CN106273570A - The production technology of resin lens - Google Patents

The production technology of resin lens Download PDF

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Publication number
CN106273570A
CN106273570A CN201610759743.6A CN201610759743A CN106273570A CN 106273570 A CN106273570 A CN 106273570A CN 201610759743 A CN201610759743 A CN 201610759743A CN 106273570 A CN106273570 A CN 106273570A
Authority
CN
China
Prior art keywords
parts
resin lens
mould
degrees celsius
carry out
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Pending
Application number
CN201610759743.6A
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Chinese (zh)
Inventor
刘德兴
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
DONGXING HUAHONG OPTICAL TECHNOLOGY Co Ltd
Original Assignee
DONGXING HUAHONG OPTICAL TECHNOLOGY Co Ltd
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by DONGXING HUAHONG OPTICAL TECHNOLOGY Co Ltd filed Critical DONGXING HUAHONG OPTICAL TECHNOLOGY Co Ltd
Priority to CN201610759743.6A priority Critical patent/CN106273570A/en
Publication of CN106273570A publication Critical patent/CN106273570A/en
Pending legal-status Critical Current

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Classifications

    • BPERFORMING OPERATIONS; TRANSPORTING
    • B29WORKING OF PLASTICS; WORKING OF SUBSTANCES IN A PLASTIC STATE IN GENERAL
    • B29DPRODUCING PARTICULAR ARTICLES FROM PLASTICS OR FROM SUBSTANCES IN A PLASTIC STATE
    • B29D11/00Producing optical elements, e.g. lenses or prisms
    • B29D11/00009Production of simple or compound lenses

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  • Engineering & Computer Science (AREA)
  • Health & Medical Sciences (AREA)
  • Manufacturing & Machinery (AREA)
  • Ophthalmology & Optometry (AREA)
  • Mechanical Engineering (AREA)
  • Eyeglasses (AREA)
  • Compositions Of Macromolecular Compounds (AREA)

Abstract

The present invention provides the production technology of a kind of resin lens, comprises the following steps: with raw material;First dimethyl isophthalate, Merlon, methyl styrene are added sequentially in reactor; carry out 110 ± 2 degrees Celsius of constant temperature under nitrogen protection and stir 1 1.5 hours; then dibutylphosphoric acid ester, UV absorbent, catalyst, sclerosing agent are added sequentially in reactor, continue to carry out 120 ± 2 degrees Celsius of constant temperature under nitrogen protection and stir 0.5 1.2 hours and carry out being thoroughly mixed to form mixture;The compound being uniformly mixed is poured into after using nitrogen pressure filtration in the mould with rubber belt sealing, air pressure≤0.10MPa;Being put into by the mould poured into a mould in curing oven and solidify, the temperature of solidification controls below 50 degrees Celsius, and hardening time is 12 hours;After demoulding, resin lens is carried out stiffened plated film and saline boiling test.The eyeglass light transmission that the present invention makes is good, anti-fog properties by force.

Description

The production technology of resin lens
Technical field
The present invention relates to resin lens technical field, be specifically related to the production technology of a kind of resin lens.
Background technology
At present, refractive index be the ordinary resin eyeglass of 1.56 after plated film, its heatproof can reach 80 DEG C, through supersalt Can present dawdle be full of cracks and stripping phenomenon in various degree after water boil test, this explanation eyeglass heatproof is inadequate, causes eyeglass to hold The most aging.
Summary of the invention
For the variety of problems faced described in background technology, it is an object of the invention to provide a kind of light transmission good, antifog The production technology of the resin lens that property is strong.
For reaching above-mentioned purpose, the technical solution adopted in the present invention is: the production technology of a kind of resin lens, including with Under
Step: step 1: with raw material: dimethyl isophthalate 20-25 part, Merlon 40-60 part, methyl styrene 10- 15 parts, dibutylphosphoric acid ester 12-15 part, UV absorbent 5-10 part, catalyst 3-5 part, sclerosing agent 5-8 part;Step 2: first will Dimethyl isophthalate, Merlon, methyl styrene are added sequentially in reactor, carry out 110 ± 2 under nitrogen protection Degree Celsius constant temperature stirs 1-1.5 hour, then dibutylphosphoric acid ester, UV absorbent, catalyst, sclerosing agent is added sequentially to In reactor, continue to carry out 120 ± 2 degrees Celsius of constant temperature stirrings under nitrogen protection and be thoroughly mixed to form for 0.5-1.2 hour Mixture;Step 3: the compound being uniformly mixed is poured into after using nitrogen pressure filtration with the mould of rubber belt sealing In, air pressure≤0.10MPa;Step 4: being put into by the mould poured into a mould in curing oven and solidify, the temperature of solidification controls 50 Below degree Celsius, hardening time is 1-2 hour;Step 5: after demoulding, carries out stiffened plated film and the examination of salt water boil to resin lens Test.
Further, in step 1, raw material includes the component of following weight portion: dimethyl isophthalate 22 parts, poly-carbonic acid Ester 50 parts, methyl styrene 12 parts, dibutylphosphoric acid ester 13 parts, UV absorbent 5 parts, catalyst 3 parts, sclerosing agent 5 parts.
Further, step 1 also includes raw material: inorganic oxide.
Yet further, inorganic oxide is zinc oxide, and zinc oxide is as in the mixture of dispersant to step 2.
The method have the advantages that present invention process is simple, the eyeglass light transmission made is good, anti-fog properties By force, improve the ageing-resistant performance of resin lens, possess superpower shock resistance.
Detailed description of the invention
Below in conjunction with specific embodiment, the production technology of resin lens of the present invention is described further.
Embodiment 1
The production technology of resin lens of the present invention, comprises the following steps:
Step 1: with raw material: dimethyl isophthalate 20 parts, Merlon 40 parts, methyl styrene 10 parts, di(2-ethylhexyl)phosphate fourth Ester 12 parts, UV absorbent 7 parts, catalyst 4 parts, sclerosing agent 6 parts;
Step 2: first dimethyl isophthalate, Merlon, methyl styrene are added sequentially in reactor, protects at nitrogen Protect down and carry out 110 ± 2 degrees Celsius of constant temperature stirrings 1 hour, then by dibutylphosphoric acid ester, UV absorbent, catalyst, sclerosing agent It is added sequentially in reactor, continues to carry out 120 ± 2 degrees Celsius of constant temperature stirrings under nitrogen protection and fully mix for 0.5 hour Close and form mixture;
Step 3: the compound being uniformly mixed is poured into after using nitrogen pressure filtration in the mould with rubber belt sealing, Air pressure≤0.10MPa;
Step 4: being put into by the mould poured into a mould in curing oven and solidify, the temperature of solidification controls below 50 degrees Celsius, Gu The change time is 1-2 hour;Step 5: after demoulding, carries out stiffened plated film and saline boiling test to resin lens.
Embodiment 2
The production technology of resin lens of the present invention, comprises the following steps:
Step 1: with raw material: dimethyl isophthalate 22 parts, Merlon 50 parts, methyl styrene 12 parts, di(2-ethylhexyl)phosphate fourth Ester 13 parts, UV absorbent 5 parts, catalyst 3 parts, sclerosing agent 5 parts;
Step 2: first dimethyl isophthalate, Merlon, methyl styrene are added sequentially in reactor, protects at nitrogen Protect down and carry out 110 ± 2 degrees Celsius of constant temperature stirrings 1.2 hours, then by dibutylphosphoric acid ester, UV absorbent, catalyst, hardening Agent is added sequentially in reactor, continues to carry out 120 ± 2 degrees Celsius of constant temperature stirrings under nitrogen protection and within 0.8 hour, carries out fully It is mixed to form mixture;
Step 3: the compound being uniformly mixed is poured into after using nitrogen pressure filtration in the mould with rubber belt sealing, Air pressure≤0.10MPa;
Step 4: being put into by the mould poured into a mould in curing oven and solidify, the temperature of solidification controls below 50 degrees Celsius, Gu The change time is 1-2 hour;Step 5: after demoulding, carries out stiffened plated film and saline boiling test to resin lens.
Embodiment 3
The production technology of resin lens of the present invention, comprises the following steps:
Step 1: with raw material: dimethyl isophthalate 25 parts, Merlon 60 parts, methyl styrene 15 parts, di(2-ethylhexyl)phosphate fourth Ester 15 parts, UV absorbent 10 parts, catalyst 5 parts, sclerosing agent 8 parts;
Step 2: first dimethyl isophthalate, Merlon, methyl styrene are added sequentially in reactor, protects at nitrogen Protect down and carry out 110 ± 2 degrees Celsius of constant temperature stirrings 1.5 hours, then by dibutylphosphoric acid ester, UV absorbent, catalyst, hardening Agent is added sequentially in reactor, continues to carry out 120 ± 2 degrees Celsius of constant temperature stirrings under nitrogen protection and fully mixes for 1 hour Close and form mixture;
Step 3: the compound being uniformly mixed is poured into after using nitrogen pressure filtration in the mould with rubber belt sealing, Air pressure≤0.10MPa;
Step 4: being put into by the mould poured into a mould in curing oven and solidify, the temperature of solidification controls below 50 degrees Celsius, Gu The change time is 1-2 hour;Step 5: after demoulding, carries out stiffened plated film and saline boiling test to resin lens.
Embodiment 4
The production technology of resin lens of the present invention, comprises the following steps:
Step 1: with raw material: dimethyl isophthalate 25 parts, Merlon 60 parts, methyl styrene 15 parts, di(2-ethylhexyl)phosphate fourth Ester 15 parts, UV absorbent 10 parts, catalyst 5 parts, sclerosing agent 8 parts, zinc oxide 5 parts;
Step 2: first dimethyl isophthalate, Merlon, methyl styrene are added sequentially in reactor, protects at nitrogen Protect down and carry out 110 ± 2 degrees Celsius of constant temperature stirrings 1.5 hours, then by dibutylphosphoric acid ester, UV absorbent, catalyst, hardening Agent is added sequentially in reactor, continues to carry out 120 ± 2 degrees Celsius of constant temperature stirrings under nitrogen protection and fully mixes for 1 hour Close and form mixture, inorganic oxide zinc oxide is distributed in mixture;
Step 3: the compound being uniformly mixed is poured into after using nitrogen pressure filtration in the mould with rubber belt sealing, Air pressure≤0.10MPa;
Step 4: being put into by the mould poured into a mould in curing oven and solidify, the temperature of solidification controls below 50 degrees Celsius, Gu The change time is 1-2 hour;Step 5: after demoulding, carries out stiffened plated film and saline boiling test to resin lens.

Claims (4)

1. the production technology of a resin lens, it is characterised in that comprise the following steps:
Step 1: with raw material: dimethyl isophthalate 20-25 part, Merlon 40-60 part, methyl styrene 10-
15 parts, dibutylphosphoric acid ester 12-15 part, UV absorbent 5-10 part, catalyst 3-5 part, sclerosing agent 5-8 part;
Step 2: first dimethyl isophthalate, Merlon, methyl styrene are added sequentially in reactor, at nitrogen
Carry out 110 ± 2 degrees Celsius of constant temperature under protection and stir 1-1.5 hour, then by dibutylphosphoric acid ester, UV absorbent, urge Agent, sclerosing agent are added sequentially in reactor, continue to carry out 120 ± 2 degrees Celsius of constant temperature stirring 0.5-1.2 under nitrogen protection Hour carry out being thoroughly mixed to form mixture;
Step 3: the compound being uniformly mixed is poured into after using nitrogen pressure filtration in the mould with rubber belt sealing, Air pressure≤0.10MPa;
Step 4: being put into by the mould poured into a mould in curing oven and solidify, the temperature of solidification controls below 50 degrees Celsius,
Hardening time is 1-2 hour;
Step 5: after demoulding, carries out stiffened plated film and saline boiling test to resin lens.
The production technology of resin lens the most according to claim 1, it is characterised in that: in step 1, raw material includes following heavy The component of amount part: dimethyl isophthalate 22 parts, Merlon 50 parts, methyl styrene 12 parts, dibutylphosphoric acid ester 13 parts, purple Ultraviolet absorbers 5 parts, catalyst 3 parts, sclerosing agent 5 parts.
The production technology of resin lens the most according to claim 2, it is characterised in that: step 1 also includes raw material: inorganic Oxide.
The production technology of resin lens the most according to claim 3, it is characterised in that: inorganic oxide is zinc oxide, oxygen Change zinc as in the mixture of dispersant to step 2.
CN201610759743.6A 2016-08-30 2016-08-30 The production technology of resin lens Pending CN106273570A (en)

Priority Applications (1)

Application Number Priority Date Filing Date Title
CN201610759743.6A CN106273570A (en) 2016-08-30 2016-08-30 The production technology of resin lens

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
CN201610759743.6A CN106273570A (en) 2016-08-30 2016-08-30 The production technology of resin lens

Publications (1)

Publication Number Publication Date
CN106273570A true CN106273570A (en) 2017-01-04

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Cited By (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN109839346A (en) * 2017-11-26 2019-06-04 丹阳康斯特光学元件有限公司 A kind of eyeglass film layer firmness detection method
CN109943048A (en) * 2017-12-20 2019-06-28 杨运海 A kind of fine definition eyeglass and preparation method thereof
CN110837138A (en) * 2019-07-15 2020-02-25 漳州东利光学科技有限公司 Lens coated with oil-proof and water-proof function and manufacturing process thereof

Citations (5)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN1548988A (en) * 2003-05-14 2004-11-24 上海康耐特光学有限公司 Method for producing optical resin material with high-refractivity
CN101405339A (en) * 2006-03-17 2009-04-08 木本股份有限公司 Binder composition for polyester film and optical film using same
CN103448265A (en) * 2013-09-17 2013-12-18 朱回军 Method for producing resin lens
CN104497547A (en) * 2014-11-28 2015-04-08 李国金 High-toughness and impact-resistant resin eyeglass and preparation method thereof
CN105176042A (en) * 2015-10-11 2015-12-23 浙江方氏眼镜制造有限公司 Resin lens with good fog resistance and preparation method thereof

Patent Citations (5)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN1548988A (en) * 2003-05-14 2004-11-24 上海康耐特光学有限公司 Method for producing optical resin material with high-refractivity
CN101405339A (en) * 2006-03-17 2009-04-08 木本股份有限公司 Binder composition for polyester film and optical film using same
CN103448265A (en) * 2013-09-17 2013-12-18 朱回军 Method for producing resin lens
CN104497547A (en) * 2014-11-28 2015-04-08 李国金 High-toughness and impact-resistant resin eyeglass and preparation method thereof
CN105176042A (en) * 2015-10-11 2015-12-23 浙江方氏眼镜制造有限公司 Resin lens with good fog resistance and preparation method thereof

Non-Patent Citations (1)

* Cited by examiner, † Cited by third party
Title
劳动和社会保障部职业技能鉴定中心,中国眼镜协会: "《眼镜定配工职业资格培训教程(高级)》", 31 July 2002, 海洋出版社 *

Cited By (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN109839346A (en) * 2017-11-26 2019-06-04 丹阳康斯特光学元件有限公司 A kind of eyeglass film layer firmness detection method
CN109943048A (en) * 2017-12-20 2019-06-28 杨运海 A kind of fine definition eyeglass and preparation method thereof
CN110837138A (en) * 2019-07-15 2020-02-25 漳州东利光学科技有限公司 Lens coated with oil-proof and water-proof function and manufacturing process thereof

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Application publication date: 20170104