CN106234448A - 一种新型植物源果树杀虫剂 - Google Patents

一种新型植物源果树杀虫剂 Download PDF

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CN106234448A
CN106234448A CN201610618428.1A CN201610618428A CN106234448A CN 106234448 A CN106234448 A CN 106234448A CN 201610618428 A CN201610618428 A CN 201610618428A CN 106234448 A CN106234448 A CN 106234448A
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韦波
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Abstract

本发明公开了一种新型植物源果树杀虫剂，包括以下原料：秦皮、毒鱼藤、阴香叶、印楝、曼陀罗、苦楝、苦皮藤、臭椿、莴苣、薄荷、蓖麻、钾盐、磷盐、氮盐、钙盐、镁盐、碘盐、硼盐、钼盐、锌盐、锰盐、铜盐、铁盐、维生素、氨基酸、吲哚丁酸、赤霉素、6‑苄基腺膘呤、萘乙酸、琼脂、激动素、聚乙烯吡咯烷酮、亚甲基双萘磺酸钠、美国杜邦EEA2112AC相容剂、蚯蚓粉、烷基硫酸酯钾、丙烯酸酯、环氧丙氧丙基三甲氧基硅烷、黄原胶、乙醇。本发明的新型植物源果树杀虫剂对尺蠖、黄蜘蛛、长白蚧植物害虫的一次杀灭率均在97.14%以上，高于常规新型植物源果树杀虫剂杀灭率，并且没有耐药用性，可以5‑8年；同时使用本新型植物源果树杀虫剂，还可提高产量和含糖量。

Description

一种新型植物源果树杀虫剂
技术领域
本发明属于杀虫剂制备技术领域，具体涉及一种多功能新型植物源果树杀虫剂。
背景技术
目前防治农业害虫大多都使用化学杀虫剂，随着人民生活水平的提高，对农产品质量要求高了，不仅要吃好，而且要吃出健康。高毒化学农药所引发的农药残留问题越来越成为社会关注的热点。高毒农药是影响农产品质量安全的核心和关键，不仅影响农产品质量，直接危害人民群众的身体健康，还影响农民增收。由于高毒农药的毒性大，以前造成人畜中毒的事件时有发生。对妇女和儿童的影响极大，致畸致残的儿童很多。此外，随着世界各国对人类生存环境和自然生态的保护意识日益增强，高毒高残留杀虫剂将进一步受到限制。农药的不合理使用对农产品的质量安全构成威胁，因此，减少农药使用特别是高毒农药使用，对提高农产品质量和市场竞争力，促进我国农业持续发展，保障广大人民群众的生命安全和构建和谐社会都有着十分重大的意义。
由于化学农药很容易引起害虫的抗药性，为了防治效果好不断增加使用药量，杀害了很多天敌与有益生物，而且也污染了我们赖以生存生活环境，国家对环境保护的越来越重视，对农产品中的农药残留检测将会愈加严格，因此，大力发展无毒无公害的高效植物源农药是今后农药发展的方向。此外，常规的杀虫剂功能性单一，无法满足需求。
发明内容
本发明提供一种新型植物源果树杀虫剂，以解决使用化学农药防治害虫引起害虫抗药性及污染环境，规的杀虫剂功能性单一，无法满足需求等问题，本发明的新型植物源果树杀虫剂对尺蠖、黄蜘蛛、长白蚧植物害虫的一次杀灭率均在97.24%以上，高于常规新型植物源果树杀虫剂杀灭率，并且没有耐药用性，可以5-8年；同时使用本新型植物源果树杀虫剂，还可提高产量和含糖量。
为解决以上技术问题，本发明采用以下技术方案：
一种新型植物源果树杀虫剂，以重量份为单位，包括以下原料：秦皮84-96份、毒鱼藤84-96份、阴香叶62-86份、印楝60-90份、曼陀罗50-80份、苦楝50-80份、苦皮藤40-70份、臭椿40-70份、莴苣35-60份、薄荷35-60份、蓖麻30-50份、钾盐2-3份、磷盐1-3份、氮盐1-2份、钙盐0.6-0.9份、镁盐0.6-0.9份、碘盐0.2-0.4份、硼盐0.2-0.4份、钼盐0.2-0.4份、锌盐0.2-0.4份、锰盐0.2-0.4份、铜盐0.2-0.4份、铁盐0.2-0.4份、维生素0.2-0.4份、氨基酸0.2-0.3份、吲哚丁酸0.06-0. 09份、赤霉素0.06-0.09份、6-苄基腺膘呤0.06-0.08份、萘乙酸0.04-0.06份、琼脂0.1-0.3份、激动素0.04-0.06份、聚乙烯吡咯烷酮0.8-2.4份、亚甲基双萘磺酸钠0.6-1.8份、美国杜邦EEA2112AC相容剂1-1.5份、蚯蚓粉0.6-1.5份、烷基硫酸酯钾0.4-1.4份、丙烯酸酯0.5-0.8份、环氧丙氧丙基三甲氧基硅烷0.6-1.6份、黄原胶0.5-1.5份、乙醇2000-6000份；
所述钾盐由以下组分组成：氯化钾0.6-0.8份、硫酸钾0.5-0.6份、硝酸钾0.4-0.6份、碳酸钾0.3-0.5份、碳酸氢钾0.2-0.5份；
所述磷盐由以下组分组成：磷酸钙0.3-0.8份、磷酸镁0.3-0.8份、磷酸铁0.2-0.7份、磷酸锌0.2-0.7份；
所述氮盐由以下组分组成：碳酸氢铵0.4-0.8份、碳酸铵0.3-0.6份、氯化铵0.3-0.6份；
所述钙盐由以下组分组成：甘氨酸钙0.3-0.4份、氯化钙0.2-0.3份、硫酸亚钙0.1-0.2份；
所述镁盐由以下组分组成：甘氨酸镁0.3-0.4份、氯化镁0.2-0.3份、硫酸亚镁0.1-0.2份；
所述碘盐由以下组分组成：碘化钠0.1-0.2份、碘酸钾0.1-0.2份；
所述维生素由以下组分组成：生素A0.08-0.14份、维生素 B10.08-0.12份、维生素B20.02-0.08份、维生素D0.02-0.06份；
所述氨基酸由以下组分组成：甘氨酸0.08-0.1份、胱氨酸0.06-0.08份、脯氨酸0.04-0.07份、丝氨酸0.02-0.05份；
所述聚乙烯吡咯烷酮为助溶剂；
所述亚甲基双萘磺酸钠为分散剂；
所述蚯蚓为粉调理剂；
所述烷基硫酸酯钾为渗透剂；
所述丙烯酸酯为调节剂；
所述环氧丙氧丙基三甲氧基硅烷为增粘剂；
所述黄原胶为稳定剂；
所述的新型植物源果树杀虫剂的制备方法，包括以下步骤：
S1：将秦皮、毒鱼藤、阴香叶、印楝、曼陀罗、苦楝、苦皮藤、臭椿、莴苣、薄荷、蓖麻混合粉碎，得到混合物Ⅰ，将混合物Ⅰ加入到乙醇中，在料液比为1:14-16，超声波功率为200-300W，乙醇浓度为65%-80%，提取温度为66-72℃下提取药液18-24min，制得药液；
S2：将步骤S1制得的药液过3000-5000目筛子，制得滤液；
S3：将步骤S2制得的滤液添加钾盐、磷盐、氮盐、钙盐、镁盐、碘盐、硼盐、钼盐、锌盐、锰盐、铜盐、铁盐、维生素、氨基酸、吲哚丁酸、赤霉素、6-苄基腺膘呤、萘乙酸、琼脂、激动素、聚乙烯吡咯烷酮、亚甲基双萘磺酸钠、美国杜邦EEA2112AC相容剂、蚯蚓粉、烷基硫酸酯钾、丙烯酸酯、环氧丙氧丙基三甲氧基硅烷、黄原胶，在温度为42-50℃，转速为100-300r/min下搅拌溶解20-30min，制得混合液；
S4：将步骤S3制得的混合液在温度为60-80℃下浓缩至含水量≤22%，制得混合物Ⅱ；
S5：将步骤S4制得的混合物Ⅱ在温度为84-88℃下干燥至含水量≤6%，接着粉碎，过120-260目筛子，所得粉末采用脉动真空压力蒸气灭菌器在温度为134-136℃，压力为210-230KPa下灭菌3-4min，制得新型植物源果树杀虫剂。
进一步地，所述硼盐为硼酸钾。
进一步地，所述钼盐为钼酸钾。
进一步地，所述锌盐为氯化锌。
进一步地，所述锰盐为甘氨酸锰。
进一步地，所述铜盐为甘氨酸铜。
进一步地，所述铁盐为硫酸亚铁。
本发明具有以下有益效果：
（1）本发明的新型植物源果树杀虫剂成分无毒，无残留，不会带来环境污染；
（2）本发明的新型植物源果树杀虫剂对尺蠖、黄蜘蛛、长白蚧植物害虫的一次杀灭率均在97.14%以上，高于常规新型植物源果树杀虫剂杀灭率，并且没有耐药用性，可以5-8年；同时使用本新型植物源果树杀虫剂，还可提高产量和含糖量；
（3）本发明的新型植物源果树杀虫剂生产方法简单，成本低，使用方便，应用效果好，有利于推广应用。
具体实施方式
为便于更好地理解本发明，通过以下实施例加以说明，这些实施例属于本发明的保护范围，但不限制本发明的保护范围。
在实施例中，所述新型植物源果树杀虫剂，以重量份为单位，包括以下原料：秦皮84-96份、毒鱼藤84-96份、阴香叶62-86份、印楝60-90份、曼陀罗50-80份、苦楝50-80份、苦皮藤40-70份、臭椿40-70份、莴苣35-60份、薄荷35-60份、蓖麻30-50份、钾盐2-3份、磷盐1-3份、氮盐1-2份、钙盐0.6-0.9份、镁盐0.6-0.9份、碘盐0.2-0.4份、硼盐0.2-0.4份、钼盐0.2-0.4份、锌盐0.2-0.4份、锰盐0.2-0.4份、铜盐0.2-0.4份、铁盐0.2-0.4份、维生素0.2-0.4份、氨基酸0.2-0.3份、吲哚丁酸0.06-0. 09份、赤霉素0.06-0.09份、6-苄基腺膘呤0.06-0.08份、萘乙酸0.04-0.06份、琼脂0.1-0.3份、激动素0.04-0.06份、聚乙烯吡咯烷酮0.8-2.4份、亚甲基双萘磺酸钠0.6-1.8份、美国杜邦EEA2112AC相容剂1-1.5份、蚯蚓粉0.6-1.5份、烷基硫酸酯钾0.4-1.4份、丙烯酸酯0.5-0.8份、环氧丙氧丙基三甲氧基硅烷0.6-1.6份、黄原胶0.5-1.5份、乙醇2000-6000份；
所述钾盐由以下组分组成：氯化钾0.6-0.8份、硫酸钾0.5-0.6份、硝酸钾0.4-0.6份、碳酸钾0.3-0.5份、碳酸氢钾0.2-0.5份；
所述磷盐由以下组分组成：磷酸钙0.3-0.8份、磷酸镁0.3-0.8份、磷酸铁0.2-0.7份、磷酸锌0.2-0.7份；
所述氮盐由以下组分组成：碳酸氢铵0.4-0.8份、碳酸铵0.3-0.6份、氯化铵0.3-0.6份；
所述钙盐由以下组分组成：甘氨酸钙0.3-0.4份、氯化钙0.2-0.3份、硫酸亚钙0.1-0.2份；
所述镁盐由以下组分组成：甘氨酸镁0.3-0.4份、氯化镁0.2-0.3份、硫酸亚镁0.1-0.2份；
所述碘盐由以下组分组成：碘化钠0.1-0.2份、碘酸钾0.1-0.2份；
所述硼盐为硼酸钾；
所述钼盐为钼酸钾；
所述锌盐为氯化锌；
所述锰盐为甘氨酸锰；
所述铜盐为甘氨酸铜；
所述铁盐为硫酸亚铁；
所述维生素由以下组分组成：生素A0.08-0.14份、维生素 B10.08-0.12份、维生素B20.02-0.08份、维生素D0.02-0.06份；
所述氨基酸由以下组分组成：甘氨酸0.08-0.1份、胱氨酸0.06-0.08份、脯氨酸0.04-0.07份、丝氨酸0.02-0.05份；
所述聚乙烯吡咯烷酮为助溶剂；
所述亚甲基双萘磺酸钠为分散剂；
所述蚯蚓为粉调理剂；
所述烷基硫酸酯钾为渗透剂；
所述丙烯酸酯为调节剂；
所述环氧丙氧丙基三甲氧基硅烷为增粘剂；
所述黄原胶为稳定剂；
所述的新型植物源果树杀虫剂的制备方法，包括以下步骤：
S1：将秦皮、毒鱼藤、阴香叶、印楝、曼陀罗、苦楝、苦皮藤、臭椿、莴苣、薄荷、蓖麻混合粉碎，得到混合物Ⅰ，将混合物Ⅰ加入到乙醇中，在料液比为1:14-16，超声波功率为200-300W，乙醇浓度为65%-80%，提取温度为66-72℃下提取药液18-24min，制得药液；
S2：将步骤S1制得的药液过3000-5000目筛子，制得滤液；
S3：将步骤S2制得的滤液添加钾盐、磷盐、氮盐、钙盐、镁盐、碘盐、硼盐、钼盐、锌盐、锰盐、铜盐、铁盐、维生素、氨基酸、吲哚丁酸、赤霉素、6-苄基腺膘呤、萘乙酸、琼脂、激动素、聚乙烯吡咯烷酮、亚甲基双萘磺酸钠、美国杜邦EEA2112AC相容剂、蚯蚓粉、烷基硫酸酯钾、丙烯酸酯、环氧丙氧丙基三甲氧基硅烷、黄原胶，在温度为42-50℃，转速为100-300r/min下搅拌溶解20-30min，制得混合液；
S4：将步骤S3制得的混合液在温度为60-80℃下浓缩至含水量≤22%，制得混合物Ⅱ；
S5：将步骤S4制得的混合物Ⅱ在温度为84-88℃下干燥至含水量≤6%，接着粉碎，过120-260目筛子，所得粉末采用脉动真空压力蒸气灭菌器在温度为134-136℃，压力为210-230KPa下灭菌3-4min，制得新型植物源果树杀虫剂。
下面通过更具体的实施例加以说明。
实施例1
一种新型植物源果树杀虫剂，以重量份为单位，包括以下原料：秦皮90份、毒鱼藤90份、阴香叶75份、印楝75份、曼陀罗65份、苦楝65份、苦皮藤55份、臭椿55份、莴苣50份、薄荷50份、蓖麻40份、钾盐2.5份、磷盐2份、氮盐1.5份、钙盐0.8份、镁盐0.8份、碘盐0.3份、硼盐0.3份、钼盐0.3份、锌盐0.3份、锰盐0.3份、铜盐0.3份、铁盐0.3份、维生素0.3份、氨基酸0.2份、吲哚丁酸0.08份、赤霉素0.08份、6-苄基腺膘呤0.07份、萘乙酸0.05份、琼脂0.2份、激动素0.05份、聚乙烯吡咯烷酮1.6份、亚甲基双萘磺酸钠1.2份、美国杜邦EEA2112AC相容剂1.2份、蚯蚓粉1份、烷基硫酸酯钾1份、丙烯酸酯0.7份、环氧丙氧丙基三甲氧基硅烷1.2份、黄原胶1份、乙醇4000份；
所述钾盐由以下组分组成：氯化钾0.7份、硫酸钾0.5份、硝酸钾0.4份、碳酸钾0.5份、碳酸氢钾0.4份；
所述磷盐由以下组分组成：磷酸钙0.6份、磷酸镁0.6份、磷酸铁0.5份、磷酸锌0.3份；
所述氮盐由以下组分组成：碳酸氢铵0.6份、碳酸铵0.5份、氯化铵0.4份；
所述钙盐由以下组分组成：甘氨酸钙0.3份、氯化钙0.3份、硫酸亚钙0.2份；
所述镁盐由以下组分组成：甘氨酸镁0.3份、氯化镁0.3份、硫酸亚镁0.2份；
所述碘盐由以下组分组成：碘化钠0.2份、碘酸钾0.1份；
所述硼盐为硼酸钾；
所述钼盐为钼酸钾；
所述锌盐为氯化锌；
所述锰盐为甘氨酸锰；
所述铜盐为甘氨酸铜；
所述铁盐为硫酸亚铁；
所述维生素由以下组分组成：生素A0.1份、维生素 B10.1份、维生素B20.05份、维生素D0.05份；
所述氨基酸由以下组分组成：甘氨酸0.08份、胱氨酸0.06份、脯氨酸0.04份、丝氨酸0.02份；
所述聚乙烯吡咯烷酮为助溶剂；
所述亚甲基双萘磺酸钠为分散剂；
所述蚯蚓为粉调理剂；
所述烷基硫酸酯钾为渗透剂；
所述丙烯酸酯为调节剂；
所述环氧丙氧丙基三甲氧基硅烷为增粘剂；
所述黄原胶为稳定剂；
所述的新型植物源果树杀虫剂的制备方法，包括以下步骤：
S1：将秦皮、毒鱼藤、阴香叶、印楝、曼陀罗、苦楝、苦皮藤、臭椿、莴苣、薄荷、蓖麻混合粉碎，得到混合物Ⅰ，将混合物Ⅰ加入到乙醇中，在料液比为1:15，超声波功率为250W，乙醇浓度为75%，提取温度为68℃下提取药液20min，制得药液；
S2：将步骤S1制得的药液过4000目筛子，制得滤液；
S3：将步骤S2制得的滤液添加钾盐、磷盐、氮盐、钙盐、镁盐、碘盐、硼盐、钼盐、锌盐、锰盐、铜盐、铁盐、维生素、氨基酸、吲哚丁酸、赤霉素、6-苄基腺膘呤、萘乙酸、琼脂、激动素、聚乙烯吡咯烷酮、亚甲基双萘磺酸钠、美国杜邦EEA2112AC相容剂、蚯蚓粉、烷基硫酸酯钾、丙烯酸酯、环氧丙氧丙基三甲氧基硅烷、黄原胶，在温度为46℃，转速为200r/min下搅拌溶解25min，制得混合液；
S4：将步骤S3制得的混合液在温度为70℃下浓缩至含水量为22%，制得混合物Ⅱ；
S5：将步骤S4制得的混合物Ⅱ在温度为86℃下干燥至含水量为6%，接着粉碎，过200目筛子，所得粉末采用脉动真空压力蒸气灭菌器在温度为135℃，压力为220KPa下灭菌3.5min，制得新型植物源果树杀虫剂。
实施例2
一种新型植物源果树杀虫剂，以重量份为单位，包括以下原料：秦皮84份、毒鱼藤84份、阴香叶62份、印楝60份、曼陀罗50份、苦楝50份、苦皮藤40份、臭椿40份、莴苣35份、薄荷35份、蓖麻30份、钾盐2份、磷盐1份、氮盐1份、钙盐0.6份、镁盐0.6份、碘盐0.2份、硼盐0.2份、钼盐0.2份、锌盐0.2份、锰盐0.2份、铜盐0.2份、铁盐0.2份、维生素0.2份、氨基酸0.2份、吲哚丁酸0.06份、赤霉素0.06份、6-苄基腺膘呤0.06份、萘乙酸0.04份、琼脂0.1份、激动素0.04份、聚乙烯吡咯烷酮0.8份、亚甲基双萘磺酸钠0.6份、美国杜邦EEA2112AC相容剂1份、蚯蚓粉0.6份、烷基硫酸酯钾0.4份、丙烯酸酯0.5份、环氧丙氧丙基三甲氧基硅烷0.6份、黄原胶0.5份、乙醇2000份；
所述钾盐由以下组分组成：氯化钾0.6份、硫酸钾0.5份、硝酸钾0.4份、碳酸钾0.3份、碳酸氢钾0.2份；
所述磷盐由以下组分组成：磷酸钙0.3份、磷酸镁0.3份、磷酸铁0.2份、磷酸锌0.2份；
所述氮盐由以下组分组成：碳酸氢铵0.4份、碳酸铵0.3份、氯化铵0.3份；
所述钙盐由以下组分组成：甘氨酸钙0.3份、氯化钙0.2份、硫酸亚钙0.1份；
所述镁盐由以下组分组成：甘氨酸镁0.3份、氯化镁0.2份、硫酸亚镁0.1份；
所述碘盐由以下组分组成：碘化钠0.1份、碘酸钾0.1份；
所述硼盐为硼酸钾；
所述钼盐为钼酸钾；
所述锌盐为氯化锌；
所述锰盐为甘氨酸锰；
所述铜盐为甘氨酸铜；
所述铁盐为硫酸亚铁；
所述维生素由以下组分组成：生素A0.08份、维生素 B10.08份、维生素B20.02份、维生素D0.02份；
所述氨基酸由以下组分组成：甘氨酸0.08份、胱氨酸0.06份、脯氨酸0.04份、丝氨酸0.02份；
所述聚乙烯吡咯烷酮为助溶剂；
所述亚甲基双萘磺酸钠为分散剂；
所述蚯蚓为粉调理剂；
所述烷基硫酸酯钾为渗透剂；
所述丙烯酸酯为调节剂；
所述环氧丙氧丙基三甲氧基硅烷为增粘剂；
所述黄原胶为稳定剂；
所述的新型植物源果树杀虫剂的制备方法，包括以下步骤：
S1：将秦皮、毒鱼藤、阴香叶、印楝、曼陀罗、苦楝、苦皮藤、臭椿、莴苣、薄荷、蓖麻混合粉碎，得到混合物Ⅰ，将混合物Ⅰ加入到乙醇中，在料液比为1:14，超声波功率为200W，乙醇浓度为65%，提取温度为66℃下提取药液24min，制得药液；
S2：将步骤S1制得的药液过3000目筛子，制得滤液；
S3：将步骤S2制得的滤液添加钾盐、磷盐、氮盐、钙盐、镁盐、碘盐、硼盐、钼盐、锌盐、锰盐、铜盐、铁盐、维生素、氨基酸、吲哚丁酸、赤霉素、6-苄基腺膘呤、萘乙酸、琼脂、激动素、聚乙烯吡咯烷酮、亚甲基双萘磺酸钠、美国杜邦EEA2112AC相容剂、蚯蚓粉、烷基硫酸酯钾、丙烯酸酯、环氧丙氧丙基三甲氧基硅烷、黄原胶，在温度为42℃，转速为100r/min下搅拌溶解30min，制得混合液；
S4：将步骤S3制得的混合液在温度为60℃下浓缩至含水量为20%，制得混合物Ⅱ；
S5：将步骤S4制得的混合物Ⅱ在温度为84℃下干燥至含水量为5%，接着粉碎，过120目筛子，所得粉末采用脉动真空压力蒸气灭菌器在温度为134℃，压力为210KPa下灭菌4min，制得新型植物源果树杀虫剂。
实施例3
一种新型植物源果树杀虫剂，以重量份为单位，包括以下原料：秦皮96份、毒鱼藤96份、阴香叶86份、印楝90份、曼陀罗80份、苦楝80份、苦皮藤70份、臭椿70份、莴苣60份、薄荷60份、蓖麻50份、钾盐3份、磷盐3份、氮盐2份、钙盐0.9份、镁盐0.9份、碘盐0.4份、硼盐0.4份、钼盐0.4份、锌盐0.4份、锰盐0.4份、铜盐0.4份、铁盐0.4份、维生素0.4份、氨基酸0.3份、吲哚丁酸0. 09份、赤霉素0.09份、6-苄基腺膘呤0.08份、萘乙酸0.06份、琼脂0.3份、激动素0.06份、聚乙烯吡咯烷酮2.4份、亚甲基双萘磺酸钠1.8份、美国杜邦EEA2112AC相容剂1.5份、蚯蚓粉1.5份、烷基硫酸酯钾1.4份、丙烯酸酯0.8份、环氧丙氧丙基三甲氧基硅烷1.6份、黄原胶1.5份、乙醇6000份；
所述钾盐由以下组分组成：氯化钾0.8份、硫酸钾0.6份、硝酸钾0.6份、碳酸钾0.5份、碳酸氢钾0.5份；
所述磷盐由以下组分组成：磷酸钙0.8份、磷酸镁0.8份、磷酸铁0.7份、磷酸锌0.7份；
所述氮盐由以下组分组成：碳酸氢铵0.8份、碳酸铵0.6份、氯化铵0.6份；
所述钙盐由以下组分组成：甘氨酸钙0.4份、氯化钙0.3份、硫酸亚钙0.2份；
所述镁盐由以下组分组成：甘氨酸镁0.4份、氯化镁0.3份、硫酸亚镁0.2份；
所述碘盐由以下组分组成：碘化钠0.2份、碘酸钾0.2份；
所述硼盐为硼酸钾；
所述钼盐为钼酸钾；
所述锌盐为氯化锌；
所述锰盐为甘氨酸锰；
所述铜盐为甘氨酸铜；
所述铁盐为硫酸亚铁；
所述维生素由以下组分组成：生素A0.14份、维生素 B10.12份、维生素B20.08份、维生素D0.06份；
所述氨基酸由以下组分组成：甘氨酸0.1份、胱氨酸0.08份、脯氨酸0.07份、丝氨酸0.05份；
所述聚乙烯吡咯烷酮为助溶剂；
所述亚甲基双萘磺酸钠为分散剂；
所述蚯蚓为粉调理剂；
所述烷基硫酸酯钾为渗透剂；
所述丙烯酸酯为调节剂；
所述环氧丙氧丙基三甲氧基硅烷为增粘剂；
所述黄原胶为稳定剂；
所述的新型植物源果树杀虫剂的制备方法，包括以下步骤：
S1：将秦皮、毒鱼藤、阴香叶、印楝、曼陀罗、苦楝、苦皮藤、臭椿、莴苣、薄荷、蓖麻混合粉碎，得到混合物Ⅰ，将混合物Ⅰ加入到乙醇中，在料液比为1:16，超声波功率为300W，乙醇浓度为80%，提取温度为72℃下提取药液18min，制得药液；
S2：将步骤S1制得的药液过5000目筛子，制得滤液；
S3：将步骤S2制得的滤液添加钾盐、磷盐、氮盐、钙盐、镁盐、碘盐、硼盐、钼盐、锌盐、锰盐、铜盐、铁盐、维生素、氨基酸、吲哚丁酸、赤霉素、6-苄基腺膘呤、萘乙酸、琼脂、激动素、聚乙烯吡咯烷酮、亚甲基双萘磺酸钠、美国杜邦EEA2112AC相容剂、蚯蚓粉、烷基硫酸酯钾、丙烯酸酯、环氧丙氧丙基三甲氧基硅烷、黄原胶，在温度为50℃，转速为300r/min下搅拌溶解20min，制得混合液；
S4：将步骤S3制得的混合液在温度为80℃下浓缩至含水量为16%，制得混合物Ⅱ；
S5：将步骤S4制得的混合物Ⅱ在温度为84-88℃下干燥至含水量为4%，接着粉碎，过260目筛子，所得粉末采用脉动真空压力蒸气灭菌器在温度为136℃，压力为230KPa下灭菌3min，制得新型植物源果树杀虫剂。
为验证本发明新型植物源果树杀虫剂的效果，通过以下实验验证。
采用实施例1-3的新型植物源果树杀虫剂和常规的杀虫剂（对照组），按1g杀虫剂配45g水的比例使用，进行柑橘一次防治尺蠖、黄蜘蛛、长白蚧植物害虫的试验，结果见下表。
从上表可见，本发明实施例1-3的新型植物源果树杀虫剂对尺蠖、黄蜘蛛、长白蚧植物害虫的一次杀灭率均在97.14%以上，高于常规新型植物源果树杀虫剂杀灭率，使用效果好；同时使用本新型植物源果树杀虫剂，还可提高产量和含糖量。
以上内容不能认定本发明具体实施只局限于这些说明，对于本发明所属技术领域的普通技术人员来说，在不脱离本发明构思前提下，还可以做出若干简单推演或替换，都应当视为属于本发明由所提交的权利要求书确定的专利保护范围。

Claims (7)

1.一种新型植物源果树杀虫剂，其特征在于，以重量份为单位，包括以下原料：秦皮84-96份、毒鱼藤84-96份、阴香叶62-86份、印楝60-90份、曼陀罗50-80份、苦楝50-80份、苦皮藤40-70份、臭椿40-70份、莴苣35-60份、薄荷35-60份、蓖麻30-50份、钾盐2-3份、磷盐1-3份、氮盐1-2份、钙盐0.6-0.9份、镁盐0.6-0.9份、碘盐0.2-0.4份、硼盐0.2-0.4份、钼盐0.2-0.4份、锌盐0.2-0.4份、锰盐0.2-0.4份、铜盐0.2-0.4份、铁盐0.2-0.4份、维生素0.2-0.4份、氨基酸0.2-0.3份、吲哚丁酸0.06-0. 09份、赤霉素0.06-0.09份、6-苄基腺膘呤0.06-0.08份、萘乙酸0.04-0.06份、琼脂0.1-0.3份、激动素0.04-0.06份、聚乙烯吡咯烷酮0.8-2.4份、亚甲基双萘磺酸钠0.6-1.8份、美国杜邦EEA2112AC相容剂1-1.5份、蚯蚓粉0.6-1.5份、烷基硫酸酯钾0.4-1.4份、丙烯酸酯0.5-0.8份、环氧丙氧丙基三甲氧基硅烷0.6-1.6份、黄原胶0.5-1.5份、乙醇2000-6000份；
所述钾盐由以下组分组成：氯化钾0.6-0.8份、硫酸钾0.5-0.6份、硝酸钾0.4-0.6份、碳酸钾0.3-0.5份、碳酸氢钾0.2-0.5份；
所述磷盐由以下组分组成：磷酸钙0.3-0.8份、磷酸镁0.3-0.8份、磷酸铁0.2-0.7份、磷酸锌0.2-0.7份；
所述氮盐由以下组分组成：碳酸氢铵0.4-0.8份、碳酸铵0.3-0.6份、氯化铵0.3-0.6份；
所述钙盐由以下组分组成：甘氨酸钙0.3-0.4份、氯化钙0.2-0.3份、硫酸亚钙0.1-0.2份；
所述镁盐由以下组分组成：甘氨酸镁0.3-0.4份、氯化镁0.2-0.3份、硫酸亚镁0.1-0.2份；
所述碘盐由以下组分组成：碘化钠0.1-0.2份、碘酸钾0.1-0.2份；
所述维生素由以下组分组成：生素A0.08-0.14份、维生素 B10.08-0.12份、维生素B20.02-0.08份、维生素D0.02-0.06份；
所述氨基酸由以下组分组成：甘氨酸0.08-0.1份、胱氨酸0.06-0.08份、脯氨酸0.04-0.07份、丝氨酸0.02-0.05份；
所述的新型植物源果树杀虫剂的制备方法，包括以下步骤：
S1：将秦皮、毒鱼藤、阴香叶、印楝、曼陀罗、苦楝、苦皮藤、臭椿、莴苣、薄荷、蓖麻混合粉碎，得到混合物Ⅰ，将混合物Ⅰ加入到乙醇中，在料液比为1:14-16，超声波功率为200-300W，乙醇浓度为65%-80%，提取温度为66-72℃下提取药液18-24min，制得药液；
S2：将步骤S1制得的药液过3000-5000目筛子，制得滤液；
S3：将步骤S2制得的滤液添加钾盐、磷盐、氮盐、钙盐、镁盐、碘盐、硼盐、钼盐、锌盐、锰盐、铜盐、铁盐、维生素、氨基酸、吲哚丁酸、赤霉素、6-苄基腺膘呤、萘乙酸、琼脂、激动素、聚乙烯吡咯烷酮、亚甲基双萘磺酸钠、美国杜邦EEA2112AC相容剂、蚯蚓粉、烷基硫酸酯钾、丙烯酸酯、环氧丙氧丙基三甲氧基硅烷、黄原胶，在温度为42-50℃，转速为100-300r/min下搅拌溶解20-30min，制得混合液；
S4：将步骤S3制得的混合液在温度为60-80℃下浓缩至含水量≤22%，制得混合物Ⅱ；
S5：将步骤S4制得的混合物Ⅱ在温度为84-88℃下干燥至含水量≤6%，接着粉碎，过120-260目筛子，所得粉末采用脉动真空压力蒸气灭菌器在温度为134-136℃，压力为210-230KPa下灭菌3-4min，制得新型植物源果树杀虫剂。
2.根据权利要求1所述的新型植物源果树杀虫剂，其特征在于，所述硼盐为硼酸钾。
3.根据权利要求1所述的新型植物源果树杀虫剂，其特征在于，所述钼盐为钼酸钾。
4.根据权利要求1所述的新型植物源果树杀虫剂，其特征在于，所述锌盐为氯化锌。
5.根据权利要求1所述的新型植物源果树杀虫剂，其特征在于，所述锰盐为甘氨酸锰。
6.根据权利要求1所述的新型植物源果树杀虫剂，其特征在于，所述铜盐为甘氨酸铜。
7.根据权利要求1所述的新型植物源果树杀虫剂，其特征在于，所述铁盐为硫酸亚铁。
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Application publication date: 20161221