CN106268122A - A kind of cold-rolling emulsion device for purifying gas with peculiar smell and method - Google Patents
A kind of cold-rolling emulsion device for purifying gas with peculiar smell and method Download PDFInfo
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- CN106268122A CN106268122A CN201510362874.6A CN201510362874A CN106268122A CN 106268122 A CN106268122 A CN 106268122A CN 201510362874 A CN201510362874 A CN 201510362874A CN 106268122 A CN106268122 A CN 106268122A
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Abstract
The present invention relates to a kind of cold-rolling emulsion waste gas purification apparatus and method thereof, this device includes: blower fan (1), demister, enrichment method reactor (6), oxidant generating means (7), discharge opeing collection device (8), air vent (9), by the gas with foreign flavor that emulsion produces being removed oil mist removing, oxidized off flavor gas, removing smell substance, the gas with foreign flavor of fog discharge system during cold rolling is further purified, is reduced the final odor concentration discharging gas with foreign flavor and Volatile organic emissions concentration.
Description
Technical field:
The invention belongs to environmental protection technical field, be specifically related to the produced gas with foreign flavor of emulsion waste gas during cold rolling
Carry out the apparatus and method purified.
Background technology
In cold-rolling process, need to apply emulsion, and emulsion can be formed when high temperature strip steel surface evaporation and part cracking
Gas with foreign flavor, causes and has abnormal flavour in ambient air.This gas with foreign flavor complicated component, mass concentration is the highest, mainly with molecular weight
Relatively large hydro carbons and the aldehydes of semi-oxidation state, ketone and alkoxide are main.
The fog discharge system that general cold rolling industry milling train is arranged there is oil mist filter, but does not remove the equipment of gas with foreign flavor, although
Within 2015, country implements " steel rolling industrial atmosphere pollutant emission standard (GB 28,665 2012) ", only defines rolling unit
The emission limit of mist of oil, and the discharge to the gas with foreign flavor in air does not limit, but mill area and the emulsifying of floss hole periphery
Liquid gas with foreign flavor is objective reality.
Traditional gas with foreign flavor suppression technology has Physical, chemical method and bioanalysis.Wherein, physical method mainly include masking method,
Absorption method.Masking method is typically to admix with abnormal flavour foul smell with abnormal flavour with more intensive aromatic odor or other pleasant abnormal smells from the patient,
To shelter abnormal flavour or to change the character of abnormal flavour, make abnormal smells from the patient become able to as people and accepted, or use one can to offset or neutralize
The additive of stench, to alleviate abnormal flavour, the effect of masking method is different and variant because of each one impression degree.Absorption method is the most suitable
Process low concentration, the smell substance that pollutional load is the highest, the device initial stage of putting into operation eliminates the unusual smell effective, but along with the time of use
The growth effect that eliminates the unusual smell substantially weaken, and it is relatively costly and there is secondary pollution to change adsorbent.Chemical method is mainly wrapped
Including chemical washing method, oxidizing process, burning method, it is high, applied widely that the method has efficiency, but equipment investment, operating cost
Higher, it is suitable for the occasion that some concentration are of a relatively high.Biological method mainly includes Biological fitler method, biosorption process, soil
Composting process and biological deodorant etc., have the advantages such as simple, the less secondary pollution of technique, but the method exist screening and cultivates bacterium
Plant difficulty, take effect slowly, the defects such as biofilter floor space is big.These traditional smell pollutions control technology and are respectively arranged with its advantage drawn game
Limit.
Have developed plasma purifying method and photocatalytic oxidation in recent years, broadly fall into normal temperature oxidation method.Plasma is clean
Change technology system utilizes isoionic activity, and its ultimate principle is: put by the high-voltage pulse corona of steep-front, nanoscale narrow spaces
The modes such as electricity, obtain nonequilibrium plasma at normal temperatures and pressures, i.e. produce substantial amounts of high energy electron and O free radical, and OH is certainly
By base isoreactivity particle, smell pollution thing is aoxidized the structure destroying malodor molecule, thus reaches to eliminate the purpose of abnormal flavour.
Photochemical catalytic oxidation system, by luminous energy and the common effect of semiconductor catalyst, forms oxidation-reduction potential, produces OH free radical etc.
Active group, reacts with smell substance.Both approaches has certain effect for the gas with foreign flavor that molecular structure is fairly simple
Really, and operational management is convenient, but because being normal temperature oxidation, it is therefore desirable to the longer response time can be only achieved the effect of setting.
Therefore the time of staying inadequate or uneven time may produce incomplete oxidation product, the often association of the most this kind of device is the denseest
The ozone of degree, if do not taked appropriate gas removal ozone measure also can form secondary pollution.
In order to solve these problems, people take many corrective measures, including the method in various patents.In Chinese patent Shen
Please number 201210279387.X, " a kind of energy-efficient abnormal flavour exhaust gas purification and treatment device ", by single for the oxidation of pre-filtering activated carbon catalysis
The equipment that unit, energetic ion generator and ultraviolet light unit integrate, wherein, prefilter is using activated carbon as absorption
Medium, it is impossible to be used for oil-containing waste gas is processed, and the catalyst of catalytic oxidation unit is easily in dirty by the particulate matter in gas
Contaminating and lost efficacy, whole device structure is complicated, and investment is big.As can be seen here, current techniques equipment is not met by current industrial undertaking
In for the demand of stench purified treatment.
Summary of the invention
The problem of emulsion gas with foreign flavor produced for cold rolling process, the invention provides a kind of to cold rolling during
Gas with foreign flavor produced by emulsion waste gas carries out the devices and methods therefor purified, by the emulsifying of fog discharge system during cold rolling
Liquid gas with foreign flavor is further purified, and reduces the final odor concentration discharging gas and Volatile organic emissions concentration.And
And, blower fan 1 is joined directly together with cold rolling mill fog discharge system pipeline 10, and the gas with foreign flavor that emulsion produces first passes through blower fan 1 again
Filtering, whole gas with foreign flavor carries out purifier and works under positive pressure, requires low to the air-tightness of purifier, and gas with foreign flavor is not
Easily reveal.Meanwhile, gas with foreign flavor flowing velocity is relatively slow, and the stop in catalysis packing material 4 is long for time of contact, oxygen
Change reaction effect more preferable, go to eliminate the unusual smell more thorough.
A kind of cold-rolling emulsion device for purifying gas with peculiar smell of the present invention, comprising: blower fan 1, demister, enrichment method are anti-
Answer device 6, oxidant generating means 7, discharge opeing collection device 8, air vent 9;
The inlet duct of described blower fan 1 is connected with cold rolling mill fog discharge system pipeline 10, the abnormal flavour produced by emulsion during rolling
Demister is sent into after gas pressurized;
The described arrival end of enrichment method reactor 6 is connected with the outlet conduit of demister, fills in enrichment method reactor 6
There are catalysis packing material 4, the smell substance in absorption and oxidized off flavor gas;
Described enrichment method reactor 6 is provided with oxidant dog-house 5, oxidant dog-house 5 and oxidant generating means 7
It is connected, oxidant generating means 7 is produced-go the oxidant eliminating the unusual smell required to send in enrichment method reactor 6;
Described discharge opeing collection device 8 is all connected with the bottom of demister and enrichment method reactor 6, for discharging except mist fills
Put the waste liquid produced in abnormal flavour purification process with enrichment method reactor 6;
Described air vent 9 is connected with described enrichment method reactor 6 port of export, the waste gas after discharging removing abnormal flavour.
Preferential, demister is filtering type machinery oil mist removing device 3, for removing the mist of oil in gas with foreign flavor.
Preferential, demister also includes that centrifugal oil mist removing device 2, described centrifugal oil mist removing device 2 are positioned at filtering type machine
The windward end of tool oil mist removing device 3, i.e. gas with foreign flavor first pass through described centrifugal oil mist removing device 2, then through filtering type machinery
Oil mist removing device, wherein,
Centrifugal oil mist removing device 2 removes the oil mist particles that in the emulsion gas with foreign flavor after blower fan 1 pressurizes, granularity is bigger;
Filtering type machinery oil mist removing device 3 removes the mist of oil in the gas with foreign flavor of centrifugal oil mist removing device further.
Described centrifugal oil mist removing device 2, for Conventional rotary helical filter, utilizes centrifugal force to remove oil mist particles, model
Optional HCY-W2 type oil mist filter.
Described filtering type machinery oil mist removing device 3, for conventional mechanical formula filter, its principle is to utilize filtering material to remove oil mist removing
Granule, general filtering material is made up of 2 metafiltration nets, and ground floor is metal gauze, and model is NITTED MESH TYPE SL-STYLE,
The second layer is that metal gauze adds glass fibre, and model is NITTED MESH TYPE GS-STYLE.
Preferential, discharge opeing collection device 8 and the link position of demister are at centrifugal oil mist removing device 2 and filtering type machinery
Between oil mist removing device 3.
Preferential, enrichment method reactor 6 is equipped with catalysis packing material 4, and wherein catalysis packing material 4 comprises activated carbon and urges
Agent, the smell substance in absorption and oxidized off flavor gas.
Preferential, catalyst is oxide or the salt of the transition metal such as ferrum, manganese.
Preferential, the weight of catalyst accounts for the 0.01~5.00% of catalysis packing material.
Preferential, oxidant dog-house 5 is positioned at upstream or the centre of catalysis packing material 4.
Preferential, oxidant generating means 7 interval produces oxidant, every other day opens oxidant generating means 20-30min.
Preferential, oxidant is ozone, H2O2Or potassium permanganate.
A kind of method using above-mentioned cold-rolling emulsion device for purifying gas with peculiar smell to carry out cold-rolling emulsion gas with foreign flavor purification, comprises
Following steps:
(1) send into oil mist removing device after the gas with foreign flavor that emulsion produces is pressurizeed by blower fan 1 and remove oil mist removing;
(2) total volatile organism (TVOCs) measured according to outlet controls the opening time of oxidant generating means 7, control
The generating capacity of oxygenerating agent;
(3) gas with foreign flavor after oil mist removing is gone to be passed through enrichment method reactor 6, absorption and oxidized off flavor material;
(4) waste gas after removing abnormal flavour is discharged by outlet 9;
(5) waste liquid produced in abnormal flavour purification process is discharged by discharge opeing collection device 8.
Preferential, step (1) is gone oil mist removing be: to remove the mist of oil in gas with foreign flavor by filter type;Demister was
Filter formula machinery oil mist removing device 3.
Preferential, step (1) is gone oil mist removing can first pass through centrifugal oil mist removing device 2 and remove the breast after blower fan 1 pressurizes
Change the oil mist particles that in liquid gas with foreign flavor, granularity is bigger;Again through filtering type machinery oil mist removing device 3 further remove through from
Mist of oil in the gas with foreign flavor of core type oil mist removing device.
Preferential, absorption and oxidation step (3) be by being catalyzed in packing material 4 catalyst by smell substance oxygen by oxidant
Change removing.
Preferential, gas with foreign flavor is 0.1~1.5m/s by the superficial velocity scope of enrichment method reactor 6, and strength load stops
Time range is 0.1~5.0s.The strength load time of staying refer to gas with foreign flavor in enrichment method reactor 6 when averagely stopping
Between.
The present invention is directed to low concentration, the feature of macromole emulsion abnormal flavour waste gas that cold rolling process produces, use enrichment method
Reactor, on the one hand effectively increases the smell substance time of staying in reactor, on the other hand can be significantly by enrichment
Improve the reactant concentration of conversion zone, improve reaction efficiency, compared with the technique of existing low-temperature plasma and photochemical catalytic oxidation,
Gas residence time adds 103~104Times, reactant concentration increases by 102~104Times, due to the downstream of oxidant dog-house 5
It is present in catalysis packing material 4, the problem that oxidant leaks will not occur.The present invention can effectively remove in cold rolling production all kinds of
All kinds of particulate form mist of oils in the produced gas of emulsion high-temperature heating or water droplet, thus decrease the dirt of subsequent reactions purifier
Dye thing load.
Use technique scheme, cold rolling and silicon steel can be produced belt steel rolling technical process fog discharge system off gas and carry out further
Purification, reduce odor concentration and the Volatile organic emissions concentration of final exhaust ventilation, reduce and be close to emission point neighboring area
Abnormal flavour risk.
Accompanying drawing explanation
Fig. 1 is cold-rolling emulsion waste gas purification apparatus structural representation.
Description of reference numerals: (1) blower fan;(2) centrifugal oil mist removing device;(3) filtering type machinery oil mist removing device;(4)
Catalysis packing material;(5) oxidant dog-house;(6) enrichment method reactor;(7) oxidant generating means;(8) discharge opeing
Collection device;(9) air vent;(10) cold rolling mill fog discharge system pipeline.
Detailed description of the invention
The volatile organic matter concentration of the fog discharge systematic collection carried by cold rolling mill is not more than 30mg/m3, temperature 20-40 DEG C,
Humidity 60-95%, odor concentration in 3000 (dimensionless) below and in wave characteristic.
As it is shown in figure 1, blower fan 1 inlet duct of the cold-rolling emulsion device for purifying gas with peculiar smell of the abnormal flavour present invention and cold rolling mill
Waste gas system airduct 10 is connected, and sucks emulsion gas with foreign flavor when blower fan 1 runs, and sends into demister after pressurization, subsequently into
Enrichment method reactor 6 is discharged by air vent 9 after removing abnormal flavour.Enrichment method reactor upstream or centre arrange oxidizer source
Dog-house 5, oxidant is produced by oxidant generating means 7, and enrichment method reactor 6 is built with catalysis packing material 4.Except mist
It is provided with discharge opeing collection device 8 bottom device and enrichment method reactor 6.
Embodiment
Baogang Stocks Trading Co. is cold rolling rolls the waste gas that the operation of rolling produces, and discharges after the fog discharge systematic collection that milling train carries, waste gas oil
Mist content≤20mg/m3, temperature 20~40 DEG C, humidity 60~95%, odor concentration is less than 1500 (dimensionless), reaches state
Family existing " emission standard for odor pollutants (GB14554-93) ", but under specific meteorological condition, air vent nearby residents district
Still there will be appreciable emulsion taste (greasy smell).
Emulsion waste gas pressurizes through blower fan 1, oil moisture content is little after centrifugal oil mist removing device 2 and filtering type machinery demister 3
In 1 μ g/m3, catalysis packing material 4 is activated carbon and the Fe as catalyst2O3, wherein activated carbon is that carbon tetrachloride absorption is held
Measuring 40~the activated carbon adsorbing material of 60%, catalyst weight accounts for the 0.20% of catalysis packing material, and oxidant is ozone,
Gas with foreign flavor controls 1.2~1.5m/s through the superficial velocity of encapsulant layer, and the strength load time of staying is 0.1s, and catalysis is filled out
Filling material 4 packed height is 12cm, and it is at 5cm that oxidant dog-house 5 is arranged at catalysis packing material height, by throwing in
Oxidant, in upper and lower two the catalysis oxide layers of catalysis encapsulant layer intermediate formation.Every about 72 hours unlatching ozonators
30~45min, it is interrupted and adds oxidant, and control ozonator with the ozone concentration of air vent 9 detection so that air vent
Ozone concentration is 80~100ppb.
The assay device shown in embodiment and method is used to process this emulsion of rolling mill waste gas (waste gas oil moisture content 20mg/m3, temperature
Spend 30 DEG C, humidity 85%, odor concentration about 800 (dimensionless)), detect with magnificent auspicious ppb RAE 3000 type VOC detector
Emulsion waste gas TVOCs imported and exported by the cold-rolling emulsion waste gas purification apparatus of the present invention, by the method for national regulations to air vent 9
Carry out odor concentration detection.Record the entrance ppb and outlet ppb of each time point, and calculate TVOCs clearance, on-the-spot continuous
Test abnormal flavour purge cases is as shown in table 1, and the average removal rate of TVOCs can reach 80%, and air vent odor concentration controls
50 (dimensionless) are below.
Table 1 gas with foreign flavor purification result
Run duration device air vent does not smells emulsion abnormal smells from the patient, and that tests continuously detects that device is arranged in the 52nd day and the 65th day
The odor concentration of QI KOU 9 is between 23-41 (dimensionless).Result above shows, the purifier of the technical program offer and side
Method, the waste gas for cold rolling process discharge has good abnormal flavour removal effect.
Claims (10)
1. a cold-rolling emulsion device for purifying gas with peculiar smell, it is characterised in that including: blower fan (1), demister, concentration
Enrichment reactor (6), oxidant generating means (7), discharge opeing collection device (8), air vent (9);
The inlet duct of described blower fan (1) is connected with cold rolling mill fog discharge system pipeline (10), and when will roll, emulsion produces
Gas with foreign flavor pressurization after send into demister;
The arrival end of described enrichment method reactor (6) is connected with the outlet conduit of demister, enrichment method reactor (6)
In equipped with catalysis packing material (4), for absorption and oxidized off flavor gas in smell substance;
Described enrichment method reactor (6) is provided with oxidant dog-house (5), oxidant dog-house (5) and oxidant
Generating means (7) is connected, and the oxidant going to eliminate the unusual smell required produced by oxidant generating means (7) is sent into and concentrated richness
In collection reactor (6);
Described discharge opeing collection device (8) is all connected with the bottom of demister and enrichment method reactor (6), is used for discharging
The waste liquid that demister and enrichment method reactor (6) produce in abnormal flavour purification process;
Described air vent (9) is connected with described enrichment method reactor (6) port of export, after discharging removing abnormal flavour
Waste gas.
Cold-rolling emulsion device for purifying gas with peculiar smell the most according to claim 1, it is characterised in that: described demister
For filtering type machinery oil mist removing device (3), filtering type machinery oil mist removing device (3) removes the mist of oil in gas with foreign flavor.
Cold-rolling emulsion device for purifying gas with peculiar smell the most according to claim 1, it is characterised in that: described demister
It is made up of centrifugal oil mist removing device (2) and filtering type machinery oil mist removing device (3), described centrifugal oil mist removing device (2)
It is positioned at the upstream of filtering type machinery oil mist removing device (3), wherein
Centrifugal oil mist removing device (2) removes the mist of oil that in the emulsion gas with foreign flavor after blower fan (1) pressurizes, granularity is bigger
Granule;
Filtering type machinery oil mist removing device (3) removes the mist of oil in the gas with foreign flavor of centrifugal oil mist removing device (2) further.
Cold-rolling emulsion device for purifying gas with peculiar smell the most according to claim 1, it is characterised in that: described catalysis is filled
Material (4) comprises activated carbon and catalyst.
Cold-rolling emulsion device for purifying gas with peculiar smell the most according to claim 4, it is characterised in that: described catalyst is
Ferrum, the oxide of manganese transition metal or salt.
Cold-rolling emulsion device for purifying gas with peculiar smell the most according to claim 4, it is characterised in that: described catalyst accounts for
The percentage by weight of catalysis packing material is 0.01~5.00%.
Cold-rolling emulsion device for purifying gas with peculiar smell the most according to claim 1, it is characterised in that: described oxidant is thrown
Material mouth (5) is positioned at upstream or the centre of catalysis packing material (4).
Cold-rolling emulsion device for purifying gas with peculiar smell the most according to claim 1, it is characterised in that: described oxidant is
Ozone, H2O2Or potassium permanganate.
9. one kind use cold-rolling emulsion device for purifying gas with peculiar smell according to any one of claim 1-8 carry out cold rolling emulsified with
The method that lower liquid gas with foreign flavor purifies, comprises step:
(1) send into oil mist removing device after the gas with foreign flavor that emulsion produces is pressurizeed by blower fan (1) and remove oil mist removing;
(2) total volatile organism measured according to air vent (9) controls the opening time of oxidant generating means (7), control
The generating capacity of oxygenerating agent;
(3) gas with foreign flavor after oil mist removing is gone to be passed through enrichment method reactor (6), absorption and oxidized off flavor material;
(4) waste gas after removing abnormal flavour is discharged by air vent (9);
(5) waste liquid produced in gas with foreign flavor purification process is discharged by discharge opeing collection device (8).
Cold-rolling emulsion gas with foreign flavor purification method the most according to claim 9, it is characterised in that: gas with foreign flavor passes through
The superficial velocity scope of described enrichment method reactor (6) is 0.1~1.5m/s, strength load residence time ranges be 0.1~
5.0s。
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Cited By (1)
Publication number | Priority date | Publication date | Assignee | Title |
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CN112387012A (en) * | 2019-08-13 | 2021-02-23 | 宝山钢铁股份有限公司 | Waste emulsion system of power station pulverized coal boiler and steam-water separation method thereof |
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