CN106244320A - A kind of Longaacting fragrance-aretaining fabric detergent spice with mosquito repellent function and preparation method thereof - Google Patents
A kind of Longaacting fragrance-aretaining fabric detergent spice with mosquito repellent function and preparation method thereof Download PDFInfo
- Publication number
- CN106244320A CN106244320A CN201610600054.0A CN201610600054A CN106244320A CN 106244320 A CN106244320 A CN 106244320A CN 201610600054 A CN201610600054 A CN 201610600054A CN 106244320 A CN106244320 A CN 106244320A
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- China
- Prior art keywords
- spice
- essence
- aretaining
- preparation
- fragrance
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
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Classifications
-
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11B—PRODUCING, e.g. BY PRESSING RAW MATERIALS OR BY EXTRACTION FROM WASTE MATERIALS, REFINING OR PRESERVING FATS, FATTY SUBSTANCES, e.g. LANOLIN, FATTY OILS OR WAXES; ESSENTIAL OILS; PERFUMES
- C11B9/00—Essential oils; Perfumes
-
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11B—PRODUCING, e.g. BY PRESSING RAW MATERIALS OR BY EXTRACTION FROM WASTE MATERIALS, REFINING OR PRESERVING FATS, FATTY SUBSTANCES, e.g. LANOLIN, FATTY OILS OR WAXES; ESSENTIAL OILS; PERFUMES
- C11B9/00—Essential oils; Perfumes
- C11B9/0003—Compounds of unspecified constitution defined by the chemical reaction for their preparation
-
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11B—PRODUCING, e.g. BY PRESSING RAW MATERIALS OR BY EXTRACTION FROM WASTE MATERIALS, REFINING OR PRESERVING FATS, FATTY SUBSTANCES, e.g. LANOLIN, FATTY OILS OR WAXES; ESSENTIAL OILS; PERFUMES
- C11B9/00—Essential oils; Perfumes
- C11B9/0007—Aliphatic compounds
- C11B9/0015—Aliphatic compounds containing oxygen as the only heteroatom
-
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
- C11D3/00—Other compounding ingredients of detergent compositions covered in group C11D1/00
- C11D3/16—Organic compounds
- C11D3/38—Products with no well-defined composition, e.g. natural products
- C11D3/382—Vegetable products, e.g. soya meal, wood flour, sawdust
-
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
- C11D3/00—Other compounding ingredients of detergent compositions covered in group C11D1/00
- C11D3/48—Medical, disinfecting agents, disinfecting, antibacterial, germicidal or antimicrobial compositions
-
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
- C11D3/00—Other compounding ingredients of detergent compositions covered in group C11D1/00
- C11D3/50—Perfumes
-
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
- C11D7/00—Compositions of detergents based essentially on non-surface-active compounds
- C11D7/22—Organic compounds
- C11D7/40—Products in which the composition is not well defined
- C11D7/44—Vegetable products
Landscapes
- Chemical & Material Sciences (AREA)
- Life Sciences & Earth Sciences (AREA)
- Engineering & Computer Science (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Wood Science & Technology (AREA)
- Oil, Petroleum & Natural Gas (AREA)
- Organic Chemistry (AREA)
- General Chemical & Material Sciences (AREA)
- Treatments For Attaching Organic Compounds To Fibrous Goods (AREA)
- Detergent Compositions (AREA)
- Fats And Perfumes (AREA)
Abstract
The invention discloses a kind of Longaacting fragrance-aretaining fabric detergent spice with mosquito repellent function and preparation method thereof, it is to be prepared by the raw material of following weight parts: Fructus Citri Limoniae essence 0.3 0.5, jasmin essence 0.3 0.5, ambrotone 0.5 1, Oleum Folium Artemisiae Argyi 0.5 1, Herba Eupatorii Fortunei oil 0.3 0.5, safflower oil 0.1 0.2, starch octenyl succinate anhydride 20 30, citric acid 0.3 0.5, VTES 12, tetraethyl orthosilicate 0.2 0.4, Konjaku plucosidopolyose 0.1 0.15.The fabric detergent spice of the present invention had both had that fabric retention is good, durability degree is high, the feature of lasting fragrance, moreover it is possible to playing effect of anophelifuge, anthelmintic, fragrance is pure and fresh pleasant, soft comfortable.
Description
Technical field
The present invention relates to daily use chemicals spice technical field, particularly relate to a kind of Longaacting fragrance-aretaining fabric washing with mosquito repellent function
Agent spice and preparation method thereof and preparation method thereof.
Background technology
In fabric detergent, add spice, on the one hand user can be allowed to feel comfortably cool, on the other hand can be clear as fabric
Clean signal, makes washed fabric have pleasant fragrance.But clean at fabric with in subsequent processes, due to water
The link such as wash, be dried and have lost substantial amounts of spice, the problem such as low, poor durability of utilization rate causing spice.Therefore, how to improve
The stability of fabric detergent spice and durability, make fragrance energy more longlasting, become an important problem.CN99807528
By modified starch, Oleum sesami is encapsulated, spice can be protected in washing cycle, reduce the loss of spice, and can make to process
Fabric there is initial and lasting fragrance effects.But, this method is not improved spice and to the adhesion of fabric and is stayed
The property, long-lasting to fragrance and spice utilization rate lifting is limited.
Summary of the invention
The object of the invention is contemplated to make up the defect of prior art, it is provided that a kind of fabric retention is good, durability degree is high, fragrant
What taste was lasting Longaacting fragrance-aretaining fabric detergent spice with mosquito repellent function and preparation method thereof and preparation method thereof.
The present invention is achieved by the following technical solutions:
A kind of Longaacting fragrance-aretaining fabric detergent spice with mosquito repellent function and preparation method thereof, it is former by following weight parts
Material prepares:
Fructus Citri Limoniae essence 0.3-0.5, jasmin essence 0.3-0.5, ambrotone 0.5-1, Oleum Folium Artemisiae Argyi 0.5-1, Herba Eupatorii Fortunei oil 0.3-0.5 are red
Caul-fat 0.1-0.2, starch octenyl succinate anhydride 20-30, citric acid 0.3-0.5, VTES 1-2, positive silicon
Acetoacetic ester 0.2-0.4, Konjaku plucosidopolyose 0.1-0.15.
A kind of preparation method of the Longaacting fragrance-aretaining fabric detergent spice with mosquito repellent function and preparation method thereof, including with
Lower step:
(1) weigh raw material by weight, first Fructus Citri Limoniae essence, jasmin essence, Oleum Folium Artemisiae Argyi, Herba Eupatorii Fortunei oil, safflower oil and ambrotone are mixed
Uniformly obtain mixing essence, stir after starch octenyl succinate anhydride is mixed with dehydrated alcohol by solid-liquid weight ratio 1:0.5-1:1
Mix 10-15min, be subsequently adding described mixing essence stirring 0.5-1h, be eventually adding citric acid, VTES
Stirring 10-15min is continued with tetraethyl orthosilicate；
(2) material in (1) is slowly dropped in the water of 1.5-2.5 times of weight and in 40-50 DEG C, 300-400r/min stir 1-
2h, adds remaining raw material stirring mix homogeneously after cooling, pH be adjusted to neutrality and stand 0.5-1h in room temperature, being then fed into spraying
Drying tower is spray-dried under the conditions of inlet temperature 145-155 DEG C, leaving air temp 85-95 DEG C, must have anophelifuge merit
The Longaacting fragrance-aretaining fabric detergent spice of effect.
The invention have the advantage that
The present invention, using VTES, tetraethyl orthosilicate as presoma, is led in conjunction with starch octenyl succinate anhydride
Cross spray drying method mixing essence is coated with, improve perfume particle to the retention of fabric and slow release durability；Dragon saliva
Ketone soft aroma and, persistently, thoroughly send out, not only contribute to promote the odor prolongation of spice, moreover it is possible to play in neutralization fragrance component and sting
Swash the effect of property abnormal smells from the patient, make fragrance more mildness, comfortable；Again by Fructus Citri Limoniae essence, jasmin essence, Oleum Folium Artemisiae Argyi, Herba Eupatorii
Oil, safflower oil complex role so as to get fabric detergent spice both had that fabric retention is good, durability degree is high, fragrance is held
Long feature, moreover it is possible to play effect of anophelifuge, anthelmintic, fragrance is pure and fresh pleasant, soft comfortable.
Detailed description of the invention
A kind of Longaacting fragrance-aretaining fabric detergent spice with mosquito repellent function and preparation method thereof, by following weight (kg)
Component raw material is prepared from:
Fructus Citri Limoniae essence 0.3, jasmin essence 0.3, ambrotone 0.5, Oleum Folium Artemisiae Argyi 0.5, Herba Eupatorii Fortunei oil 0.3, safflower oil 0.1, octenyl amber
Amber acid-starch ester 20, citric acid 0.3, VTES 1, tetraethyl orthosilicate 0.2, Konjaku plucosidopolyose 0.1.
A kind of preparation method of the Longaacting fragrance-aretaining fabric detergent spice with mosquito repellent function and preparation method thereof, including with
Lower step:
(1) weigh raw material by weight, first Fructus Citri Limoniae essence, jasmin essence, Oleum Folium Artemisiae Argyi, Herba Eupatorii Fortunei oil, safflower oil and ambrotone are mixed
Uniformly obtain mixing essence, starch octenyl succinate anhydride is pressed and stirs after solid-liquid weight ratio 1:0.5 mixes with dehydrated alcohol
10min, is subsequently adding described mixing essence stirring 0.5h, is eventually adding citric acid, VTES and positive silicon
Acetoacetic ester continues stirring 10min；
(2) material in (1) is slowly dropped in the water of 1.5 times of weight and in 40 DEG C, 300r/min stir 1h, after cooling add
Remaining raw material stirring mix homogeneously, is adjusted to pH neutrality and stands 0.5h in room temperature, being then fed in spray drying tower in air intake
It is spray-dried under the conditions of temperature 145 DEG C, leaving air temp 85 DEG C, must have the Longaacting fragrance-aretaining fabric detergent of mosquito repellent function
Spice.
Being added to by fabric detergent spice obtained above common without in fragrant detergent, addition is detergent gross weight
0.5%, after washing, aroma retaining effect test result shows that fabric washing still has obvious odor characteristic after drying three months.
Claims (2)
1. Longaacting fragrance-aretaining fabric detergent spice with mosquito repellent function and preparation method thereof, it is characterised in that its be by
The raw material of following weight parts prepares:
Fructus Citri Limoniae essence 0.3-0.5, jasmin essence 0.3-0.5, ambrotone 0.5-1, Oleum Folium Artemisiae Argyi 0.5-1, Herba Eupatorii Fortunei oil 0.3-0.5 are red
Caul-fat 0.1-0.2, starch octenyl succinate anhydride 20-30, citric acid 0.3-0.5, VTES 1-2, positive silicon
Acetoacetic ester 0.2-0.4, Konjaku plucosidopolyose 0.1-0.15.
A kind of Longaacting fragrance-aretaining fabric detergent spice with mosquito repellent function the most according to claim 1 and preparation method thereof
Preparation method, it is characterised in that comprise the following steps:
(1) weigh raw material by weight, first Fructus Citri Limoniae essence, jasmin essence, Oleum Folium Artemisiae Argyi, Herba Eupatorii Fortunei oil, safflower oil and ambrotone are mixed
Uniformly obtain mixing essence, stir after starch octenyl succinate anhydride is mixed with dehydrated alcohol by solid-liquid weight ratio 1:0.5-1:1
Mix 10-15min, be subsequently adding described mixing essence stirring 0.5-1h, be eventually adding citric acid, VTES
Stirring 10-15min is continued with tetraethyl orthosilicate；
(2) material in (1) is slowly dropped in the water of 1.5-2.5 times of weight and in 40-50 DEG C, 300-400r/min stir 1-
2h, adds remaining raw material stirring mix homogeneously after cooling, pH be adjusted to neutrality and stand 0.5-1h in room temperature, being then fed into spraying
Drying tower is spray-dried under the conditions of inlet temperature 145-155 DEG C, leaving air temp 85-95 DEG C, must have anophelifuge merit
The Longaacting fragrance-aretaining fabric detergent spice of effect.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201610600054.0A CN106244320A (en) | 2016-07-28 | 2016-07-28 | A kind of Longaacting fragrance-aretaining fabric detergent spice with mosquito repellent function and preparation method thereof |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201610600054.0A CN106244320A (en) | 2016-07-28 | 2016-07-28 | A kind of Longaacting fragrance-aretaining fabric detergent spice with mosquito repellent function and preparation method thereof |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| CN106244320A true CN106244320A (en) | 2016-12-21 |
Family
ID=57604413
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN201610600054.0A Pending CN106244320A (en) | 2016-07-28 | 2016-07-28 | A kind of Longaacting fragrance-aretaining fabric detergent spice with mosquito repellent function and preparation method thereof |
Country Status (1)
| Country | Link |
|---|---|
| CN (1) | CN106244320A (en) |
Citations (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN105002009A (en) * | 2015-07-23 | 2015-10-28 | 安徽省三环纸业集团香料科技发展有限公司 | Rheumatism-relieving washing powder perfume and preparing method thereof |
| CN105002010A (en) * | 2015-07-23 | 2015-10-28 | 安徽省三环纸业集团香料科技发展有限公司 | Skin-caring health caring washing powder perfume and preparing method thereof |
| CN105039017A (en) * | 2015-07-23 | 2015-11-11 | 安徽省三环纸业集团香料科技发展有限公司 | Washing powder perfume for improving immunity and preparation method thereof |
| CN105062713A (en) * | 2015-07-23 | 2015-11-18 | 安徽省三环纸业集团香料科技发展有限公司 | Spice used for mosquito repellent detergent powder and preparation method for spice |
-
2016
- 2016-07-28 CN CN201610600054.0A patent/CN106244320A/en active Pending
Patent Citations (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN105002009A (en) * | 2015-07-23 | 2015-10-28 | 安徽省三环纸业集团香料科技发展有限公司 | Rheumatism-relieving washing powder perfume and preparing method thereof |
| CN105002010A (en) * | 2015-07-23 | 2015-10-28 | 安徽省三环纸业集团香料科技发展有限公司 | Skin-caring health caring washing powder perfume and preparing method thereof |
| CN105039017A (en) * | 2015-07-23 | 2015-11-11 | 安徽省三环纸业集团香料科技发展有限公司 | Washing powder perfume for improving immunity and preparation method thereof |
| CN105062713A (en) * | 2015-07-23 | 2015-11-18 | 安徽省三环纸业集团香料科技发展有限公司 | Spice used for mosquito repellent detergent powder and preparation method for spice |
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| Date | Code | Title | Description |
|---|---|---|---|
| C06 | Publication | ||
| PB01 | Publication | ||
| C10 | Entry into substantive examination | ||
| SE01 | Entry into force of request for substantive examination | ||
| RJ01 | Rejection of invention patent application after publication |
Application publication date: 20161221 |
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| RJ01 | Rejection of invention patent application after publication |