and stores under high pure nitrogen environment by described method, makes sample in deblocking, processes and preserve
All the time be in during Deng in high vacuum environment, high pure nitrogen environment, make sample few as far as possible by outside of the earth environment (as water,
Oxygen etc.) impact, it is to avoid objects outside Earth sample contamination.
The purpose of the present invention is realized by techniques below scheme:
A kind of method unsealing objects outside Earth sample sealing packaging containers, described method comprises the steps:
Step one:
Release the compliant section of described solution batten down and the connection of lower end rigid section, and compress described compliant section so that it is lower end
The distance of the end face of tip to face distance lower end rigid section is fixing more than after the height of described objects outside Earth sample sealing packaging containers；Open
Push-pull valve, opens gas circulating purifying device, and maintaining and stating the pressure in operational window is 101.325KPa ± 2000Pa, by described mistake
The gas displacement crossed in cabin, operational window reconciliation batten down is high pure nitrogen, closes push-pull valve；
Step 2:
Described objects outside Earth sample sealing packaging containers is positioned in transfer chamber, described transfer chamber is evacuated to
Pressure is less than 10Pa；Opening the vacuum valve on pipeline between transfer chamber and operational window, described gas circulating purifying device is by behaviour
Make cabin and be filled with high pure nitrogen to transfer chamber, during pressure balance between two cabins, close described vacuum valve；
Step 3:
Open push-pull valve, objects outside Earth sample sealing packaging containers is moved in operational window, close push-pull valve；By described
The top of outer celestial body sample sealing packaging containers is connected with the lid solution sealing mechanism of described solution batten down, and bottom and lower end rigid section are solid
Fixed connection；
Step 4:
Connecting described compliant section and described lower end rigid section, now, described solution batten down forms an independence in operational window
Sealing space, described solution batten down is carried out evacuation, the pressure in batten down to be solved be less than 5 × 10-3During Pa, stop evacuation；
Regulation lid unseals mechanism, is rotated and upgraded by the lid of objects outside Earth sample sealing packaging containers, makes lid and objects outside Earth sample
Product sealing packaging containers separates, and completes deblocking；
Step 5:
Opening operation cabin and the vacuum valve solved between batten down on pipeline, described gas circulating purifying device by operational window to
Solve batten down and be filled with high pure nitrogen, during pressure balance between two cabins, close described vacuum valve；
Step 6:
Release the compliant section of described solution batten down and the connection of lower end rigid section, and compress described compliant section so that it is lower end
The distance of the end face of tip to face distance lower end rigid section is fixing more than after the height of described objects outside Earth sample sealing packaging containers；To solve
Take out in the objects outside Earth sample sealing packaging containers being honored as a queen moves to operational window and by objects outside Earth sample, it is carried out at filing
It is placed on after reason in sample protection device.
Described method is based on following device: described device includes that transfer chamber, operational window, solution batten down, gas circularly purifying fill
Put, gas cylinder and vacuum pump；
Wherein, the upper and lower surface of described operational window is all machined with through hole；
Described solution batten down divides and is made up of upper end rigid section and middle flexible section and lower end rigid section；Described compliant section and lower end
Rigid section removably connects, and when described compliant section is connected with lower end rigid section, described solution batten down forms confined space；
Described transfer chamber is connected with described operational window by push-pull valve, and passes through pipeline between described transfer chamber and operational window
Connection；Described transfer chamber is connected with vacuum pump by pipeline；Described gas-recycling plant is respectively by pipeline and described operational window
Connect with described gas cylinder；The upper end rigid section of described solution batten down and lower end rigid section are respectively by the upper and lower surface of described operational window
Through hole affixed with operational window, and described lower rigid section is connected with vacuum pump by pipeline；Described solution batten down passes through pipeline and institute
State operational window connection.
Further, the material of described compliant section is compressible corrugated tube.
Further, described device also includes the hoisting mechanism for promoting described compliant section.
Beneficial effect
(1) the method for the invention can under high vacuum environment (vacuum :≤5 × 10-3Pa) close to objects outside Earth sample
Envelope packaging container unseals, and under high pure nitrogen environment, (water content≤5ppm, oxygen content≤5ppm in high pure nitrogen) over the ground
Outer celestial body sample processes and stores, and makes sample in deblocking, processes and be in high vacuum environment, height all the time during preservation etc.
In pure nitrogen gas environment, sample is made to be affected by outside of the earth environment (such as water, oxygen etc.) as far as possible less, it is to avoid objects outside Earth sample
Pollute.
(2) the method for the invention applied range, applies also for the deblocking of other rare samples, processes and store
Deng.
(3) stage casing that in device of the present invention, solution batten down is is dismountable flexible structure so that described solution batten down can
In operational window, form independent sealing space, optimize structure and the design of existing deblocking device, decrease vacuum movement machine
Structure, reduces the risk of bite when motion runs in vacuum environment, improves the reliability of equipment, simplify ground simultaneously
The deblocking flow process of outer celestial body sample sealing packaging containers, shortens the operating time, improves work efficiency, reduce objects outside Earth
The risk that sample pollutes in deblocking, process and storing process.
Accompanying drawing explanation
Fig. 1 is the structural representation of device described in embodiment 1；
Wherein, 1-transfer chamber, 2-operational window, 3-solves batten down, 4-gas circulating purifying device, 5-gas cylinder, 6-vacuum pump, 7-
Upper end rigid section, 8-middle flexible section, 9-lower end rigid section, 10-hoisting mechanism, 11-objects outside Earth sample sealing packaging containers.
Detailed description of the invention
The present invention is described in detail in detail with specific embodiment below in conjunction with the accompanying drawings, but is not limited to this.
Embodiment 1
A kind of method unsealing objects outside Earth sample sealing packaging containers, described method comprises the steps:
Step one:
Release the compliant section of described solution batten down and the connection of lower end rigid section, and compress described compliant section so that it is lower end
The distance of the end face of tip to face distance lower end rigid section is fixing more than after the height of described objects outside Earth sample sealing packaging containers；Open
Push-pull valve, opens gas circulating purifying device, and maintaining and stating the pressure in operational window is 101.325KPa ± 2000Pa, by described mistake
The gas displacement crossed in cabin, operational window reconciliation batten down is high pure nitrogen, closes push-pull valve；
Step 2:
Described objects outside Earth sample sealing packaging containers is positioned in transfer chamber, described transfer chamber is evacuated to
Pressure is less than 10Pa；Opening the vacuum valve on pipeline between transfer chamber and operational window, described gas circulating purifying device is by behaviour
Make cabin and be filled with high pure nitrogen to transfer chamber, during pressure balance between two cabins, close described vacuum valve；
Step 3:
Open push-pull valve, objects outside Earth sample sealing packaging containers is moved in operational window, close push-pull valve；By described
The top of outer celestial body sample sealing packaging containers is connected with the lid solution sealing mechanism of described solution batten down, and bottom and lower end rigid section are solid
Fixed connection；
Step 4:
Connecting described compliant section and described lower end rigid section, now, described solution batten down forms an independence in operational window
Sealing space, described solution batten down is carried out evacuation, the pressure in batten down to be solved be less than 5 × 10-3During Pa, stop evacuation；
Regulation lid unseals mechanism, is rotated and upgraded by the lid of objects outside Earth sample sealing packaging containers, makes lid and objects outside Earth sample
Product sealing packaging containers separates, and completes deblocking；
Step 5:
Opening operation cabin and the vacuum valve solved between batten down on pipeline, described gas circulating purifying device by operational window to
Solve batten down and be filled with high pure nitrogen, during pressure balance between two cabins, close described vacuum valve；
Step 6:
Release the compliant section of described solution batten down and the connection of lower end rigid section, and compress described compliant section so that it is lower end
The distance of the end face of tip to face distance lower end rigid section is fixing more than after the height of described objects outside Earth sample sealing packaging containers；To solve
Take out in the objects outside Earth sample sealing packaging containers being honored as a queen moves to operational window and by objects outside Earth sample, it is carried out at filing
It is placed on after reason in sample protection device.
Described method realizes based on following device, and described device includes: transfer chamber 1, operational window 2, solution batten down 3, gas follow
Ring purifier 4, gas cylinder 5 and vacuum pump 6；
Wherein, the upper and lower surface of described operational window 2 is all machined with through hole；
Described solution batten down divides and is made up of upper end rigid section 7 and middle flexible section 8 and lower end rigid section 9；Described compliant section with
Lower end rigid section 9 removably connects, and when described compliant section is connected with lower end rigid section 9, described solution batten down forms confined space；
Described transfer chamber 1 is connected with described operational window 2 by push-pull valve, and passes through between described transfer chamber 1 and operational window 2
Pipeline communication；Described transfer chamber 1 is connected with vacuum pump 6 by pipeline；Described gas-recycling plant passes through pipeline respectively with described
Operational window 2 connects with described gas cylinder 5；The upper end rigid section 7 of described solution batten down and lower end rigid section 9 are respectively by described operational window
The through hole on 2 upper and lower surfaces is affixed with operational window 2, and described lower rigid section is connected with vacuum pump 6 by pipeline；Described solution batten down
Connected with described operational window 2 by pipeline.
Wherein, the material of described compliant section is compressible corrugated tube.
Described device also includes the hoisting mechanism 10 for promoting described compliant section.
The present invention includes but not limited to above example, every any equivalent carried out under the principle of spirit of the present invention
Replace or local improvement, all will be regarded as within protection scope of the present invention.
Claims (2)
1. a method based on described device deblocking objects outside Earth sample sealing packaging containers, it is characterised in that: described method
Comprise the steps:
Step one:
Release the compliant section of described solution batten down and the connection of lower end rigid section, and compress described compliant section so that it is the end face of lower end
The distance of the end face away from lower end rigid section is fixing more than after the height of described objects outside Earth sample sealing packaging containers；Open plate
Valve, opens gas circulating purifying device, and maintaining and stating the pressure in operational window is 101.325KPa ± 2000Pa, by described transition
The gas displacement that cabin, operational window are conciliate in batten down is high pure nitrogen, closes push-pull valve；
Step 2:
Described objects outside Earth sample sealing packaging containers is positioned in transfer chamber, described transfer chamber is evacuated to pressure
Less than 10Pa；Opening the vacuum valve on pipeline between transfer chamber and operational window, described gas circulating purifying device passes through operational window
It is filled with high pure nitrogen to transfer chamber, during pressure balance between two cabins, closes described vacuum valve；
Step 3:
Open push-pull valve, objects outside Earth sample sealing packaging containers is moved in operational window, close push-pull valve；By described extraterrestrial sky
The top of body sample sealing packaging containers is connected with the lid solution sealing mechanism of described solution batten down, and bottom and lower end rigid section are fixing even
Connect；
Step 4:
Connect described compliant section and described lower end rigid section, now, described solution batten down formed in operational window one independent close
Envelope space, carries out evacuation to described solution batten down, and the pressure in batten down to be solved is less than 5 × 10-3During Pa, stop evacuation；Regulation
Lid solution sealing mechanism, rotates and upgrades the lid of objects outside Earth sample sealing packaging containers, makes lid close with objects outside Earth sample
Envelope packaging container separates, and completes deblocking.
A kind of method based on described device deblocking objects outside Earth sample sealing packaging containers the most according to claim 1,
It is characterized in that: described method is further comprising the steps of:
Step 5:
Opening operation cabin and the vacuum valve solved between batten down on pipeline, described gas circulating purifying device passes through operational window to deblocking
Cabin is filled with high pure nitrogen, during pressure balance between two cabins, closes described vacuum valve；
Step 6:
Release the compliant section of described solution batten down and the connection of lower end rigid section, and compress described compliant section so that it is the end face of lower end
The distance of the end face away from lower end rigid section is fixing more than after the height of described objects outside Earth sample sealing packaging containers；Solution is honored as a queen
Objects outside Earth sample sealing packaging containers move to take out, after it is carried out filing process in operational window and by objects outside Earth sample
It is placed in sample protection device.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201610796926.5A CN106276743B (en) | 2016-08-31 | 2016-08-31 | A method of deblocking objects outside Earth sample sealing packaging containers |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201610796926.5A CN106276743B (en) | 2016-08-31 | 2016-08-31 | A method of deblocking objects outside Earth sample sealing packaging containers |
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| Publication Number | Publication Date |
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| CN106276743A true CN106276743A (en) | 2017-01-04 |
| CN106276743B CN106276743B (en) | 2018-10-02 |
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| CN201610796926.5A Active CN106276743B (en) | 2016-08-31 | 2016-08-31 | A method of deblocking objects outside Earth sample sealing packaging containers |
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Cited By (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN111084027A (en) * | 2019-12-26 | 2020-05-01 | 重庆大学 | Housing assembly for a biological growth system for an off-ground space |
| CN114276929A (en) * | 2021-12-29 | 2022-04-05 | 中国科学院国家空间科学中心 | Biological exposure device for near space scientific experiment |
| CN114572494A (en) * | 2022-03-03 | 2022-06-03 | 中国科学院国家天文台 | Deblocking equipment and deblocking method |
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| JP2000292321A (en) * | 1999-04-02 | 2000-10-20 | Ono Sokki Co Ltd | Extracting and diluting device and sample collecting device |
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| CN103693256A (en) * | 2013-12-17 | 2014-04-02 | 兰州空间技术物理研究所 | Device and method for unsealing sample sealing device |
| CN105667914A (en) * | 2016-01-28 | 2016-06-15 | 兰州空间技术物理研究所 | Extraterrestrial celestial body sampling device unsealing table |
| CN105716931A (en) * | 2016-02-16 | 2016-06-29 | 兰州空间技术物理研究所 | Unsealing method of extraterrestrial celestial sample collection sealed container |
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| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| DE2736830A1 (en) * | 1977-08-16 | 1979-02-22 | Alkem Gmbh | PROTECTIVE DEVICE FOR WORK ON CONTAINERS |
| JP2000292321A (en) * | 1999-04-02 | 2000-10-20 | Ono Sokki Co Ltd | Extracting and diluting device and sample collecting device |
| DE20022430U1 (en) * | 2000-04-01 | 2001-11-29 | Spanner Stephan | Protection device for the assembly and disposal of workbench filters |
| CN103693256A (en) * | 2013-12-17 | 2014-04-02 | 兰州空间技术物理研究所 | Device and method for unsealing sample sealing device |
| CN105667914A (en) * | 2016-01-28 | 2016-06-15 | 兰州空间技术物理研究所 | Extraterrestrial celestial body sampling device unsealing table |
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Cited By (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN111084027A (en) * | 2019-12-26 | 2020-05-01 | 重庆大学 | Housing assembly for a biological growth system for an off-ground space |
| CN114276929A (en) * | 2021-12-29 | 2022-04-05 | 中国科学院国家空间科学中心 | Biological exposure device for near space scientific experiment |
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| CN114572494A (en) * | 2022-03-03 | 2022-06-03 | 中国科学院国家天文台 | Deblocking equipment and deblocking method |
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| Publication number | Publication date |
|---|---|
| CN106276743B (en) | 2018-10-02 |
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